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Articles 781 - 810 of 5710

Full-Text Articles in Engineering Science and Materials

Atmospheric Hydrochloric And Nitric Acid Leaching Of A Limonite Ore From The Wolo Mine Area, Southeast Sulawesi, Indonesia, Sufriadin -, Malyanus Yepta, Irzal Nur, Purwanto -, Rizky Amalia, Ulva Ria Irfan, Djabal Nur Basir, Tsubasa Otake Jan 2024

Atmospheric Hydrochloric And Nitric Acid Leaching Of A Limonite Ore From The Wolo Mine Area, Southeast Sulawesi, Indonesia, Sufriadin -, Malyanus Yepta, Irzal Nur, Purwanto -, Rizky Amalia, Ulva Ria Irfan, Djabal Nur Basir, Tsubasa Otake

Journal of Metals, Materials and Minerals

The atmospheric acid leaching studies of a limonite ore sample from the Wolo mine area, Southeast Sulawesi, Indonesia, have been performed using hydrochloric acid (HCl) and nitric acid (HNO3). The objectives of these studies were to compare the leaching degree of metals (Ni, Co, Fe, and Al) and to analyze the dissolution behavior of minerals under different acid concentrations. Mineralogical characterization of the ore sample was conducted using optical microscopy, scanning electron microscopy (SEM), and X-ray diffraction, whereas chemical composition was determined by X-ray fluorescence (XRF) spectrometry and atomic absorption spectroscopy (AAS), respectively. An atmospheric leaching test was done with …

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In Vitro And Vivo Biocompatibility And Degradability Of Low-Alloyed Mg-Zn-Ca-Mgo Composite As Bone Repair Biomaterials, Shuquan Zhang, Jiangtao Feng, Chaokun Tang, Ran Pang, Xinglong Zhang, Chenguang Li, Weihao Zhang, Fengxin Zhou, Feng Xue, Shaoyuan Lyu, Minfang Chen, Hao Wang Jan 2024

In Vitro And Vivo Biocompatibility And Degradability Of Low-Alloyed Mg-Zn-Ca-Mgo Composite As Bone Repair Biomaterials, Shuquan Zhang, Jiangtao Feng, Chaokun Tang, Ran Pang, Xinglong Zhang, Chenguang Li, Weihao Zhang, Fengxin Zhou, Feng Xue, Shaoyuan Lyu, Minfang Chen, Hao Wang

Journal of Metals, Materials and Minerals

Magnesium alloys have gained attention as biodegradable bone repair biomaterials. Unlike non-biodegradable materials like titanium and tantalum, biodegradable implants offer advantages in promoting bone healing and minimizing chronic inflammatory reactions. However, the impact of the implant's degradation on the osteogenic environment remains a concern. The Mg-Zn-Ca-MgO composite, being biocompatible and containing osteogenic ions, is a promising candidate. This study assesses the degradability and in vitro/in vivo biocompatibility of two Mg-Zn-Ca-MgO composites with varying degradation rates. The Mg-1Zn-0.2Ca-1.0MgO composite was prepared, and leaching solutions were created following standard protocols. MC3T3-E1 cell cultures were conducted to assess cell toxicity, alkaline phosphatase (ALP) …

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Modification Of Gas Atomized Metal Powders Through Mechanical Chemical Bonding Technique, Philip Thomas Mallory Jan 2024

Modification Of Gas Atomized Metal Powders Through Mechanical Chemical Bonding Technique, Philip Thomas Mallory

Graduate Theses, Dissertations, and Problem Reports (ETD)

Additive Manufacturing (AM) has become popular for commercial applications where high-performance parts can now be created, tested, and modified more efficiently thus expediting the design process. Because of its relatively easy access today a lot of research and improvements are coming out yearly for improved AM machines and the material used. At WVU, a new way of modifying as-receive commercial gas-atomized metal powders used in AM has been developed using Mechanical Chemical Bonding (MCB) methodology which uses high rotational blades to create an environment where it increases the particle-on-particle interaction. During this high energetic process all irregular shaped particles, with …

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Inherently Porous Metal Structures With Sufficient Mechanical Properties Through Direct Writing Of Bio-Based Inks, Havva Eda Aysal Jan 2024

Inherently Porous Metal Structures With Sufficient Mechanical Properties Through Direct Writing Of Bio-Based Inks, Havva Eda Aysal

Graduate Theses, Dissertations, and Problem Reports (ETD)

There is currently a burgeoning interest in developing 3D printed metal structures with inherent porosity and sufficient mechanical properties for mass customization in the biomedical field. Current approaches for 3D printing of biocompatible metals rely on powder-bed fusion methods which are energy intensive and utilize large amounts of metal powder that is challenging to recycle. In addition, such methods aim on producing dense parts and porosity generation, within the printed part, is challenging due to the complex physics of the melting pool. Here, a relatively new and promising approach is undertaken to study the 3D printing of inherently porous structures …

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Hot Corrosion Behavior Of Mg2 Sio4 Ceramic Exposed To Molten Na2so4 At 900℃ To 1100℃, Hamza Milles, Louafi Snani, Amel Oulabbas, Khaled Toualbia Jan 2024

Hot Corrosion Behavior Of Mg2 Sio4 Ceramic Exposed To Molten Na2so4 At 900℃ To 1100℃, Hamza Milles, Louafi Snani, Amel Oulabbas, Khaled Toualbia

Journal of Metals, Materials and Minerals

Thermal barriers are used as protective coating for critical components working at high temperature of gas turbines. Forsterite (Mg2SiO4) ceramic is proposed by researchers as a novel thermal barrier coating (TBC), due to its low thermal conductivity and good thermal expansion. Hot corrosion results from the molten salts effect on the TBC’s surface, accumulated during the combustion processes. In this study, Mg2SiO4 samples were exposed to Na2SO4 molten salt at 900℃, 1000℃ and 1100℃ for 6 h in air. Samples were investigated and compared using scanning electron microscope (SEM) and X-Ray diffractometer (XRD). MgSO4 was the predominant corrosion product observed …

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A Contribution To The Exploration Of The Chemical Durability, Thermal Stability, And Structural Ability Of Glasses From The Fe2o3-K2o-Moo3-P2o5 Quaternary System, Asmae Er-Rafai, Yasmina Alaoui, Mohamed Laourayed, Mohamed Ounacer, Mouloud El Moudane, Mohammed Sajieddine, Abdelkbir Bellaouchou Jan 2024

A Contribution To The Exploration Of The Chemical Durability, Thermal Stability, And Structural Ability Of Glasses From The Fe2o3-K2o-Moo3-P2o5 Quaternary System, Asmae Er-Rafai, Yasmina Alaoui, Mohamed Laourayed, Mohamed Ounacer, Mouloud El Moudane, Mohammed Sajieddine, Abdelkbir Bellaouchou

Journal of Metals, Materials and Minerals

The relationships between the properties and structure of xFe2O3-(40-x)K2O-10MoO3-50P2O5 glasses have been reported in this paper. Homogeneous glasses are formed for different Fe2O3 contents. The density and molar volume evolution of these glasses shows that Fe2O3 acts as a glass former and strengthens the structural bonds of the glass. Experimental 57Fe Mössbauer spectroscopy graphs suggest the existence of divalent Iron (FeII) and trivalent Iron (FeIII). The boost in chemical durability agrees with the growth in glass transition temperature due to more powerful bonding in the structural network. P-O-Fe bonds replace P-O-P bonds when Fe2O3 is present in the phosphate network.

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Incorporating Novel Bio-Mineral Materials Of Silicone-Arrowroot Modified Starch For Compressed Powder, Pirada Sudprasert, Ananthaya Sansawat, Piangkhwan Kruapoo Jan 2024

Incorporating Novel Bio-Mineral Materials Of Silicone-Arrowroot Modified Starch For Compressed Powder, Pirada Sudprasert, Ananthaya Sansawat, Piangkhwan Kruapoo

Journal of Metals, Materials and Minerals

Incorporating novel bio-mineral materials of silicone-arrowroot modified starch (SA) is an environmentally friendly technique to create compressed powder, thereby integrating biodiversity with sustainability and responding to the Bio-Circular-Green (BCG) economy. The SA had improved flowability and water resistance compared with non-modified arrowroot flour (A0), concurring with the Fourier Transform Infrared (FTIR), scanning electron microscope (SEM) analyses that indicated more hydrophobic properties. To investigate the formulated dust and compressed powder, three types of binders including magnesium stearate (Ms), isopropyl myristate (Im), and mineral oil (Mo) were examined. Powder samples of all binders at each concentration gave high water resistance with floating …

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The Effects Of Copper On The Mechanical Properties Of Ti-10mo Alloy Prepared By Powder Metallurgy Method, Aji Abdillah Kharisma, Haris Rudianto, Achmad Benny Mutiara, Sulistyo Puspitodjati, Fahamsyah Hamdan Latief, Agus Sukarto Wismogroho, Wahyu Bambang Widayatno, Didik Aryanto, Cherly Firdharini Jan 2024

The Effects Of Copper On The Mechanical Properties Of Ti-10mo Alloy Prepared By Powder Metallurgy Method, Aji Abdillah Kharisma, Haris Rudianto, Achmad Benny Mutiara, Sulistyo Puspitodjati, Fahamsyah Hamdan Latief, Agus Sukarto Wismogroho, Wahyu Bambang Widayatno, Didik Aryanto, Cherly Firdharini

Journal of Metals, Materials and Minerals

Titanium alloys are currently widely explored and produced for applications in various engineering fields. Alloying metal elements such as Mo, Cu, and Mn bring more advantages among them to help improve the mechanical properties of titanium alloys. This study is intended for the evaluation of mechanical properties through compression and hardness testing performed on a Ti-10Mo alloy with copper addition by powder metallurgy. Ti-10Mo alloys with the addition of copper contents of 3 wt% Cu, 6 wt% Cu, and 9 wt% Cu were prepared to optimize the properties of Ti-10Mo-xCu alloys. With the addition of 3 wt% copper, the compressive …

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First-Principles Study On Structural And Electronic Properties Of P3ht-Graphene, Fia Amalia, Ari Dwi Nugraheni, Sholihun Sholihun Jan 2024

First-Principles Study On Structural And Electronic Properties Of P3ht-Graphene, Fia Amalia, Ari Dwi Nugraheni, Sholihun Sholihun

Journal of Metals, Materials and Minerals

Based on density functional theory, calculations have been carried out to study the structural and electronic properties of the polymer Poly (3-hexylthiophene) (P3HT) interacting with monolayer graphene as an active layer. (P3HT)1-graphene and (P3HT)2-graphene are optimized on graphene using the generalized-gradient-approximation type of the exchange-correlation functional. Adsorption energy, band gap, and charge transfer are calculated. The calculated adsorption energy shows that all systems have negative adsorption energy, indicating that the reaction is exothermic. Compared to (P3HT)1-graphene, (P3HT)2-graphene has a lower band gap. As for the charge transfer calculation, a negative ΔN indicates that electron transfers from P3HT to graphene.

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Integration Of Jackfruit Seed-Derived Carbon Dots And Electronic Nose For A Sensitive Detection Of Formaldehyde Vapor, Thitarat Prathumsuwan, Sumana Kladsomboon, Alfred Antony Christy, Insik In, Xiao Liang, Shufeng Song, Yao Wang, Thitirat Inprasit, Peerasak Paoprasert, Natee Sirisit Jan 2024

Integration Of Jackfruit Seed-Derived Carbon Dots And Electronic Nose For A Sensitive Detection Of Formaldehyde Vapor, Thitarat Prathumsuwan, Sumana Kladsomboon, Alfred Antony Christy, Insik In, Xiao Liang, Shufeng Song, Yao Wang, Thitirat Inprasit, Peerasak Paoprasert, Natee Sirisit

Journal of Metals, Materials and Minerals

The preparation of carbon dots from jackfruit seeds through a pyrolysis method at 280℃ and their use for the detection of formaldehyde were reported. The as-prepared carbon dots showed a high fluorescence efficiency with a quantum yield of 12.7% and excellent photostability and dispersibility in aqueous solution with a zeta potential of ‒62.5 mV. The integration of carbon dot thin film and a home-made optical electronic nose system possessed sensitivity towards formaldehyde vapor with a detection limit of 24.7%v/v across a linear range of 25%v/v to 100%v/v. Furthermore, the sensor showed the highest sensitivity towards formaldehyde against other volatile organic …

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Nano-Zno Prepared By Using Chaya And Mango Leaves Extract For Photocatalyst Of Methylene Blue, Sri Wahyu Suciyati, Junaidi Junaidi, Rudy Situmeang, Posman Manurung Jan 2024

Nano-Zno Prepared By Using Chaya And Mango Leaves Extract For Photocatalyst Of Methylene Blue, Sri Wahyu Suciyati, Junaidi Junaidi, Rudy Situmeang, Posman Manurung

Journal of Metals, Materials and Minerals

This research aimed to synthesize nano-ZnO from chaya (Cnidoscolus aconitifolius) and mango leaves extract (Mangifera indica) as environmentally friendly photocatalysts. Nano-ZnO was synthesized using green synthesis, with leaves extracts as reducing agents and nanoparticle size stabilizers. The samples were prepared using two methods, namely nano-ZnO-1 and nano-ZnO-2. The results of Fourier transform infrared spectroscopy (FTIR) analysis showed the contribution of metabolite compounds in nano-ZnO synthesis. X-ray diffraction (XRD) and transmission electron microscopy (TEM) showed the crystal size in nano range, with spherical nanorod morphology observed. Ultraviolet-visible diffuse reflectance spectroscopy (UV-Vis DRS) determined the band gap energy …

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Photocatalytic Degradation Of Ciprofloxacin Drug Utilizing Novel Pvdf/Polyaniline/ Lanthanum Strontium Manganate@Ag Composites, Swayam Aryam Behera, Ali Amanat, P. Ganga Raju Achary Jan 2024

Photocatalytic Degradation Of Ciprofloxacin Drug Utilizing Novel Pvdf/Polyaniline/ Lanthanum Strontium Manganate@Ag Composites, Swayam Aryam Behera, Ali Amanat, P. Ganga Raju Achary

Journal of Metals, Materials and Minerals

Poly (vinylidene fluoride) (PVDF) is the first-choice ferroelectric support or membrane material. The lanthanum strontium manganite (LSMO) is a well-known electrode material in the class of the solid oxide fuel cell (SOFC) materials. A set of four polymer composites PVDF-LSMO-PANI(5.0 wt%) with different amount of silver doping were fabricated with the silver nitrate and reducing agent. The characterization of these four novel PVDF based composites were characterized by the XRD, FTIR, SEM, UV-Visible DRS. The present communication highlights: (I) the effect of PANI in the PVDF-LSMO-PANI (PLP) composites towards the photocatalytic degradation of ciprofloxacin drug. (II) the effect of Ag …

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The Effect Of Two-Stage Heat Treatment On The Microstructure And Mechanical Properties Of High Chrome Austenitic Manganese Steel, Mohammad Reza Hermawan, Budi Hartono Setiamarga, Ilham Nur Hakim, Rizka Mulia Anggraeni Jan 2024

The Effect Of Two-Stage Heat Treatment On The Microstructure And Mechanical Properties Of High Chrome Austenitic Manganese Steel, Mohammad Reza Hermawan, Budi Hartono Setiamarga, Ilham Nur Hakim, Rizka Mulia Anggraeni

Journal of Metals, Materials and Minerals

In this research, heat-treatment was used to determine changes in the microstructure and mechanical characteristics of austenitic manganese steel equivalent to ASTM A128-C. Carbide formed in as-cast conditions is transformed into dispersed hardened austenite to increase the toughness of the material because it can inhibit dislocation movement. Heat treatment is carried out in two heating stages. The first stage of heating was carried out at a temperature of 625°C with a holding time varying by 2.5, 3.5, and 4.5 h, and the second stage was carried out at a temperature of 1000°C with a constant holding time of 1.5 h. …

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Microstructural And Dielectric Characteristics Of The Ce-Doped Bi2femno6, Laxmidhar Sahoo, Swayam Aryam Behera, Rajesh Kumar Singh, Santosh Kumar Parida, Patnala Ganga Raju Achary Jan 2024

Microstructural And Dielectric Characteristics Of The Ce-Doped Bi2femno6, Laxmidhar Sahoo, Swayam Aryam Behera, Rajesh Kumar Singh, Santosh Kumar Parida, Patnala Ganga Raju Achary

Journal of Metals, Materials and Minerals

A double-perovskite material Bi2FeMn0.94Ce0.06O6 (BFMCO) was synthesized by solid state reaction technique and characterized it by various techniques (structural, microstructural, dielectric, impedance and modulus properties). The material has an orthorhombic crystal structure with an average crystallite size of 52.4 nm, as revealed by X-ray diffraction data (XRD). The scanning electron microscope (SEM) image shows the presence of nano rod-shaped grains and well-defined grain boundaries in this material, with an average grain size of 21.8 µm. The Energy dispersive X-ray (EDX) analysis and color mapping confirm the purity and the composition of the material. The dielectric, impedance and modulus properties are …

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Green Synthesis Of Bimetallic Cuo@Nio Nanocomposite For The Removal Of Glyphosate, Kornkanok Boonserm, Anan Sutcha, Rarm Phinjaroenphan Jan 2024

Green Synthesis Of Bimetallic Cuo@Nio Nanocomposite For The Removal Of Glyphosate, Kornkanok Boonserm, Anan Sutcha, Rarm Phinjaroenphan

Journal of Metals, Materials and Minerals

Green synthesis of photocatalyst bimetallic CuO@NiO nanocomposite for eliminating organic hazardous glyphosate (Gly) solution has been introduced. The nanocomposite has been successfully developed from mango (Mangifera indica L.) peel extracted solution by a simultaneous reduction process. HRTEM, XRD, and EDX have also been used to explore the nanostructure, crystal conformation, and chemical compositions of CuO@NiO. Using UV-vis spectrometer, we have observed the photo-catalytic activity and kinetic removal rate constant of CuO@NiO in terms of glyphosate elimination under UV light illumination. Compared with pure CuO and NiO nanoparticles, CuO@NiO displayed improved and enhanced photocatalytic activity. This work demonstrates an …

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Possibility Of Using Boric Acid And Glutinous Rice Flour As Additive For Producing Silicon Carbide Ceramic Via Pressureless Solid-State Sintering, Apichart Jinnapat, Auamporn Rattanasing, Nithiwach Nawaukkaratharnant, Kritkeaw Somton, Kannigar Dateraksa Jan 2024

Possibility Of Using Boric Acid And Glutinous Rice Flour As Additive For Producing Silicon Carbide Ceramic Via Pressureless Solid-State Sintering, Apichart Jinnapat, Auamporn Rattanasing, Nithiwach Nawaukkaratharnant, Kritkeaw Somton, Kannigar Dateraksa

Journal of Metals, Materials and Minerals

This research aimed to investigate the possibility of using the mixture of boric acid and glutinous rice flour as a cost-efficient alternative additive for producing silicon carbide (SiC) ceramic sintered at 1800℃ via pressureless solid-state sintering. The results indicated that the addition of boric acid- glutinous rice flour mixture (10 wt%) in an appropriate ratio (0.5 by molar ratio) into the SiC mixture (90 wt%) enhanced the densification and flexural strength of sintered SiC samples. However, increasing boric acid/glutinous rice flour ratio reduces density and flexural strength. The 5.45 wt% carbon content was sufficient to remove the oxide layer of …

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Development Of Antioxidant Film Based On Gelatin And Carboxymethylcellulose Incorporated With Tecoma Stans (L.) Juss. Ex Kunth Petals Extract For Biodegradable Food Packaging, Pacharawan Ratanasongtham, Passara Sukplee, Yutthana Wongnongwa Jan 2024

Development Of Antioxidant Film Based On Gelatin And Carboxymethylcellulose Incorporated With Tecoma Stans (L.) Juss. Ex Kunth Petals Extract For Biodegradable Food Packaging, Pacharawan Ratanasongtham, Passara Sukplee, Yutthana Wongnongwa

Journal of Metals, Materials and Minerals

The aim of this research was to develop a novel combination of antioxidant blended film for use as biodegradable packaging in the food industry.  The antioxidant film was prepared based on gelatin (G) and carboxymethyl cellulose (CMC) incorporated with Tecoma stans (L.) Juss. ex Kunth petals extract (TKE) at various concentrations (0.5, 1.0, and 2.0 mg∙L‒1) via solution casting method. The structural and surface morphology of G/CMC-TKE film were characterized using FTIR spectrometry technique and scanning electron microscopy (SEM), including determining antioxidant activity, water solubility, water vapor permeability, and biodegradability. According to FTIR analysis, the significant interaction between the gelatin …

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The Effect Of Mixing Sequence On Synthesis Of Pp-G-Gma Compatibilizer For Multilayer Packaging (Mlp) Compounding, Fitri Ayu Radini, Firda Apriyani, Yogi Angga Swasono, Reza Pahlevi Rudianto, Nonni Soraya Sambudi, Yose Fachmi Buys Jan 2024

The Effect Of Mixing Sequence On Synthesis Of Pp-G-Gma Compatibilizer For Multilayer Packaging (Mlp) Compounding, Fitri Ayu Radini, Firda Apriyani, Yogi Angga Swasono, Reza Pahlevi Rudianto, Nonni Soraya Sambudi, Yose Fachmi Buys

Journal of Metals, Materials and Minerals

Melt recycling Multilayer Packaging (MLP) waste is difficult due to challenging separation procedures. However, blending techniques with compatibilizers can simplify MLP waste melt recycling. PP-g-GMA is a common compatibilizer in polyolefin and PET blends. PP-g-GMA compatibilizer was synthesized by utilizing an internal mixer at 175℃, 50 rpm, and 10 min using styrene as a comonomer. Titration was a method to examine effect of three different sequences of adding the BPO initiator on GMA grafting. Each sequence's PP-g-GMA samples were compounded with MLP waste using a twin-screw extruder and injection molded to make tensile test specimens. FTIR analysis shows that the …

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Evaluation Of The Effect Of Strontium And Tungsten Carbide On The Microstructure Evolution, Tribological And Mechanical Behaviour Of Al-Zn-Mg-Cu-5sr-Wc Metal Matrix Composite, Jeffin Johnson, Rosari Raja Jan 2024

Evaluation Of The Effect Of Strontium And Tungsten Carbide On The Microstructure Evolution, Tribological And Mechanical Behaviour Of Al-Zn-Mg-Cu-5sr-Wc Metal Matrix Composite, Jeffin Johnson, Rosari Raja

Journal of Metals, Materials and Minerals

The present study focused on the experimental investigation of the metallurgical, tribological, and mechanical behavior of the developed Al-Zn-Mg-Cu-Sr-WC (Al7075-Sr-WC) metal matrix composite. The effect of the reinforcements such as strontium and tungsten carbide (WC) along with a 2 wt% magnesium as the wetting agent during the stir casting of the synthesized aluminum metal matrix composite (MMC) was investigated by varying the weight percentages. The microstructure examination was characterized using field emission scanning electron microscopy (FE-SEM), scanning electron microscopy (SEM), X-ray diffraction (XRD), and energy dispersive spectroscopy (EDS) techniques. Wear analysis and mechanical testing were conducted to study the effect …

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The Effect Of Printing Parameters On The Properties Of 17-4 Ph Stainless Steel Fabricated By Material Extrusion Additive Manufacturing, Phanuphak Seensattayawong, Chanun Suwanpreecha, Natthanicha Boonlert, Sukrit Songkuea, Anchalee Manonukul Jan 2024

The Effect Of Printing Parameters On The Properties Of 17-4 Ph Stainless Steel Fabricated By Material Extrusion Additive Manufacturing, Phanuphak Seensattayawong, Chanun Suwanpreecha, Natthanicha Boonlert, Sukrit Songkuea, Anchalee Manonukul

Journal of Metals, Materials and Minerals

The 17-4PH stainless steel filament was characterised and utilised to study the effect of printing parameters, i.e. printing temperature, layer thickness, infill pattern and extrusion multiplier on the physical properties. The as-printed and as-sintered internal structures were analysed. The results showed that the as-printed density increases with increasing printing temperature and extrusion multiplier and decreasing layer thickness. The use of the line infill pattern also provided slightly higher as-printed density than the concentric infill pattern due to the low fraction of void between deposited paths. After sintering, the trace of these voids can be observed together with smaller-size residual pores …

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The Mechanochemistry Of Lanthanum Dihydride (Lah2) With Hydrogen (H2) Using The Ball-Mill Process And The Effect Of Oxidation On The Resulting Products, Andika Widya Pramono, Satrio Herbirowo, Agung Imaduddin, Iwan Dwi Antoro, Heri Nugraha, Hendrik -, Anung Syampurwadi, Ines Hayatun Nufus, Nihayatul Umna, Silvia Farah Diba, Fina Fitratun Amaliyah Jan 2024

The Mechanochemistry Of Lanthanum Dihydride (Lah2) With Hydrogen (H2) Using The Ball-Mill Process And The Effect Of Oxidation On The Resulting Products, Andika Widya Pramono, Satrio Herbirowo, Agung Imaduddin, Iwan Dwi Antoro, Heri Nugraha, Hendrik -, Anung Syampurwadi, Ines Hayatun Nufus, Nihayatul Umna, Silvia Farah Diba, Fina Fitratun Amaliyah

Journal of Metals, Materials and Minerals

The complex behavior of LaH2 during ball milling was investigated in this study, with its mechanical, chemical, and morphological changes explored. The relationship between milling time and hydrogen pressure reduction was uncovered through detailed experiments, reflecting the dynamic nature of the process. A transient yet significant event was observed upon unsealing the milling jar post-milling: the emergence of a minor fire ember, indicative of the interplay between mechanical forces and chemical reactivity within the LaH2 powder. Profound changes in the structure, composition, and shape were unraveled using advanced techniques such as X-ray diffraction (XRD), scanning electron microscopy coupled with energy-dispersive …

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Enhancing The Efficiency Of Hemp Fiber Dyeing With Natural Dyes: Indigo And Lac, Jadsadaporn Chouytan, Rajapol Thirawat, Dhea Khotradha, Tanawat Ruangteprat, Ing-Orn Sittitanadol, Somchai Udon Jan 2024

Enhancing The Efficiency Of Hemp Fiber Dyeing With Natural Dyes: Indigo And Lac, Jadsadaporn Chouytan, Rajapol Thirawat, Dhea Khotradha, Tanawat Ruangteprat, Ing-Orn Sittitanadol, Somchai Udon

Journal of Metals, Materials and Minerals

Hemp fibers dyed with natural dyes are environmentally sustainable, but it is typically difficult to achieve an intense shade and washing durability. In this study, mercerization and cationization using polyelectrolyte, Poly-diallyldimethylammonium chloride (polyDADMAC), were chosen to enhance the dyeing efficiency and mechanical properties. Indigo and lac were chosen as natural dyes due to their widespread use. SEM demonstrated that untreated fibers contained the non-cellulose boundary layer on the surfaces, but after mercerization, the surfaces were smoother, making them suitable for absorbing natural dyes. In agreement with the FT-IR, the spectra of non-cellulose disappeared after mercerizing. Following cationization, the FT-IR spectra …

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Development Of Pla/Ha Porous Scaffolds With Controlled Pore Sizes Using The Combined Freeze Drying And Sucrose Leaching Technique For Bone Tissue Engineering, Sunisa Singhawannurat, Panuwat Lawtae, Catleya Rojviriya, Chalermluck Phoovasawat Jan 2024

Development Of Pla/Ha Porous Scaffolds With Controlled Pore Sizes Using The Combined Freeze Drying And Sucrose Leaching Technique For Bone Tissue Engineering, Sunisa Singhawannurat, Panuwat Lawtae, Catleya Rojviriya, Chalermluck Phoovasawat

Journal of Metals, Materials and Minerals

The combination of freeze drying and sucrose leaching technique was employed to fabricate PLA/HA scaffolds with controlled pore size. The influence of the HA content and sucrose size on the scaffold properties was investigated. The fabricated scaffolds showed porous properties with a porosity of 44% to 58% and pore size of 461 μm to 688 μm. The results indicated that the scaffolds possessed favorable porous properties, illustrated by good interconnectivity, appropriate pore size, and suitable porosity. These characteristics were crucial for facilitating bone cell growth and promoting the formation of new tissue within the scaffold structure. The compressive modulus of …

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Leonardite Humic Acid Activated Carbon/Mno Composite Nanostructures For Supercapacitors, Artit Ausavasukhi, Thanchanok Siriphala, Wanwisa Limphirat, Sukanya Nilmoung Jan 2024

Leonardite Humic Acid Activated Carbon/Mno Composite Nanostructures For Supercapacitors, Artit Ausavasukhi, Thanchanok Siriphala, Wanwisa Limphirat, Sukanya Nilmoung

Journal of Metals, Materials and Minerals

This work reports the preparation and electrochemical studies of activated carbon derived from leonardite humic acid composited with MnO2 for supercapacitors. Activated carbon contains high conductivity, high specific surface area, and accommodates large volume expansion/contraction during charging/discharging process. Meanwhile, MnO2 has very high theoretical specific capacity (1370 F∙g‒1). Their composite could significantly improve both the storage performance and cycle stability of supercapacitors. Moreover, humic acid from leonardite was selected to add value to this waste and reduce environmental pollution.  By varying the carbonization temperature (500℃ to 800℃), the prepared samples carbonized at 800℃ exhibited fascinating properties. The oxidation state of …

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Biosynthesis Of Zinc Oxide Nanoparticles Using Water Hyacinth Extracts: Characterization, Evaluation Of Antimicrobial And Dye Removal, Phiphat Sonthongphithak, Chonchanok Muangnapoh, Chalita Ratanatawanate, Teerasak E-Kobon, Akkharadet Piyasaengthong, Piyorot Hongsachart, Manop Sriuttha, Nipaporn Sengkhamparn, Anto Cordelia Tanislaus Anthony Dhanapal, Kitiyaporn Wittayanarakul Jan 2024

Biosynthesis Of Zinc Oxide Nanoparticles Using Water Hyacinth Extracts: Characterization, Evaluation Of Antimicrobial And Dye Removal, Phiphat Sonthongphithak, Chonchanok Muangnapoh, Chalita Ratanatawanate, Teerasak E-Kobon, Akkharadet Piyasaengthong, Piyorot Hongsachart, Manop Sriuttha, Nipaporn Sengkhamparn, Anto Cordelia Tanislaus Anthony Dhanapal, Kitiyaporn Wittayanarakul

Journal of Metals, Materials and Minerals

In nanobiotechnology, synthesizing metal nanoparticles (NPs) using plant extracts has recently been increasing because of eco-friendly and low-cost methods. For this work, zinc oxide nanoparticles (ZnO NPs) have been synthesized by biosynthesis process using water hyacinth extracts (WHE). The water hyacinth (WH) was chosen because the WH is fast-growing and the most toxic aquatic plant in the world. Therefore, this work aims to apply these WHE to be a precursor in the biosynthesis of ZnO NPs (ZnOBio-NPs) based on the research of a sustainable environment. The ZnO NPs synthesized by the WHE were investigated for their antibacterial and photocatalytic activities. …

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Natural Wound Dressing Films Prepared From Acetylated Starch/Κ-Carrageenan Blend Incorporated With Mandelic Acid, Wimolsiri Sriphochai, Jutarat Prachayawarakorn Jan 2024

Natural Wound Dressing Films Prepared From Acetylated Starch/Κ-Carrageenan Blend Incorporated With Mandelic Acid, Wimolsiri Sriphochai, Jutarat Prachayawarakorn

Journal of Metals, Materials and Minerals

Due to several limitations of acetylated starch film for wound dressing applications such as low mechanical properties and no antibacterial activity, acetylated starch film was, therefore, modified by different contents of κ-carrageenan and mandelic acid. Infrared spectra confirmed the presence of κ-carrageenan and mandelic acid in the modified acetylated starch films. In addition, the decreased crystallinity of the carrageenan modified acetylated starch films led to more smooth film, as observed by scanning electron images. Besides, the addition of various amounts of κ-carrageenan in the modified acetylated starch films caused the improvement of mechanical properties, moisture uptake, water vapor transmission rate …

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A Review On The Development Of Metals-Doped Vanadium Oxides For Zinc-Ion Battery, Kittima Lolupima, Jin Cao, Dongdong Zhang, Chenwu Yang, Xinyu Zhang, Jiaqian Qin Jan 2024

A Review On The Development Of Metals-Doped Vanadium Oxides For Zinc-Ion Battery, Kittima Lolupima, Jin Cao, Dongdong Zhang, Chenwu Yang, Xinyu Zhang, Jiaqian Qin

Journal of Metals, Materials and Minerals

Rechargeable zinc-ion batteries (ZIBs) are emerging as promising energy storage devices for various applications, including large-scale energy storage, due to their environmental friendliness, enhanced safety, and low cost. A key challenge in ZIB development is creating cathode materials that reduce the solubility of active materials in aqueous electrolytes, increase electrical conductivity, and extend life cycles for high performance. Vanadium-based compounds, with their diverse structures and multiple oxidation states (+2, +3, +4, and +5), have been extensively studied as effective cathodes for ZIBs. This mini review highlights recent research on doping transition metals into vanadium oxide materials to achieve superior electrochemical …

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Comparative Studies Of Radio Transparency And Dielectric Characteristics Of Polymer Composites, Azira Yermakhanova, Aidar Kenzhegulov, Berdiyar Baiserikov, Мohammed Meiirbekov, Nurlan Boguspayev Jan 2024

Comparative Studies Of Radio Transparency And Dielectric Characteristics Of Polymer Composites, Azira Yermakhanova, Aidar Kenzhegulov, Berdiyar Baiserikov, Мohammed Meiirbekov, Nurlan Boguspayev

Journal of Metals, Materials and Minerals

Aramid-epoxy composites and glass fiber reinforced plastics are widely used in the manufacturing of the fairing design for modern aerospace vehicles due to their excellent mechanical properties combined with radio transparency in wave transfer. In this paper, aramid-epoxy composite and fiberglass were fabricated by the vacuum infusion method for a comparative study on radio transparency and dielectric characteristics. The radio transparency of the studied materials was evaluated by free-space measurements in the frequency range of 1 GHz to 8.5 GHz. According to the radio transparency results, the aramid-epoxy composite undergoes less electromagnetic wave loss than glass fiber reinforced plastic. Modifying …

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Effect Of Hatch Spacing In Selective Laser Melting Process Of Ti-6al-4v Alloy On Finished Surface Roughness: A Computational Study, Reettiporn Thongpron, Patiparn Ninpetch, Prasert Chalermkarnnon, Pruet Kowitwarangkul Jan 2024

Effect Of Hatch Spacing In Selective Laser Melting Process Of Ti-6al-4v Alloy On Finished Surface Roughness: A Computational Study, Reettiporn Thongpron, Patiparn Ninpetch, Prasert Chalermkarnnon, Pruet Kowitwarangkul

Journal of Metals, Materials and Minerals

The Selective Laser Melting (SLM) process is a promising additive manufacturing technology for producing complex metal parts. However, this process has certain limitations, including lack of fusion and defects, which can hinder its industrial applications. These challenges can be addressed by determining the appropriate overlap percentage parameters. This study used numerical simulation to explore the effect of overlap percentage on multi-track melting in the SLM process for Ti-6Al-4V. The simulation results categorize the multi-track melting morphologies into two distinct groups. The first group, (0% to 40% overlap), displays consistent surface roughness with an average Ra value of 7 µm. In …

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Use Of Commercial Synthetic Filament Waste To Reinforce Biobased Poly(Butylene Succinate) With The Aid Of Compatibilizers, Nattakarn Hongsriphan, Alongkorn Popanna Jan 2024

Use Of Commercial Synthetic Filament Waste To Reinforce Biobased Poly(Butylene Succinate) With The Aid Of Compatibilizers, Nattakarn Hongsriphan, Alongkorn Popanna

Journal of Metals, Materials and Minerals

Since poly(butylene succinate) (PBS) has low rigidity for engineering application, this research attempted to reinforce PBS with poly(ethylene terephthalate) (PET) and polyamide-6 (nylon6) filaments with the reservation of polymer toughness. Filaments were chopped to be short fibers (length of 2 mm to 4 mm) and melt compounded with PBS pellets in the weight ratio of 1 wt%, 5 wt%, and 7 wt% using a twin-screw extruder that the temperature profile was set high enough for melting only PBS matrix. Two types of compatibilizers; hexamethylene diisocyanate (HMDI) or hexamethylene diamine (HMDA) of 0.05 wt% were used to treat fiber surface. It …

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