Process Control and Systems Commons^™

Developing Process Control Experiments For Undergraduate Chemical Engineering Laboratories, Chase M. Swaffar

Graduate Theses and Dissertations

It is the intent of this work to develop a process control apparatus and series of experiments that will help students visualize the PID (Proportional-Integral-Derivative) control of a process and enhance their understanding of the subject. The apparatus is a computer-controlled PID mixing system that responds quickly to set point changes and process disturbances which are directly observable. The system can easily be simulated with a transfer function model in Matlab's Simulink, so that the controller can be optimized for the desired system response. Four experiments can be conducted with this system including: exploration of system modeling and controller optimization …

Tin Sensitization For Electroless Plating, Xingfei Wei

Graduate Theses and Dissertations

The tin sensitization process has been used in electroless plating since 1940s Brenner and Riddell developed the electroless plating for surface metallization method. It was found to be an interesting topic to study tin sensitization for chemically controlling metal deposition on different substrates, because the tin sensitization process had critical effects on the electroless plated metal thin films. Nowadays electroless plating metal deposition is still an important method for depositing metals. It has a few advantages over the vapor deposition and electrodeposition method, such as work in an ambient condition, on nonconductive substrates, and without extra power input. Applying electroless …

Low Volume Dispensing With High Speed Dispensers, Sunny Agarwal

Graduate Dissertations and Theses

With the high pace of innovation in the semiconductor manufacturing industry, there has been an increasing demand for more energy efficient and environmental friendly products. This research relates to a complex process of fluid dispensing at low volumes on a printed circuit board. Currently, a more refined non-contact dispensing terminology named “Streaming” is widely used to stream out material at low volumes for various applications. The key solution is to frame a dispensing method that lends itself most closely to the requirements of a specific production process.

This study represents a detailed approach of dispensing low volumes of materials in …

Development Of A High Precision Quantum Dot Synthysis Method Utilizing A Microfluidic Reactor And In-Line Fluorescence Cell, Harry Lafferty, Jonny Hoadley

Materials Engineering

Quantum dots show great potential for use as spectral converters in solar cells, lighting applications and biological imaging. These applications require precise control of quantum dot size to maximize performance. The fluorescence profile of quantum dots in solution correlates directly with particle size. An alternative, high precision process was developed for the synthesis of cadmium-selenide quantum dots using a microfluidic reactor and fluorescence flow through cell. The process required creating separate cadmium and selenium precursors that were then mixed in a nitrogen environment at 17± 1°C. Using an NE-300^® syringe pump, the solution was pumped through a microfluidic reactor …

Energy Audit In Wastewater Aeration System, Dinesh R. Kandel, Jacimaria R. Batista, Sajjad Ahmad

College of Engineering: Graduate Celebration Programs

To evaluate the energy consumption air to aeration basins in wastewater treatment aeration system and to compare the standard computations of oxygen demand and blower power requirements with the actual plant data.

Froth Flotation Performance Enhancement By Feed Cavitation And Magnetic Plastic Particle Addition, Mehmet Saracoglu

Theses and Dissertations--Mining Engineering

Froth flotation is the most commonly used process to recover and upgrade the portion of the coal preparation plant feed that has a particle size smaller than 150 microns. Problems that occur when employing froth flotation in the coal industry include i) coal surfaces that are weakly-to-moderately hydrophobic, and ii) flotation systems that are overloaded and limited by insufficient retention time.

Research was performed to evaluate techniques that could be implemented to improve flotation performance under the aforementioned scenarios. Pre-aeration of flotation feed using a cavitation system was extensively evaluated in laboratory and full-scale test programs. The benefits of adding …

Modeling, Fabrication And Characterization Of Scalable Electroless Gold Plated Nanostructures For Enhanced Surface Plasmon Resonance, Gyoung Gug Jang

Graduate Theses and Dissertations

The scientific and industrial demand for controllable thin gold (Au) film and Au nanostructures is increasing in many fields including opto-electronics, photovoltaics, MEMS devices, diagnostics, bio-molecular sensors, spectro-/microscopic surfaces and probes. In this study, a novel continuous flow electroless (CF-EL) Au plating method is developed to fabricate uniform Au thin films in ambient condition. The enhanced local mass transfer rate and continuous deposition resulting from CF-EL plating improved physical uniformity of deposited Au films and thermally transformed nanoparticles (NPs). Au films and NPs exhibited improved optical photoluminescence (PL) and surface plasmon resonance (SPR), respectively, relative to batch immersion EL (BI-EL) …

New Approaches In Automation, Allen Lam

Hong Kong Innovative Users Group Meetings

No abstract provided.

A Review Of Some Subtleties Of Practical Relevance, Keqin Gu

SIUE Faculty Research, Scholarship, and Creative Activity

This paper reviews some subtleties in time-delay systems of neutral type that are believed to be of particular relevance in practice. Both traditional formulation and the coupled differential-difference equation formulation are used. The discontinuity of the spectrum as a function of delays is discussed. Conditions to guarantee stability under small parameter variations are given. A number of subjects that have been discussed in the literature, often using different methods, are reviewed to illustrate some fundamental concepts. These include systems with small delays, the sensitivity of Smith predictor to small delay mismatch, and the discrete implementation of distributed-delay feedback control. The …

A Direct Sampling Particle Filter From Approximate Conditional Density Function Supported On Constrained State Space, Sridhar Ungarala

Chemical & Biomedical Engineering Faculty Publications

Constraints on the state vector must be taken into account in the state estimation problem. Recently, acceptance/rejection and projection methods are proposed in the particle filter framework for constraining the particles. A weighted least squares formulation is used for constraining samples in unscented and ensemble Kalman filters. In this paper, direct sampling from an approximate conditional probability density function (pdf) is proposed. It is obtained by approximating the a priori pdf as a Gaussian. The support of the conditional density is a subset of the intersection of two supports, the 3-sigma bounds of the priori Gaussian and the constrained state …

Applied Control Strategies At A Cogeneration Plant, Joseph William Burns

Master's Theses

The purpose of this paper is to demonstrate the effectiveness of “classical strategies for dynamic control” on authentic cogeneration processes. These strategies are applied to several processes at the University of Connecticut’s cogeneration plant. Case studies of their applications are presented in this paper. Strategies that are applied include the following:

1) The classical SISO feedback structure

2) The First Order Plus Dead Time (FOPDT) process model

3) The Internal Model Control (IMC) correlations for PI controller tuning

4) Static feed forward with feedback trim

5) Cascade Control

Running Head: Analysis Of The Just In Time Inventory System At Uhs Wilson Medical Center, Kyle P. Roeber

MPA Capstone Projects 2006 - 2015

In November 2007, United Health Services Materials Management implemented a Just in Time Inventory system to have a tighter control of their supply chain. This project examines the accuracy of the par levels currently employed by the United Health Services and the financial impact of operating a Just in Time inventory system using inaccurate inventory and par levels. In addition, the project researches other hospitals using JIT inventory management systems to compare implementation and management practices of JIT process.

Electrodeposition Of Tin Using Tin (Ii) Methanesulfonate From Mixture Of Ionic Liquid And Methane Sulfonic Acid., Yang Kok Kee

Student Works (2010-2019)

The electrodeposition of tin from Tin(II) Methane Sulfonate (MSA) with varying concentration in air and water stable 1-butyl-1-methyl-pyrrolidinium trifluoromethanesulfonate, (BMPOTF) ionic liquid at room temperature was studied. Cyclic Voltammetry served to characterize the electrochemical behavior of tin reduction and oxidation. The diffusion coefficient of stannous ions in the mixture of BMPOTF ionic liquid and MSA based electrolyte obtained via Randles-Sevcik and Cottrell equation was 2 × 10-7 cm2/s. Electroplating on copper panel was conducted under different current densities to determine BMPOTF based tin plating solution current efficiency. Mixture of BMPOTF and MSA based tin plating solution gave current efficiency as …

Optimization Of Inductively Coupled Plasma Dry Etching For Planar Waveguide Fabrication., Lim Weng Hong

Student Works (2010-2019)

Optimization of the Inductively Coupled Plasma (ICP) dry etching process parameters has been carried out. Seven main etching characteristics were considered in order to produce good etching quality. These characteristics are glass etching rates, selectivity of chromium to glass etching rate, channel side wall roughness, channel side wall vertical profile, channel cleanliness, critical dimension and resolution. Several ICP parameters that are affecting the etching characteristic were optimized in this work. These optimised ICP parameters obtained from this work are ICP power (880 W), bias power (45 W), operating chamber pressure (10 mtorr), reactant gas composition, reactant gas flow rate (35sccm …

Retrofit Of Distillation Columns In Biodiesel Production Plants, Nghi Nguyen, Yaşar Demirel

Yaşar Demirel Publications

Column grand composite curves and the exergy loss profiles produced by the Column-Targeting Tool of the Aspen Plus simulator are used to assess the performance of the existing distillation columns, and reduce the costs of operation by appropriate retrofits in a biodiesel production plant. Effectiveness of the retrofits is assessed by means of thermodynamics and economic improvements. We have considered a biodiesel plant utilizing three distillation columns to purify biodiesel (fatty acid methyl ester) and byproduct glycerol as well as reduce the waste. The assessments of the base case simulation have indicated the need for modifications for the distillation columns. …

Calibration Of Hdm-4 For Use In Pavement Management Systems (Pms), Nurdin Mushule

Tanzania Journal of Engineering and Technology (TJET)

One of major problems of road management in developing countries is the lack of decision making tools for preparing road maintenance programmes. This results in poor resource allocation and poor utilisation of existing assets. Pavement management systems (PMS) have been developed around the world in order to assist with the pavement management process in a co-ordinated and systematic manner. Some developed countries have derived pavement performance models that are suited to local conditions by setting up long term pavement performance studies. Conversely, most developing countries do not have the resources required to set up similar large-scale field experiments. However, validation …

A Systemic Framework For Implementation Of Tqm Programmes, Emanuel Mjema

Tanzania Journal of Engineering and Technology (TJET)

The purpose of this paper is to present a systemic framework for implementation of TQM program in a manufacturing organisation that produces motor vehicle components in Port Elizabeth - South Africa. The approach used included conceptualisation of the systemic framework and then involvement of the stakeholders in adding scenarios to be considered in the design and implementing the framework in the real field. The findings obtained during the implementation of the systemic framework established that reduction of scrap rate, reduction of production costs, reduction of cycle time and employee motivation could be achieved through the implementation of a Systemic Framework …

Computing Arrival Cost Parameters In Moving Horizon Estimation Using Sampling Based Filters, Sridhar Ungarala

Chemical & Biomedical Engineering Faculty Publications

Moving horizon estimation (MHE) is a numerical optimization based approach to state estimation, where the joint probability density function (pdf) of a finite state trajectory is sought, which is conditioned on a moving horizon of measurements. The joint conditional pdf depends on the a priori state pdf at the start of the horizon, which is a prediction pdf based on historical data outside the horizon. When the joint pdf is maximized, the arrival cost is a penalty term based on the a priori pdf in the MHE objective function. Traditionally, the a priori pdf is assumed as …

Letter To The Editor, Sridhar Ungarala

Chemical & Biomedical Engineering Faculty Publications

No abstract provided.

Comments On "Robust And Reliable Estimation Via Unscented Recursive Nonlinear Dynamic Data Reconciliation", Sridhar Ungarala

Chemical & Biomedical Engineering Faculty Publications

No abstract provided.

The Use Of A Cell Filter For State Estimation In Closed-Loop Nmpc Of Low Dimensional Systems, Sridhar Ungarala, Keyu Li

Chemical & Biomedical Engineering Faculty Publications

Combining variants of the Kalman filter and moving horizon estimation (MHE) with nonlinear MPC has been studied before. The MHE is appealing due to its ability to impose constraints and demonstrated superiority over extended Kalman filter. However, nonlinear MPC based on MHE requires solutions to two back to back nonlinear programs. In this paper we propose to use the cell filter (CF) to provide state feedback to the MPC regulator. The cell filter is a piecewise constant approximation of the conditional probability density of the states, whose temporal evolution is modeled by an aggregate Markov chain. Since the CF …

The Multivariate Statistical Analysis Of Abiotic Parameters Of The Lake Tanganyika Sub Catchment, Hudson Nkotagu

Tanzania Journal of Engineering and Technology (TJET)

Results from multivariate statistical analysis of abiotic parameters conducted during the dry season at 20 accessible sites on 8 rivers, 2 lakes and a dam covering the Lake Tanganyika sub catchment are discussed. Standard methods were used to determine the levels of abiotic parameters from water samples. Physical parameters including DO, EC, Eh, turbidity, temperature, pH and secchi transparency were measured in situ while chlorophyll a was determined in the laboratory. Nutrients such as NO3-, SiO2, PO4 3- and Fe2+ were determined along with HCO3-. Factor analysis resulted in four factors including increased primary productivity, redox conditions, dissolution, and reduction …

Bayesian Estimation Via Sequential Monte Carlo Sampling-Constrained Dynamic Systems, Lixin Lang, Wen-Shiang Chen, Bhavik R. Bakshi, Prem K. Goel, Sridhar Ungarala

Chemical & Biomedical Engineering Faculty Publications

Nonlinear and non-Gaussian processes with constraints are commonly encountered in dynamic estimation problems. Methods for solving such problems either ignore the constraints or rely on crude approximations of the model or probability distributions. Such approximations may reduce the accuracy of the estimates since they often fail to capture the variety of probability distributions encountered in constrained linear and nonlinear dynamic systems. This article describes a practical approach that overcomes these shortcomings via a novel extension of sequential Monte Carlo (SMC) sampling or particle filtering. Inequality constraints are imposed by accept/reject steps in the algorithm. The proposed approach provides samples representing …

Application Of Iso Tank In Chemimcal Logisitcs In China And Relative Issues, Hao Zhang

World Maritime University Dissertations

No abstract provided.

Research On Establishment Of Oil Spill Emergency Response System In China Qingdao Port Based On Ann, Ge Zhang

World Maritime University Dissertations

No abstract provided.

Biotechnology, Life Sciences And Control Engineering:Some Synthesis Issues, Aidan O'Dwyer

Conference papers

The synthesis of biotechnology, life sciences and control engineering is receiving increasing interest. The purpose of this contribution (and the associated poster) is to raise awareness of some of this synthesis work.

Sensors For The Detection Of Hazardous Emissions, Aidan O'Dwyer

Conference papers

This contribution will detail recent developments in sensor technology for the detection of hazardous emissions. The accurate measurement of such emissions is necessary if they are to be controlled to the appropriate regulations.

Socio-Economic Impacts Of Computer Viruses In Tanzania, M Victor

Tanzania Journal of Engineering and Technology (TJET)

This paper reports on a research project conducted with an objective of identifying and assessing various approaches used by different computer users (Management, System Administrators and end users) in Tanzania to combat computer viruses (CVs), and to assess users' awareness level on CVs. Specifically, the study aimed at assessing the awareness level on CVs to the Tanzanian business community; analyze the socio -economic impact caused by CVs in Tanzania and; assess existing methods, capacity and limitations on controlling CVs in Tanzania. Data was collected using both questionnaires and interview from financial institutions such as NBC and BOT, and telecommunications sector …

Degradation Of Waterfront Reinforced Concrete Structures At The Port Of Dar Es Salaam, I Sanga

Tanzania Journal of Engineering and Technology (TJET)

The paper summarises the results of an investigation done on piers at the Dar es Salaam Port. The problem facing these structures and marine facilities is their exposure to aggressive environmental phenomena. The paper presents an investigation of the strength and corrosion of concrete seaport piers so as to determine degradation of the reinforced concrete waterfront structures in the port of Dar es Salaam. For instance the structures at a dhow quay terminal had been in use for about 100 years. The facility was in bad condition as the concrete had been badly damaged due to corrosion. Some of the …

Stability Of Transport And Rate Processes [Review], Yaşar Demirel

Papers in Thermal Mechanics

About fifty years ago, the Turing instability demonstrated that even simple reaction-diffusion systems might lead to spatial order and differentiation, while the Rayleigh-Bénard instability showed that the maintenance of nonequilibrium might be the source of order in fluids subjected to a thermodynamic force above a critical value. Therefore, distance from global equilibrium in the form of magnitude of a thermodynamic force emerges as another constraint of stability; some systems may enhance perturbations, and evolve to highly organized states called the dissipative structures after a critical distance on the thermodynamic branch. Although the kinetics and transport coefficients represent short-range interactions, chemical …