Materials Science and Engineering Commons^™

The Influence Of The Reference Area Of Aileron On The N2xx Aircraft Using Computational Fluid Dynamics, Siti Nur Rahmah, Gaguk Jatisukamto, Hary Sutjahjono

Journal of Mechanical Engineering Science and Technology (JMEST)

Aileron is a control surface that functions as a regulator of roll motion. The movements of the ailerons are opposite to the left and right sides. Previous studies have shown that graphs of hinge moment coefficient (Chm) values increases with increasing angle of attack. This study is to determine the aerodynamic characteristics of aileron by combining the surface area of the vane into the aileron by varying the aileron’s deflection. The calculation is performed using a numerical method in two dimensions (2D) commercial CFD simulation software. The results of the study concluded that the hinge moment coefficient for modified airfoil …

The Effect Of Heat Treatment To The Erosion Rate Of Brass Composite, Aminnudin Aminnudin, Solichin Solichin

Journal of Mechanical Engineering Science and Technology (JMEST)

Brass composites can be improved their mechanical properties by the heat treatment process. The improvement of the mechanical properties of this technique is expected to increase the resistance of the composite to erosion that occurs in the environment of flow water. Brass composites used are compositeswith fly ash 5, 10, 15, and 20%. The heat treatment process was carried out using electric furnace withoutprotective gas. Composite heat up to 350°C and 400°C for 30 min. and quenching with water. Before and after the erosion test, the weight of the test specimen was weighed with analytical scales. The treatment process affects …

Protein And Polysaccharide-Based Fiber Materials Generated From Ionic Liquids: A Review., Christopher R Gough, Ashley Rivera-Galletti, Darrel A Cowan, David Salas-De La Cruz, Xiao Hu

College of Science & Mathematics Departmental Research

Natural biomacromolecules such as structural proteins and polysaccharides are composed of the basic building blocks of life: amino acids and carbohydrates. Understanding their molecular structure, self-assembly and interaction in solvents such as ionic liquids (ILs) is critical for unleashing a flora of new materials, revolutionizing the way we fabricate multi-structural and multi-functional systems with tunable physicochemical properties. Ionic liquids are superior to organic solvents because they do not produce unwanted by-products and are considered green substitutes because of their reusability. In addition, they will significantly improve the miscibility of biopolymers with other materials while maintaining the mechanical properties of the …

Methods Of Uncertainty Quantification For Physical Parameters, Kellin Rumsey

Mathematics & Statistics ETDs

Uncertainty Quantification (UQ) is an umbrella term referring to a broad class of methods which typically involve the combination of computational modeling, experimental data and expert knowledge to study a physical system. A parameter, in the usual statistical sense, is said to be physical if it has a meaningful interpretation with respect to the physical system. Physical parameters can be viewed as inherent properties of a physical process and have a corresponding true value. Statistical inference for physical parameters is a challenging problem in UQ due to the inadequacy of the computer model. In this thesis, we provide a comprehensive …

Nanohybrid Membrane Synthesis With Phosphorene Nanoparticles: A Study Of The Addition, Stability And Toxicity, Joyner Eke, Philip Alexander Mills, Jacob Ryan Page, Garrison P. Wright, Olga V. Tsyusko, Isabel C. Escobar

Center of Membrane Sciences Faculty Publications

Phosphorene is a promising candidate as a membrane material additive because of its inherent photocatalytic properties and electrical conductance which can help reduce fouling and improve membrane properties. The main objective of this study was to characterize structural and morphologic changes arising from the addition of phosphorene to polymeric membranes. Here, phosphorene was physically incorporated into a blend of polysulfone (PSf) and sulfonated poly ether ether ketone (SPEEK) doping solution. Protein and dye rejection studies were carried out to determine the permeability and selectivity of the membranes. Since loss of material additives during filtration processes is a challenge, the stability …

Synthesis, Self-Assembly And High-Pressure Properties Of Nanoparticles And Hybrid Nanocomposites, Lingyao Meng

Nanoscience and Microsystems ETDs

Nanoparticles have gained significant scientific interests owing to their unique structural dimensions, size- and shape-tunable properties, and numerous fascinating applications, from opto-electronics, sensor devices, to energy, environmental, and medical fields. Furthermore, the synergistic integration of other materials, including organic polymers, with nanoparticles provides new opportunities and strategies to obtain nanocomposites with superior properties and functionalities. While there is already significant research on the synthesis and characterizations of nanoparticles and hybrid nanocomposites, some research questions, such as how to design and control the interfacial morphology in polymer/nanoparticle hybrid nanocomposites, how to synthesize metal- organic framework (MOF) nanoparticles in well-defined and uniform …

High‐Tensile Strength, Composite Bijels Through Microfluidic Twisting, S. P. Kharal, Robert P. Hesketh, Martin F. Haase

Henry M. Rowan College of Engineering Departmental Research

Rope making is a millennia old technique to collectively assemble numerous weak filaments into flexible and high tensile strength bundles. However, delicate soft matter fibers lack the robustness to be twisted into bundles by means of mechanical rope making tools. Here, weak microfibers with tensile strengths of a few kilopascals are combined into ropes via microfluidic twisting. This is demonstrated for recently introduced fibers made of bicontinuous interfacially jammed emulsion gels (bijels). Bijels show promising applications in use as membranes, microreactors, energy and healthcare materials, but their low tensile strength make reinforcement strategies imperative. Hydrodynamic twisting allows to produce continuous …

Tacky Elastomers To Enable Tear-Resistant And Autonomous Self-Healing Semiconductor Composites, Song Zhang, Yu-Hsuan Cheng, Luke Galuska, Anirban Roy, Matthias Lorenz, Beibei Chen, Shaochuan Luo, Yen-Ting Li, Chih-Chien Hung, Zhiyuan Qian, Peter Blake Joseph St. Onge, Gage T. Mason, Lewis Cowen, Dongshan Zhou, Sergei I. Nazarenko, Robson F. Storey, Bob C. Schroeder, Simon Rondeau-Gagné, Yu-Cheng Chiu, Xiaodan Gu

Faculty Publications

Mechanical failure of π-conjugated polymer thin films is unavoidable under cyclic loading conditions, due to intrinsic defects and poor resistance to crack propagation. Here, the first tear-resistant and room-temperature self-healable semiconducting composite is presented, consisting of conjugated polymers and butyl rubber elastomers. This new composite displays both a record-low elastic modulus (

A Spatially Distributed Fiber-Optic Temperature Sensor For Applications In The Steel Industry, Muhammad Roman, Damilola Balogun, Yiyang Zuang, Rex E. Gerald Ii, Laura Bartlett, Ronald J. O'Malley, Jie Huang

Materials Science and Engineering Faculty Research & Creative Works

This paper presents a spatially distributed fiber-optic sensor system designed for demanding applications, like temperature measurements in the steel industry. The sensor system employed optical frequency domain reflectometry (OFDR) to interrogate Rayleigh backscattering signals in single-mode optical fibers. Temperature measurements employing the OFDR system were compared with conventional thermocouple measurements, accentuating the spatially distributed sensing capability of the fiber-optic system. Experiments were designed and conducted to test the spatial thermal mapping capability of the fiber-optic temperature measurement system. Experimental simulations provided evidence that the optical fiber system could resolve closely spaced temperature features, due to the high spatial resolution and …

Synthesis Of Carbide Ceramics Via Reduction And Carburization Of Oxyanions Adsorbed Onto An Activated Carbon Matrix, Grant Wallace

Graduate Theses & Non-Theses

Carbide ceramics rank high among the hardest and most chemically resistant materials. Their ability to resist physical and chemical attack under conditions where more traditional materials fail make them very desirable for a number of industrial applications. Their use is limited, however, due to the expensive and energy-intensive methods required to produce them commercially.

A more versatile and energy-efficient process for commercial carbide production has been developed by synthesizing micron/sub-micron carbide ceramic particles through the adsorption and subsequent carburization of anions on an activated carbon matrix. Oxyanion solutions containing sodium tungstate, sodium molybdate, or sodium metasilicate are adsorbed onto activated …

Prediction Of Isotropic Strain Hardening Material Properties Using Gradient Boosted Regression Tree Method And Hyperparameter Optimization, Darren R. Promer

Masters Theses

In this study a new technique is proposed for the determination of elastic-plastic stress-strain relations for isotropic materials using the force-displacement output from an instrumented indentation test, finite element simulation, and machine learning methods. This non-destructive testing methodology has promising potential for industry implementation. Applications to benefit from this method include the characterization of localized material properties on surface engineered components, and the post-manufacturing assessment of material properties for items such as additively manufactured metallic components and load-bearing welded joints.

Currently, the capability of the instrumented indentation test for determining material properties is limited to the elastic modulus and surface …

A Multiscale Thermomechanical Metal Additive Manufacturing Simulation And The Impact Of Geometry On Residual Stress And Distortion, Luis Fernando Silva Velasco

Masters Theses

Metal additive manufacturing is an enabling technology for the rapid prototyping and manufacturing of geometrically complex parts that would otherwise be difficult or impossible to manufacture. However, the manufacturing process can produce undesired residual stresses and distortions. The first part of the work describes the implementation of a multiscale, thermo-mechanical simulation modeling the metal powder bed fusion additive manufacturing process. NASA’s Micromechanics Analysis Code was is to incorporate the microscale effects of an evolving material porosity on the predicted macroscale residual fields. The simulation shows that modeling an evolving material porosity, as the material transitions from a metal powder to …

Precipitate Characterization In Model Al-Zn-Mg-(Cu) Alloys Using Small-Angle X-Ray Scattering, Daniel Freiberg, Wenhui Zhu, Jun Sang Park, Jonathan D. Almer, Paul Sanders

Michigan Tech Publications, Part 1

Model 7000 series alloys with and without copper were fabricated into sheets to study precipitation hardening behavior under isothermal aging conditions. Samples of each alloy were subjected to 3 h annealing treatments at various temperatures to produce a range of precipitate size distributions. Hardness, electrical conductivity, and small-angle X-ray scattering (SAXS) were used to characterize the aging behavior of the two alloys. Precipitate size distributions were modeled from the scattering curves for each annealing condition using a maximum entropy method (MEM) and compared to select transmission electron microscopy (TEM) results. The measured average precipitate diameters from TEM were in good …

International Year Of Glass, Bill Fahrenholtz

Materials Science and Engineering Faculty Research & Creative Works

No abstract provided.

Predicting Effective Fracture Toughness Of Zrb₂-Based Ultra-High Temperature Ceramics By Phase-Field Modeling, Arezoo Emdadi, Jeremy Lee Watts, William Fahrenholtz, Greg Hilmas, Mohsen Asle Zaeem

Materials Science and Engineering Faculty Research & Creative Works

The effective fracture toughness (EFT) of ZrB₂-C ceramics with different engineered microarchitectures was numerically evaluated by phase-field modeling. To verify the model, fibrous monoliths (elongated hexagonal ZrB₂-rich cells in a continuous C-rich matrix) with different volume fractions of a C-rich phase were considered. Architectures containing 10 and 30 vol% of C-rich phase showed EFT values about 42% more than that of pure ZrB₂. Increasing the C-rich phase to 50 vol%, dropped toughness significantly, which is in agreement with the experimental results. Replacing hexagonal cells with cylindrical, triangular, or square cells of the same cross-sectional …

Piezoresistive Hybrid Nanocomposites For Strain And Damage Sensing: Experimental And Numerical Analysis, Audrey Jean-Miche Gbaguidi

Doctoral Dissertations and Master's Theses

Carbon nanomaterials such as carbon nanotubes (CNTs) and graphite nanoplatelets (GNPs) demonstrate remarkable electrical and mechanical properties, which suggest promising structural and functional applications as fillers for polymer nanocomposites.

The piezoresistive behavior of these nanocomposites makes them ideal for sensing applications. Besides, hybrid nanocomposites with multiple fillers like carbon nanotubes (CNTs) and graphite nanoplatelets (GNPs) are known to exhibit improved electrical and mechanical performance when compared to mono-filler composites.

To comprehensively understand the mechanisms of electrical percolation, conductivity, and piezoresistivity in hybrid nanocomposites, the author develops a two-dimensional (2D) and a three-dimensional (3D) computational Monte Carlo percolation network models for …

Synthesis And Application Of Ceramic Paste For High-Temperature Electronic Packaging, Ardalan Nasiri

Graduate Theses and Dissertations

This dissertation research focused on the synthesis and application of ceramic paste for high-temperature applications. An alumina paste material comprising aluminum dihydric phosphate and alumina powder was developed for high-temperature electronic packaging. Nano aluminum nitride and nano-silica powders were embedded to promote the paste curing process, limit the grain growth, and increase its bond shear strength. The chip-to-substrate bond strength was enhanced and met the MIL-STD requirements for die-attach assembly. Its encapsulation property was improved with fewer cracks compared to similar commercial ceramic encapsulants. The die-attach material and encapsulation properties tested at 500°C showed no defect or additional cracks. Thermal …

Preventing Delayed Cracks In Sus304 Deep Drawn Cups Using Extreme Blank Holding Forces Aided By Nanolubrication, Ibrahim Muhammad Shafiq

Student Works (2020-2029)

This study was to investigate the formation and reformation of delayed cracks of SUS304 cylindrical drawn cups under elevated blank holding force (BHF) from 8~32 kN with 1~3 wt% SiO2 nanolubricants concentrations. The widest crack-free BHF range i.e. from 29 ~ 31 kN was determined for 2 wt% of SiO2 in the experiment. Delayed cracks were also observed below and beyond this BHF range. There was an increment of frictional force at the cup flange region when entering the crack-free BHF range, as proven by the rebound in sidewall thickness, relative intensity of α′-martensite, elongated height and drawing force beyond …

Microstructural Characteristics And Mechanical Properties Of Sn-Ag-Cu Solders With Minor Additions Of Al And Zn, Yee Mei Leong

Student Works (2020-2029)

Driven by the recent trend towards miniaturization of lead free electronic products, researchers are putting immense efforts to improve the properties and reliability of Sn based solders. Recently, much interest has been shown on low silver (Ag) content solder SAC 105 (Sn-1.0Ag-0.5Cu) solder because of economic reasons and improvement of impact resistance as compared to SAC387(Sn-3.8Ag-0.7Ag). The present work investigates the effect of minor (0.1-0.5wt.%) Aluminium (Al) and Zinc (Zn) addition to SAC105 on the bulk and interfacial structure between solder and copper substrate during reflow and after thermal aging , the mechanical properties of the solder joint and the …

Engineering Properties And Microstructural Characteristics Of Cement And Geopolymer Based Mortars Using Nontraditional Supplementary Cementitious Materials, Mathialagan Sumesh

Student Works (2020-2029)

The concrete repair and rehabilitation industry grows rapidly due to deterioration, damage and defects in concrete structures. For various reasons, the concrete construction industry is not sustainable; because it consumes huge quantities of virgin materials, the usage of Portland cement as prime binder. The production of cement is a major contributor to greenhouse gas emissions. In addition, the high cost of commercial repair material. Therefore, it is necessary to develop cost-effective alternative repair materials for concrete repairs. There have been many standard repair materials available in the market, which are costly and not affordable to common people. However, research works …

Development Of Nano Carbon And Conducting Polymers Based Ternary Composites For Supercapattery, Iqbal Javed

Student Works (2020-2029)

Although significant efforts have been devoted on the development of energy storage systems such as batteries and fuel cells in the past decades, the low power density, short cyclic life and high maintenance cost have kept them away from many applications. Alternatively, supercapattery which has the characteristic features of batteries as well as supercapacitors has gained much attention because of its rapid charge/discharge mechanism, long life cycle, and high power density. However, supercapattery generally suffers from poor energy density. This research aims to develop carbon and conducting polymers based ternary nanocomposites for high performance supercapattery. Pristine metal oxide nanostructures suffer …

Research Of The Process Of Deformation Of Extractional Phosphoric Acid From Phosphorites Of Central Kyzylkum, Khodjamkulov Sakhomiddin, Mirzakulov Kholtura, Melikulova Gavkhar, Usmanov Ilkham

CHEMISTRY AND CHEMICAL ENGINEERING

The purpose of this research was to determine the optimal technological parameters for the purification of extraction phosphoric acid based on phosphorites of Central Kyzylkum from fluorine by precipitation with sodium salts. The influence of the norm of sodium silicate and the total norm of sodium carbonate and sodium metasilicate salts on the chemical composition and degree of precipitation of sodium silicofluoride was research. It is shown that the optimal norm of sodium metasilicate is the stoichiometric norm for binding fluorine present in the extraction phosphoric acid to silicofluoride and the total norm of sodium salts is 120-140%, the temperature …

Modeling Of Craft Oil- Water Emulsion Under Laboratory Conditions, Arslanov Sharafutdin, Dengaev Aleksey, Getalov Andrey, Sarigin Boris

CHEMISTRY AND CHEMICAL ENGINEERING

The purpose of this research is to study the possibilities of modeling oil-water emulsion in the laboratory. The study of the ratio of components and conditions of dispersion (formation) of oil-water emulsions on their stability at different settling temperatures using a laboratory model can optimize the separation of oil-water emulsions in field conditions. The possibility of modeling commercial oil and water emulsions in laboratory conditions is investigated, the average diameters of water globules in simulated oil and water emulsions at different times of their formation are determined, and the obtained average globule diameters are compared with the average diameter of …

The Possibilities Of Using Loess Clay Of Kattabog Deposit In The Production Of Ceramic Products, Ruzibaev Bahrom, Saloxidinova Salima

CHEMISTRY AND CHEMICAL ENGINEERING

The aim of the research was to determine the properties of loess clay in Kattabog deposit (Uzbekistan) to identify possible areas of use. Modern methods of physicochemical analysis are used: spectroscopic, x-ray phase, electron microscopic methods of analysis. The research results showed that the main phases of clay are hydromica, quartz, kaolinite, calcite and orthoclase. Based on the research, it can be stated that the clay of Kattabog deposit has good physical and technical properties and mineralogical composition, which is a valuable raw material for the production of various ceramics, bricks, tiles, majolica and other products.

Influence Of The Aluminum Oxide Additive On The Phase Composition Of Mullit-Forming Aluminosilicate Minerals, Mkrtchyan Ripsime, Aripova Mastura

CHEMISTRY AND CHEMICAL ENGINEERING

The aim of the research is to determine the effect of alumina on the phase composition of shale of the Jerdanak deposit and the quartz-pyrophyllite rock of the Baynaksay deposit during high-temperature firing. X-ray phase analysis determined changes in the phase composition of rocks with additives from 5 to 20% aluminum oxide as a result of firing at 1300 and 1400 °C. A comparative analysis revealed the absence of cristobalite formation, a decrease in the quartz content, and an increase in the amount of mullite for shale samples. No positive effect of alumina additives on the phase composition of quartz-pyrophyllite …

Coordination Compounds Of Copper, Cobalt And Nickel Formates With Formamide And Carbamide, Jumaniyazova Mukaddas, Azizov Tohir

CHEMISTRY AND CHEMICAL ENGINEERING

The synthesis of mixed ligand coordination compounds of copper, cobalt and nickel formates with formamide and urea in an aqueous solution was carried out. The metal content in the complexes was determined by complexometric titration. Using IR spectroscopy, it was proved that the coordination of formamide and urea with the complexing atom is carried out through the oxygen atom of the carbonyl group. The absorption spectrum of coordinated water is also present in the IR spectrum. The nature of the change in the frequency of stretching vibrations of the –OH group in the composition of water indicates its location in …

Configuration And Competitive Reactivity Of Ligands In Mixed Ligand Complexes Of Dialkylditiophosphates And Aminobenbenzimidazole (Part I: Au, Pt, Ag), Esbergenova Botakoz, Daminova Shakhlo, Kadirova Zuhra, Sharipov Khasan

CHEMISTRY AND CHEMICAL ENGINEERING

With the aim of determination of electronic and geometrical structures of mixed-ligand complexes, theoretical modeling of the structures of coordination compounds of transition metals with dialkyldithiophosphate chelating ligands with aminobenzimidazoles carried out using quantum chemical methods. Using BIOVIA Materials Accelrys Studio 2017 software packages, the geometry, electron density distribution, and frontier orbitals calculated for the mixed ligand complexes of Au(III), Pt(II), Ag(I), Cu(II), Ni(II), Fe(III), which are necessary for understanding the electronic structure of coordination compounds with chelating ligands.

Educational Cluster - Foundation Of The National Economy And Regional Innovation System, Usmonov Botir, Kushiev Khabibjon

CHEMISTRY AND CHEMICAL ENGINEERING

The paper analyzes the available resources for the creation of a cluster approach to the integration of education, science and industry in order to create a mechanism to bring the development of the economy to the level of modern requirements. The article describes the collaboration of science, education and industry through the clustering process. Ways to introduce clustering in the national innovation system are described. At the same time, the role of the integration of education, science and industry with the elements of the National Innovation System is analyzed. In conclusion, the role of the education cluster in the regional …

The Impact Of Composition And Morphology On Ionic Conductivity Of Silk/Cellulose Bio-Composites Fabricated From Ionic Liquid And Varying Percentages Of Coagulation Agents., Bailey Blessing, Cory Trout, Abneris Morales, Karleena Rybacki, Stacy A Love, Guillaume Lamoureux, Sean M O'Malley, Xiao Hu, David Salas-De La Cruz

College of Science & Mathematics Departmental Research

Blended biocomposites created from the electrostatic and hydrophobic interactions between polysaccharides and structural proteins exhibit useful and unique properties. However, engineering these biopolymers into applicable forms is challenging due to the coupling of the material’s physicochemical properties to its morphology, and the undertaking that comes with controlling this. In this particular study, numerous properties of the Bombyx mori silk and microcrystalline cellulose biocomposites blended using ionic liquid and regenerated with various coagulation agents were investigated. Specifically, the relationship between the composition of polysaccharide-protein bio-electrolyte membranes and the resulting morphology and ionic conductivity is explored using numerous characterization techniques, including scanning …

Influence Of Deposition Temperature On Properties Of Multilayered Gallium Doped Zinc Oxide Films Prepared By Dc Magnetron Sputtering Technique, Elisante Maloda, Anayesu Malisa

Tanzania Journal of Science

Multilayered transparent conducting films based on ZnO: Ga were deposited onto glass substrate by DC magnetron sputtering technique. The films were prepared from alloy (Zn: Ga) and ceramic (ZnO: Ga) targets with gallium composition of 3 at% and 4 at%, respectively. Crystal structure and phase analysis were measured using X-ray diffractometer (XRD). The XRD structural analysis results indicated that all multilayered films were polycrystalline with (002) orientation slightly shifted of diffracting angles due to gallium dopant concentrations as increase in the deposition temperatures. The films were hexagonal wurtzite structure, having preferred growth orientation in c-axis perpendicular to the substrate surface. …