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Hydrophobic Deep Eutectic Solvents: Liquid-Liquid Extraction Of Organic Water Pollutants, Abigail Louise Maletta 2024 Western Michigan University

Hydrophobic Deep Eutectic Solvents: Liquid-Liquid Extraction Of Organic Water Pollutants, Abigail Louise Maletta

Masters Theses

Pollution is a topic of significant research within the scientific community. The massive demand for industrial processes to deliver the technology and resources we rely on has opened numerous avenues for pollutants to enter the environment, affecting air, water, soil, and the food chain. Oftentimes, these pathways are intertwined, and the interplay between water and air currents spreads pollution globally, creating a cascade of environmental impacts. Water, a vital resource for all forms of life, is particularly susceptible to industrial pollution. Among the most prevalent water pollutants are heavy metals, such as lead and mercury, and organic compounds, often released …


Investigating Ocean Carbonate System Changes Across Latitudes In The North Atlantic Basin With A Time-Series Mooring System, Anna Trujillo 2024 SIT Study Abroad

Investigating Ocean Carbonate System Changes Across Latitudes In The North Atlantic Basin With A Time-Series Mooring System, Anna Trujillo

Independent Study Project (ISP) Collection

The world ocean, specifically the Arctic, serves as one of the greatest mitigators for anthropogenic carbon dioxide release, making the study of high latitude ocean carbonate chemistry an increasingly important topic. While much work has been done concerning the science of acidification and future model projections, analyzing data to detect decadal anthropogenic trends and effects is also highly important. Aiming to add to this data pool, this study investigated the ocean carbonate system at three North Atlantic mooring locations at polar, subtropical, and tropical latitudes from 2013 - 2021. Time series datasets of the pH and pCO₂ of surface water …


Efficient Removal Of Chemical Organic Demand And Total Organic Carbon From Leachate Using Heterogeneous Fenton Catalyst Based On Activated Carbon, Amar IDIR, Mounir ZIATI, Mohamed Bouzid 2024 Research Unit: Materials, Processes and Environment, Faculty of Technology, M’hamed Bougara University, Boumerdes 35000, Algeria

Efficient Removal Of Chemical Organic Demand And Total Organic Carbon From Leachate Using Heterogeneous Fenton Catalyst Based On Activated Carbon, Amar Idir, Mounir Ziati, Mohamed Bouzid

Emirates Journal for Engineering Research

Organic components contained in leachates resulting from decomposition of waste are difficult to degrade. Leachate volume and its composition vary depending on biogeochemistry of site type of deposited residues, and the age of sanitary landfill. The present study aims to develop efficient heterogeneous Fenton oxidation of organic matter, expressed in terms of chemical organic demand (COD) and total organic carbon (TOC) of leachate using the newly synthesized iron-modified activated carbon. The characterization of catalyst revealed that the Fe(II) was successfully introduced onto the original activated carbon (AC) and diversified the material’s surface morphology and elemental compounds. The heterogeneous Fenton oxidation …


Advanced Oxidation Of Tert-Butanol With Ultraviolet Light Emitting Diodes And Hydrogen Peroxide, Lauren R. Mainolfi 2024 Air Force Institute of Technology

Advanced Oxidation Of Tert-Butanol With Ultraviolet Light Emitting Diodes And Hydrogen Peroxide, Lauren R. Mainolfi

Theses and Dissertations

Tert-butanol (TBA), a versatile chemical widely used in industrial processes, poses exposure risks through inhalation, ingestion, and skin contact. Environmental contamination, often from industrial activities, emphasizes the importance of robust waste management and monitoring to protect water supplies from potential TBA migration and ensure drinking water safety. This study employed hydrogen peroxide (H2O2): TBA molar ratios of 100, 200, 400, and 500:1 in a Continuous Flow Stirred-Tank Reactor (CSTR) with UV-LED as the TBA degradation mechanism in an Advanced Oxidation Process (AOP). The UV-LEDs and H2O2 were synergistically employed to generate hydroxyl radicals in an advanced oxidation process. Gas chromatography–mass …


Advanced Oxidation Of Methyl Tert Butyl Ether With Ultraviolet Light Emitting Diodes, Aaron R. Neal 2024 Air Force Institute of Technology

Advanced Oxidation Of Methyl Tert Butyl Ether With Ultraviolet Light Emitting Diodes, Aaron R. Neal

Theses and Dissertations

Methyl Tert-Butyl Ether (MTBE) is a volatile, soluble, organic compound introduced to gasoline within the United States as a fuel oxygenator in 1979. MTBE is a common groundwater pollutant due to its high water solubility and resistance to bio-degradation; it commonly infiltrates groundwater sources via leaking underground storage tanks or fuel spills. This research employed ultraviolet light emitting diodes (UV-LEDs) and hydrogen peroxide (H2O2) induced advanced oxidation process (AOP) to treat MTBE contaminated water at the bench scale. Using four H2O2:MTBE molar peroxide ratios (100:1, 200:1, 400:1, 500:1), MTBE degradation was induced …


Toward A Coordinated Understanding Of Hydro-Biogeochemical Root Functions In Tropical Forests For Application In Vegetation Models, Daniela F. Cusack, Bradley Christoffersen, Chris M. Smith-Martin, Kelly M. Andersen, Amanda L. Cordeiro, Katrin Fleischer, S. Joseph Wright, Nathaly R. Guerrero-Ramírez, Laynara F. Lugli, Lindsay A. McCulloch, Mareli Sanchez-Julia, Sarah A. Batterman, Caroline Dallstream, Claire Fortunel, Laura Toro, Lucia Fuchslueger, Michelle Y. Wong, Daniela Yaffar, Joshua B. Fisher, Marie Arnaud, Lee H. Dietterich, Shalom D. Addo-Danso, Oscar J. Valverde-Barrantes, Monique Weemstra, Jing Cheng Ng, Richard J. Norby 2024 Colorado State University - Fort Collins

Toward A Coordinated Understanding Of Hydro-Biogeochemical Root Functions In Tropical Forests For Application In Vegetation Models, Daniela F. Cusack, Bradley Christoffersen, Chris M. Smith-Martin, Kelly M. Andersen, Amanda L. Cordeiro, Katrin Fleischer, S. Joseph Wright, Nathaly R. Guerrero-Ramírez, Laynara F. Lugli, Lindsay A. Mcculloch, Mareli Sanchez-Julia, Sarah A. Batterman, Caroline Dallstream, Claire Fortunel, Laura Toro, Lucia Fuchslueger, Michelle Y. Wong, Daniela Yaffar, Joshua B. Fisher, Marie Arnaud, Lee H. Dietterich, Shalom D. Addo-Danso, Oscar J. Valverde-Barrantes, Monique Weemstra, Jing Cheng Ng, Richard J. Norby

Biology, Chemistry, and Environmental Sciences Faculty Articles and Research

Tropical forest root characteristics and resource acquisition strategies are underrepresented in vegetation and global models, hampering the prediction of forest–climate feedbacks for these carbon-rich ecosystems. Lowland tropical forests often have globally unique combinations of high taxonomic and functional biodiversity, rainfall seasonality, and strongly weathered infertile soils, giving rise to distinct patterns in root traits and functions compared with higher latitude ecosystems. We provide a roadmap for integrating recent advances in our understanding of tropical forest belowground function into vegetation models, focusing on water and nutrient acquisition. We offer comparisons of recent advances in empirical and model understanding of root characteristics …


Lotic-Sipco2: Adaptation Of An Open-Source Co2 Sensor System And Examination Of Associated Emission Uncertainties Across A Range Of Stream Sizes And Land Uses, Andrew L. Robison, Lauren E. Koenig, Jody D. Potter, Lisle E. Snyder, Christopher W. Hunt, William H. McDowell, Wilfred M. Wollheim 2024 Ecole Polytechnique Fédérale de Lausanne

Lotic-Sipco2: Adaptation Of An Open-Source Co2 Sensor System And Examination Of Associated Emission Uncertainties Across A Range Of Stream Sizes And Land Uses, Andrew L. Robison, Lauren E. Koenig, Jody D. Potter, Lisle E. Snyder, Christopher W. Hunt, William H. Mcdowell, Wilfred M. Wollheim

Faculty Publications

River networks play a crucial role in the global carbon cycle, as relevant sources of carbon dioxide (CO2) to the atmosphere. Advancements in high-frequency monitoring in aquatic environments have enabled measurement of dissolved CO2 concentration at temporal resolutions essential for studying carbon variability and evasion from these dynamic ecosystems. Here, we describe the adaptation, deployment, and validation of an open-source and relatively low-cost in situ pCO2 sensor system for lotic ecosystems, the lotic-SIPCO2. We tested the lotic-SIPCO2 in 10 streams that spanned a range of land cover and basin size. Key system adaptations for lotic environments included prevention of biofouling, …


Univariate Optimization Of Dispersive Liquid-Liquid Microextraction For Preconcentration Of Lead From Environmental Matrices, Samawah Region Prior To Quantification Using Flame Atomic Absorption Spectroscopy, Zaman Sahb Mehdi, Saher A. Ali Alshamkhawy 2024 Department of Chemistry, College of Science, University of Thi-Qar, Thi-Qar, 64001, Iraq.

Univariate Optimization Of Dispersive Liquid-Liquid Microextraction For Preconcentration Of Lead From Environmental Matrices, Samawah Region Prior To Quantification Using Flame Atomic Absorption Spectroscopy, Zaman Sahb Mehdi, Saher A. Ali Alshamkhawy

Al-Bahir

In this work, a procedure based on dispersive liquid₋liquid microextraction for lead (Pb) preconcentration and quantification in an environmental matrix by flame atomic absorption spectroscopy (FAAS) was applied. A case-study approach was chosen to obtain further in-depth information on the Pb levels. The green chemistry principles have been applied for the pretreatment and preparation of real samples by focusing on some features such as the volume of reagents/sample, employ of energy efficient equipment, and production of waste. A univariate strategy was utilized to achieve the optimum extraction conditions. 1750 µL of acetonitrile containing 100 µL of carbon tetrachloride, were rapid …


Sulfate Enhances The Adsorption And Retention Of Cu(Ii) And Zn(Ii) To Dispersed And Aggregated Iron Oxyhydroxide Nanoparticles, Emma M. Kocik, Abigail Kim, Miranda L. Aiken, Lauren Smith, Christopher S. Kim 2024 University of Pennsylvania

Sulfate Enhances The Adsorption And Retention Of Cu(Ii) And Zn(Ii) To Dispersed And Aggregated Iron Oxyhydroxide Nanoparticles, Emma M. Kocik, Abigail Kim, Miranda L. Aiken, Lauren Smith, Christopher S. Kim

Biology, Chemistry, and Environmental Sciences Faculty Articles and Research

The adsorption and retention of metal ions to nanoscale iron (hydr)oxides in aqueous systems is significantly influenced by prevailing environmental conditions. We examined the influence of sulfate, the second most common anion in seawater that is present in many other natural aquatic systems, on the adsorption and retention of Cu(II) and Zn(II) to synthetic iron oxyhydroxide nanoparticles (NPs) and their aggregates. Batch uptake experiments with monodisperse NPs and NPs aggregated by changes in pH, ionic strength, and temperature were conducted over sulfate concentrations ranging from 0 to 0.30 M. The introduction of 0.03 M sulfate significantly increased the initial adsorption …


Simple Sars-Cov-2 Concentration Methods For Wastewater Surveillance In Low Resource Settings, Mohammad Dehghan Banadaki, Soroosh Torabi, Alexus Lori Rockward, William Strike, Ann Noble, James W. Keck, Scott M. Berry 2024 University of Kentucky

Simple Sars-Cov-2 Concentration Methods For Wastewater Surveillance In Low Resource Settings, Mohammad Dehghan Banadaki, Soroosh Torabi, Alexus Lori Rockward, William Strike, Ann Noble, James W. Keck, Scott M. Berry

UK CARES Faculty Publications

Wastewater-based epidemiology (WBE) measures pathogens in wastewater to monitor infectious disease prevalence in communities. Due to the high dilution of pathogens in sewage, a concentration method is often required to achieve reliable biomarker signals. However, most of the current concentration methods rely on expensive equipment and labor-intensive processes, which limits the application of WBE in low-resource settings. Here, we compared the performance of four inexpensive and simple concentration methods to detect SARS-CoV-2 in wastewater samples: Solid Fraction, Porcine Gastric Mucin-conjugated Magnetic Beads, Calcium Flocculation- Citrate Dissolution (CFCD), and Nanotrap® Magnetic Beads (NMBs). The NMBs and CFCD methods yielded the highest …


Thin-Film Nanocomposite Membranes With Alumina Nanoparticles For Textile Wastewater Treatment Applications, Amr Mohamed Tayel 2024 American University in Cairo

Thin-Film Nanocomposite Membranes With Alumina Nanoparticles For Textile Wastewater Treatment Applications, Amr Mohamed Tayel

Theses and Dissertations

Thin-film nanocomposite (TFN) membranes are gaining great interest in industrial wastewater treatment due to their superior performance, especially for higher water flux and pollutants’ rejection, as well as improved chemical, thermal and mechanical stabilities, compared to other types of membranes. The performance of TFN membranes can be enhanced using different types of nanofillers, among which ceramic nanomaterials, such as Al2O3, offer a promising potential for applications involving treatment of industrial wastewater such as textile effluents, and this is due to their stability, hydrophilicity, and relative low cost. The study of the TFN membrane properties and structure allows the optimization and …


Intercalibration: A Cornerstone Of The Success Of The Geotraces Program, Ana Aguilar-Islas, Hélène Planquette, Maeve C. Lohan, Walter Geibert, Gregory Cutter 2024 University of Alaska, Fairbanks

Intercalibration: A Cornerstone Of The Success Of The Geotraces Program, Ana Aguilar-Islas, Hélène Planquette, Maeve C. Lohan, Walter Geibert, Gregory Cutter

OES Faculty Publications

The international GEOTRACES program was developed to enhance knowledge about the distribution of trace elements and their isotopes (TEIs) in the ocean and to reduce the uncertainty about their sources, sinks, and internal cycling. Recognizing the importance of intercalibration from the outset, GEOTRACES implemented intercalibration efforts early in the program, and consensus materials were generated that included the full range of TEIs dissolved in seawater, in suspended particles, and from aerosols. The GEOTRACES section cruises include “crossover station(s)” that are occupied by two or more sections and whereby all aspects of sample collection, preservation, and processing can be compared and …


Editorial: The Marine Iodine Cycle, Past, Present, And Future, Rosie Chance, Gregory A. Cutter, Dalton S. Hardisty, Anoop S. Mahajan 2024 University of York, York, United Kingdom

Editorial: The Marine Iodine Cycle, Past, Present, And Future, Rosie Chance, Gregory A. Cutter, Dalton S. Hardisty, Anoop S. Mahajan

OES Faculty Publications

In this Research Topic, we bring together ten articles from the diverse research communities interested in the marine iodine cycle, including paleoceanographers, atmospheric chemists, and biogeochemists. The physical chemistry underpinning iodine’s chemical speciation and transformations in the ocean is reviewed by Luther; this paper provides a theoretical basis for the field observations presented in this Research Topic.


Marine Emissions Of Methanethiol Increase Aerosol Cooling In The Southern Ocean, Charel Wohl, Julián Villamayor, Martí Galí, Anoop S. Mahajan, Rafael P. Fernández, Carlos A. Cuevas, Adriana Bossolasco, Qinyi Li, Anthony J. Kettle, Tara Williams, Roland Sarda-Esteve, Valérie Gros, Rafel Simó, Alfonso Saiz-Lopez 2024 University of East Anglia

Marine Emissions Of Methanethiol Increase Aerosol Cooling In The Southern Ocean, Charel Wohl, Julián Villamayor, Martí Galí, Anoop S. Mahajan, Rafael P. Fernández, Carlos A. Cuevas, Adriana Bossolasco, Qinyi Li, Anthony J. Kettle, Tara Williams, Roland Sarda-Esteve, Valérie Gros, Rafel Simó, Alfonso Saiz-Lopez

OES Faculty Publications

Ocean-emitted dimethyl sulfide (DMS) is a major source of climate-cooling aerosols. However, most of the marine biogenic sulfur cycling is not routed to DMS but to methanethiol (MeSH), another volatile whose reactivity has hitherto hampered measurements. Therefore, the global emissions and climate impact of MeSH remain unexplored. We compiled a database of seawater MeSH concentrations, identified their statistical predictors, and produced monthly fields of global marine MeSH emissions adding to DMS emissions. Implemented into a global chemistry-climate model, MeSH emissions increase the sulfate aerosol burden by 30 to 70% over the Southern Ocean and enhance the aerosol cooling effect while …


Impact Of Solar Radiation On Perchlorate Formation In The Atmosphere: Evidence From Ice Core Measurements, Bishnu Kunwar 2024 South Dakota State University

Impact Of Solar Radiation On Perchlorate Formation In The Atmosphere: Evidence From Ice Core Measurements, Bishnu Kunwar

Electronic Theses and Dissertations

Perchlorate, which derives from both anthropogenic and natural sources in the current environment, poses a substantial health hazard to humans as it competes with iodine uptake in the thyroid gland. Consequently, there has been considerable concern about minimizing human exposure to environmental perchlorate by restricting its release from man-made sources. However, the absence of a clear understanding regarding the respective contributions of man-made and natural sources has hindered widespread regulation efforts. A 300-year (1700–2007) Summit, Greenland ice core record from a previous study showed relatively stable perchlorate concentrations in Greenland snow prior to 1980, with some elevated perchlorate levels associated …


Assessment Of The Extraction And Quantification Of Pfbs From Sprague Dawley Rat Adipose Tissues, Joshua O. Osaghae 2024 Georgia Southern University

Assessment Of The Extraction And Quantification Of Pfbs From Sprague Dawley Rat Adipose Tissues, Joshua O. Osaghae

Honors College Theses

Per- and polyfluoroalkyl substances (PFAS) are a group of complex synthetic chemicals that have applications ranging from automotives to consumer products. PFAS have been found to bioaccumulate in the ecosystem as their carbon-fluorine bonds are among the strongest bonds in organic chemistry. Perfluorobutanesulfonic acid (PFBS) compounds are used as surfactants in water- and stain-repellent coatings for fabrics and carpets, cleaning agents, and paints. The persistence of PFAS has led to their accumulation in sources of groundwater, making them ubiquitous drinking water contaminants of concern with evidence linking PFAS exposure to adverse health effects, including reduced kidney function, thyroid disruption, and …


The Effect Of Ions On The Adsorption Of So2 On A Water Nanoparticle, Nathaniel W. Gillispie 2024 Western Kentucky University

The Effect Of Ions On The Adsorption Of So2 On A Water Nanoparticle, Nathaniel W. Gillispie

Mahurin Honors College Capstone Experience/Thesis Projects

Secondary Organic Aerosols (SOAs) have been of interest to atmospheric chemists for their harmful effects on human health and implications for climate change. Here, we explore a likely system from the early stages of SOA formation. Using compu- tational methods, water nanoparticles with and without ions were simulated. We observe the effects of ions on the adsorption of SO2 on this system. SO2 in the at- mosphere is associated with greater production of SOAs, so its study is important to SOA formation. We find that the overall structure of water is the most important observable affecting the location of SO2 …


Permafrost Carbon: Progress On Understanding Stocks And Fluxes Across Northern Terrestrial Ecosystems, Claire C. Treat, Anna-Maria Virkkala, Eleanor Burke, Lori Bruhwiler, Abhishek Chatterjee, Joshua B. Fisher, Josh Hashemi, Frans-Jan W. Parmentier, Brendan M. Rogers, Sebastian Westermann, Jennifer D. Watts, Elena Blanc-Betes, Matthias Fuchs, Stefan Kruse, Avni Malhotra, Kimberley Miner, Jens Strauss, Amanda Armstrong, Howard E. Epstein, Bradley Gay, Mathias Goeckede, Aram Kalhori, Dan Kou, Charles E. Miller, Susan M. Natali, Youmi Oh, Sarah Shakil, Oliver Sonnentag, Ruth K. Varner, Scott Zolkos, Edward A.G. Schuur, Gustaf Hugelius 2024 Alfred Wegener Institute Helmholtz Center for Polar and Marine Research

Permafrost Carbon: Progress On Understanding Stocks And Fluxes Across Northern Terrestrial Ecosystems, Claire C. Treat, Anna-Maria Virkkala, Eleanor Burke, Lori Bruhwiler, Abhishek Chatterjee, Joshua B. Fisher, Josh Hashemi, Frans-Jan W. Parmentier, Brendan M. Rogers, Sebastian Westermann, Jennifer D. Watts, Elena Blanc-Betes, Matthias Fuchs, Stefan Kruse, Avni Malhotra, Kimberley Miner, Jens Strauss, Amanda Armstrong, Howard E. Epstein, Bradley Gay, Mathias Goeckede, Aram Kalhori, Dan Kou, Charles E. Miller, Susan M. Natali, Youmi Oh, Sarah Shakil, Oliver Sonnentag, Ruth K. Varner, Scott Zolkos, Edward A.G. Schuur, Gustaf Hugelius

Biology, Chemistry, and Environmental Sciences Faculty Articles and Research

Significant progress in permafrost carbon science made over the past decades include the identification of vast permafrost carbon stocks, the development of new pan-Arctic permafrost maps, an increase in terrestrial measurement sites for CO2 and methane fluxes, and important factors affecting carbon cycling, including vegetation changes, periods of soil freezing and thawing, wildfire, and other disturbance events. Process-based modeling studies now include key elements of permafrost carbon cycling and advances in statistical modeling and inverse modeling enhance understanding of permafrost region C budgets. By combining existing data syntheses and model outputs, the permafrost region is likely a wetland methane …


Wildfire Effects On The Fate Of Deposited Nitrogen In A Boreal Larch Forest, Weili Liu, Jiaxing Zu, B. Liu, Lin Qi, Wei Huang, Yunting Fang, Jian Yang 2024 Fujian Polytechnic Normal University

Wildfire Effects On The Fate Of Deposited Nitrogen In A Boreal Larch Forest, Weili Liu, Jiaxing Zu, B. Liu, Lin Qi, Wei Huang, Yunting Fang, Jian Yang

Earth and Environmental Sciences Faculty Publications

The effects of nitrogen (N) deposition on forests largely depend on the ecosystem N status and the fates of deposited N. Boreal forests are typically N-limited ecosystems and are considered to be more efficient in retaining deposited N relative to temper- ate and tropical forests. As a primary disturbance in boreal forests, wildfires may alleviate N limitation in the burned ecosystem and increase mineralization, resulting in the altered outcomes of the N deposition.


The Surface Chemistry And Binding Interactions Of Lignin With Polymer-Encapsulated Gold Nanoparticles Acting As Model Microplastics, Oluwaseun Ayodeji Akinsola 2024 Central Washington University

The Surface Chemistry And Binding Interactions Of Lignin With Polymer-Encapsulated Gold Nanoparticles Acting As Model Microplastics, Oluwaseun Ayodeji Akinsola

All Master's Theses

This study investigates the surface chemistry and molecular-level interactions between lignin, a special type of natural organic matter, and polymer-capped gold nanoparticles, shedding light on the strength of adsorption between lignin and nanoscale polymer surfaces. Specifically, the study presents a variety of nanoscale polymer surfaces displaying different charged functional groups, using layer-by-layer assembly of three polyelectrolytes (polyallylamine hydrochloride (PAH)), polyacrylic acid (PAA), and poly(diallyldimethylammonium chloride (PDADMAC)) on 90 nm citrate-stabilized gold nanoparticles (AuNPs). This approach provides a library of polymer-encapsulated AuNPs for investigating the binding interactions of lignin to nanoscale polymers via spectroscopic techniques. ζ-potential, dynamic light scattering (DLS), …


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