Metallurgy Commons^™

Timeline - History Of The Metallurgy / Mineral Processing Programs (1900-2022), Jerome Downey, Larry G. Twidwell

Metallurgy

No abstract provided.

History Of The Metallurgy / Mineral Processing Programs (1900-2022), Jerome Downey, Larry G. Twidwell

Metallurgy

No abstract provided.

Treatment Of Arsenic-Bearing Minerals And Fixation Of Recovered Arsenic Products: An Updated Review, Larry G. Twidwell

Metallurgy

Mineral processing and extractive metallurgical operations have created and are creating appreciable arsenic bearing wastewater and waste solid products that have to be handled, treated for recycle, or treated for environmentally safe disposal. At present there are intense research and operational activities being conducted to provide the best viable processing procedures to ensure that the mineral processing and extractive metallurgical industries are profitable and environmentally secure. The focus of this presentation is on the element arsenic, even though many other deleterious elements may also be present in ores and concentrates. Numerous base metal resources contain arsenic bearing minerals, especially resources …

Physics-Based Crystal Plasticity Model For Predicting Microstructure Evolution And Dislocation Densities, Juyoung Jeong

LSU Doctoral Dissertations

This work presents three different studies investigating plastic deformation mechanisms in metals and alloys using crystal plasticity finite element (CPFE) modeling. The first study presents a new nonlocal crystal plasticity model for face-centered cubic single crystals under heterogeneous inelastic deformation. The model incorporates generalized constitutive relations that incorporate the thermally activated and drag mechanisms to cover different kinetics of viscoplastic flow in metals and describes the plastic flow and yielding of single-crystals using dislocation densities. The model is compared to micropillar compression experiments for copper single crystals and clarifies the complex microstructural evolution of dislocation densities in metals. The second …

Use Of Electrochemical Techniques And Statistical Analysis To Investigate The Pitting Probability Of Copper, Sina Matin

Electronic Thesis and Dissertation Repository

The development of a safe permanent disposal plan is essential for the long-term disposal of used fuel bundles. Nuclear Waste Management Organization (NWMO) has been investigating the deep geologic disposal of nuclear waste which offers the optimum passive safety system with a negligible probability of release of radionuclides into the environment.

The proposed used fuel containers (UFC) for the permanent disposal of high-level nuclear waste in Canada is comprised of a carbon steel vessel coated with a 3 mm corrosion-resistant copper layer deposited using a combination of electrodeposition and cold spray deposition. Although copper is often considered to be thermodynamically …

Atomistic Simulation Studies Of Thin Film Growth And Plastic Deformation In Metals And Metal/Ceramic Nanostructures, Reza Namakian

LSU Doctoral Dissertations

Despite the significant improvements in manufacturing and synthesis processes of metals and ceramics in the past decades, there are still areas in which the procedure is still frequently more of an art or skill rather than a science. Therefore, systematic and combined experimental and computational studies are required to facilitate the development of techniques that offer thorough understanding of the events taking place during manufacturing and synthesis processes. With regard to these issues, it is paramount to address microscale characterizations and atomic scale understanding of the events during fabrication processes. One of the focuses of this study is unraveling fundamental …

Effect Of Austenization And Repeated Quenching On The Microstructures And Mechanical Properties Of Wear-Resistant Steel, Yanuar Nugraha, Myrna Ariati Mochtar

Journal of Materials Exploration and Findings (JMEF)

This study was focused on determining the effect of repeated austenitization and quenching on mechanical properties and microstructure. The experiment was carried out in a rolled quencher facility with a heat treatment process of one to two times, with parameters of an austenizing temperature of 9500C and quenching at a temperature of 8500C with pressurized water media. Testing of specimens, including microstructure observations and hardness testing. The repeated heat treatment process showed an increase in hardness of 0.79% on one-time repeated heat treatment and 1.65% on two repeated heat treatments. This occurs due to the presence accompanied by refinement of …

The Effect Of Graphite And Activated Carbon As Dispersed Particle In Base Fluid As Quench Medium On The Hardness Of S45c Carbon Steel, Wahyuaji Narottama Putra, Danika Aprilia Somadinata, Ghiska Ramahdita

Journal of Materials Exploration and Findings (JMEF)

Adding a solid particle dispersion into a base fluid could increase its thermal conductivity, hence increasing the heat transfer characteristics. One example of this thermally enhanced fluid is in heat treatment industry as quench medium. By controlling the amount of the dispersed particle, the cooling rate of the quench medium can be altered, and could affect steel hardness after heat treatment. In this research, the dispersed particle used was commercially available graphite and activated carbon particle. As for the base fluid, distilled water and common engine oil were compared. The concentration of the dispersed particle was 0.1, 0.3, 0.5 weight …

Microstructure Evolution And Austenitic Grain Refinement Of Ti-Modified High Mn Steels During Solution Annealing Heat Treatment, Abhinav Karanam, Arnab Sarkar, Erik Nenzen, Viraj Ashok Athavale, Mark Watson, Laura Nicole Bartlett, Lukas Bichler

Materials Science and Engineering Faculty Research & Creative Works

Austenitic high manganese (Mn) steels are often used in harsh environments due to their high toughness and wear resistance. Heat treatments are performed to engineer the microstructure of the steels and optimize their performance for the desired service conditions. This study investigated the effect of titanium (Ti) and heat treatment on the microstructure of cast high Mn steel (HMS) alloys. The results reveal that Ti addition contributed to grain refinement in the as cast and heat-treated conditions. In-situ observation of microstructure evolution up to 1125 °C confirmed the stability of precipitated TiC particles, while revealing a new mechanism of grain …

Performance Evaluation Of Composite Sandwich Structures With Additively Manufactured Aluminum Honeycomb Cores With Increased Bonding Surface Area, M. Rangapuram, S. K. Dasari, Joseph William Newkirk, K. Chandrashekhara, H. Misak, P. R. Toivonen, D. Klenosky, T. Unruh, J. Sam

Materials Science and Engineering Faculty Research & Creative Works

Modern aerostructures, including wings and fuselages, increasingly feature sandwich structures due to their high-energy absorption, low weight, and high flexural stiffness. The face sheet of these sandwich structures are typically thin composite laminates with interior honeycombs made of Nomex or aluminum. Standard cores are structurally efficient, but their design cannot be varied throughout the structure. With additive manufacturing (AM) technology, these core geometries can be altered to meet the design requirements that are not met in standard honeycomb cores. This study used a modified aluminum honeycomb core, with increased surface area on the top and bottom, as the core material …

Investigation Of Oxidation And Corrosion Resistance Of Ni-Based Alloys And Stainless Steels Under Co2 Environments At Elevated Temperatures, Spencer Roy Fultineer

Graduate Theses, Dissertations, and Problem Reports

High mechanical strength integrity, high robustness towards oxidation, and high resistance to carburization under CO2 environments at elevated temperatures are usually required for metallic systems that are employed for power generation. INCONEL 625 is a nickel-based superalloy that started development in the 1950s. This material was designed with the distinct purpose of use in high-temperature and high-pressure systems. While various materials possess the physical properties to handle these conditions, the creation of IN625 addresses the need for a material to withstand the highly corrosive properties of these kinds of environments. In order to evaluate the oxidation and corrosion resistance of …

Characterization Of Virgin, Re-Used, And Oxygen-Reduced Copper Powders Processed By The Plasma Spheroidization Process, M. Hossein Sehhat, David Perez-Palomino, Connor Wiedemeier, Tristan Cullom, Joseph William Newkirk

Materials Science and Engineering Faculty Research & Creative Works

Fabrication of parts with high mechanical properties heavily depend on the quality of powder deployed in the fabrication process. Copper powder in three different powder types were spheroidized using radio-frequency inductively coupled plasma (ICP) spheroidization process (TekSphero-15 system). The characterized powders include virgin powder as purchased from the powder manufacturer, powder used in electron beam powder bed fusion (EB-PBF) process, and reconditioned powder, which was used powder that underwent an oxygen-reduction treatment. The goal of spheroidizing these powder types was to evaluate the change in powder morphology, the possibility of enhancing the powder properties back to their as-received conditions, and …

A Study On The Impact Of Silicon And Manganese On Peritectic Behavior In Low Alloy Steels Assisted By Mold Thermal Mapping Technology And Shell Growth Measurements, Damilola Balogun, Muhammad Roman, Rex E. Gerald, Laura Bartlett, Jie Huang, Ronald O'Malley

Materials Science and Engineering Faculty Research & Creative Works

Non-Uniform Shell Growth Commonly Caused by the Peritectic Transformation in Low Carbon and Low Alloy Steels Has Been Directly Correlated with Mold Thermal Maps using a Mold Immersion Test into a Molten Steel Alloy. Mold Thermal Maps Were Obtained by Performing Real-Time Temperature Measurements with Optical Fibers Embedded 1 Mm from the Mold Working Surface. Shell Growth Measurements Were Obtained by 3D Optical Scanning of the Recovered Steel Shell Following Immersion Testing. the Effects of Silicon and Manganese on the Shell Growth and Mold Temperature Maps Have Been Examined in Relation to the Peritectic Transformation for Varying Carbon Contents. Results …

Cascaded Sapphire Fiber Bragg Gratings Inscribed By Femtosecond Laser For Molten Steel Studies, Dinesh Reddy Alla, Deva Prasad Neelakandan, Farhan Mumtaz, Rex E. Gerald, Laura Bartlett, Ronald J. O'Malley, Jeffrey D. Smith, Jie Huang

Electrical and Computer Engineering Faculty Research & Creative Works

This research reports a distributed fiber optic high-temperature sensing system tailored for applications in the steel industry and various other sectors. Recent advancements in optical sensor technology have led to the exploration of sapphire crystal fibers as a solution for sensing in harsh environments. Utilizing a femtosecond (fs) laser, cascaded fiber Bragg gratings (FBGs) were meticulously fabricated within a multimode sapphire optical fiber. These FBGs endowed the system with distributed sensing capabilities and underwent rigorous testing under extreme temperatures, reaching up to 1,800 °C. The study delves into the investigation of the FBG reflection spectrum, facilitated by the development of …

Characterization Of Virgin, Re-Used, And Oxygen-Reduced Copper Powders Processed By The Plasma Spheroidization Process, M. Hossein Sehhat, David Perez-Palomino, Connor Wiedemeier, Tristan Cullom, Joseph William Newkirk

Mathematics and Statistics Faculty Research & Creative Works

Fabrication of parts with high mechanical properties heavily depend on the quality of powder deployed in the fabrication process. Copper powder in three different powder types were spheroidized using radio-frequency inductively coupled plasma (ICP) spheroidization process (TekSphero-15 system). The characterized powders include virgin powder as purchased from the powder manufacturer, powder used in electron beam powder bed fusion (EB-PBF) process, and reconditioned powder, which was used powder that underwent an oxygen-reduction treatment. The goal of spheroidizing these powder types was to evaluate the change in powder morphology, the possibility of enhancing the powder properties back to their as-received conditions, and …

Phenomenological Analysis Of Surface Degradation Of Metallic Materials In Extreme Environment, Simon N. Lekakh, Oleg Neroslavsky

Materials Science and Engineering Faculty Research & Creative Works

The resistance to surface degradation in metallic alloys plays an important role for the lifetime of the components working in harsh environments. The mechanisms involved in degradation of metallic surface in a high-temperature aggressive gaseous atmosphere include the following: forming adherent to the surface multiphase oxide layer, partial spallation, and possible vaporization of formed compounds. The governing equation, which describes a parabolic growth of adherent layer, time-dependent vaporization, and cross-linked to instantaneous thickness of adherent layer spallation rate, was suggested and analyzed. The several relationships between the kinetic constants were defined from analysis of the governing equation. Design of routes …

Residual Stress Distribution, Distortion, And Crack Initiation In Conventional And Intensive Quench Practices, Kingsley Tochukwu Amatanweze, Mario F. Buchely, Viraj Ashok Athavale, Laura Bartlett, Ronald J. O'Malley, Toshi Suzuki

Materials Science and Engineering Faculty Research & Creative Works

This study evaluates the effect of two different quench practices on distortion, sensitivity to quench cracking, development and distribution of residual stress, microstructural uniformity, and hardenability of standardized test castings. Navy C-rings made of AISI 4340 were quenched in this experiment. Some rings were quenched in a conventional draft tube immersion quench bath, and others were quenched in an intensive quench spray system to compare with the results from the conventional immersion quench bath. The rings were measured with a coordinate measuring machine, for distortion and flatness, before and after quenching. Hardness profiles of the quenched rings showed through hardness …

An Updated Analytical Method For Predicting The Bracing Behavior Of Z-Purlin Supported Standing Seam Diaphragm Systems, Michael W. Seek

Engineering Technology Faculty Publications

Roof systems utilizing Z-purlins as a secondary member supporting a standing seam panel system are used extensively by the metal building industry. The Z-purlins rely on the diaphragm action in the standing seam panel system to provide lateral support and transfer forces to anchorages. The behavior of the standing seam system is highly nonlinear making prediction of the interaction between the Z-purlin and the standing seam system difficult. To better understand the behavior of the interaction between the purlins and the panel system, a series of non-linear shell finite element models were developed based on the test results of simple …

Cold-Formed Steel Strength Predictions For Combined Bending And Torsion, Yu Xia, Robert S. Glauz, Benjamin W. Schafer, Michael Seek, Hannah B. Blum

Engineering Technology Faculty Publications

Locally slender cross-section members, such as cold-formed steel Cee and Zee sections, are susceptible to significant twisting and high warping torsion stresses. Torsion considerations are complicated by whether it is derived as a first-order effect from loading or a second-order effect from instability. The current design for combined bending and torsion interaction has some limitations, including only considering the first yield in torsion and ignoring the cross-section slenderness in torsion. Previous work has derived a simple uniform equation to predict the bimoment capacity and two bimoment strength curves for local and distortional buckling under torsion only. This work is extended …

Elastic Properties Of The Non-Mixing Copper Donor Assisted Material In Friction Stir Welding Of Aluminum Alloys Using Nanoindentation, M. Ojha, A. H. Al-Allaq, Y. S. Mohammed, S. N. Bhukya, Z. Wu, A. A. Elmustafa

Mechanical & Aerospace Engineering Faculty Publications

Friction stir welding of high-strength materials such as steels is the impeded by the lack of the vast heat input needed to start the process. Contact friction is considered the most dominant source of heat generation for FSW steels which tends to cause severe wear conditions of the tool hear. To relieve the extreme wear conditions that occur on the tool heads because of FSW steels, we introduce the non-mixing Cu donor stir material to friction stir welding of aluminum alloys. The elastic properties of the Cu donor assisted friction stir welded aluminum alloys are measured using nanoindentation. The hardness …