Metallurgy Commons^™

Cassava Pulp As A Biofuel Feedstock Of An Enzymatic Hydrolysis Proces, Djuma’Ali Djuma’Ali, Nonot Soewarno, Sumarno Sumarno, Dyah Primarini, Wahono Sumaryono

Makara Journal of Technology

Cassava pulp, a low cost solid byproduct of cassava starch industry, has been proposed as a high potential ethanolic fermentation substrate due to its high residual starch level, low ash content and small particle size of the lignocellulosic fibers. As the economic feasibility depends on complete degradation of the polysaccharides to fermentable glucose, the comparative hydrolytic potential of cassava pulp by six commercial enzymes were studied. Raw cassava pulp (12% w/v, particle size <320 >μm) hydrolyzed by both commercial pectinolytic (1) and amylolytic (2) enzymes cocktail, yielded 70.06% DE. Hydrothermal treatment of cassava pulp enhanced its susceptibility to enzymatic cleavageas compared …

Fabrication Of Size-Tunable Metallic Nanoparticles Using Plasmid Dna As A Biomolecular Reactor, Jacopo Samson, Irene Piscopo, Alex Yampolski, Patrick Nahirney, Andrea Parpas, Amit Aggarwal, Raihan Saleh, Charles Michael Drain

Publications and Research

Plasmid DNA can be used as a template to yield gold, palladium, silver, and chromium nanoparticles of different sizes based on variations in incubation time at 70 °C with gold phosphine complexes, with the acetates of silver or palladium, or chromium acetylacetonate. The employment of mild synthetic conditions, minimal procedural steps, and aqueous solvents makes this method environmentally greener and ensures general feasibility. The use of plasmids exploits the capabilities of the biotechnology industry as a source of nanoreactor materials.

A Quantitative Study Of The Weldability Of Inconel 718 Using Gleeble And Varestraint Test Methods, Sean Quigley

Master's Theses

Nickel super alloy Inconel 718 was tested and compared to Haynes 230 using Gleeble and Varestraint mechanical test methods. Hot cracking susceptibility was examined in either alloy using a sub-scale Varestraint test method at 5 augmented strain levels: 0.25%, 05.%, 1%, 2%, and 4%. Maximum crack length, total crack length, and number of cracks were measured for each strain level. Gleeble hot ductility on-heating and on-cooling tests were performed on both alloys. Inconel 718 was tested on-heating at target temperatures of 1600˚F, 2000˚F, 2100˚F, 2200˚F, and on cooling at 1600˚F, 1700˚F, 1800˚F, 1900˚F, and 2100˚F. Haynes 230 was tested on-heating …

Study Of Mechanical Behaviors And Structures Of Bulk Metallic Glasses With High-Energy Synchrotron X-Ray Diffraction, Feng Jiang

Doctoral Dissertations

This dissertation addresses two critical issues in the mechanical behaviors and structures of bulk-metallic glasses (BMGs): (1) the effect of composition, fabrication method, and pretreatment of plastic deformation on mechanical properties and structures of BMGs; (2) the mechanical response and structural evolution of BMGs in the elastic and plastic region.

(Cu₅₀Zr₅₀)₉₄Al₆ and (Cu₅₀Zr₅₀)₉₂Al₈ amorphous alloys were used to study the effect of composition on mechanical properties and structures of BMGs. The (Cu₅₀Zr₅₀)₉₄Al₆ alloy exhibits lower yield stress and Young’s …

Effect Of Au Content On Microstructural Evolution Of Snagcu Solder Joints That Undergo Isothermal Aging And Reliability Testing, Patrick J. Hyland

Master's Theses

Electronics, especially, printed circuit boards (PCBs) are a widespread technology. Metal coatings or “surface finishes” are often added to PCB board pads and component leads during manufacturing to improve their performance. Electroplated nickel/gold over copper is a popular surface finish for printed circuit boards and component leads. The presence of gold in solder joints, however, is known to have detrimental effects referred to as gold embrittlement. It is generally understood that tin-lead solder joints with less than 3 weight percent (wt%) of gold will not experience reliability issues. The acceptable level of gold in lead-free solder joints, however, is less …

Design, Fabrication, And Characterization Of A Thin-Film Nickel-Titanium Shape Memory Alloy Diaphragm For Use In Micro-Electro-Mechanical Systems, Brian Joel Alvarez

Master's Theses

Previous work done at Cal Poly has shown that thin-film nickel-titanium (NiTi) can be easily sputtered onto silicon wafers and annealed to create a crystallized shape memory alloy (SMA) film. Initial work on creating devices yielded cantilevers that were highly warped due to thin-film stress created during the sputtering process. The objective of this work was to create a thin-film NiTi SMA device that could be better characterized. A membrane was selected due to the simplicity of fabrication and testing which would also oppose the thin-film stress due to the increase in attachment points to the substrate.

Silicon wafers were …

Time-Dependent Crack Growth Behavior Of Alloy 617 And Alloy 230 At Elevated Temperatures, Shawoon Kumar Roy

UNLV Theses, Dissertations, Professional Papers, and Capstones

Two Ni-base solid-solution-strengthened superalloys: INCONEL 617 and HAYNES 230 were studied to check sustained loading crack growth (SLCG) behavior at elevated temperatures appropriate for Next Generation Nuclear Plant (NGNP) applictaions with constant stress intensity factor (K _max = 27.75 MPa[checkmark]m) in air. The results indicate a time-dependent rate controlling process which can be characterized by a linear elastic fracture mechanics (LEFM) parameter - stress intensity factor (K). At elevated temperatures, the crack growth mechanism was best described using a damage zone concept. Based on results and study, SAGBOE (stress accelerated grain boundary oxidation embrittlement) is considered the primary reason for …

The Effects Of Heat Treatment On Area Percent Porosity And Corrosion Behavior Of High-Nickel Thermal Spray Coatings, Travis Crowe, Alec Guraydin

Materials Engineering

Samples of two Thermal Spray Coating (TSC) alloys on a low carbon steel substrate were obtained: alloy C276 and Nicko-Shield 200. Specimens of each alloy were subjected to heat treatments at temperatures at 1100° for 60 minutes and 1200° for 10 minutes, with some specimens left in the as-sprayed condition. Three replicates were prepared for each condition. Thin 1” strips were cut using a diamond wafering blade for porosity measurements and 2” x 1” specimens were cut for corrosion testing using a SiC abrasive saw. The porosity specimens were mounted in acrylic resin, polished, and examined using SEM. From these …

Characterization Of The Relationship Between The Microstructure And Tensile Strength Of Annealed Ti-6al-4v, Aldo Corona

Materials Engineering

Tensile coupons of Ti-6Al-4V were heat treated at varying annealing temperatures from 1200°F (648°C) to 1450°F (787°C) at 50°F (23°C) increments for 1 hour. The samples were air cooled to room temperature or furnace cooled to 800°F (426°C) followed by air cooling to room temperature. Four tensile coupons were treated at each annealing temperature and cooling rate. Alpha case was observed to form on the surface of the samples post heat treatment with a maximum depth of 25 µm (.001 in). Samples were tensile tested for their ultimate tensile strength, yield strength, and percent elongation. Samples across all annealing temperatures …

Dissimilar Metal Weld Variability Due To Lot Differences In Nitinol/ Stainless Steel Interface, Matthew R. Rudow

Materials Engineering

Abstract

An experiment was conducted to determine and reduce the causes of variation between a 304 Stainless Steel and super elastic Nickel Titanium dissimilar metal weld. Six factors were established to understand the cause of variation: perpendicularity, final grind, surface finish, weld force, weld pulse duration, and alignment. Using a rotational test with an air piston break pressures were established and charted in Minitab to identify trends. It was shown that weld force and weld pulse duration were the two factors that had the most influence on break strength. This data also showed that higher strength groups had less variability. …

Process Refinement Through Design Of Experiments (Taguchi) To Reduce Porosity Levels Of Thin Flame Spray Nicrbsi Coatings On Cast Aluminium Alloys, David Culliton, David Kennedy, Tony Betts

Conference Papers

Thin(16matrix of key deposition parameters was constructed to develop the optimum spray parameters. The effects of parameter variations on the porosity levels of these coatings were assessed. Key parameter interactions were reported. Quantifiable interactions between the selected parameters were noted for the LM24 substrate. However, on the LM25 substrate these interactions were much less defined. Corrosion performance of the optimised coatings, based on electrochemical impedance spectroscopy, was reported. The presence of through-pores in the coatings were shown to reduce the corrosion resistance of the coated systems by a factor of 10, in dilute NaCl solutions, compared to bulk 316L stainless …

The Effect Of The Environment On The Corrosion Products And Corrosion Rates On Gas Transmission Pipelines, Brent Sherar

Electronic Thesis and Dissertation Repository

This thesis reports a series of investigations examining external corrosion processes along gas transmission pipelines. TransCanada PipeLines Ltd. (TCPL) has developed six proposed corrosion scenarios to describe external pipeline corrosion, based primarily on corrosion products and corrosion rates (CRs) observed at field sites. The six proposed corrosion scenarios can be divided into two groups: abiotic and biotic. The three abiotic corrosion scenarios are (1) anaerobic corrosion, (2) aerobic corrosion, and (3) anaerobic corrosion turning aerobic; while (4) anaerobic corrosion with microbial effects, (5) aerobic corrosion turning anaerobic with microbial effects, and (6) anaerobic corrosion with microbial effects turning aerobic comprise …

Review Of The Maxus 8 Sounding Rocket Experiment To Investigate Solidification In A Ti-Al-Nb Alloy, Robin Mooney, David Browne, Olga Budenkova, Yves R. Fautrelle, Ludo Froyen, Andrey Kartavykh, Stephan Rex, Burkhard Schmitz, Daniella Voss, Shaun Mcfadden

Conference Papers

A review of the MAXUS 8 sounding rocket microgravity experiment to investigate solidification structures in a Ti-Al-Nb intermetallic alloy is presented. The experiment was part of the Intermetallic Materials Processing in Relation to Earth and Space Solidification (IMPRESS) EU FP6 project. Key objectives were to investigate columnar and equiaxed solidification, and to achieve Columnar-to-Equiaxed Transition (CET) in the alloy. A microgravity experiment was designed to achieve this using a controlled power-down method. Two alloys were tested: one inoculated with a grain refiner and the other without grain refinement. Unrefined samples displayed axial and radial columnar growth. Boride inoculated samples displayed …

Growth Of Oriented Nickel-Manganese-Gallium Single Crystals Via The Bridgman Method, Douglas Leroy Kellis

Boise State University Theses and Dissertations

A Bridgman furnace was designed and built to grow oriented single crystals of nickel-manganese-gallium. The starting alloys were produced from high purity elements. The compositions of the alloys and single crystals were determined with energy dispersive x-ray spectroscopy. Oxygen concentration of the starting elements, the alloys, and single crystal were determined with the LECO combustion method. Starting seeds were produced from single crystal ingots produced at ETH Zurich, Switzerland, and from a single crystal grown from these seeds. Crystallographic orientation of the starting seeds and the single crystals were determined with x-ray diffraction. Mechanical testing was performed on a single …

The Formation Design Of Noise Reducers From Plywood, Foam, Tray, Dan Coconut Fiber For Static Sources, Melati Ferianita Fachrul, Wisnu Eka Yulyanto, Asharani Merya

Makara Journal of Technology

The Formation Design of Noise Reducers from Plywood, Foam, Tray, dan Coconut Fiber for Static Sources. Research was conducted in a semi-anechoic room using a method referring to the ISO 3745. The design used is the Hemisphere in which the source of noise is analogous to engines in an industry. The value reduction in the rate of sound power is obtained by comparing the sound power level before and after control is given. The noise control test materials used consist of layers of plywood, foam, fiber and tray (egg box). The effectiveness of these materials is tested by measuring the …

Production Of Lovastatin And Sulochrin By Aspergillus Terreus Using Solid State Fermentation, Rizna Triana Dewi, Nina Artanti, Hani Mulyani, Puspa Dewi Narrij Lotulung, Minarti Minarti

Makara Journal of Technology

Lovastatin is an anti-cholesterol agent that was produced by Aspergillus terreus using solid state fermentation (SSF). During this fermentation process, sulochrin is also produced as an unwanted co-metabolite. However, our previous result showed that sulochrin had potential as antidiabetes because it is an inhibitor agent of α-glucosidase. In this paper, we reported our observation on lovastatin and sulochrin production pattern in relation with inhibitor α-glucosidase activity during eleven days fermentation of A. terreus koji (SSF) ethyl acetate extract. Koji obtained from solid state fermentation with rice as the substrate and incubated at room temperature, sample is taken daily for eleven …

The Zonation Of Abration Speed Characteristics And Its Handling Technique Of Jalinbar Of North Bengkulu As Vital Band Transportation, Suwarsono Suwarsono, Supiyati Supiyati, Suwardi Suwardi

Makara Journal of Technology

The Zonation of Abration Speed Characteristics and its Handling Technique of Jalinbar of North Bengkulu as Vital Band Transportation. Jalinbar Bengkulu is a vital infrastructure for traffic service, goods, agriculture products, mining, plantation and oils distribution. Abration due to scour of seawater often make these roads jammed and discrupts the peoples economy movement. The aims of this research was to investigate the abration speed of all segment of Jalinbar. The research method was a combination of two methods: A determination of swash energy of sea water using photometer and determination of rocks binding energy using douche method. The result shows …

Determining The Standard Value Of The Oily Distortion Of Acquisition The Fingerprint Images, Rahmat Syam, Mochamad Hariadi, Mauridhi Hery Purnomo

Makara Journal of Technology

Determining the Standard Value of the Oily Distortion of Acquisition the Fingerprint Images. This research describes a novel procedure for determining the standard value of the oily distortion of acquisition the fingerprint images based on the score of clarity and ridge-valley thickness ratio. The fingerprint image is quantized into blocks size 32 x 32 pixels. Inside each block, an orientation line, which perpendicular to the ridge direction, is computed. The center of the block along the ridge direction, a two-dimension (2-D) vector V1 (slanted square) with the pixel size 32 x 13 pixels can be extracted and transformed to a …

Ergonomic Analysis Of Garment Industry Using Posture Evaluation Index (Pei) In Virtual Environment, Erlinda Muslim, Boy Nurtjahyo, Romadhani Ardi

Makara Journal of Technology

Ergonomic Analysis of Garment Industry using Posture Evaluation Index (PEI) in Virtual Environment. This research tried to study, in a virtual environment, the ergonomics of four divisions in garment industry: cutting division, sewing division, button division, and finishing division. Variables that influence the working conditions in each division are different; depend on the real situations that happened. The purpose is to assess the real working conditions based on ergonomics study using Posture Evaluation Index (PEI). PEI integrates the scores of low back analysis (LBA), ovako working posture (OWAS), and rapid upper limb assessment (RULA). Analysis phase was done using digital …

The Solvent Effectiveness On Extraction Process Of Seaweed Pigment, Warkoyo Warkoyo, Elfi Anis Saati

Makara Journal of Technology

Eucheuma cottonii seaweed is a species of seaweed cultured in Indonesian waters, because its cultivation is relatively easy and inexpensive. It has a wide variety of colors from green to yellow green, gray, red and brown, indicating photosynthetic pigments, such as chlorophyll and carotenoids. An important factor in the effectiveness of pigment extraction is the choice of solvent. The correct type of solvent in the extraction method of specific natural materials is important so that a pigment with optimum quality that is also benefical to the society can be produced. The target of this research is to obtain a high …