Materials Science and Engineering Commons^™

Synchrotron X-Ray Diffraction Method For Continuous Strain Analysis Across Heterogenous Material Interface Layers, Sierra Damon

Discovery Day - Daytona Beach

Synchrotron X-ray diffraction method for continuous strain analysis across heterogenous material interface layers   The transfer of strain across a material interface is a relevant concept to quantify for numerous aerospace applications that involve coatings applied to substrates of different materials, particularly in the field of high temperature materials. X-ray diffraction (XRD) is a metrology technique capable of resolving strain within an arbitrary material by quantifying the shifts of Bragg peaks with respect to an unstrained sample and has seen increased use due to the capability of XRD to perform in-situ measurements on materials in extreme environments. Since different materials have …

Spark Plasma Sintering Of Alumina With Controlled Porosity, Harshail Patet

Discovery Day - Daytona Beach

Alumina is one of the most widely used advanced ceramics, serving applications that range from dense structural and wear-resistant components to porous thermal insulation and filtration systems. Porosity is a defining microstructural feature that governs mechanical strength, thermal conductivity, and permeability, meaning different applications demand different porosity levels from the same material. Spark plasma sintering (SPS) enables rapid consolidation by simultaneously applying pulsed electric current and uniaxial pressure, offering precise control over density, grain size, and porosity in significantly shorter processing times than conventional sintering. While prior studies have investigated the individual effects of SPS parameters on alumina densification, a …

Advanced Manufacturing And Materials Of A Bio-Mimetic Hoof For Space Robotics Applications, Benjamin Heckel

Discovery Day - Daytona Beach

Planetary surfaces often feature steep, uneven, and unpredictable terrain conditions that resemble some of the most challenging natural environments on Earth. In these terrestrial settings, certain animals have evolved to navigate complex landscapes with remarkable agility. One example is the mountain goat, an animal whose hooves have evolved for stable and precise movement across rocky, inclined surfaces. This biological adaptation provides a useful model for improving robotic mobility in planetary exploration. This study draws inspiration from that natural adaptation to develop a bio-mimetic robotic hoof designed to enhance traction, durability, and adaptability for extraterrestrial exploration. By replicating the mechanical properties …

Additive Manufacturing Of Metals: Mechanical Properties And Their Implications, Sean Chih

Discovery Day - Daytona Beach

Additive manufacturing of metals is a relatively new and groundbreaking approach to manufacturing high-performance components. However, variability in mechanical properties from the process creates a barrier before this manufacturing technique can be widely applied. Understanding when and where to use this manufacturing is also important to create components with efficiency and without harmful defects. The objective of this research is to evaluate the effects of build orientation, printing parameters, internal defects, thermal history, and residual stresses, post-processing heat treatments, and fatigue behavior on additively manufactured components. Literature-based research is conducted on commonly used metals for additive manufacturing, such as stainless …

Cavitation In Pumps And Propellers: Causes, Effects, Prevention, And Future Trends, Gillian Negron Burgos, Olivia Wilson

Discovery Day - Daytona Beach

In this research, we will explore cavitation in pumps and propellers, including its causes, effects on system performance, prevention methods, and future engineering solutions. Cavitation occurs when the local pressure of a flowing liquid drops below its vapor pressure, forming vapor-filled bubbles that collapse and damage mechanical components. Disciplines such as fluid mechanics, thermodynamics, and materials science contribute to understanding and mitigating cavitation in fluid machinery.   When vapor bubbles collapse near metal surfaces, they generate localized shock waves that cause pitting, erosion, vibration, and noise. These effects reduce efficiency, increase maintenance requirements, and shorten the lifespan of rotating machinery used …

Improving Direct Reduced Iron Briquette Properties, Abigail Clark

Honors Theses

Fines are generated during the reduction, handling, and transportation of iron oxide pellets and lump ore. These fines present significant safety concerns due to their tendency to oxidize rapidly and combust spontaneously. In addition, they contribute to material losses and reduced revenue. However, DRI fines can be recycled through briquetting and reused in downstream steelmaking processes. Briquettes are produced by agglomerating and compacting direct reduced iron (DRI) fines with binders such as molasses and lime, calcium stearate, and bentonite. Although many different binders have been developed and studied for iron oxide agglomeration and induration, far fewer studies have been conducted …

Selective Oxidation And Reduction For Recycling Samarium-Cobalt Permanent Magnets, Mitchell Harvey

Honors Theses

Samarium cobalt (SmCo) based magnets are among the strongest permanent magnets second only to neodymium iron boron (NdFeB) based magnets. While SmCo-based magnets have lower remanence and coercivity than NdFeB-based magnets at room temperature, SmCo-based magnets retain these properties better at higher temperatures. As a result, SmCo-based magnets find use in a variety of devices operating at elevated temperatures including traveling wave tubes for satellite communications, electrical generators, and control surface actuators for aviation system. With increasing geopolitical tension over the sourcing of Sm and Co, there is a renewed interest in recycling end-of-life SmCo-based magnets. This work explores a …

65th Annual Rocky Mountain Conference On Magnetic Resonance

Rocky Mountain Conference on Magnetic Resonance

Conference program, abstracts, and information about the 65th annual meeting of the Rocky Mountain Conference on Magnetic Resonance. Held in the Snowbird Resort and Conference Center, Snowbird, Utah, August 2-6, 2026.

A Semantic Data Management Framework For Uncertainty Quantification In Synchrotron Diffraction Pattern Analysis, Ayorinde E. Olatunde, Ozan Dernek, Erika I. Barcelos, Roger H. French, Anirban Mondal

Student Scholarship

Advancements in technology have enabled scientists and engineers in the synchrotron science domain to generate high-dimensional data. To conduct a machine learning study on these data, an analyst undergoes multiple analytical stages, including dimensionality reduction, predictive modelling, and uncertainty quantification (UQ).

To ensure reproducibility in science, it is necessary to document the semantic relationships among the stages of the analysis to enable provenance, interoperability, and knowledge reuse. In this work, we present a Semantic Data Management (SDM) framework rooted in FAIR principles that provides ontologies for UQ workflows. We illustrate the application of UQ ontology in synchrotron diffraction pattern analyses …

Synthesis And Characterization Of Carbon Quantum Dots And Gold Nanoparticles For Norovirus Biosensing Applications In Water Systems, Breanne Evans

Master's Theses

Rapid, reliable detection of viral pathogens remains a significant challenge across water-treatment and environmental monitoring systems, including drinking-water, wastewater, water reuse, and environmental surveillance applications. Waterborne viral contamination can pose substantial public-health risks, making early detection essential for protecting water quality and responding quickly to treatment failures or contamination events. Direct potable reuse (DPR) is one particularly demanding example because it requires continuous verification of treatment performance and the broader need for rapid virus monitoring extends across many water-treatment and environmental surveillance applications. Norovirus is a priority target because of its widespread occurrence in wastewater, environmental persistence, and exceptionally low …

Effect Of Rheology Modification On Fiber Orientation And Dispersion In 3d-Printed Ultra-High-Performance Concrete, Haodao Li, Alfred Addai-Nimoh, Seongho Han, Kamal H. Khayat

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

The extrusion process in 3D concrete printing (3DCP) facilitates horizontal alignment of steel fibers along the printing direction, thus enhancing the load-bearing capacity of printed elements. However, such shear-induced fiber alignment is highly sensitive to rheological properties. This study investigates how variations in dynamic yield stress (τd) and plastic viscosity (μ), influence the extrudability, fiber orientation and dispersion, and anisotropic mechanical behavior of ultra-high-performance concrete (UHPC). Five viscosity-modifying agent (VMA) types were incorporated at two content levels to modify the rheology of printable UHPC. Results showed that moderate VMA additions improved printability, whereas excessive contents markedly increased τd and μ; …

Review: Mechanics Of Mycelium Materials, Md Anwar Sadat Anik, Ehsanul Azim, Gerardo I. Zapata, Mohammad R. Islam

Mechanical Engineering Faculty Publications

The biological growth of fungal root structure, called mycelium, can be engineered to develop innovative fibrous and biocomposite materials. Mycelium materials have potential as sustainable alternatives to petroleum-derived materials for load-bearing applications. To realize this potential, there is an increasing effort dedicated to understanding the mechanics of mycelium materials. This work presents a systematic review of our current understanding of the mechanics of mycelium materials with a specific focus on structure–property relationships. The review first explores how the mycelium’s fiber network structure varies depending on whether it is grown as a two-dimensional (2D) membrane, a cellular foam, or as a …

Thermal Degradation Analysis Of Bagasse Fibers From Sugarcane Waste, Rashmitha Suresh, Faisal Al Nasser

Journal of Mechanical Engineering Science and Technology (JMEST)

Sugarcane is one of the important commodities in the industry where bagasse fiber as waste is abundantly available.   Sugarcane bagasse fiber has high cellulose, a key element in the utilization of bagasse. Chemical pretreatment is important to prepare the natural fiber before used as composite reinforcement. The purpose of the study is to analyze the thermal degradation of bagasse fiber after being treated using NaOH and TEMPO solution. The manufacturing method was carried out by a series of washing bagasse with distilled water and NaOH solution, subsequently soaking it in 6% NaOH and 2,2,6,6-tetramethylpiperidine-l-oxyl (TEMPO) solution, and conducted oven-dried. Thermogravimetric …

Investigating The Corrosion Behavior Of Stainless Steel 316 In Static Lead Lithium Eutectic Under Applied Stressed Conditions, Daniel E. Levario

Nuclear Engineering ETDs

As fusion power moves closer to feasibility, identifying structural materials compatible with breeding blanket environments remains a critical challenge. Lead-lithium eutectic (LLE) is a leading candidate breeder and coolant material due to its low melting point and combined tritium breeding and neutron multiplication capability. However, the corrosive nature of LLE toward structural steels at elevated temperatures must be characterized before these systems can be reliably deployed. This study investigates the corrosion behavior of Type 316 stainless steel in static LLE under applied stress conditions at 550°C using C-ring stress corrosion specimens. Post exposure analysis via optical microscopy, SEM, EDS, and …

Dynamic Reconstruction Engineering Of Anti-Corrosion Ni-Based Anodes For Alkaline Seawater Electrolysis, Yi-Gang Zhang, Wen-Wen Xu, Tian-Yu Zhang, Zhi-Yi Lu

Journal of Electrochemistry

Green hydrogen production via alkaline seawater electrolysis offers an environmentally sustainable and potentially cost-effective route to address both energy and climate challenges. Achieving long-term anode stability under complex ionic environments and industrial current densities remains a central bottleneck. Specifically, Ni-based anodes exhibit intense surface reconstruction during the oxygen evolution reaction, necessitating dynamic anti-corrosion strategies. This mini review systematically summarizes reconstruction engineering approaches to develop anti-corrosion Ni-based anodes of alkaline seawater electrolysis across increasingly complex ionic environments from simulated seawater to real seawater: (i) Cl^– dominated; (ii) Cl^– with co-existing oxyanions, and (iii) Cl^–  with co-existing Br^{– …}

Preparation And Performance Study Of In-Situ Self-Assembled Biphasic Smmn2O5-Nimn2O4 Composite Cathode, Neng-Chu Xia, Yu Zhou, Qin Wang, Jia-You Zhang, Chun Yu, Yang Zhang, Wan-Bing Guan, Jian-Xin Wang

Journal of Electrochemistry

Mullite-structured oxides exhibit excellent oxygen reduction reaction activity, possess a low thermal expansion coefficient due to their unique crystal structure, and can eliminate the need for a barrier layer and simplify the preparation process as they contain no alkaline earth elements. Thus, they hold great promise as novel cathode materials for solid oxide fuel cells. In this work, a mullite-spinel-structured SmMn₂O₅-NiMn₂O₄ (SMO-NMO) composite cathode was one-step synthesized via a solid-liquid composite route, and its in-situ self-assembly enabled good compatibility with the electrolyte without any barrier layer. Characterization results showed that the SMO:NMO = …

In-Situ Stm Visualization Of Molecular Structural Evolution During Electrochemical Oxidation Coupling Of Para-Aminothiophenol On Au(111), Zi-Wei Ma, Tai-Rui Wu, An-Ni Zheng, Lai-Ke Chen, Yuan-Hui Xiao, Zhao-Bin Chen, Qing-Na Zheng, Jian-Zhang Zhou, Jia-Wei Yan, De-Yin Wu

Journal of Electrochemistry

Para-aminothiophenol (PATP) is not only a widely-used probe molecule in the field of surface-enhanced Raman spectroscopy (SERS), but also an important model molecule for interfacial reactions, exhibiting distinct photo- and electro-oxidation pathways, so that PATP is selectively activated under different external fields. The evolution of products and intermediates during electrochemical oxidative coupling remains unknown. In this study, we have investigated the dynamic electrochemical oxidation process of PATP on the Au(111) surface using cyclic voltammetry, electrochemical (EC)-SERS, and in situ electrochemical scanning tunneling microscopy (EC-STM). The results showed that PATP forms an unsaturated adsorption coverage on Au(111) in an acidic solution. …

A Multidimensional Conceptual Framework For Supportive Outdoor Environments In Healthcare Settings, Mona Ali, Dalia A. Beheiry, Rowaida Kamel, Hammam Serageldin

HBRC Journal

The integration of supportive outdoor environments (SOEs) in healthcare settings has gained increasing attention for their potential to enhance patient recovery, support staff well-being, and contribute to holistic therapeutic outcomes. This scoping review examines design recommendations for inclusive outdoor environments in healthcare settings that impact user health and experience. Guided by the Joanna Briggs Institute (JBI) framework for scoping reviews, a comprehensive search was conducted across five databases (Google Scholar, PubMed, ScienceDirect, JSTOR, Sage), yielding 697 records. Following screening and applying the inclusion and exclusion criteria, 18 articles were selected for analysis. This scoping review identified consistent evidence linking outdoor …

Analysis Of Electronic Control Unit Optimization On The Performance Of A 150 Cc Motorcycle Engine Using Ethanol-Blended Fuel, Agus Achmad Syaiful, Annisa Bhikuning, Muhammad Rizal Baihaqi, Muhammad Aulia Rafli

Journal of Mechanical Engineering Science and Technology (JMEST)

The use of ethanol-blended fuel in a standard vehicle can reduce combustion quality, which has an impact on decreasing vehicle performance. At the above 20% blend level, it affects vehicle performance and requires adjustments to engine settings or the Electronic Control Unit (ECU) before use on conventional engines. This study investigates the effect of aftermarket ECU settings on the performance of a 150 cc motorcycle operating on a gasoline-ethanol blend. Four fuel variations were tested: Pertalite (P100), revvo 90 (R100), and 30% ethanol blends (PE30 and RE30). This study analyzes the effects of optimizing injection duration and ignition timing settings …

Chemical Composition Stability Of Cu–Sn And Cu–Zn Journal Bechemical Composition Stability Of Cu–Sn And Cu–Zn Alloys Fabricated By Sand And Permanent Mold Casting With Nickel Alloying, Erwin Erwin, Didik Sugiyanto, Juan Pratama, Trisna Ardi Wiradinata, Abdul Rachmadhan, Muhammad Fikri Andika

Journal of Mechanical Engineering Science and Technology (JMEST)

The processes of moulding and reinforcing chemical elements have a big impact on the balance of chemical composition in copper-based bearing alloys. This has a direct impact on how well the material works. This study examines Cu–Sn alloys produced via sand casting and Cu–Zn alloys fabricated through permanent mould casting, with the incorporation of nickel, which remains uncommon. The objective was to examine the variations in the equilibrium of the chemical composition and the performance potential of the bearing alloy metal when subjected to different casting techniques and nickel concentrations ranging from 0% to 4%. Some of the methods used …

Effect Of Concentration And Temperature Of Tio2-Al2o3 Hybrid Nanofluid On The Corrosion Rate Of Aluminum Radiator, Ratna Monasari, Rizky Maulana Ramadhan, Nike Nur Farida, Ahmad Hanif Firdaus, Supa Kusuma Aji, Yuniarto Agus Winoko, Rizkyansyah Alif Hidayatullah

Journal of Mechanical Engineering Science and Technology (JMEST)

Corrosion of aluminum radiators can reduce cooling system reliability and shorten service life in automotive applications. This study examines the effect of TiO₂-Al₂O₃ hybrid nanofluid concentration and temperature on the corrosion rate of commercially available aluminum radiator material. Hybrid nanoparticles with a TiO₂-Al₂O₃ mass ratio of 50:50 were dispersed in distilled water at concentrations of 0.6 wt.%, 0.8 wt.%, and 1.0 wt.%. Corrosion behavior was evaluated using a 14-day accelerated immersion test at 60°C and 80°C, and the corrosion rate was determined using the gravimetric mass loss method. The results …

Straw As A Potential Vegetable Fibre Insulative Infill In Framed Constructions - Material Testing\Tnotereftnote1, Patrick Daly

Journal of Sustainable Construction Materials and Technologies

The construction sector faces increasing pressure to reduce embodied carbon and adopt circular material strategies, with bio-based materials offering a promising pathway. Straw-based insulation, particularly in loose-fill form, has gained traction in Europe, where several products have achieved certification under EAD 040138-01-1201. This study investigates the potential of Irish-processed straw chip as a bio-based insulative infill for framed construction by evaluating its material properties and thermal conductivity–density performance relative to European ETA-certified reference products. A programme of laboratory testing was undertaken on commercially available Irish straw samples, including material characterisation (moisture content, particle morphology, and dust content) and thermal conductivity …

Development And Characterization Of Mycelium-Based Biocomposites From Ganoderma Lucidum Using Spent Yerba Mate And Residual Sunflower Oil For Sustainable Insulation In Construction, Paula V. Alfieri, Guadalupe Canosa

Journal of Sustainable Construction Materials and Technologies

The construction industry urgently requires sustainable alternatives to petroleum-based insulation materials such as expanded polystyrene (EPS) and mineral wool. Mycelium-based biocomposites offer a promising solution by valorizing agricultural waste while delivering competitive thermal and acoustic performance. In this study, developed and characterized biocomposites using Ganoderma lucidum mycelium combined with spent yerba mate and residual sunflower oil (70 g/30 mL), both commonly generated as waste in Argentine institutions. Two formulations were evaluated: high density (HD: 280 ± 5 kg/m³) and low density (LD: 185 ± 5 kg/m³). Samples were cultivated for 90 days at 28 °C and 65% relative humidity and …

Comparative Life Cycle Assessment Of Hemp Walls In Residential Construction In Morocco, Hicham Kaddouri, Rachida Elbarghmi, Firyal Latrache, Marwane Hammouti, Abderrahim Abidouche, Ismael Driouch

Journal of Sustainable Construction Materials and Technologies

This study analyzes the energy and environmental performance of hemp-based wall solutions applied to Moroccan residential buildings by combining dynamic thermal simulation and life cycle assessment (LCA). A reference building is assessed under four representative Moroccan climates (Al Hoceima, Oujda, Marrakech, and Ouarzazate), comparing a conventional wall retrofitted with hemp plaster and a wall incorporating hemp concrete. The results show that hemp concrete significantly reduces annual heating and cooling energy demands by 20–24% depending on the climate, with heating needs decreasing by up to 40% and cooling needs by approximately 15%, particularly in hot and arid regions. The LCA reveals …

Dual-Waste Integration For Geotechnical Improvement: Silica Fume And Eggshell Ash In Kaolin Soil Stabilization, Ng Jun Shen, Muzamir Hasan, Siti Sarah Eliyun, Md. Ikramul Hoque, Mohamad Afiq Jazrin Mohamad Sidek

Journal of Sustainable Construction Materials and Technologies

This study reveals the potential substitution of silica fume and eggshell ash in the technique of soil stabilization, varying across distinct proportions in the modification of geotechnical parameters. The untreated kaolinitic soil which has low soil bearing capacity in nature is frequently reflected in its mechanical instability, for instance, soil settlement and extreme compressibility. By associating the industrial and agricultural material, it is potentially to resolve the above-mentioned issues with explicit designs. A number of laboratory approaches have been implemented in the assessment of basic geotechnical properties, including grain size distribution, Atterberg limits, specific gravity, proctor properties, and shear strength …

Sustainable Hydrogel From Biowaste: Synthesis And Characterization Of Pectin And Starch-Based Hydrogels Derived From Fruit Peel, Aneesa Rasheed Anwar, Roudha Sultan Almarri, Munawwar Ali Khan, Pramod Kumbhar

All Works

Arid regions such as the United Arab Emirates face persistent challenges in agricultural productivity due to water scarcity, poor soil quality, and the overuse of chemical fertilizers. As a sustainable alternative, biodegradable hydrogels offer promising solutions owing to their high swelling capacity, water retention ability, and controlled release of water and nutrients. This study explored the synthesis and characterization of eco-friendly hydrogels derived from pectin and starch extracted from orange and banana peels, respectively. These biopolymers are cross-linked using calcium and polyvinyl alcohol, forming hydrogels suitable for agricultural applications. The quality of the extracted biopolymers was assessed by analyzing moisture …

Structural Design And Finite Element Analysis Of A 54 Ton Freight Wagon Bolster Test Rig Under Vertical Center Plate Load, Shandy Dwi Prayoga, I Dewa Gede Ary Subagia, I Ketut Adi Atmika, Abdul Rohman Farid, Yunior Lanang Satrio

Journal of Mechanical Engineering Science and Technology (JMEST)

Bolster is one of the bogie's components that receives direct loading from the car body and freight movement. One of the problems that occurs in the bolster is permanent deflection during vertical and transversal static loading. Therefore, a static loading test is required to evaluate the structural strength of the bolster. During the static loading test, a rig is required to hold the bolster so that the bolster is in a fixed position. The rig owned by PT. INKA (Persero) showed a plastic deformation at the vertical center plate load (VCP 5.22P). Therefore, a modified design of the rig is …

Numerical Simulation Of Centrifugal Pump Performance Under Impeller Blade And Suction Diameter Variations, Gunawan Budi Santoso, Susanto -, Akhmad Nuriyanis, Anang Budhi Nugroho, Rizka Noor Miftakhul Ulum, Suyono -

Journal of Mechanical Engineering Science and Technology (JMEST)

The objective of this study is to model variations in pump geometry to obtain optimal performance under the effects of cavitation. The resulting geometric variation models were then simulated using ANSYS Fluent software. The first geometric variation model used a standard 5-blade impeller with suction pipe diameter variations of 2, 2 ½, 2 ¾, 3, 3 ¼, 3 ½, and 4 inches. The second geometric variation model for simulation used a standard 3-inch suction pipe with impeller blade variations of 3, 4, 5, 6, 7, 8, and 9. The simulation results indicated that the number of blades without changes in …

Effect Of Naoh Concentration On The Structural, Morphological, And Tensile Properties Of Pineapple Stem Fibers, Ahmad Norca Kurnia Zen, Heru Suryanto, Aminnudin Aminnudin, Fajar Nusantara, Joseph Selvi Binoj

Journal of Mechanical Engineering Science and Technology (JMEST)

Natural fiber reinforced composites are increasingly being developed due to their environmentally friendly nature, low production costs, and safety for human health. However, the presence of lignin and hemicellulose reduces adhesion properties between fiber and composite matrix. Alkalization treatment is an effective way to remove lignin and hemicellulose attached to cellulose. This study aims to determine the optimum concentration of NaOH used during alkalization process of pineapple stem fiber. The methods included the retting process of fibers from pineapple stems. The obtained fibers were soaked in variations of 2%, 4%, 6%, and 8% NaOH for 4 hours,  then dried and …

Comparative Lca Of Germanium Production From Coal Fly Ash Using Chlorinated Distillation And Solvent Extraction, Dennis Dadzie, Kwame Awuah-Offei, Michael Moats, Nasib Al Habib, Weston Hartzell

Mining Engineering Faculty Research & Creative Works

Germanium is increasingly important for high-tech applications, yet its supply chain is vulnerable, with production limited to a few countries. Although prior research has explored alternative techniques for extracting and recovering germanium, the literature lacks comparative life-cycle evidence that quantifies their environmental burdens and translates findings into actionable (policy) recommendations. This paper presents a cradle-to-gate life-cycle assessment that compares the environmental burdens of producing 1 kg of single-crystal germanium from coal fly ash via chlorinated distillation (CD) and solvent extraction (SX). Under the study's assumptions, CD has lower potential impacts in 15 of 19 impact categories, while both routes show …