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Articles 691 - 720 of 5215

Full-Text Articles in Food Biotechnology

Fast Traceability Detection Of Astragalus Membranaceus Based On The Combination Of Electronic Tongue And Electronic Eye To Improve Mobilenetv3, Jin Xin-Ning, Liu Ming, Sang Heng-Liang, Ma Yun-Xia, Wang Zhi-Qiang Oct 2023

Fast Traceability Detection Of Astragalus Membranaceus Based On The Combination Of Electronic Tongue And Electronic Eye To Improve Mobilenetv3, Jin Xin-Ning, Liu Ming, Sang Heng-Liang, Ma Yun-Xia, Wang Zhi-Qiang

Food and Machinery

Objective: To realize the rapid traceability detection of Astragalus membranaceus from different origins. Methods: This study proposed a rapid detection method for the origin of Astragalus membranaceus based on the improved MobileNetv3 network based on the combination of electronic tongue and electronic eye. The electronic tongue and electronic eye were used to collect the one-dimensional fingerprint and two-dimensional appearance image information of different samples of Astragalus membranaceus. The Gramian Angular Field (GAF) was used to convert the one-dimensional electronic tongue signal into two-dimensional image information, retain the time series related features in the electronic tongue signal, and then fused …

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Simultaneous Determination Of 6 Pesticide Residues In Tea By Quechers-Gs-Ms/Ms, Wu Han-Bin Oct 2023

Simultaneous Determination Of 6 Pesticide Residues In Tea By Quechers-Gs-Ms/Ms, Wu Han-Bin

Food and Machinery

Objective: This study aimed to establish a method by using QuEChERS-gas chromatography tandem mass spectrometry (GC-MS/MS), to determine six pesticide residues in tea, including: hydroprene, kinoprene, genite, fluronitrofen, cycloprate, and chlornitrofen. Methods: The samples were pretreated by QuEChERS method. They were separated by gas chromatographic, detected by multiple reaction monitoring (MRM) mode and quantified by the external method. Results: All the pesticide residues showed good linearity with correlation coefficients above 0.999 when the concentration falls in the range 0.025~2.000 mg/kg, and the limits of quantitation were in the range of 0.000 6 ~0.007 2 mg/kg. In the recovery experiment of …

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Uncertainty Evaluation For The Determination Of Three Pyrethroid Pesticide Residues In Fresh Tea Leaves, Zhang Li, Liu Teng-Fei, Yao Ling-Yi, Chen Yu-Yang, Jiang Li Oct 2023

Uncertainty Evaluation For The Determination Of Three Pyrethroid Pesticide Residues In Fresh Tea Leaves, Zhang Li, Liu Teng-Fei, Yao Ling-Yi, Chen Yu-Yang, Jiang Li

Food and Machinery

Objective: The uncertainty of determination of three pyrethroid pesticides （cypermethrin, fenvalerate and deltamethrin） in fresh tea leaves by gas chromatography was evaluated. Methods: A mathematical model was established according to the determination process of the experiment, and the uncertainties caused by various factors in the model were identified. The sources are mainly the following 7 aspects: repeated determination of samples, fitness of standard curve, recovery rate, standard solution preparation, sample weighing and pretreatment, and the measurement of instrument. Results: At the spiking level of 0.10 mg/kg, the expanded uncertainty of measured values of cypermethrin, fenvalerate, and deltamethrin were 0.011, 0.011 …

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Simultaneous Determination Of 80 Veterinary Drug Residues In Chicken By Quechers-Uplc-Ms/Ms, Li Hong, Xiang Jun, Li Dan, Li Li-Juan, He Qing-Ke Oct 2023

Simultaneous Determination Of 80 Veterinary Drug Residues In Chicken By Quechers-Uplc-Ms/Ms, Li Hong, Xiang Jun, Li Dan, Li Li-Juan, He Qing-Ke

Food and Machinery

Objective: This study aimed to establish a method for the simultaneous determination of 80 veterinary drugs including quinolones, sulfonamides, receptor agonists, glucocorticoids, macrolides, tetracyclines, antiviral drugs in chicken by QuEChERS - ultra high performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS）. Methods: The samples were extracted by 1% formic acid acetonitrile aqueous solution, purified by QuEChERS multi-veterinary drug residue purification column, detected by ultra-high performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS） multi-reaction monitoring mode, and quantified by matrix standard curve external standard method. Results: The results showed that 80 kinds of veterinary drugs were highly responsive under specific mass spectrometry conditions, and the …

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Determination Of 57 Organic Pollutants In Edible Vegetable Oil By Gas Chromatography-Triple Quadrupole Mass Spectrometry, Liu Yu-Xing, Yi Shou-Fu, Xu Wen-Yang, Tang Wan-Li, Kang Shao-Ying, Wang Xia-Li Oct 2023

Determination Of 57 Organic Pollutants In Edible Vegetable Oil By Gas Chromatography-Triple Quadrupole Mass Spectrometry, Liu Yu-Xing, Yi Shou-Fu, Xu Wen-Yang, Tang Wan-Li, Kang Shao-Ying, Wang Xia-Li

Food and Machinery

Objective: Establish a high throughput method for the determination of 57 organic pollutants in edible vegetable oil. Methods: The target compounds were extracted by acetonitrile-hexane solution and purified by disperse solid phase extraction and solid phase extraction, after that the contents of 16 polycyclic aromatic hydrocarbons, 17 phthalates, 8 organochlorines and 16 polychlorinated biphenyls in edible oil were detected by gas chromatography triple quadrupole mass spectrometry. Results: All target components had an excellent linearity within the linear range of 0.001～0.1 μg/mL （r2＞0.998）, and the limits of detection was between 0.16～2.0 μg/kg, meanwhile the average recovery rate of …

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Study On The Rapid Detection Of Pseudomonas Aeruginosa By Real-Time Fluorescence Quantitative Pcr In Packaged Drinking Water, Wang Fang-Mei, Xu Yue, Lin Dan, Zhu Qiu-Yan, Hong Zhen-Bai, Jiang Wei Oct 2023

Study On The Rapid Detection Of Pseudomonas Aeruginosa By Real-Time Fluorescence Quantitative Pcr In Packaged Drinking Water, Wang Fang-Mei, Xu Yue, Lin Dan, Zhu Qiu-Yan, Hong Zhen-Bai, Jiang Wei

Food and Machinery

Objective: The molecular biological test has the advantage of fast and sensitive, which can effectively make up for the defects of the traditional microbial test method. Methods: According to the conserved sequences of the V3~V4 region of the virulence gene pcrL and the universal gene 16S rRNA of Pseudomonas aeruginosa in GB 8538—2022, primers and probes were designed and synthesized, and a real-time fluorescent PCR kit was established in this study. Results: The results showed that the common standard reserve strain 16S rRNA was amplified, and the virulence gene pcrL was only effective for nucleic acid detection of Pseudomonas aeruginosa …

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Optimization Approaches To Legal Supervision Of Import And Export Food Safety In China, Chen He-Fang Oct 2023

Optimization Approaches To Legal Supervision Of Import And Export Food Safety In China, Chen He-Fang

Food and Machinery

At present, China has preliminarily established a food safety supervision system for imports and exports, with the current 21 year Food Safety Law as the basic law and the inspection and quarantine department as the main regulatory body. However, there are still problems such as low food safety standards, low management and technical level of regulatory departments, and lack of necessary coordination with major trading partners. In this regard, we can optimize and construct the legal supervision of China's import and export food safety from the dimensions of building scientific food safety standards that are in line with international standards, …

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Structural Design And Experiment Of Automatic Cooking Machine, Zhang Fan, Ning Meng, Deng Qian Oct 2023

Structural Design And Experiment Of Automatic Cooking Machine, Zhang Fan, Ning Meng, Deng Qian

Food and Machinery

Objective: In view of the problems of large size and low heating uniformity of the existing cooking machine, a miniaturized drum-type automatic cooking machine with electromagnetic heating was designed to reduce the equipment volume and improve the cooking effect. Methods: The modular design method oriented to function and structure was adopted to design each module mechanism of the frying machine. Then, based on Biot-Savart law, the relationship between the magnetic field generated by the coil in space and the current and distance is obtained, and the distribution curves of magnetic field intensity and temperature on the surface of the cooker …

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Design And 3d Flow Field Analysis Based On Ansys/Cfx Stepwise Acceleration Twin Screw, Tian Dong, Guo Shu-Guo, Wang Li-Yan Oct 2023

Design And 3d Flow Field Analysis Based On Ansys/Cfx Stepwise Acceleration Twin Screw, Tian Dong, Guo Shu-Guo, Wang Li-Yan

Food and Machinery

Objective: To improve the mixing efficiency and working performance of the new twin-screw extruder. Methods: A new twin-screw extruder with embedded planetary gear train and kneading block was designed. A three-dimensional model was established by SolidWorks, and the flow field analysis of the flow channel was performed by ANSYS/CFS finite element analysis software based on the finite volume method. The Macroscopic pressure diagram, velocity vector diagram, velocity flow diagram were gotten, which was compared with the traditional twin-screw extruder three-dimensional flow field. Results: Under the gradual action of the planetary gear train and the kneading block, the mixing performance and …

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Design Of Appearance Quality Grading System For Apricot Mushroom Based On Machine Vision, Liu Hao, Lin Xin-Hua, Zhu Ya-Nan, Zhou Zhu, Wang Min, Chen Xue-Yong Oct 2023

Design Of Appearance Quality Grading System For Apricot Mushroom Based On Machine Vision, Liu Hao, Lin Xin-Hua, Zhu Ya-Nan, Zhou Zhu, Wang Min, Chen Xue-Yong

Food and Machinery

Objective: This study aimed to induce the machine vision technology into the appearance detection of Pleurotus eryngii. Methods: A bilateral filter was proposed to replace Gaussian filter as image smoothing filter, and Ostu maximum inter-class variance method was proposed to replace the improved Canny operator, based on fixed double threshold segmentation, and used as edge detection algorithm. HALCON operator and color space conversion were used to extract the length, diameter, curvature, evenness, color and cap defects of P. erynii, and the development and design of visual software function modules were completed, under the VS 2017 development environment with HALCON …

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Design Of Fruit Grading System Based On Machine Vision, Liu Jia-Hao, Gao Jun-Wei, Zhang Bing-Xing, Wang Jian-Chong Oct 2023

Design Of Fruit Grading System Based On Machine Vision, Liu Jia-Hao, Gao Jun-Wei, Zhang Bing-Xing, Wang Jian-Chong

Food and Machinery

Objective: In order to solve the problems of low efficiency and high false detection rate of current fruit classification detection methods, a fruit classification system based on machine vision was designed with apples as the sorting object. Methods: The apple image collected in real time was preprocessed, the improved Canny edge detection algorithm was used to extract the edge, and the radius of the apple cross-section was obtained by fitting the edge coordinates with the minimum peripheral circle method. The acquired RGB image was converted to HSI image, and the proportion of red region is calculated according to the range …

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Effects Of Different Sterilization Treatments On The Quality Of Fermented Jujube Juice, Zhang Li-Hua, Feng Lu-Yao, Tang Pei-Xin, Li Shun-Feng, Zong Wei Oct 2023

Effects Of Different Sterilization Treatments On The Quality Of Fermented Jujube Juice, Zhang Li-Hua, Feng Lu-Yao, Tang Pei-Xin, Li Shun-Feng, Zong Wei

Food and Machinery

Objective: This study aimed to compare the effects of different sterilization on the quality of fermented jujube juice. Methods: The effects of cold plasma sterilization (CPS) and pulsed strong light sterilization (PLS) on the quality of jujube juice before and after fermentation were studied, with high pressure sterilization (SA) jujube juice as the control. Results: The contents of total sugar, reducing sugar and soluble solid in jujube juice before and after fermentation by CPS treatment were significantly higher than those of the other two sterilization methods, and the contents of total sugar, reducing sugar and soluble solid in jujube juice …

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Effect Of Water Content On The Growth Of A. Flavus And Aflatoxin M1 Accumulation During Storage Of Fresh Walnut In Xinjiang, Wang Yuan-Meng, Bai Yu-Jia, Feng Zuo-Shan, Cheng Huan Oct 2023

Effect Of Water Content On The Growth Of A. Flavus And Aflatoxin M1 Accumulation During Storage Of Fresh Walnut In Xinjiang, Wang Yuan-Meng, Bai Yu-Jia, Feng Zuo-Shan, Cheng Huan

Food and Machinery

Objective: To improve the storage safety of Xinjiang fresh walnut. Methods: Xinjiang "Xin 2" thin-skinned walnut was used as material, sterile water was inoculated as a control group, and Aspergillus flavus was inoculated as an experimental group. The Aspergillus flavus isolated and purified from naturally moldy walnut was artificially inoculated into Xinjiang thin-skinned fresh walnut with different water content （10%, 15%, 20%, 25%, 30%） to investigate the growth and toxicity of Aspergillus flavus. Results: The water content of walnut which was suitable for the growth of Aspergillus flavus and the secretion of Aflatoxin M1 was 15%. With the …

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Effect Of Different Drying Methods On The Quality Of Rugao Black Pakchoi, Du Xin-Yu, Wan Jin-Qing, Wang Yuan-Yuan, Wang You-Jun, Sun Xiao-Lin, Tong Nian Oct 2023

Effect Of Different Drying Methods On The Quality Of Rugao Black Pakchoi, Du Xin-Yu, Wan Jin-Qing, Wang Yuan-Yuan, Wang You-Jun, Sun Xiao-Lin, Tong Nian

Food and Machinery

Objective: This study aimed to investigated the effect of ice-temperature vacuum drying on the powder quality of selenium-rich Rugao black pakchoi. Methods: After pretreatment, the fresh black pakchoi was dried to the moisture content of (5.0±0.5) %, and the physical and chemical indexes were investigated, comparing to the control groups of hot-air drying, vacuum drying and freeze-vacuum drying. Results: The vitamin C content of vacuum drying at ice temperature was 554.60 mg/100 g, and the retention rate reached 83.96%, which was 43.11%, 33.57% and 1.61% higher than that of hot-air drying, vacuum drying and freeze-vacuum drying, respectively. Glutathione peroxidase had …

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Research On Apple Defect Detection Method Based On Improved Cnn, Du Guo-Zhen, Lu Ming-Xing, Ji Ze-Xu, Liu Ji-Chao Oct 2023

Research On Apple Defect Detection Method Based On Improved Cnn, Du Guo-Zhen, Lu Ming-Xing, Ji Ze-Xu, Liu Ji-Chao

Food and Machinery

Objective: To solve the problems of low accuracy and poor efficiency in existing apple defect detection methods. Methods: Based on a fruit image acquisition system, an improved convolutional neural network was proposed for detecting surface defects in apples. Deep separable convolution was Introduced to replace the original network standard convolution, to improve the speed of feature extraction. The Leaky ReLU activation function was introduced to replace the ReLU activation function to improve the calculation efficiency and accuracy. Global average pooling was introduced to replace the fully connected layer, to reduce the computational complexity of the network model. After each layer …

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Effects Of Dry Ice Freezing On Ice Crystal And Quality Of Large Yellow Croaker （Pseudosciaena Crocea） During Frozen Storage, Jia Shi-Liang, Yang Yue, Zheng Ya-Dan, Yang Peng, Ding Yu-Ting Oct 2023

Effects Of Dry Ice Freezing On Ice Crystal And Quality Of Large Yellow Croaker （Pseudosciaena Crocea） During Frozen Storage, Jia Shi-Liang, Yang Yue, Zheng Ya-Dan, Yang Peng, Ding Yu-Ting

Food and Machinery

Objective: The effects of freezing method and storage temperature on the quality of large yellow croaker during storage were investigated. Methods: Fresh large yellow croaker fillets were frozen with dry ice and air freezing (-40 ℃) to the central temperature of -18 ℃, and then stored at -40 ℃ and -18 ℃, respectively. Physical and chemical indexes such as freezing curve, ice crystal morphology, pH value, volatile base nitrogen, K value, Ca2+-ATPase activity, total sulfhydryl group, carbonyl group, protein degradation and texture characteristics of large yellow croaks were determined after freezing and during freezing storage. Results: The time …

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Inhibition Of Psoriasis-Like Inflammation In Mice By Sesamol, Chen Xue, Liu Xue-Bo, Wang Yu-Xuan Oct 2023

Inhibition Of Psoriasis-Like Inflammation In Mice By Sesamol, Chen Xue, Liu Xue-Bo, Wang Yu-Xuan

Food and Machinery

Objective: This study aimed to explore the improvement effect of sesamol on skin lesions caused by psoriasis. Methods: The psoriasis model was constructed by using 5% imiquimod cream applied to the backs of mice for seven consecutive days, with sesamol intervention used from one week before to the end of modelling to explore the protective effect of sesamol on the skin. Then, observed and measured skin thickness, PASI score, spleen index, pathological tissue sections, cytokines (IL-17, IL-23, TNF-α and other inflammatory factors and chemokines like CXCL1 and CCL20), and inflammatory factors (IL-17, TNF-α) in plasma of mice …

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Optimization Of Preparation Process Of Fermented Peanut Milk Complexed With Hypoallergenic Protein Ara H 1 And Probiotics, Sun Chang, Lu Chen-Yu, Li Tie-Zhu, Hu Ji-Mei, Huang Wei Oct 2023

Optimization Of Preparation Process Of Fermented Peanut Milk Complexed With Hypoallergenic Protein Ara H 1 And Probiotics, Sun Chang, Lu Chen-Yu, Li Tie-Zhu, Hu Ji-Mei, Huang Wei

Food and Machinery

Objective: This study aimed to develop a kind of fermented hypoallergenic peanut milk with lactic acid bacteria. Methods: The crude protein content and Ara h 1 concentration in different peanut varieties were determined by the kit, and the peanut varieties with the lowest Ara h 1 content were selected to make fermented milk. Response surface method was used to optimize the preparation process of fermented peanut milk with the maximum reduction of sensitizing protein Ara h 1 content with different inoculation amount, inoculation species, fermentation time and sugar addition amount as factors. The compound fermented peanut milk with probiotics was …

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Optimization Of Compound Shrimp Mince Gel Based On Texture Properties, Man Hao, Liu Fu-Jun, Ge Jing-Hui, Guo Xuan, Li Dong-Mei Oct 2023

Optimization Of Compound Shrimp Mince Gel Based On Texture Properties, Man Hao, Liu Fu-Jun, Ge Jing-Hui, Guo Xuan, Li Dong-Mei

Food and Machinery

Objective: To promote the intensive processing of Antarctic Krill and enrich the types of minced shrimp products. Methods: Using Krill meat and prawn meat as main raw materials, waxy corn acetylated distarch adipate, egg white powder, soy protein isolate, glutamine transaminase and other adjuvants were added, and the optimal preparation ratio of shrimp balls was obtained through single factor test and response surface test. Results: The optimal preparation ratio of shrimp balls was 6.00% waxy corn acetylated distarch adipate, 5.00% egg white powder, 5.00% soy protein isolate, 0.50% glutamine transaminase and 0.20% konjac gum. Conclusion: The two-stage heating method is …

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Research Advances On The Functions Of Probiotic Fermented Milk In Regulating Body Health, Zhao Cui-Yu, Wu Zi-Jian, Li Shu-Sen, Liu Ju-Long, Zhang Xin-Yu, Sun Er-Na, Wen Yan Oct 2023

Research Advances On The Functions Of Probiotic Fermented Milk In Regulating Body Health, Zhao Cui-Yu, Wu Zi-Jian, Li Shu-Sen, Liu Ju-Long, Zhang Xin-Yu, Sun Er-Na, Wen Yan

Food and Machinery

Probiotic fermented milk is an important carrier of probiotics. It enhances the nutritional and health properties of fermented milk by improving the balance of host intestinal microflora and promoting the metabolism of beneficial ingredients. This review expounds the auxiliary effects of probiotics fermented milk in improving intestinal function, regulating body immunity, assisting in treating metabolic diseases and improving mental system diseases, etc., in order to provide theoretical support for expanding the application of probiotics fermented milk.

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Research Progress Of Blunt Enzyme Technology For Radiofrequency Sterilization Of Agricultural Products, Dong Yi-Fei, Ling Jian-Gang, Zhu Lin, Li Su-Hong Oct 2023

Research Progress Of Blunt Enzyme Technology For Radiofrequency Sterilization Of Agricultural Products, Dong Yi-Fei, Ling Jian-Gang, Zhu Lin, Li Su-Hong

Food and Machinery

Agricultural products usually contain a large number of spoilage bacteria and endogenous enzymes, which can adversely affect the quality of agricultural products. Radio frequency is a kind of dielectric heating technology, which has fast heating speed and high efficiency, can effectively inactivate microorganisms and endogenous enzymes in agricultural products and has little influence on the quality of agricultural products， such as color, texture and nutritional composition, etc. This review summarized the mechanism of action of radiofrequency sterilization blunt enzyme technology and its application in agricultural products processing in recent years, and the shortcomings and solutions of radiofrequency sterilization blunt enzyme …

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Research Progress On Physicochemical Properties And Biological Activity Of Theabrownin, Dai Li-Feng, Jiang Jie-Lin, Guan Xing-Li, Zou Xiao-Lin, Fu Zong-Lin, Luo Sai, Yang Zhi Oct 2023

Research Progress On Physicochemical Properties And Biological Activity Of Theabrownin, Dai Li-Feng, Jiang Jie-Lin, Guan Xing-Li, Zou Xiao-Lin, Fu Zong-Lin, Luo Sai, Yang Zhi

Food and Machinery

Theabrownin, a kind of water-soluble, non-dialysable, highly polymerised brown substance, mainly composed of polyphenol, polysaccharide, protein and nucleic acid, which is closely related to the color and functional activity of fermented tea. Due to the complexity of the formation mechanism, its chemical structure is still unclear. In this review, the structural characteristics, formation mechanism, extraction and detection methods, and functional activity of theophylcin were discussed, and the future research direction was also prospected.

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Application Progress Of Gas Chromatography-Mass Spectrometry In Food Analysis, Xing Qian-Qian, Liu Zhen-Min, Hong Qing, You Chun-Ping Oct 2023

Application Progress Of Gas Chromatography-Mass Spectrometry In Food Analysis, Xing Qian-Qian, Liu Zhen-Min, Hong Qing, You Chun-Ping

Food and Machinery

Gas chromatography-mass spectrometry combines the advantages of efficient and rapid gas chromatography and accurate identification by mass spectrometry. Gas chromatography-mass spectrometry has been widely used in the separation and analysis of volatile components in food recently. This paper reviewed the application progress of GC in food analysis, introduces the separation mechanism of GC, the types of GC columns and the classification of detectors. The application progress of GC-MS in food analysis was reviewed, and the separation process of gas chromatography, the classification of chromatographic columns and the classification of detectors were introduced. Moreover, the applications of gas chromatography-mass spectrometry in …

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Research On The Characteristics And Application Of Food Materials In Food 3d Printing, Tong Qiang, Jiang Yu, Tong Yao, Meng Yu-Xiang, Dong Xiu-Ping Oct 2023

Research On The Characteristics And Application Of Food Materials In Food 3d Printing, Tong Qiang, Jiang Yu, Tong Yao, Meng Yu-Xiang, Dong Xiu-Ping

Food and Machinery

Food material is the key factor of food 3D printing. This review summarized the characteristics of food materials (protein, starch, hydrogel and fat) commonly used in food 3D printing at present, analyzed the influence of different material combinations on the forming performance. Moreover, suggestions on how to improve the printing effect of difficult printing materials were also provided, and the technical bottleneck of food materials development faced in food 3D printing nowadays were noticed. Finally, the direction of food 3D printing technology in the future was prospected.

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Whole Genome Analysis And Molecular Traceability Of Pseudomonas Aeruginosa In Drinking Water, Guo Kun-Peng, Zhang Hai-Yun, He Juan, Gao Han, Yang Tao, Song Sheng Oct 2023

Whole Genome Analysis And Molecular Traceability Of Pseudomonas Aeruginosa In Drinking Water, Guo Kun-Peng, Zhang Hai-Yun, He Juan, Gao Han, Yang Tao, Song Sheng

Food and Machinery

Objective: Provide data support for the source tracing and pollution prevention of Pseudomonas aeruginosa in drinking water in Hunan Province. Methods: According to the national food safety standards of GB 8538—2016, the bottled water was tested randomly collected from partial cities and counties in Hunan Province, and the whole genome sequencing and molecular traceability of the 18 strains of Pseudomonas aeruginosa were detected. The carrying of virulence genes and drug resistance genes was detected. Results: It was confirmed that four strains of Pseudomonas aeruginosa showed consistency in terms of geographical distance, genetic distance, pathogenic and drug-resistant genotypes, and it was …

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Purification Of Polyphenols From Wormwood By Macroporous Resin And Inhibitory Activity Of Its Against Α-Glucosidase, Wu Ping-Xiang, Wei Ming, Ding Kai-Li, Nie Feng Oct 2023

Purification Of Polyphenols From Wormwood By Macroporous Resin And Inhibitory Activity Of Its Against Α-Glucosidase, Wu Ping-Xiang, Wei Ming, Ding Kai-Li, Nie Feng

Food and Machinery

Objective: This study aimed to purify crude polyphenols from wormwood and to study inhibitory activity of its against α-glucosidase. Methods: The adsorption-desorption properties of wormwood polyphenols by seven kinds of macroporous resins were studied. The suitable resin for separating and purifying Wormwood polyphenols was obtained and the purification parameters were optimized. Using different concentration ethanol solution for dynamic elution, the inhibitory activity of different elution fractions on α-glucosidase was investigated. Results: The results indicated that D101 resin was a suitable material for purifying wormwood polyphenols and the macroporous resin reached equilibrium within 120 min. The optimal conditions for …

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Taste Evaluation Of Chinese Oolong Tea “Baiyaqilan” Based On Physiological Signals And Multivariate Statistics, Yang Bo-Kai, Shen Li-Juan, Yang Jing-Min Oct 2023

Taste Evaluation Of Chinese Oolong Tea “Baiyaqilan” Based On Physiological Signals And Multivariate Statistics, Yang Bo-Kai, Shen Li-Juan, Yang Jing-Min

Food and Machinery

Objective: Investigate young people's taste preference for white bud kiran tea and design tea drinks accordingly. Methods: Design a combination of electroencephalogram （EEG）, electrodermal activity （EDA）, heart rate variability （HRV） multivariate statistical analysis and sensory evaluation to allow 24 subjects （12 of each gender） to evaluate the taste preference of seven batches of white bud kiran tea of different grams and brewing lengths. Results: the mean values of power spectral density, HRV and EDA of EEG can predict the taste preference of the subjects more accurately, and the mean values are negatively correlated with the liking level. A two-way analysis …

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Simultaneous Determination Of 21 Perfluorinated Compounds In Animal-Derived Food By Uplc-Ms/Ms, Tang Yun-Xi, Bai Ya-Min, Liu Lu-Lu, Yu Jie Oct 2023

Simultaneous Determination Of 21 Perfluorinated Compounds In Animal-Derived Food By Uplc-Ms/Ms, Tang Yun-Xi, Bai Ya-Min, Liu Lu-Lu, Yu Jie

Food and Machinery

Objective: To established a method for determination of 21 perfluorinated compounds in animal-derived food by ultra-performance liquid chromatography-tandem mass spectrometry （UPLC-MS/MS）. Methods: The sample was extracted with 1% formic acid-acetonitrile, cleaned up with a sorbent mixture of N-propylethylenediamine （PSA）, octadecyl bonded silica gel （C18） and graphitized carbon black （GCB）, then separated by acetonitrile-5mmol/L ammonium acetate aqueous solution and Acquity UPLC BEH C18, detected by liquid chromatography tandem mass spectrometry in negative mode using the multiple reaction monitoring （MRM） mode. Results: The calibration curves were linear in the range of 0.2~10 ng/mL for the 21 …

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Modified Quechers Method Combined With Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry For Simultaneous Determination Of 19 Quinolones And Sulfonamides In Aquatic Products, Sun Juan, Yang Jing, Zhao Chun-Hui, Shen Yuan, Li Ying, Fang Fang Oct 2023

Modified Quechers Method Combined With Ultra-High Performance Liquid Chromatography-Tandem Mass Spectrometry For Simultaneous Determination Of 19 Quinolones And Sulfonamides In Aquatic Products, Sun Juan, Yang Jing, Zhao Chun-Hui, Shen Yuan, Li Ying, Fang Fang

Food and Machinery

Objective: A simultaneous determination method was established for detecting 19 kinds of quinolones and sulfonamides in aquatic products simultaneously, by using QuEChERS combined with UPLC-MS/MS. Methods: Samples were extracted with 1.0% formic acid acetonitrile solution, ultrasonic for 1 min, and purified by QuEChERS multi-function needle filter. The sample purification and filtering were performed simultaneously. The Mass spectrometry was conducted by using positive (ESI+) electrospray ionization and multi-reactions monitoring (MRM) models, with external standard method. Results: The detection limit of 19 kinds of sulfonamides and quinolones is from 0.5 to 1.0 μg/kg. Compared with the national standard method, the detection sensitivity …

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Rapid Determination Of 56 Pesticide Residues In Dendrobium Officinale By Mpfc-Quechers Method Combined With Ultra-Performance Liquid Chromatography-Tandem Mass Spectrometry, Li Zhan-Bin, Zhao Li-Jun, Huang Yong-Qiao, Wang Xue, Lu Yang Oct 2023

Rapid Determination Of 56 Pesticide Residues In Dendrobium Officinale By Mpfc-Quechers Method Combined With Ultra-Performance Liquid Chromatography-Tandem Mass Spectrometry, Li Zhan-Bin, Zhao Li-Jun, Huang Yong-Qiao, Wang Xue, Lu Yang

Food and Machinery

Objective: In order to analyze the risk of pesticide residues in D. officinale, a method for rapid determination of 56 pesticide residues in D. officinale by a kind of ultrafiltration purification column（MPFC-QuEChERS） combined with ultra-performance liquid chromatography- tandem mass spectrometry（UHPLC-MS/MS）was developed. Methods: The samples were extracted with acetonitrile contained 0.1% formic acid, salted out, shaken, centrifuged, and single-step purified by a MPFC-QuEChERS purification column. Mass spectrometer was operated in the positive and negative ion mode using select reaction monitoring for qualitative and quantitative analysis. Results: The result showed that, the 56 kinds of pesticides showed good linearity when they …

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