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Articles 5341 - 5370 of 16386

Full-Text Articles in Materials Science and Engineering

Radiopaque Activity Of Iodine Containing Methylene-Bis-Carbamate, Baltabaev Ubaydulla, Djuraev Abdukahhor, Abduvakilov Jahongir, Abdullaeva Matluba Jun 2020

Radiopaque Activity Of Iodine Containing Methylene-Bis-Carbamate, Baltabaev Ubaydulla, Djuraev Abdukahhor, Abduvakilov Jahongir, Abdullaeva Matluba

CHEMISTRY AND CHEMICAL ENGINEERING

Considering that many derivatives of bis carbamates have different biological activity, it was intuitive to produce a targeted synthesis of new derivatives of bis carbamates by the interaction of hexamethylene diisocyanate with 3,5-diode-4-hydroxybenzoic acid and 2,4,6-triiodophenol (1: 2 mol, respectively) in freshly distilled dry pyridine at 95-110 оC for 6 hours, the corresponding derivatives were obtained - methylene bis carbamates. Experimental studies have been conducted to identify the acute toxicity and radiopaque properties of the synthesized new N, -hexamethylene bis (2,6-diode-4-carboxyphenylcarbamate).

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Modification Of Lithium Lubricants, Azimova Shodiyakhon, Arslanov Sharafutdin, Aripdjanov Oybek, Azimov Dilmurod Jun 2020

Modification Of Lithium Lubricants, Azimova Shodiyakhon, Arslanov Sharafutdin, Aripdjanov Oybek, Azimov Dilmurod

CHEMISTRY AND CHEMICAL ENGINEERING

The aim is to study the effect of the presence of free alkalis and acids on the properties of the complex lithium greases and the choice of the optimal dispersion medium, which provides the required physicochemical characteristics of the developed grease. The dispersed phase of lithium greases studied in the polyalphaolefin oils media. It was found that the use of a mixture of polyalphaolefin oil-4 and polyalphaolefin oil-40 as a percentage of 23/77 with a total content of 83.0% provides a relatively low effective viscosity of the lubricant at low temperatures and a relatively high tensile strength at high temperature.

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Effective Oil Extraction From Bombyx Mori Silkworm Pupae And Its Structural Characteristics, Avazova Oynavod, Yugai Sveta, Rashidova Sayora Jun 2020

Effective Oil Extraction From Bombyx Mori Silkworm Pupae And Its Structural Characteristics, Avazova Oynavod, Yugai Sveta, Rashidova Sayora

CHEMISTRY AND CHEMICAL ENGINEERING

The conditions for the effective isolation of oil from the silkworm Bombyx mori pupae, based on the extraction of extracted oil with organic reagents, have been studied. The quantitative content of oil was determined in the samples. It is revealed that the oils extracted using gasoline have a high fat-wax composition compared with ethyl alcohol and hexane. When dried pupae processed with gasoline, it is possible to extract up to 16% of fatty substances as much as possible. Physical-chemical characteristics of the oil from silkworm pupae are characterized by high quality indicators. In particular, the presence of unsaturated fatty acids …

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Composition Of Liquid Paraffins For Flotation Enrichment Of Potassium Chloride, Vaqqosov Sobir, Xolmuratov Shamsitdin, Buxarov Shuhrat, Kodirov Orifjon Jun 2020

Composition Of Liquid Paraffins For Flotation Enrichment Of Potassium Chloride, Vaqqosov Sobir, Xolmuratov Shamsitdin, Buxarov Shuhrat, Kodirov Orifjon

CHEMISTRY AND CHEMICAL ENGINEERING

The purpose of this work is to determine the source of liquid paraffins from secondary products of the local chemical industry, compare the performance properties and use the resulting products as apolar co-reagents in silvinite flotation. The experiments were conducted with secondary used hexane and pyrocondensation. To improve the efficiency of flotation, the dependences of the order of reagent’s supply into the process and the time of action were studied. Experiments have shown that when adding tetradecane and pentadecane in an amount of 2.5 to 7.5% to hexane liquid paraffins, it is possible to reduce the tail of KCl to …

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Influence Of Technological Parameters On The Chemical Composition Of Calcium Polyphosphates From Phosphorites Central Kyzylkum, Ulugberdieva Ziyada, Khujamberdiev Sherzod, Mirzakulov Kholtura, Usmanov Ilkham Jun 2020

Influence Of Technological Parameters On The Chemical Composition Of Calcium Polyphosphates From Phosphorites Central Kyzylkum, Ulugberdieva Ziyada, Khujamberdiev Sherzod, Mirzakulov Kholtura, Usmanov Ilkham

CHEMISTRY AND CHEMICAL ENGINEERING

The aim of the research was to study the effect of temperature, the ratio of P2O5EPA:P2O5PRM and the duration of calcination on the content of various forms of P2O5 in calcium polyphosphate. The effect of calcination temperature from 150 to 300 °C, the ratio of P2O5EPA:P2O5FRM from 2,15 to 4,50 and the duration of the process from 20 to 120 minutes on the changes in various forms of P2O5 were studied. It was shown that with increasing temperature to 200-250 °C the content of the total (ortho + poly) assimilable form of Р2О5 increases and then decreases, passing through a …

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Bases Of Development Of Technologies Of Synthesis Of Oxide Materials In Big Solar Furnace (Parkent), Gulamova Dilbara, Baxronov Khayot, Bobokhulov Sirojiddin, Eshonkulov Elyor Jun 2020

Bases Of Development Of Technologies Of Synthesis Of Oxide Materials In Big Solar Furnace (Parkent), Gulamova Dilbara, Baxronov Khayot, Bobokhulov Sirojiddin, Eshonkulov Elyor

CHEMISTRY AND CHEMICAL ENGINEERING

The advantages of synthesis of complex oxide compounds by solar energy, the possibility of obtaining highly textured nano materials are shown. The development of heliomaterial science, aimed at the synthesis of new materials, is inextricably linked with the use of effective optical energy systems. On the example of obtaining superconducting materials of nominal composition Bi1.7Pb0.3Sr2Ca(n-1)CunOy (n = 3-20), optimization of the parameters of the optical-energy system of the Big Solar Furnace (Parkent) is shown. The ideology of developing heliotechnology for the synthesis of inorganic materials in a solar furnace is presented. The properties of a superconducting material of nominal Bi1.7Pb0.3Sr2Ca(n1)CunOy …

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Study And Characterization Of Conductive Elastomers For Biomedical Applications, Hadis Gharacheh Jun 2020

Study And Characterization Of Conductive Elastomers For Biomedical Applications, Hadis Gharacheh

Theses and Dissertations

Health issues have always been one of humankind's biggest challenges. Over the last century, there has been significant and monumental progress in health and biomedical science, with the end goal of alleviating and eliminating illnesses and ailments. For developing biomedical devices, polymers and elastomers group among other types of biomaterials have been highlighted to be used due to high flexibility, stability, biocompatibility, and mechanical and rheological characteristics. In this work, the characterization of acrylated poly glycerol_sebacate (PGSA) polymer conjugated with bio ionic liquid (BIL) was investigated. Results showed high biocompatibility, high printability with tunable mechanical, adhesive, and conductivity properties. For …

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In Vivo Biosynthesis Of Inorganic Nanomaterials Using Eukaryotes - A Review, Ashiqur Rahman, Julia Lin, Francisco E. Jaramillo, Dennis A. Bazylinski, Clayton Jeffryes, Si Amar Dahoumane Jun 2020

In Vivo Biosynthesis Of Inorganic Nanomaterials Using Eukaryotes - A Review, Ashiqur Rahman, Julia Lin, Francisco E. Jaramillo, Dennis A. Bazylinski, Clayton Jeffryes, Si Amar Dahoumane

Life Sciences Faculty Research

Bionanotechnology, the use of biological resources to produce novel, valuable nanomaterials, has witnessed tremendous developments over the past two decades. This eco-friendly and sustainable approach enables the synthesis of numerous, diverse types of useful nanomaterials for many medical, commercial, and scientific applications. Countless reviews describing the biosynthesis of nanomaterials have been published. However, to the best of our knowledge, no review has been exclusively focused on the in vivo biosynthesis of inorganic nanomaterials. Therefore, the present review is dedicated to filling this gap by describing the many different facets of the in vivo biosynthesis of nanoparticles (NPs) using living eukaryotic …

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Resistive Switching In Atomic Layer Deposited Hfo2/Zro2 Nanolayer Stacks, Lin Tang, Hiraku Maruyama, Taihao Han, Juan C. Nino, Yonghong Chen, Dou Zhang Jun 2020

Resistive Switching In Atomic Layer Deposited Hfo2/Zro2 Nanolayer Stacks, Lin Tang, Hiraku Maruyama, Taihao Han, Juan C. Nino, Yonghong Chen, Dou Zhang

Materials Science and Engineering Faculty Research & Creative Works

The resistive switching properties of HfO2/ZrO2 nanolayers with the total thickness of 16 nm prepared using atomic layer deposition (ALD) were investigated. Current-voltage behavior, pulse time mode measurement, retention and endurance tests were carried out to characterize the memristive (memory-resistive) properties. Resistive switching was observed in all nanolayer stacks, and the set voltage (Vset) decreased with increasing the number of layers (i.e., increasing number of hafnia-zirconia interfaces). Grazing incidence x-ray diffraction (GI-XRD) results demonstrate that the hafnia transforms from monoclinic to orthorhombic crystal structure during the post metallization annealing. Shifts in the binding energy of the x-ray …

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Demonstration Of A Distributed Bragg Reflector For Polyvinylcarbazole And Cadmium Sulfide Layers: Modeling And Comparison To Experimental Results, Javier E. Hasbun, L. Ajith Desilva Jun 2020

Demonstration Of A Distributed Bragg Reflector For Polyvinylcarbazole And Cadmium Sulfide Layers: Modeling And Comparison To Experimental Results, Javier E. Hasbun, L. Ajith Desilva

Georgia Journal of Science

Light wave propagation in a periodically stratified medium has many applications in physics, mathematics, and engineering. The subject is of interest to students, teachers, and researchers, as it presents a great opportunity to focus on principles of optics and to understand the basics of mathematical modeling. A complete theory of wave propagation can be derived using Born’s optics theory. We employed that theory to determine the reflectivity of a one-dimensional distributed Bragg reflector (DBR) and do simulations using MATLAB. A DBR is a photonic crystal consisting of alternating layers of materials with different refractive indices. In this study, we modeled …

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Cancer Biomarker Detection In Human Plasma By Integrating Surface Acoustic Wave And Metal-Enhanced Fluorescence, Yuqi Huang Jun 2020

Cancer Biomarker Detection In Human Plasma By Integrating Surface Acoustic Wave And Metal-Enhanced Fluorescence, Yuqi Huang

USF Tampa Graduate Theses and Dissertations

This thesis includes data and discussion about the technique of metal-enhanced fluorescence (MEF) to lower the detection limit of carcinoembryonic antigen (CEA). The detection limit goes down to 100pg/mL level when using MEF substrate made by rapid thermally annealed silver film covered by silica, which has great promise in diagnosing certain types of cancer that uses CEA as detection biomarker, such as pancreatic cancer and colon cancer. To further address the issue of background noises from non-specifically bound proteins (NSB) in complex media, such as plasma, serum, urine and blood, MEF is integrated with surface acoustic wave (SAW) streaming in …

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Investigation Of Neoprene Medical Gloves: Analysis Of Material Properties, Durability, And Bacterial Barrier Efficacy, Amanda Agui Jun 2020

Investigation Of Neoprene Medical Gloves: Analysis Of Material Properties, Durability, And Bacterial Barrier Efficacy, Amanda Agui

Honors Scholar Theses

This work aims to investigate the material properties, durability, and bacterial barrier efficacy of neoprene for applications in the healthcare/medical field. A special focus on material stiffness and fatigue failure will be explored. Additionally, manufacturer regulations and testing will be inspected to ensure medical gloves made of neoprene blends have a proper lifespan for its desired application in the healthcare community. The resistance of protective gloves and its ability to withstand perforation failure will be investigated to guarantee the safety of users holds extreme importance. Lastly, an analysis of the bacterial barrier efficacy of neoprene gloves will be determined.

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Preparation Of Glass Ionomer Cement From Recycled Low Alumina Glass, Sura S. Al-Tae'e, Ola M. Almitwalli, Saad B. H. Farid Jun 2020

Preparation Of Glass Ionomer Cement From Recycled Low Alumina Glass, Sura S. Al-Tae'e, Ola M. Almitwalli, Saad B. H. Farid

Karbala International Journal of Modern Science

Fluoroaluminosilicate glass was prepared from recycled low alumina glass, with the additions of AlF3 and CaF. That was to provide a cheap source of proper glass required to prepare glass ionomer cement GIC. Three batches of the fluoroaluminosilicate glass were prepared with different additions of CaF varied at the expense of AlF3. i.e., the glass was prepared with three different CaO contents. The prepared glasses were used as an essential part of GICs. It was found that a crystalline phase (fluorapatite) appeared as part of the set cement matrix. The XRD of the set cements indicated that …

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Recent Advances In Electrospun Sustainable Composites For Biomedical, Environmental, Energy, And Packaging Applications., Hao Liu, Christopher R Gough, Qianqian Deng, Zhenggui Gu, Fang Wang, Xiao Hu Jun 2020

Recent Advances In Electrospun Sustainable Composites For Biomedical, Environmental, Energy, And Packaging Applications., Hao Liu, Christopher R Gough, Qianqian Deng, Zhenggui Gu, Fang Wang, Xiao Hu

College of Science & Mathematics Departmental Research

Electrospinning has gained constant enthusiasm and wide interest as a novel sustainable material processing technique due to its ease of operation and wide adaptability for fabricating eco-friendly fibers on a nanoscale. In addition, the device working parameters, spinning solution properties, and the environmental factors can have a significant effect on the fibers' morphology during electrospinning. This review summarizes the newly developed principles and influence factors for electrospinning technology in the past five years, including these factors' interactions with the electrospinning mechanism as well as its most recent applications of electrospun natural or sustainable composite materials in biology, environmental protection, energy, …

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Fabrication Of Magnetocaloric La(Fe,Si)13 Thick Films, N H. Dung, N B. Doan, P De Rango, L Ranno, Karl G. Sandeman, N M. Dempsey Jun 2020

Fabrication Of Magnetocaloric La(Fe,Si)13 Thick Films, N H. Dung, N B. Doan, P De Rango, L Ranno, Karl G. Sandeman, N M. Dempsey

Publications and Research

La(Fe,Si)13–based compounds are considered to be very promising magnetocaloric materials for magnetic refrigeration applications. Many studies have focused on this material family but only in bulk form. In this paper we report on the fabrication of thick films of La(Fe,Si)13, both with and without post-hydriding. These films exhibit magnetic and structural properties comparable to bulk materials. We also observe that the ferromagnetic phase transition has a negative thermal hysteresis, a phenomenon not previously found in this material but which may have its origins in the availability of a strain energy reservoir, as in the cases of …

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Tribological Properties Of Polymeric Composites: A Review, Yusuf Şahin, Hakan Şahin Jun 2020

Tribological Properties Of Polymeric Composites: A Review, Yusuf Şahin, Hakan Şahin

Journal of Metals, Materials and Minerals

Tribology deals with interacting surfaces in sliding, rolling or any others types of motions, which is much importance in designing for machine components to improve their durability's of mechanical engineering systems. This study overviews the most recent studies on the tribological behavior of polymeric based materials containing different fillers. Some microstructural and mechanical properties of the epoxy composite are introduced. In addition, mechanisms of increasing wear resistance and reducing friction coefficient for polymeric composites are reviewed. An overview is also covered the process optimization for the dry wear results of polymeric composites using Taguchi Method (TM) and Response Surface Method …

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Ceramic And Glass-Ceramic Fillers In Dental Composites: A Review, Sumana Ghosh Jun 2020

Ceramic And Glass-Ceramic Fillers In Dental Composites: A Review, Sumana Ghosh

Journal of Metals, Materials and Minerals

Dental composite fillings are most popular fillings wherein various fillers have been suitably dispersed in a polymerizable resin. Major challenges are to make choice of suitable filler and their distribution in the resin matrix in the development of the dental fillings. Apart from traditional fillers ceramic whiskers, glass fibres, branched fibres and nanoporous powders have also been investigated as fillers in dental composites. Recently, ceramic, and glass-ceramic fillers are attracting attention of the researchers due to their suitable combination of material properties. In the current paper, the prospect of ceramic and glass-ceramics as fillers in fabricating dental composites has been …

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Synthesis And Characterization Of Ball-Milled Eggshell And Al2o3 Reinforced Hybrid Green Composite Material, Shrawan Kumar, Shashi Prakash Dwivedi, Vijay Kumar Dwived Jun 2020

Synthesis And Characterization Of Ball-Milled Eggshell And Al2o3 Reinforced Hybrid Green Composite Material, Shrawan Kumar, Shashi Prakash Dwivedi, Vijay Kumar Dwived

Journal of Metals, Materials and Minerals

Eggshell is a by-product (a secondary product derived from a production process) which produces lots of environment pollution. However, some environment pollution can be reduced by utilizing this waste. In the present investigation, an attempt was made to utilize eggshell as the reinforcement material with alumina (Al2O3) in the development of composite material. Carbonized eggshell particles and Al2O3 ceramic particles were ball-milled up to 100 hours to obtain a uniform particle size of reinforcement particles. Results showed that by using Al2O3 with eggshell in the development of aluminium based composite material after the ball-milling, mechanical properties were significantly improved. However, …

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Green-Based Corrosion Protection For Mild Steel In 3.5% Nacl And Distilled Water Medias: Jatropha Curcas And Roselle Extracts, Muhammad A. Afandi, Safaa N. Saud, Esah Hamzah Jun 2020

Green-Based Corrosion Protection For Mild Steel In 3.5% Nacl And Distilled Water Medias: Jatropha Curcas And Roselle Extracts, Muhammad A. Afandi, Safaa N. Saud, Esah Hamzah

Journal of Metals, Materials and Minerals

In this study, the natural sources of Jatropha curcas and Hibiscus Sabdariffa calynx (Roselle) extracts as green corrosion inhibitors were employed to improve the corrosion resistance of mild steel in simulated (3.5% NaCl) and distilled water medias. The inhibiting performance of two types of extracts was studied by visual inspection, microscope analysis, and various electrochemical measurements and the data of corrosion rate were statistically analyzed. The main phenolic compounds of Jatropha and Roselle extracts were confirmed via a liquid chromatography-mass spectrometry. Meanwhile, the functional groups of active phytochemical compounds were characterized via attenuated total reflection spectroscopy (ATR). The results of …

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Optimization And Longevity Of Functionalized Multi-Walled Carbon Nanotube-Enabled Membranes For Water Treatment, Madeleine Michael Isabella White Jun 2020

Optimization And Longevity Of Functionalized Multi-Walled Carbon Nanotube-Enabled Membranes For Water Treatment, Madeleine Michael Isabella White

Master's Theses

Water scarcity is a growing concern at the global scale. Large scale water reuse is growing both in necessity and popularity. Before water reuse can be performed efficiently on a large scale or be used for potable supply, even indirectly, contaminants of emerging concern (CECs) will need to be treated at the full scale. Advanced oxidation processes (AOPs) are a form of advanced water treatment capable of treating a wide range of CECs. This study contributes to the growing field of AOPs and more specifically AOPs using ozone combined with functionalized multi-walled carbon nanotubes (MWCNTs). Ozonation of MWCNTs has been …

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Thermal Properties Of Sodium Borosilicate Glasses As A Function Of Sulfur Content, Jason M. Lonergan, Charmayne Lonergan, Joshua Silverstein, Pornsinee Cholsaipant, John Mccloy Jun 2020

Thermal Properties Of Sodium Borosilicate Glasses As A Function Of Sulfur Content, Jason M. Lonergan, Charmayne Lonergan, Joshua Silverstein, Pornsinee Cholsaipant, John Mccloy

Materials Science and Engineering Faculty Research & Creative Works

Sulfur trioxide (SO3) additions, up to 3.0 mass%, were systematically investigated for effects on the physical properties of sodium borosilicate glass melted in air, with a sulfur-free composition of 50SiO2–10Al2O3–12B2O3–21Na2O–7CaO (mass%). Solubility measurements, using electron microscopy chemical analysis, determined the maximum loading to be ~1.2 mass% SO3. It was found that measured sulfur (here as sulfate) additions up to 1.18 mass% increased the glass transition temperature by 3%, thermal diffusivity by 11%, heat capacity by 10%, and thermal conductivity by 20%, and decreased the …

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Prediction Of Flotation Efficiency Of Metal Sulfides Using An Original Hybrid Machine Learning Model, Rachel Cook, Keitumetse Cathrine Monyake, Muhammad Badar Hayat, Aditya Kumar, Lana Alagha Jun 2020

Prediction Of Flotation Efficiency Of Metal Sulfides Using An Original Hybrid Machine Learning Model, Rachel Cook, Keitumetse Cathrine Monyake, Muhammad Badar Hayat, Aditya Kumar, Lana Alagha

Materials Science and Engineering Faculty Research & Creative Works

Froth flotation process is extensively used for selective separation of base metal sulfides from uneconomic mineral resources. Reliable prediction of process outcomes (metal recovery and grade) is vital to ensure peak performance. This work employs an innovative hybrid machine learning (ML) model—constructed by combining the random forest model and the firefly algorithm—to predict froth flotation efficiency of galena and chalcopyrite in relation to various experimental process parameters. The hybrid model's prediction performance was rigorously evaluated and compared against four different standalone ML models. The outcomes of this study illustrate that the hybrid ML model has the prediction ability to process …

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Development Of Reduced Chemical Kinetic Models For The Numerical Simulation Of Combustion And Emissions Behavior Of Representative Conventional And Bio-Derived Fuels, Mazen A. Eldeeb Jun 2020

Development Of Reduced Chemical Kinetic Models For The Numerical Simulation Of Combustion And Emissions Behavior Of Representative Conventional And Bio-Derived Fuels, Mazen A. Eldeeb

Mineta Transportation Institute

The study addresses two of the main challenges facing combustion modeling for transportation fuels: simultaneous simulation of non-related combustion problems and reducing the computational cost of the modeling process itself. To address the first challenge, researchers determine a characteristic flame time from thermal diffusivity and laminar burning velocity. Researchers examine parametric dependence of flame time and ignition delay time on pressure, temperature and equivalence ratio for methane, based on validated chemical kinetic mechanisms. The study reveals flame time and ignition delay time show similar temperature dependence, flame time has stronger dependence on equivalence ratio and weaker dependence on pressure than …

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Design For Additive Manufacturing, Michael Charonnat, Leonardo Franco-Muñoz, Sam Noble, J.P. Purdom Jun 2020

Design For Additive Manufacturing, Michael Charonnat, Leonardo Franco-Muñoz, Sam Noble, J.P. Purdom

Mechanical Engineering

This document outlines the critical design details and timeline for the Design for Additive Manufacturing Senior Project sponsored by Solar Turbines, Inc. The scope of this project encompasses the redesign of two of Solar Turbine’s cast parts for metal additive manufacturing in order to minimize lead time, cost, and weight. With the overall objective of performing in-depth analysis exploring affordability & feasibility, this redesign process will aid Solar Turbines in expanding their knowledge of Design for Additive Manufacturing principles and enable them to further incorporate the use of additive manufacturing into their production processes. The first part that the team …

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Xas Analysis Of Copper Binding In Soils, Wapakorn Siriwong, Penphitcha Amonpattaratkit, Wantana Klysubun Jun 2020

Xas Analysis Of Copper Binding In Soils, Wapakorn Siriwong, Penphitcha Amonpattaratkit, Wantana Klysubun

Journal of Metals, Materials and Minerals

Ecological distribution of copper from soil is depended on its bioavailability and mobility. Copper binding on heterogeneous soil composition is a key information for understanding the long-term fate benefiting suitable management practice for copper in the environment. X-ray absorption spectroscopy (XAS) techniques were used to provide microscopic scale information of copper-binding on different soils. Soil samples containing 14.9-56.6% clay and 0.5-3.4% organic matter were studied. Dry-powder soil samples containing approximated 0.3% copper from batch equilibrated equilibrium experiments were analyzed. Copper K-edge spectrum were collected at the Synchrotron light research institute (SLRI), Thailand in X-ray absorption near edge structure (XANES) and …

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Preparation Of Alginate/2-Hydroxyethyl Methacrylate Composite Beads: Role Of Fillers And Characteristics Of Bead Formation, Somkiet Urusetthanon, Somchai Udon, Boonsri Kusuktham Jun 2020

Preparation Of Alginate/2-Hydroxyethyl Methacrylate Composite Beads: Role Of Fillers And Characteristics Of Bead Formation, Somkiet Urusetthanon, Somchai Udon, Boonsri Kusuktham

Journal of Metals, Materials and Minerals

In this research, alginate composite beads were prepared. The objective was to study the effect of particle size of fillers on the viscosity of alginate solution and bead formation. The sodium alginate solution with and without 2-hydroxyethyl methacrylate was dropped into calcium chloride to form the beads. The polymerization of the 2-hydroxyethyl methacrylate in the alginate matrix was occurred by using potassium persulphate as an initiator and N,N/-methylenebisacrylamide as a crosslinking agent and N,N,N/,N/ -tetramethylethylenediamine in the calcium chloride solution as an accelerator. For the preparation of the composite beads, the cotton dust, and sawdust at various ratios were mixed …

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Synthesis And Fabrication Of Polyaniline/Eggshell Composite In Ammonia Detection, Nurul Aqilla Mazlan, Jamil M. Sapari, Kavirajaa Pandian Sambasevam Jun 2020

Synthesis And Fabrication Of Polyaniline/Eggshell Composite In Ammonia Detection, Nurul Aqilla Mazlan, Jamil M. Sapari, Kavirajaa Pandian Sambasevam

Journal of Metals, Materials and Minerals

This study focuses on the measurement and performance of bio-filler composite based on polyaniline (PANI)/chicken eggshell (CES). The composite films were prepared via ex-situ polymerisation using DBSA as its dopant. The PANI solution was distributed equally before mixing it with three different ratios of CES powder. Characterisations of the composite films were analysed using Fourier-transform infrared spectroscopy (FTIR) and Ultraviolet-visible spectroscopy (UV-Vis), Scanning electron microscope/energy dispersive x-ray (SEM/EDX) and multimeter. PANI film that contained 20mg CES filler possessed the highest conductivity and the fastest time to achieve 90% of sensitivity. The film was also very selective towards ammonia gas and …

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Dry-Sliding Wear Of The 316l/H-Bn Composites Produced Under Crack Ammonia Atmosphere, Ekkarat Chusong, Panya Kansuwan, Naoto Ohtake, Pongsak Wila, Nattaya Tosangthum, Ruangdaj Tongsri Jun 2020

Dry-Sliding Wear Of The 316l/H-Bn Composites Produced Under Crack Ammonia Atmosphere, Ekkarat Chusong, Panya Kansuwan, Naoto Ohtake, Pongsak Wila, Nattaya Tosangthum, Ruangdaj Tongsri

Journal of Metals, Materials and Minerals

Wear is one of different problems in mechanical failures of moving components. When a component encounters friction force on its surface, crack initiation tends to occur and wear follows crack propagation. Thus, the moving parts of automobiles should have proper wear resistance for long-time services, in addition to having high strength and hardness for heavy load operation. A self-lubricating material with compromised tribological and mechanical properties is important for some moving components. In this work, self-lubricating composites, metal matrix composites embedded with a solid lubricant, made from 316L stainless steel powder mixed with different hexagonal boron nitride (h-BN) contents of …

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Synthesis Of Hydroxyapatite From Cuttlebone Under Various Ph Conditions: An Approach For Medical Materials, Sineenart Kangkan, Premjit Arpornmaeklong, Sarute Ummartyotin Jun 2020

Synthesis Of Hydroxyapatite From Cuttlebone Under Various Ph Conditions: An Approach For Medical Materials, Sineenart Kangkan, Premjit Arpornmaeklong, Sarute Ummartyotin

Journal of Metals, Materials and Minerals

To support the bio-based economy, development on hydroxyapatite from cuttlebone was investigated. Cuttlebone is naturally occurring source of calcium. We calcined it at 700°C for 4 h to form a calcium oxide powder. Hydroxyapatite was coprecipitated with calcium oxide powder and phosphoric acid. The effect of the pH ranging from 6 - 10 was controlled by adding ammonium hydroxide. Fourier transform infrared and X-ray diffraction were employed to characterize the structural properties of the hydroxyapatite. Changes in pH did not affect the structural properties of the hydroxyapatite. Thermogravimetric analysis revealed that the hydroxyapatite was thermally stable up to 700°C. At …

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Insearchfornear-Room-Temperaturesuperconductingcriticaltemperatureofmetalsuperhydridesunderhighpressure: A Review, Udomsilp Pinsook Jun 2020

Insearchfornear-Room-Temperaturesuperconductingcriticaltemperatureofmetalsuperhydridesunderhighpressure: A Review, Udomsilp Pinsook

Journal of Metals, Materials and Minerals

An overview and the latest status of the superconductivity of metal superhydrides under high pressure are discussed in this review article. The searching for near-room-temperature superconductors have been one of the most enthusiastic fields in physics. This is because of several key factors in both theoretical and experimental sides. By advanced experiment innovation, pressure exceeded that of the earth's core can be generated in laboratories. This allows scientists to explore new physics of materials under high pressure. In the synergy form, the theoretical calculation gives accountable predictions on the structural and electronic properties which can be served as a practical …

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