Petroleum Engineering Commons^™

Vibro-Seismic Approach For Remediation Of Near-Wellbore Damage, Mounira Ahmed Abdallah

Theses and Dissertations

The research highlights the importance of vibro-seismic technology in the oil and gas industry. The primary objective of this study is to demonstrate how the vibro-seismic method enhances formation properties which are porosity, and permeability. Ultimately, this will lead to improved productivity and its application to remove the wellbore damage.

The research discusses whether or not the formation properties will be enhanced by the optimized acoustic vibration formation parameters. The thesis details laboratory experiments on core plugs, and four key findings are presented. The experimental work first showed that the use of the proper and optimum parameters enhanced the porosity …

Investigations Of Carbon Dioxide Storage In Low-Temperature Reservoirs For Non-Leaking Storage, Md Nahin Mahmood

Doctoral Dissertations

Carbon dioxide (CO₂) injection into subsea or low-temperature water zones has emerged as a promising strategy for long-term, non-leaking CO₂ storage through the formation of solid hydrates. This research investigates CO₂ injection into Berea sandstone cores saturated with water under simulated subsea conditions, focusing on hydrate formation behavior across varying temperatures, pressures, and injection flow rates. Experimental results demonstrate that CO₂ hydrate formation under dynamic (flowing) conditions occurs at significantly higher pressure compared to static conditions reported previously. At temperatures ranging from 0 °C to 5 °C, dynamic hydrate formation pressures were observed to be approximately double. This can be …

Geological Carbon Storage In Deep, Low Permeable Shale Reservoirs: Insights From The Haynesville Formation, Louisiana, Himakshi Goswami

Masters Theses

As global initiatives to mitigate greenhouse gas emissions intensify, depleted unconventional shale gas formations have emerged as critical candidates for large-scale geological carbon storage (GCS). This study investigates the feasibility, dynamic trapping mechanisms, and operational optimization of CO₂ sequestration in deep, low-permeability shale reservoirs, using the Upper Jurassic Haynesville Shale in northwest Louisiana as a comprehensive case study. Compositional reservoir simulation (CMG GEM 2021.10) was performed using the SPE Haynesville dataset, with CO₂ injected at a rate of 10,000 ft³/day across single and multiple depth intervals spanning 11,290–11,314 feet. Results demonstrate that multi-depth injection significantly improves residual trapping, reduces buoyancy-driven …

Mitigating Surfactant-Gas Interactions In Associated Gas Reservoirs: A Simulation And Machine Learning Guided Approach, Francis Dela Nuetor

Masters Theses

Surfactant flooding is a promising chemical enhanced oil recovery (EOR) method for mobilizing residual oil through interfacial tension reduction and wettability alteration. However, its performance in associated-gas reservoirs can be limited by salinity, gas composition, surfactant adsorption, and possible chemical instability. This study investigates the effect of salinity on surfactant flooding efficiency using an integrated reservoir simulation and machine learning workflow. A synthetic three-dimensional reservoir model was developed in ECLIPSE using a 10 × 10 × 3 Cartesian grid to simulate surfactant flooding over a 300-day production period under salinity conditions ranging from 100 to 50,000 ppm. Key outputs, including …

Optimizing Co₂ Wag Flooding Parameters For Enhanced Oil Recovery And Formation Damage Control In Asphaltene Reservoirs Using Soft Experimentation, Derrick Amoah Oladele

Masters Theses

CO₂ Water Alternating Gas flooding has become an important enhanced oil recovery process in increasing oil production in medium to heavy oil reservoirs. However, CO₂ injections have the potential to cause asphaltene destabilization, leading to precipitation, deposition, and pore plugging. This study evaluated and optimized the effect of CO₂ flooding parameters to maximize oil recovery and minimized formation damage. Eclipse 300 compositional reservoir simulator was used to assess the effect of CO₂ Water Alternating Gas (WAG) Injection Rate, WAG Ratio, and CO₂ Water Alternating Gas (WAG) Injection Pressure on the reservoir. Predictive models for Cumulative Oil Production (FOPT) and Asphaltene …

Mechanism Of Improved Miscibility Of Co2–Oil Systems By Multiester-Headgroup Surfactants, Ning Xu, Yanling Wang, Baojun Bai, Yu Zhang, Wenjing Shi, Zhaonian Zhang, Wenhui Ding, Peixu Ma, Zan Gao

Geosciences and Geological and Petroleum Engineering Faculty Research & Creative Works

In the pursuit of carbon neutrality, the CO₂-enhanced oil recovery provides dual benefits by enabling both carbon sequestration and incremental oil production. However, its application is limited by high minimum miscibility pressure. CO₂-philic and oil-affinitive surfactants have emerged as an effective, low-dosage, and cost-efficient strategy to reduce the minimum miscibility pressure. In this study, macroscopic phase behavior experiments combined with molecular dynamics simulations were employed to systematically elucidate the influence of multiester-head surfactants on CO₂–oil miscibility. Using a modified pressure–volume–temperature apparatus equipped with optical power monitoring, we determined that multiester-head surfactants reduced the first-contact …

Utilization Of Commercial Phosphonium And Ammonium Ionic Liquids In Enhanced Oil Recovery Of Carbonate Reservoirs, Nada Berrandjia

Thesis/ Dissertation Defenses

Despite advancements in renewable energy, oil and gas still dominate global energy supply, while a substantial portion of original oil in place (OOIP) remains unrecovered through conventional recovery methods. One of the most effective approaches used to mobilize residual oil is chemical enhanced oil recovery (CEOR) through mechanisms such as reduction of interfacial tension (IFT), alteration of wettability, emulsification, and improved displacement efficiency. Recently, ionic liquids (ILs) have gained interest as alternative CEOR agents due to their tunable structure and superior stability under harsh reservoir conditions. This thesis experimentally investigates the potential of low-cost and commercially available ILs for enhanced …

Mathematical Modelling And Optimisation Of The Reactor For The Esterification Process Of Safflower Oil With N-Butyl Alcohol, Sadritdin Makhamatdinovich Turabdjanov Academician, Hasan Sadriddin Ugli Fozilov, Ozoda Bakhronovna Axmedova, Sadriddin Fayzullayevich Fozilov

Technical science and innovation

This study addresses the mathematical modelling and optimisation of a reactor for the esterification of safflower oil with n-butyl alcohol. To improve process controllability and reduce the need for numerous pilot-scale trials, an ideal-mixing continuous stirred-tank reactor (CSTR) model was adopted. Incorporating reaction kinetics, the effect of contact time on the relative viscosity of the product mixture was analysed. The modelling results indicate that achieving an acceptable degree of feedstock conversion is difficult when a single ideal-mixing reactor is used. Therefore, a CSTR cascade was proposed, and the configuration with N = 2 reactors was selected as the most appropriate …

Sustainable Cellulose Aerogels And Biofaoms From Date Palm Waste For Thermal Insulation Application, Hyder Ali Al Abdallah

Thesis/ Dissertation Defenses

This dissertation is concerned with the use of date palm waste for the preparation of green lightweight aerogels and foams. Cellulose extracted from date palm wood waste is utilized to fabricate cellulose aerogels. Moreover, wood foams are prepared from whole biomass wood waste, without any prior treatment or extraction processes. The aim of this research is to produce sustainable, green, environmentally friendly heat insulation materials the construction, to replace commercial and fossil-fuel derived heat insulators. In this research, cellulose is extracted from date palm trees waste using both traditional and green environmentally friendly solvents. After extraction, cellulose aerogels are prepared …

Gas Lift Valve Operation Under Elevated Pressure And Temperature Conditions, Pedro O. De Melo Flores

LSU Master's Theses

Gas lift valves are critical components in artificial lift systems, and their performance directly influences well unloading efficiency and long-term production. Current industry models used to correct valve opening and closing pressure for temperature rely on assumptions that have not been extensively validated against experimental data. This study experimentally investigates the opening and closing behavior of injection pressure-operated (IPO) gas lift valves under controlled elevated-temperature conditions. A load rate test bench was modified to include a heating system capable of maintaining valve temperatures up to 220°F. Five gas lift valve designs from multiple manufacturers were tested over a range of …

Controlled Gelation Of Co₂-Resistant Polymer Systems For Improved Conformance In Co₂-Eor, Maryam Sharifi Paroushi

Miners Solving for Tomorrow Research Conference

This presentation introduces a CO₂-resistant hydrogel developed to control fluid movement and improve CO₂ injection performance in subsurface reservoirs for Enhanced Oil Recovery (EOR) and Carbon Capture and Storage (CCS). Conventional polymer gels often lose strength in CO₂-rich environments, resulting in weak plugging, early breakdown, and ineffective flow control. To address this limitation, a sulfonated HPAM-based gel system crosslinked with chromium was developed. The effects of polymer concentration, molecular weight, crosslinker ratio, ionic strength, and pH were investigated to better understand gelation behavior and performance. The formulation exhibited controlled gelation, strong resistance to temperature and CO₂, and minimal shrinkage over …

Isolated Bacillus Licheniformis Sp01 From Daqing Oilfield In Reducing Chromium(Iii) Crosslinked Polymer Residue And Enhancing Oil Recovery, Xiao Hui

Student Works (2020-2029)

After polymer gel formation, the residual partially hydrolyzed polyacrylamide (HPAM) and the crosslinker (Cr3+) caused plugging and decreased oil recovery. Microorganisms can degrade HPAM to address the issues, but Cr³⁺ inhibits the process and reduces oil recovery. This study explores the underexamined biodegradation of HPAM and improved oil recovery in the presence of Cr³⁺, offering new perspectives for microbial enhanced oil recovery (MEOR) after polymer gel formation. HPAM and crude oil were innovatively used as the sole nitrogen(N) and carbon(C) sources to isolate the best-growing strain from Daqing Oilfield produced water, identified as Bacillus licheniformis SP01. The oil displacement potential …

Assessing The Geomechanical Modelling Of Underground Reservoir For Co₂ Storage Trapping Mechanisms, Bonavian Hasiholan, Mohammed Ali Farea, Elhassan Mostafa Abdallah, Sami Abdelrahman M. Yagoub, Yasir Mukhtar

Mathematical Modelling and Numerical Simulation with Applications

Effective carbon dioxide (CO₂) storage is essential for mitigating climate change amid increasing global greenhouse gas emissions. This study investigates the influence of geomechanics on CO₂ storage performance within carbon capture and storage (CCS), focusing on structural, residual, and solubility trapping mechanisms using a fully coupled modeling framework. Two numerical models, with and without geomechanical effects, are developed to evaluate impacts on reservoir behavior, CO₂ migration, and trapping efficiency. Each mechanism is analyzed separately and within an integrated framework to assess their combined contributions. Results indicate that geomechanical coupling increases reservoir pressure, reduces CO₂ flow velocity, enhances migration control, and …

Fly Ash Proppant Developed For Hydraulic Fracturing, Raz Rzgar Haydar

Theses and Dissertations

Proppants are critical components in hydraulic fracturing, used to maintain fracture conductivity and enhance reservoir stimulation. In high-pressure and harsh reservoir environments, the use of high-strength proppants is essential to ensure well performance. Conventional proppants, being sand, ceramic, and sintered bauxite can be expensive, and their use often requires costly fracture fluids. This study investigates the possibility of utalizing fly ash geopolymers as a sustainable alternative that is also cost-effective for proppants manufacturing. Fly ash, a by-product from the combustion of coal and other materials, was explored as a base material for proppants, utilizing an alkaline solution as an activator …

Effect Of Ionic Strength On Gelation Time And Strength Of Amps-Based Polymer Gels, Maryam Sharifi Paroushi, Xuyang Tian, Baojun Bai, Thomas P. Schuman, Yin Zhang, Mingzhen Wei

Geosciences and Geological and Petroleum Engineering Faculty Research & Creative Works

Polymer gel treatment has been widely applied for improving sweep efficiency and controlling excessive water and gas production. Their performance depends on gelation time and final gel strength. In most studies, brine salinity is used to describe the effect of formation water on gel behavior. However, changing salinity also changes ionic strength and ion composition at the same time. Because of this coupling, it is difficult to identify the mechanisms controlling gelation, which has led to inconsistent trends in the literature. Increasing salinity has been reported to either slow or accelerate gelation and to weaken or strengthen gels depending on …

Evaluation Of A Novel Re-Crosslinkable Preformed Particle Gel For Conformance Control In Ultra-High Temperature Reservoirs, Yanbo Liu, Tao Song, Caleb Kwasi Darko, Thomas P. Schuman, Mingzhen Wei, Baojun Bai

Chemistry Faculty Research & Creative Works

Preferential fluid flow remains a major challenge in subsurface energy production and gas storage operations, resulting in excessive water production in mature oil fields, reduced heat extraction in geothermal reservoirs, and low sweep and storage efficiency in CO₂-EOR projects. Polymer gels are widely used to mitigate high-permeability channels; however, conventional systems exhibit limited plugging efficiency and short lifetimes in ultra-high-temperature reservoirs due to poor thermal stability. This study presents a novel ultra-high-temperature-resistant preformed particle gel (UHT-PPG) developed for conformance control in reservoirs with temperatures of 150–275 °C and severe super-K or channeling problems. The material was evaluated in …

Evaluation Of Chromium-Crosslinked Amps-Hpam Copolymer Gels: Effects Of Key Parameters On Gelation Time And Strength, Maryam Sharifi Paroushi, Baojun Bai, Thomas P. Schuman, Yin Zhang, Mingzhen Wei

Geosciences and Geological and Petroleum Engineering Faculty Research & Creative Works

Controlling CO₂ channeling in heterogeneous reservoirs remains a major challenge for both enhanced oil recovery (EOR) and secure geological storage. AMPS-HPAM copolymers exhibit high-temperature resistance and brine tolerance compared with conventional HPAM gels, making them well suited for the harsh environments associated with CO₂ injection. Chromium-based crosslinkers (CrAc and CrCl₃) were investigated because sulfonic acid groups in AMPS can coordinate with trivalent chromium ions, enabling dual ionic crosslinking and the formation of a robust gel network. While organic crosslinked AMPS-HPAM gels have been widely studied, the behavior of chromium-crosslinked AMPS-containing systems, particularly their gelation kinetics under …

Solubility And Dissolution Mechanism Of Novel Multi-Ester Headgroup Surfactants In Supercritical Co2, Ning Xu, Yan Ling Wang, Baojun Bai, Shi Zhang Cui, Yu Zhang, Wen Jing Shi, Zhao Nian Zhang, Wen Hui Ding, Pei Xu Ma, Zan Gao

Geosciences and Geological and Petroleum Engineering Faculty Research & Creative Works

To address the limited solubility and applicability of conventional hydrocarbon surfactants in supercritical CO₂, a series of multi-ester headgroup surfactants were designed and synthesized by leveraging the CO₂-philic properties of ester groups. The molecular structures were characterized using Fourier transform infrared (FT-IR) spectroscopy and ¹H NMR. A custom-designed laser-based apparatus was developed to quantify surfactant solubility and systematically investigate phase behavior in CO2. Molecular dynamics (MD) simulations were employed to elucidate structure–solubility relationships across multiple scales, including solubility parameters, interaction energies, radial distribution functions (RDFs), and free volume fractions. Results indicate that, at 323.15 K, …

Optimization Of Carbon Capture And Sequestration In The Tri-State Hub West Virginia, Ohio, And Pennsylvania, Saif Abdullah Saif Al-Nabhani

Graduate Theses, Dissertations, and Problem Reports (ETD)

Carbon Capture and sequestration (CCS) is a critical way for the decarbonization of power and industrial sectors. The Tri-State area between West Virgina, Ohio and Pennsylvania are a diverse region with various CO₂ sources, deep saline, depleted reservoirs, pipeline network, and the midstream infrastructure that makes it possible for Captured CO₂ to be safely and economically moved and stored over long periods of time. This project addresses the need for an integrated optimization framework that includes CO₂ sources to potential storing sites using a transportation network design and a subsurface model that secures storage and minimizes leakage risk.

The model …

Deep Learning-Based Co-Current Upward Gas-Liquid Two-Phase Flow Regime Identification In An Annular Conduit, Joshua Robert Macomber

Graduate Theses, Dissertations, and Problem Reports (ETD)

Flow regime identification in co-current upward gas-liquid flow through annular conduits remains a significant challenge in petroleum engineering, with major safety and operational implications. It is also important across industries involving the transport of multiphase fluids. Misidentifying flow regimes can introduce major operational risk, yet regime boundaries in annular gas-liquid flow are often visually complex and context dependent.

The objective of this study was to evaluate the utility of convolutional neural network (CNN) classifiers for flow regime identification. The CNN was trained using annular flow image dataset published by Texas A&M University. The dataset consists of approximately 947 RGB images …

Utilizing Coal For Mesophase Pitch-Based Carbon Fiber Production: Precursors, Processes, And Progress, Christina M. Thompson

Theses and Dissertations--Chemistry

Graphitic materials possess unique properties due to the unique combination of layered crystalline structure and carbon’s low atomic weight. High performance carbon fiber is one such example, displaying exceptional strength-to-weight ratios, stiffness, and thermal and chemical resistance. These properties render high performance carbon fiber a critical structural reinforcement material in the manufacture of composites across various industries, such as for automotive and aerospace applications. However, balancing fiber performance with precursor and processing costs remains a challenge. As alternative carbonaceous feedstocks are explored, coal has gained interest for utilization in graphitic products as a relatively abundant and low-cost source of aromatic …

Thermo-Chemical Recycling Of Waste Plastics Containing Halogenated Polymers (Br−, Cl−, F−) Using Potential Additives, Mohamed Shafi

Thesis/ Dissertation Defenses

Plastic waste handling is a daunting task due to the presence of halogenated polymers, specifically those cluttered with bromine (Br), chlorine (Cl), and fluorine (F). Halogenated plastics can be mixed with other polymers in the general plastic waste, particularly in the recycling stream. Brominated flame retardants (BFRs) are mainly present in e-waste and from the use of flame retardants in household items, textiles, and furniture. Plastics from discarded electronics often contain significant levels of bromine and chlorine, predominantly from flame retardants and plasticizers. Being the most deployed thermoplastic worldwide, waste polyvinyl chloride (PVC) generation is expected to increase by about …

Predicting Simulation Times For Multiphase Thermal-Hydraulic Models, Andrew Yule, Andrew Taylor

SMU Data Science Review

Addressing the challenge of computationally intensive OLGA

simulations in the oil and gas industry, a machine learning framework is

developed for accurate runtime prediction. A specialized feature extraction

pipeline identifies key parameters—such as simulation time, time step,

number of branches, and section count—from OLGA input files that serve as

high-impact predictors. Multiple predictive models, including regression,

tree-based ensembles, and neural networks, are implemented to validate

accuracy and robustness. Results reveal that prioritizing simulations based on

predicted runtimes optimizes licensing resources and reduces operational

costs, making real-time scheduling more efficient. This research demonstrates

the effectiveness of data-driven runtime prediction in enhancing …

Core-Scale Study Of Miscible Co2 Foam–Oil Interactions, Kuvonchbek Abdirakhmonov

Theses

Foam is currently the most effective means for gas mobility control in a variety of geo-energy applications, including enhanced oil recovery (EOR), carbon capture, utilization and storage (CCUS), and aquifer/soil remediation. This study investigates the mobility control of miscible CO₂ foam in the presence of oil.

The primary objective is to quantify the impact of oil on CO₂ foam behavior under miscible conditions, specifically examining foam stability, strength, and flow regimes as influenced by oil composition and reservoir permeability. While most oils destabilize foam, few studies explore the coarsening mechanisms of CO₂ foam in the presence of miscible oils, which …

Laboratory Investigation Of High-Temperature Preformed Particle Gels For Fluid Control In Granite Cores For Geothermal Applications, K. Caleb Darko, Yanbo Liu, Thomas P. Schuman, Mingzhen Wei, Baojun Bai

Chemistry Faculty Research & Creative Works

To understand the applicability of high-temperature preformed particle gel (HT-PPG) for control of short-circuiting in enhanced geothermal systems (EGSs), core flooding experiments were conducted on fractured granite cores under varying fracture widths, gel particle sizes and swelling ratios. Key parameters such as injection pressure, water breakthrough pressure, and residual resistance factor were measured to evaluate HT-PPG performance. The gel exhibited strong injectability, entering granite fractures at pressure gradients as low as 0.656 MPa/m; HT-PPG yields a superior sealing performance by significantly reducing the permeability; and dehydration occurs during HT-PPG propagation, with a dehydration ratio ranging from 4.71% to 11.36%. This …

Effect Of Clays On The Spontaneous Imbibition Behavior Of Surfactant Solutions In Shale Oil Reservoirs, Ning Xu, Yanling Wang, Baojun Bai, Chuanbao Zhang, Shizhang Cui, Yu Zhang, Di Li, Wenjing Shi, Wenhui Ding

Geosciences and Geological and Petroleum Engineering Faculty Research & Creative Works

Surfactant-enhanced spontaneous imbibition is a proven method of enhancing oil recovery from shale reservoirs. However, a significant knowledge gap concerning the impact of clay minerals on surfactant-enhanced imbibition in shale reservoirs remains. Therefore, this study first analyzed the mineral composition and pore structure of the shale reservoirs. Subsequently, three surfactants were selected for spontaneous imbibition experiments. The influence of various clay minerals on the surfactant imbibition was assessed by considering various properties of the imbibition system. The results showed that the shale pores primarily consisted of macropores (44.03%) and mesopores (43.94%). Surfactants enhance the imbibition recovery by altering the wettability …

Detecting Electrical Submersible Pump (Esp) Failures And Estimating Run Life Using Artificial Neural Networks, Mostafa Ahmed Sobhy

Theses and Dissertations

Electric Submersible Pumps (ESPs) are one of the important artificial lift methods for sustaining production in mature and high-water-cut wells; but may suffer frequent failures due to mechanical, electrical, hydraulic, chemical, and operational failures. These failures can yield substantial deferred production and intervention costs. Plenty of ESP installations are fitted with downhole sensors. Yet, it is observed that the current industry practice underutilizes the wealth of available sensor and operational data and lacks standardized, explainable failure-type identification and classification.

In this thesis, a comprehensive Machine Learning (ML) and Deep Learning (DL) framework was introduced for ESPs that simultaneously estimates remaining …

Predicting Groundwater Withdrawals Using Machine Learning With Limited Metering Data: Assessment Of Training Data Requirements, Dawit Asfaw, Ryan G. Smith, Sayantan Majumdar, Katherine Grote, Bin Fang, B. B. Wilson, V. Lakshmi, J. J. Butler

Geosciences and Geological and Petroleum Engineering Faculty Research & Creative Works

The future of major aquifer systems supporting irrigated agriculture is threatened due to unsustainable groundwater pumping. Metering of pumping is key for implementing robust groundwater management, but metering is limited in most aquifers. Although machine learning methods have been used to estimate pumping over certain regions, these studies have not fully demonstrated the data quantity and input parameter requirements to accurately estimate regional groundwater pumping. This study determined the data quantity required and identified relevant features to develop Random Forests-based annual groundwater pumping estimates (2008–2020) over the Kansas High Plains aquifer. We predicted pumping at two spatial scales, i.e., point …

Upcycling Waste To Wealth: Cuo-Sio₂/Reduced Graphene Nanocomposite From Pomegranate Peels For One-Pot Low-Temperature Conversion Of Waste Oils Into Valuable Fatty Acid Monomers, Attia Attia, Shahenda Mahran Dr., Maria Centeno Prof., Basudeb Saha

Petroleum Engineering and Gas

and hence reduce the price of the fatty acid monomers. This study reports for the first time a novel, environmentally benign, highly active copper oxide-silica oxide/reduced graphene oxide (CuO-SiO2/RGO), heterogeneous nano-catalyst derived from waste pomegranate peels, for the one-pot, low-temperature synthesis of fatty acid monomers from high-acid-value waste vegetable oil (WVO). The synthesised nano-catalyst was extensively characterised using XRD, FT-IR, TEM, SEM, EDX and TGA-DTA. Further, it was utilised to synthesise fatty acidrich oleic phenoxypropyl acrylate (OPA) monomer from high acid value WVO via a single-step reaction.

Investigation Of Co-Current And Counter-Current Multiphase Flow In Upstream Drilling And Production Applications, Hazem Fleifel

LSU Doctoral Dissertations

In the domain of upstream Petroleum Engineering, the dynamics of co-current and counter-current multiphase flows present huge challenges, significantly impacting the efficiency of associated processes. This study investigates two specific applications concerning these flow behaviors, involving both laboratory experiments and transient computer simulations. This work investigates two distinct well control and production enhancement processes, involving multiphase flow dynamics: the bullheading kill procedure and liquid-assisted gas lift (LAGL).

The first topic (Topic 1) explores the bullheading process, a type of well control methods, by challenging the traditional understanding that gas removal efficiency increases monotonically with injection pump flow rate. Through 1D …