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Articles 1081 - 1110 of 3533

Full-Text Articles in Nanoscience and Nanotechnology

Synthesis And Characterization Of Molybdenum Disulfide/Conducting Polymer Nanocomposite Materials For Supercapacitor Applications, Turki S. Alamro Apr 2019

Synthesis And Characterization Of Molybdenum Disulfide/Conducting Polymer Nanocomposite Materials For Supercapacitor Applications, Turki S. Alamro

USF Tampa Graduate Theses and Dissertations

The needs for energy storage devices have kindled researchers desire to explore and synthesize nanocomposite materials. Storing energy efficiently, effectively and sustainably are the science and engineering communities’ highest priorities to develop electrochemical energy storage devices. Supercapacitors have become power solution not only because supercapacitors can bridge the gap between the traditional capacitors and rechargeable batteries but also because of many other advantages which include extraordinary electrochemical properties, wide working-temperature range, cost effective, safe operation and long/stable cycle life. They have higher current pules than batteries due to the mechanism of charging and discharging. Batteries charging and discharging via chemical …

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Numerical Simulation Of Viscoelastic Flow In Micro/Nanochannels, Lanju Mei Apr 2019

Numerical Simulation Of Viscoelastic Flow In Micro/Nanochannels, Lanju Mei

Mechanical & Aerospace Engineering Theses & Dissertations

Micro/Nanofluidic devices often involve use of biological fluids or polymeric solutions that cannot be simply treated as Newtonian fluids. The numerical simulation for the complex fluids at micro/nanoscale presents a significant computational challenge, and the inclusion of electrokinetic body force further increases the complexity. Specifically, the well-known High Weissenberg Number Problem (HWNP) has become a challenge for the numerical simulation of viscoelastic fluid. This dissertation is aimed to develop a numerical tool to simulate the behavior of viscoelastic fluid in the micro/nanochannel. The most popular log-conformation reformulation to solve the HWNP is presented and implemented in a finite volume scheme. …

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The Effect Of Defects And Surface Modification On Biomolecular Assembly And Transport, Haneen Martinez Mar 2019

The Effect Of Defects And Surface Modification On Biomolecular Assembly And Transport, Haneen Martinez

Nanoscience and Microsystems ETDs

Nanoscale transport using the kinesin-microtubule (MT) biomolecular system has been successfully used in a wide range of nanotechnological applications including self-assembly, nanofluidic transport, and biosensing. Most of these applications use the ‘gliding motility geometry’, in which surface-adhered kinesin motors attach and propel MT filaments across the surface, a process driven by ATP hydrolysis. It has been demonstrated that active assembly facilitated by these biomolecular motors results in complex, non-equilibrium nanostructures currently unattainable through conventional self-assembly methods. In particular, MTs functionalized with biotin assemble into rings and spools upon introduction of streptavidin and/or streptavidin-coated nanoparticles. Upon closer examination of these structures …

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Electrochemical Modification Of Granular Activated Carbon And Carbon Nanofibers To Determine Effect On Adsorption, Jose E. Martinez Sanchez Mar 2019

Electrochemical Modification Of Granular Activated Carbon And Carbon Nanofibers To Determine Effect On Adsorption, Jose E. Martinez Sanchez

Theses and Dissertations

Granular activated carbon and carbon nanofiber samples were tested as is and electrochemically modified to determine the effect on adsorption. An electrochemical cell was used to modify the carbon samples. The samples were then used in bench bottle tests with 2,4-dinitrotoluene (DNT), brilliant blue (BB) dye, and methylene blue (MB) dye solutions and sampled over time intervals. An ultraviolet–visible spectrophotometer was used to analyze the results of the bottle bench tests. The results indicated that electrochemically modified coal-based carbons’ adsorption were improved 25% over the adsorption of the as is carbon samples prior to modification. The electrochemical modification increased adsorption …

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Nanoparticle Synthesis For Glucose-Loaded Mesoporous Silica And Sucrose Hydrolysis Strategies For Bioanalyte Detection Applications Using A Personal Glucose Meter, Xiomar Emauel Bustos Perez Mar 2019

Nanoparticle Synthesis For Glucose-Loaded Mesoporous Silica And Sucrose Hydrolysis Strategies For Bioanalyte Detection Applications Using A Personal Glucose Meter, Xiomar Emauel Bustos Perez

USF Tampa Graduate Theses and Dissertations

Point-of-care (POC) tests are a reliable, portable, easy to use, and more affordable alternative to regular laboratory diagnostic tests. They bypass the necessity of expensive equipment, human labor, and technical expertise. The personal glucose meter (PGM) is a POC device that measures glucose levels in blood. Lately, the PGM have been used as a tool to detect other bioanalytes in different applications. There are two analytes which POC detection would be beneficial for patients: creatinine and tacrolimus. Creatinine is used to calculate glomerular filtration rate, a measurement of kidneys function that can help to diagnose kidney failure, and other nephropathies. …

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Axitinib Loaded Plga Nanoparticles For Age-Related Macular Degeneration, Priya P. Narvekar Mar 2019

Axitinib Loaded Plga Nanoparticles For Age-Related Macular Degeneration, Priya P. Narvekar

USF Tampa Graduate Theses and Dissertations

Despite of all the research going on for the treatment of ocular diseases, age-related macular degeneration (AMD) remains one of the serious vision threatening disease worldwide. Choroidal neovascularization, a pathophysiological characteristic of wet AMD, is the growth of anomalous blood vessels in the eye choroidal layer. Neovascularization is a key factor in AMD and thus anti-angiogenic therapy is beneficial in reducing the development of new abnormal blood vessels to prevent progression of AMD. Axitinib, multi-receptor tyrosine kinase inhibitor, is a small molecule that works by blocking vascular endothelial growth factor receptors (VEGFR) and platelet derived growth factor receptors (PDGFR) responsible …

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Removal Of Synthetic Azo Dye Using Bimetallic Nickel-Iron Nanoparticles, Shelby L. Foster, Katie Estoque, Michael Voecks, Nikki Rentz, Lauren F. Greenlee Mar 2019

Removal Of Synthetic Azo Dye Using Bimetallic Nickel-Iron Nanoparticles, Shelby L. Foster, Katie Estoque, Michael Voecks, Nikki Rentz, Lauren F. Greenlee

Chemical Engineering Faculty Publications and Presentations

Bimetallic nanoparticles comprised of iron (Fe) and nickel (Ni) were investigated for the removal of an azo dye contaminant in water. Morphology (core shell and alloy) and metal molar ratio (Ni2Fe10, Ni5Fe10, and Ni10Fe10) were tested as key nanoparticle properties. The shelf life of the nanoparticles was tested over a 3-week period, and the effect of initial nanoparticle concentration on dye removal was evaluated. The highest initial nanoparticle concentration (1000 mg/L) showed consistent Orange G removal and the greatest extent of dye removal, as compared to the other tested concentrations (i.e., 750 mg/L, 500 mg/L, and 250 mg/L) for the …

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Soft , Multilayered Electronics For Wearable Devices And Methods To Produce The Same, Carmel Majidi, Michael D. Bartlett, Eric J. Markvicka Mar 2019

Soft , Multilayered Electronics For Wearable Devices And Methods To Produce The Same, Carmel Majidi, Michael D. Bartlett, Eric J. Markvicka

Department of Mechanical and Materials Engineering: Faculty Publications

Disclosed herein is an efficient fabrication approach to create highly customizable wearable electronics through rapid laser machining and adhesion - controlled soft materials assembly . Well - aligned , multi - layered materials can be created from 2D and 3D elements that stretch and bend while seamlessly integrating with rigid components such as micro chip integrated circuits ( IC ) , discrete electrical components , and interconnects . These techniques are applied using commercially available materials . These materials and methods enable custom wearable electronics while offering versatility in design and functionality for a variety of bio - monitor ing …

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Analysis Of Dynamic Behaviour Of A Tensioned Carbon Nanotube In Thermal And Pressurized Environments, Ahmed Yinusa, Gbeminiyi Sobamowo Mar 2019

Analysis Of Dynamic Behaviour Of A Tensioned Carbon Nanotube In Thermal And Pressurized Environments, Ahmed Yinusa, Gbeminiyi Sobamowo

Karbala International Journal of Modern Science

In this paper, the dynamic behaviour of a tensioned single-walled carbon nanotubes (SWCNT) in thermal and pressurized environments is investigated analytically. With the applications of Bernoulli-Euler and thermal elasticity mechanics theories, the governing equation of motion are developed and solved using Laplace and Fourier transforms. The results of the close form solution in this work are in excellent agreements with past results in literature. From the parametric studies, it is established that as the magnitude of the pressure distribution at the surface increases, the deflection associated with the nanotube increases at any mode of vibration. However, a corresponding increase in …

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Å-Indentation For Non-Destructive Elastic Moduli Measurements Of Supported Ultra-Hard Ultra-Thin Films And Nanostructures, Filippo Cellini, Yang Gao, Elisa Riedo Mar 2019

Å-Indentation For Non-Destructive Elastic Moduli Measurements Of Supported Ultra-Hard Ultra-Thin Films And Nanostructures, Filippo Cellini, Yang Gao, Elisa Riedo

Publications and Research

During conventional nanoindentation measurements, the indentation depths are usually larger than 1–10 nm, which hinders the ability to study ultra-thin films (<10 >nm) and supported atomically thin two-dimensional (2D) materials. Here, we discuss the development of modulated Å-indentation to achieve sub-Å indentations depths during force-indentation measurements while also imaging materials with nanoscale resolution. Modulated nanoindentation (MoNI) was originally invented to measure the radial elasticity of multi-walled nanotubes. w, by using extremely small amplitude oscillations (<<1 Å) at high frequency, and stiff cantilevers, we show how modulated nano/Å-indentation (MoNI/ÅI) enables non-destructive measurements of the contact stiffness and indentation modulus of ultra-thin ultra-stiff films, including CVD diamond films (~1000 GPa stiffness), as well as the transverse modulus of 2D materials. Our analysis demonstrates that in presence of a standard laboratory noise floor, the signal to noise ratio of MoNI/ÅI implemented with a commercial atomic force microscope (AFM) is such that a dynamic range of 80 dB –– achievable with commercial Lock-in amplifiers –– is sufficient to observe superior indentation curves, having indentation depths as small as 0.3 Å, resolution in indentation <0.05 Å, and in normal load <0.5 nN. Being implemented on a standard AFM, this method has the potential for a broad applicability.

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Gastrointestinal Sensor Implantation System, Benjamin Terry, Weston Lewis, Wanchuan Xie, Pengbo Li, Alfred Tsubaki Mar 2019

Gastrointestinal Sensor Implantation System, Benjamin Terry, Weston Lewis, Wanchuan Xie, Pengbo Li, Alfred Tsubaki

Department of Mechanical and Materials Engineering: Faculty Publications

A gastrointestinal ( GI ) sensor deployment device is dis closed . In implementations , the sensor deployment device includes an orally - administrable capsule with a tissue cap ture device removably coupled to the orally - administrable capsule . The tissue capture device includes a plurality of fasteners for connecting the tissue capture device to GI tissue within a body . A biometric sensor is coupled to the tissue capture device for continuous or periodic monitoring of the GI tract of the body at the GI tissue attachment location . A chamber within the orally - administrable capsule is …

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Interactions Between Dislocations And Three-Dimensional Annealing Twins In Face Centered Cubic Metals, Yanxiang Liang, Xiaofang Yang, Mingyu Gong, Guisen Liu, Qing Liu, Jian Wang Mar 2019

Interactions Between Dislocations And Three-Dimensional Annealing Twins In Face Centered Cubic Metals, Yanxiang Liang, Xiaofang Yang, Mingyu Gong, Guisen Liu, Qing Liu, Jian Wang

Department of Mechanical and Materials Engineering: Faculty Publications

Annealing twins often form in metals with a face centered cubic structure during thermal and mechanical processing. Here, we conducted molecular dynamic (MD) simulations for copper and aluminum to study the interaction processes between {1 1 1}1/2 <1 1 0> dislocations and a three-dimensional annealing twin. Twin boundaries are characterized with Σ3{1 1 1} coherent twin boundaries (CTBs) and Σ3{1 1 2} incoherent twin boundaries (ITBs). MD results revealed that dislocation-ITB interactions affect slip transmission for a dislocation crossing CTBs, facilitating the nucleation of Lomer dislocation.

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Recent Developments In Surface/Interface Modulation And Structure-Performance Relationship Of Cathode Catalysts For Li-Air Batteries, Rui Gao, Jun-Kai Wang, Zhong-Bo Hu, Xiang-Feng Liu Feb 2019

Recent Developments In Surface/Interface Modulation And Structure-Performance Relationship Of Cathode Catalysts For Li-Air Batteries, Rui Gao, Jun-Kai Wang, Zhong-Bo Hu, Xiang-Feng Liu

Journal of Electrochemistry

Lithium-air battery has been considered to be one of the most promising secondary battery systems because of its high energy density. However, the sluggish kinetics of the oxygen reduction reaction (ORR) and oxygen evolution reaction (OER) on the cathode, and the high overpotential, poor cycle stability and low rate capacity have severely blocked the development and application of Li-air battery. One of the effective strategies to alleviate these issues is to develop cathode catalysts for Li-air batteries. The design and development of bifunctional cathode catalysts with high activity and efficiency on both ORR and OER is highly desired for Li-air …

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Development Of A Counter-Flow Thermal Gradient Microfluidic Device, Shayan Davani Feb 2019

Development Of A Counter-Flow Thermal Gradient Microfluidic Device, Shayan Davani

Doctoral Dissertations

This work presents a novel counter-flow design for thermal stabilization of microfluidic thermal reactors. In these reactors, precise control of temperature of the liquid sample is achieved by moving the liquid sample through the thermal zones established ideally through the conduction in the solid material of the device. The goal here is to establish a linear thermal distribution when there is no flow and to minimize the temperature change at flow condition. External convection as well as internal flowinduced effects influence the prescribed thermal distribution. The counter-flow thermal gradient device developed in this study is capable of both stabilizing the …

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Optimization Of Processing Parameters Of Nanocomposite Film For Fresh Sliced Okra Packaging, Adeshina Fadeyibi Phd, Zinash Delebo Osunde Phd, Professor, Mohammed Gana Yisa Professor Feb 2019

Optimization Of Processing Parameters Of Nanocomposite Film For Fresh Sliced Okra Packaging, Adeshina Fadeyibi Phd, Zinash Delebo Osunde Phd, Professor, Mohammed Gana Yisa Professor

Journal of Applied Packaging Research

Nanocomposite film can be regarded as an active packaging material which is capable of curtailing microbial growth and keeping food for an extended life. In this research, the optimum processing parameters of cassava starch-zinc nanocomposite film was determined for packaging fresh-sliced okra. Samples of the films, with thickness ranging between 15– 17µm, were developed from the blends of 24g of cassava starch, 0–2 % zinc nanoparticles (NP) and 45–55 % glycerol in 600 ml distilled water. The ideal film was determined by optimizing the film processing parameters using Box-Behnken Design in Surface Response Methodology. It was subsequently used to package …

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Electrical Properties And Electromagnetic Interference Shielding Effectiveness Of Interlayered Systems Composed By Carbon Nanotube Filled Carbon Nanofiber Mats And Polymer Composites, Claudia A. Ramirez-Herrera, Homero Gonzalez, Felipe De La Torre, Laura Benitez, Jose G. Cabanas-Moreno, Karen Lozano Feb 2019

Electrical Properties And Electromagnetic Interference Shielding Effectiveness Of Interlayered Systems Composed By Carbon Nanotube Filled Carbon Nanofiber Mats And Polymer Composites, Claudia A. Ramirez-Herrera, Homero Gonzalez, Felipe De La Torre, Laura Benitez, Jose G. Cabanas-Moreno, Karen Lozano

Mechanical Engineering Faculty Publications

The demand for multifunctional requirements in aerospace, military, automobile, sports, and energy applications has encouraged the investigation of new composite materials. This study focuses on the development of multiwall carbon nanotube (MWCNT) filled polypropylene composites and carbon nanofiber composite mats. The developed systems were then used to prepare interlayered composites that exhibited improved electrical conductivity and electromagnetic interference (EMI) shielding efficiency. MWCNT-carbon nanofiber composite mats were developed by centrifugally spinning mixtures of MWCNT suspended in aqueous poly(vinyl alcohol) solutions. The developed nanofibers were then dehydrated under sulfuric acid vapors and then heat treated. Interlayered samples were fabricated using a nanoreinforced …

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Deep Learning Segmentation Of Coronary Calcified Plaque From Intravascular Optical Coherence Tomography (Ivoct) Images With Application To Finite Element Modeling Of Stent Deployment, Yazan Gharaibeh, Pengfei Dong, David Prabhu, Chaitanya Kolluru, Juhwan Lee, Vlad Zimin, Hozhabr Mozafari, Hiram Bizzera, Linxia Gu, David Wilson Feb 2019

Deep Learning Segmentation Of Coronary Calcified Plaque From Intravascular Optical Coherence Tomography (Ivoct) Images With Application To Finite Element Modeling Of Stent Deployment, Yazan Gharaibeh, Pengfei Dong, David Prabhu, Chaitanya Kolluru, Juhwan Lee, Vlad Zimin, Hozhabr Mozafari, Hiram Bizzera, Linxia Gu, David Wilson

Department of Mechanical and Materials Engineering: Faculty Publications

Because coronary artery calcified plaques can hinder or eliminate stent deployment, interventional cardiologists need a better way to plan interventions, which might include one of the many methods for calcification modification (e.g., atherectomy). We are imaging calcifications with intravascular optical coherence tomography (IVOCT), which is the lone intravascular imaging technique with the ability to image the extent of a calcification, and using results to build vessel-specific finite element models for stent deployment. We applied methods to a large set of image data (>45 lesions and > 2,600 image frames) of calcified plaques, manually segmented by experts into calcified, lumen and …

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Strength And Plasticity Of Amorphous Silicon Oxycarbide, Kaisheng Ming, Chao Gu, Qing Su, Yongqiang Wang, Arezoo Zare, Don A. Lucca, Michael Nastasi, Jian Wang Jan 2019

Strength And Plasticity Of Amorphous Silicon Oxycarbide, Kaisheng Ming, Chao Gu, Qing Su, Yongqiang Wang, Arezoo Zare, Don A. Lucca, Michael Nastasi, Jian Wang

Department of Mechanical and Materials Engineering: Faculty Publications

Amorphous SiOC films were synthesized by magnetron sputtering at room temperature with/without radio frequency (RF) bias and further improved in terms of mechanical properties by ion irradiation. As-deposited SiOC films without RF bias exhibit catastrophic failure at a low stress and strain, which is ascribed to microstructural heterogeneities associated with the formation of voids during deposition, as evidenced by transmission electron microscopy. Ion irradiation unifies microstructure accompanied with eliminating the voids, resulting in a simultaneously increase in strength and plasticity (ultimate strength of 5–7 GPa and the strain to shear instability of over 20%). Homogeneous microstructures are demonstrated to ensure …

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Effect Of Crystallization Modes In Tips-Pentacene/Insulating Polymer Blends On The Gas Sensing Properties Of Organic Field-Effect Transistors, Jung Hun Lee, Yena Seo, Yeong Don Park, John E. Anthony, Do Hun Kwak, Jung Ah Lim, Sunglim Ko, Ho Won Jang, Kilwon Cho, Wi Hyoung Lee Jan 2019

Effect Of Crystallization Modes In Tips-Pentacene/Insulating Polymer Blends On The Gas Sensing Properties Of Organic Field-Effect Transistors, Jung Hun Lee, Yena Seo, Yeong Don Park, John E. Anthony, Do Hun Kwak, Jung Ah Lim, Sunglim Ko, Ho Won Jang, Kilwon Cho, Wi Hyoung Lee

Center for Applied Energy Research Faculty and Staff Publications

Blending organic semiconductors with insulating polymers has been known to be an effective way to overcome the disadvantages of single-component organic semiconductors for high-performance organic field-effect transistors (OFETs). We show that when a solution processable organic semiconductor (6,13-bis(triisopropylsilylethynyl)pentacene, TIPS-pentacene) is blended with an insulating polymer (PS), morphological and structural characteristics of the blend films could be significantly influenced by the processing conditions like the spin coating time. Although vertical phase-separated structures (TIPS-pentacene-top/PS-bottom) were formed on the substrate regardless of the spin coating time, the spin time governed the growth mode of the TIPS-pentacene molecules that phase-separated and crystallized on the …

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Nano-Biophysical Approaches For Assessing Nanoparticle Interactions With Biological Systems, Zachary Untracht Jan 2019

Nano-Biophysical Approaches For Assessing Nanoparticle Interactions With Biological Systems, Zachary Untracht

Electronic Theses and Dissertations

Understanding interactions between nanoparticles and biological systems is fundamental for the development of emerging nano-biotechnology applications. In this thesis, I present an investigation of zinc oxide (ZnO) nanoparticles interactions with biomolecules in two separate studies. The first section of my thesis covers tracking and detection of ZnO nanoparticles using sodium dodecyl sulfate polyacrylamide gel electrophoresis (SDS-PAGE). ZinkicideTM is a bactericidal ZnO nanoparticle which has been developed for agriculture. The characterization of Zinkicide in biological media and in solution has been difficult due to its high dispersibility and ultra-small size. SDS-PAGE is considered a golden standard for protein qualitative interpretations. In …

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Developments Towards High-Flux Silica Nanosphere Substrates To Support Conforming Self-Assembled Gold Nanoparticle Monolayers For Applications In Size-Selective Filtration, Ryan Baker Vincent Jan 2019

Developments Towards High-Flux Silica Nanosphere Substrates To Support Conforming Self-Assembled Gold Nanoparticle Monolayers For Applications In Size-Selective Filtration, Ryan Baker Vincent

Theses, Dissertations and Capstones

Hydrophobic thiol coated gold nanoparticles have recently been investigated for their ability to self-assemble into robust, ultra-thin, porous membranes at a liquid-vapor interface. Due to the well-ordered, hexagonal close-packed nanoparticle arrays formed during the self-assembly process, these 2-dimensional sheets have very well-defined pore structures and have been shown to span gaps of several microns under ideal conditions. While these self-assembled nanoparticle monolayers have very promising applications in the field of size-selective filtration due to their well-defined pore structure, they need to be supported by a rigid substrate with a large amount of open area. Here, tightly packed arrays of silica …

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Mesoporous Bimetallic Oxides Supported Mono And Bimetallic Catalysts For Fischer-Tropsch Studies In A Stainless-Steel Microchannel Reactor, Robert Stevens-Boyd Jan 2019

Mesoporous Bimetallic Oxides Supported Mono And Bimetallic Catalysts For Fischer-Tropsch Studies In A Stainless-Steel Microchannel Reactor, Robert Stevens-Boyd

Theses

Fischer-Tropsch (F-T) synthesis is the controlled catalyzed conversion of synthesized (syn) gas, a mixture of hydrogen and carbon monoxide, to fuel grade alkanes or hydrocarbons. One of the objectives of NSF-CREST Bioenergy Center is to develop stable catalysts for F-T synthesis with the goal of conversion of syngas enriched with CO2 in microchannel microreactors to liquid fuels. In our previous work, the effect of silica and titania sol-gel as support for F-T studies using syngas (CO:H2; 1:3 or 1:2) was investigated and significant differences in the activities of Co, Fe, and Ru catalysts were observed. In order to investigate synergistic …

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Development Of 3d Printed And 3d Metal-Based Micro/Nanofabricated, And Nano-Functionalized, Microelectrode Array (Mea) Biosensors For Flexible, Conformable, And In Vitro Applications, Charles Didier Jan 2019

Development Of 3d Printed And 3d Metal-Based Micro/Nanofabricated, And Nano-Functionalized, Microelectrode Array (Mea) Biosensors For Flexible, Conformable, And In Vitro Applications, Charles Didier

Electronic Theses and Dissertations

Emerging fields such as "Organs on a Chip", disease modeling in vitro, stem cell manufacturing and wearable bioelectronics are demanding rapid development of 3D Microelectrode Arrays (MEAs) for electrical interfacing with biological constructs. The work reported in this thesis focuses on two developmental tracks: "Dynamic 3D MEAs" and metal microfabrication for 3D MEAs. In the first part of the thesis, we explore the capabilities and limitations of 3D printed microserpentines (µserpentines) and utilize these structures to develop dynamic 3D microelectrodes. Analytical modeling of µserpentines flexibility followed by integration into a flexible Kapton® package and PDMS insulation are demonstrated. These 3D …

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Synthesis Of Two-Dimensional Molybdenum Disulfide Nanostructures Using Molybdenum Trioxide Thin Film Via Chemical Vapor Depostion, Vanessa Charles Jan 2019

Synthesis Of Two-Dimensional Molybdenum Disulfide Nanostructures Using Molybdenum Trioxide Thin Film Via Chemical Vapor Depostion, Vanessa Charles

Electronic Theses and Dissertations

Two dimensional (2D) materials-based nanostructures have attracted much attention due to their unique properties which exhibit promising prospects for application in catalysis and energy storage devices. Control growth method is important in synthesizing these nanostructures. Chemical vapor deposition (CVD) is a powerful method that provides scalability and controllable way to grow high quality 2D materials-based nanostructures. Here, we report a novel CVD growth method of 2D molybdenum disulfide (MoS2) based different structures in which thin film of molybdenum trioxide (MoO3) was used as the source of molybdenum (Mo), while sulfur (S) powder was used for the chalcogen precursor. Precise control …

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Robotic Devicewith Compact Joint Design And Related Systems And Methods, Tom Frederick, Eric Markvicka, Shane Michael Farritor, Dmitry Oleynikov Jan 2019

Robotic Devicewith Compact Joint Design And Related Systems And Methods, Tom Frederick, Eric Markvicka, Shane Michael Farritor, Dmitry Oleynikov

Department of Mechanical and Materials Engineering: Faculty Publications

The embodiments disclosed herein relate to various robotic and/or in vivo medical devices having compact joint configurations. Other embodiments relate to various medical device components, including forearms having grasper or cautery end effectors, that can be incorporated into certain robotic and/or in vivo medical devices.

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Flaw Detection With Ultrasonic Backscatter Signal Envelopes, Yongfeng Song, Christopher M. Kube, Zuoxiang Peng, Joseph A. Turner, Xiongbing Li Jan 2019

Flaw Detection With Ultrasonic Backscatter Signal Envelopes, Yongfeng Song, Christopher M. Kube, Zuoxiang Peng, Joseph A. Turner, Xiongbing Li

Department of Mechanical and Materials Engineering: Faculty Publications

Ultrasound is a prominent nondestructive testing modality for the detection, localization, and sizing of defects in engineering materials. Often, inspectors analyze ultrasonic waveforms to determine if echoes, which stem from the scattering of ultrasound from a defect, exceed a threshold value. In turn, the initial selection of the threshold value is critical. In this letter, a time-dependent threshold or upper bound for the signal envelope is developed based on the statistics governing the scattering of ultrasound from microstructure. The utility of the time-dependent threshold is demonstrated using experiments conducted on sub-wavelength artificial defects. The results are shown to enhance current …

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Glocal Integrity In 420 Stainless Steel By Asynchronous Laser Processing, Michael P. Sealy, Haitham Hadidi, Cody Kanger, X. L. Yan, Bai Cui, J. A. Mcgeough Jan 2019

Glocal Integrity In 420 Stainless Steel By Asynchronous Laser Processing, Michael P. Sealy, Haitham Hadidi, Cody Kanger, X. L. Yan, Bai Cui, J. A. Mcgeough

Department of Mechanical and Materials Engineering: Faculty Publications

Cold working individual layers during additive manufacturing (AM) by mechanical surface treatments, such as peening, effectively “prints” an aggregate surface integrity that is referred to as a glocal (i.e., local with global implications) integrity. Printing a complex, pre-designed glocal integrity throughout the build volume is a feasible approach to improve functional performance while mitigating distortion. However, coupling peening with AM introduces new manufacturing challenges, namely thermal cancellation, whereby heat relaxes favorable residual stresses and work hardening when printing on a peened layer. Thus, this work investigates glocal integrity formation from cyclically coupling LENS® with laser peening on 420 stainless steel.

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The Role Of Low-Level Image Features In The Affective Categorization Of Rapidly Presented Scenes, L. Jack Rhodes, Matthew Rios, Jacob M. Williams, Gonzalo Quinones, Prahalada K. Rao, Vladimir Miskovic Jan 2019

The Role Of Low-Level Image Features In The Affective Categorization Of Rapidly Presented Scenes, L. Jack Rhodes, Matthew Rios, Jacob M. Williams, Gonzalo Quinones, Prahalada K. Rao, Vladimir Miskovic

Department of Mechanical and Materials Engineering: Faculty Publications

It remains unclear how the visual system is able to extract affective content from complex scenes even with extremely brief (< 100 millisecond) exposures. One possibility, suggested by findings in machine vision, is that low-level features such as unlocalized, two-dimensional (2-D) Fourier spectra can be diagnostic of scene content. To determine whether Fourier image amplitude carries any information about the affective quality of scenes, we first validated the existence of image category differences through a support vector machine (SVM) model that was able to discriminate our intact aversive and neutral images with ~ 70% accuracy using amplitude-only features as inputs. This model allowed us to confirm that scenes belonging to different affective categories could be mathematically distinguished on the basis of amplitude spectra alone. The next question is whether these same features are also exploited by the human visual system. Subsequently, we tested observers’ rapid classification of affective and neutral naturalistic scenes, presented briefly (~33.3 ms) and backward masked with synthetic textures. We tested categorization accuracy across three distinct experimental conditions, using: (i) original images, (ii) images having their amplitude spectra swapped within a single affective image category (e.g., an aversive image whose amplitude spectrum has been swapped with another aversive image) or (iii) images having their amplitude spectra swapped between affective categories (e.g., an aversive image containing the amplitude spectrum of a neutral image). Despite its discriminative potential, the human visual system does not seem to use Fourier amplitude differences as the chief strategy for affectively categorizing scenes at a glance. The contribution of image amplitude to affective categorization is largely dependent on interactions with the phase spectrum, although it is impossible to completely rule out a residual role for unlocalized 2-D amplitude measures.

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Compliant Surgical Graspers And Methods Of Making And Using, Carl Nelson, Alan Goyzueta Jan 2019

Compliant Surgical Graspers And Methods Of Making And Using, Carl Nelson, Alan Goyzueta

Department of Mechanical and Materials Engineering: Faculty Publications

This disclosure describes compliant graspers for use in endoscopic surgeries.

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Self-Powered Ghz Solution-Processed Hybrid Perovskite Photodetectors, Jinsong Huang Jan 2019

Self-Powered Ghz Solution-Processed Hybrid Perovskite Photodetectors, Jinsong Huang

Department of Mechanical and Materials Engineering: Faculty Publications

Organic-inorganic hybrid perovskite (OIHP) based photo-responsive devices include an OIHP active layer disposed between a cathode layer and an anode layer, and an electron extraction layer disposed between the cathode layer and the active layer. The electron extraction layer includes a layer of C60 directly disposed on the active layer. The active layer includes an organometal trihalide perovskite layer (e.g., CH3NH3PbI2X, where X includes at least one of Cl, Br, or I).

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