Metallurgy Commons^™

Revealing Prior Austenite Grain Boundaries Of 4340 Steel, Ryan Brierly Barrows

Materials Engineering

Grain growth during austenitization has a negative effect on fatigue strength. Several methods have been investigated in order to determine an accurate method of measuring the austenite grain size of 4340 steel. The McQuaid-Ehn method, an industry standard for evaluating austenite grain size, has been recognized to produce inaccurate results due to the coarsening of grains during extended austenitizing. A method utilized for hypoeutectoid steels, outlined by the ASTM-E112 standard, is investigated to potentially obtain more accurate results by reducing the duration of austenitizing. Studies regarding effective etching procedures for revealing austenite grains without austenitizing are also addressed. Samples are …

Structural, Magnetic And Microstructural Studies Of Composition-Modified Sm–Co Ribbons, Xiujuan Jiang

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

There is an increasing interest in developing desirable microstructures in hard magnetic materials. Sm-Co-based magnets, bearing superior intrinsic magnetic properties, are good candidates for further development. Two Sm-Co-based alloys, (Sm₁₂Co₈₈)_100-x-yCr_yC_x (taking SmCo₇ phase) and SmCo_4-xFe_xB (a derivative of SmCo₅ phase), were produced using melt-spinning technique. The magnetic properties are correlated to the structural and microstructural properties.

Within the SmCo₇ stoichiometry, cumulative effects of Cr and C additions on the structural and magnetic properties have been investigated. Experimental results have shown that these additions along …

3d Printing Of Stainless Steel For Engineering Applications, Michael Doyle

Undergraduate Research Symposium

3-D metal printing has the potential to solve problems in the medical, prototyping, automotive, aerospace, defense, and other engineering industries. To reach the potential of any manufacturing process, the final product’s material characteristics and how the process affects those characteristics must be understood to meet the demands of industrial applications. There is a gap in standard testing information regarding metal based 3-D metal printing processes. The purpose of this research is to fill that gap of valuable information for this manufacturing process, so that its principles can be used to design better products. Fundamental tensile and compression tests were executed …

Dynamic Characteristic Identification Of Seismic-Excited Multi-Story Buildings Through Response-Only Technique, Agung Budipriyanto, Priyo Suprobo

Makara Journal of Technology

Identifying dynamic characteristics of civil engineering structures is still a challenging task. It intends to assess behavior of the structures under time-dependent loads. This paper discusses a methodology suitable for identifying the characteristics of multi-story buildings using only their measured response under earthquake ground excitations. Appropriateness of technique used for structural identification was corroborated through coherence of the structure’s responses. The methodology was applied for identifying the characteristics of 14-story and 20-story office buildings located in a high seismic region. Responses of these two buildings recorded during three different seismic ground motions were investigated. The buildings’ response spectral densities and …

Synthesis And Characterization Of Soy-Based Polyurethane Foam With Utilization Of Ethylene Glycol In Polyol, Flora Elvistia Firdaus

Makara Journal of Technology

The use of vegetable oils on replacing petroleum has attracted attention of many researchers. The chemical structure of vegetable oils are different from petrochemicals, so the structure of soybean oil has to be chemically modified through its unsaturated fatty acid chain in triglyceride. A two step process was conducted for the preparation of soy-polyol in designated temperatures; 50 °C, 60 °C, and 70 °C. Ethylene glycol (EG) as co-reagent was taking part in soy-polyol synthesis, and the soy-polyol was used as a sole polyol for polyurethane synthesis. Referred to the previous study, the existence of EG in polyurethane synthesis can …

Performances Of Free-Space Optical Communication System Over Strong Turbulence, Ucuk Darusalam, Purnomo Sidi Priambodo, Harry Sudibyo, Eko Tjipto Rahardjo

Makara Journal of Technology

We report an experimental of free-space optical communication (FSOC) system that use tube propagation simulator (TPS) as the turbulence medium. The FSOC system use wavelength of 1550 nm at the rate transmission of 1000 Mbps and amplified with EDFA at the output of +23 dBm. Index structure of 10-15–10-13 as the representation of atmosphere index turbulences are used for simulation of intensity distribution model or scintillation. The simulation use gammagamma and K model as well. The beam wave propagation models used in simulation are plane wave, spherical wave and Gaussian wave. Spherical wave achieves highest performance via gamma-gamma in strong …

Preparations Of Nanostructured Silicide Bundles And Oxide Arrays, Hirokazu Tatsuoka, Wen Li, Erchao Meng, Daisuke Ishikwa, Kaito Nakane, Shingo Oda, Tomoji Matsushita, Natsuki Kurebayashi

Makara Journal of Technology

A variety of nanostructured silicide bundles and oxide nanowire arrays with abundant, non-toxic materials we are prepared. The CrSi2 nanowire and Mg2Si/MgO composite nanowire bundles were synthesized using a Si substrate and a SiOx nanofiber bundle, respectively. The hexagonal MoSi2 nanosheet bundles were also synthesized using a MoS2 layered material as a template. In addition, ZnO, CuO/Cu2O and a-Fe2O3 nanowire arrays were prepared on semiconductor or metallic substrates. The growth phenomena and the structural properties of the nanostructured materials awere investigated. In addition, the preparations of axial and radial nanowire structures weare examined.

Bioethanol Production From Iles-Iles And Sorghum Starch As Raw Materials (Effect Of Cacl 2 Addition And Saccharification Time), Kusmiyati Kusmiyati, Ali Mahmudi

Makara Journal of Technology

Bioethanol produced from agricultural sources is one alternative energy that has been developed to substitute for petroleum. However, the use of food sources such as corn and cassava to produce bioethanol still face obstacles that lead to the scarcity of food and an increase in food prices. The aim of this study was to produce bioethanol from sorghum and iles-iles, which are not used by humans as food, especially in Indonesia. For both materials, the variables studied were saccharification time (4, 8, 24, and 48 h) and concentration of CaCl2 added to the liquefaction slurry (0, 100, 200, 300, and …

The Effect Of Zephyr Layer Orientation On Zephyrboard Made From Oil Palm Petiole, Lusita Wardani, Muhamad Yusram Massijaya, Yusuf Sudo Hadi, I Wayan Darmawan

Makara Journal of Technology

It is very important to utilize oil palm petiole for the production of zephyr boards. This study aimed to analyze the effect of layer orientation on zephyr board quality. Zephyr boards were made with three coating patterns (A = cross perpendicular, B= combine A and C, and C= paralell) and five zephyr layers using urea formaldehyde adhesive. They were pressed for 20 min at a pressure of 25 kgf/cm² and a temperature 120 ºC, to a target density of 0.80 g/cm³ and a size of 300 mm X 300 mm X 12 mm. Our results showed that the physical and …

Performance Evaluation Of An Optimized Floating Breakwater In Oblique Waves With A Higher-Order Boundary Element Method, Faisal Mahmuddin, Masashi Kashiwagi

Makara Journal of Technology

In the previous study, the optimal performance of a two-dimensional (2D) floating breakwater shape was obtained. The performance of this shape was also confirmed with a model experiment in a towing tank. Moreover, the shape’s performance in three dimensions (3D) was investigated in a subsequent study. However, to predict the shape’s performance in a real application more accurately, the shape’s characteristics in oblique waves must also be evaluated. In this study, the performance and characteristics of the model (hydrodynamic forces, body motions, wave elevations, and drift forces) are computed using a higher-order boundary element method (HOBEM). The HOBEM, which is …

Microstructure And Magnetic Properties Of Bulk Nanocrystalline Mnal, Anurag Chaturvedi, Rumana Yaqub, Ian Baker

Dartmouth Scholarship

MnAl is a promising rare-earth free permanent magnet for technological use. We have examined the effects of consolidation by back-pressure, assisted equal channel angular extrusion processing on mechanically-milled, gas-atomized Mn-46% at. Al powder. X-ray diffraction showed both that the extruded rod consisted mostly of metastable τ phase, with some of the equilibrium γ₂ and β phases, and that it largely retained the as-milled nanostructure. Magnetic measurements show a coercivity of ≤4.4 kOe and a magnetization at 10 kOe of ≤40 emu/g. In addition, extrusions exhibit greater than 95% of the theoretical density. This study opens a new window in …

Shape Memory Behavior Of Single And Polycrystalline Nickel Rich Nickel Titanium Alloys, Irfan Kaya

Theses and Dissertations--Mechanical and Aerospace Engineering

NiTi is the most commonly used shape memory alloy (SMA) and has been widely used for bio-medical, electrical and mechanical applications. Nickel rich NiTi shape memory alloys are coming into prominence due to their distinct superelasticity and shape memory properties as compared to near equi-atomic NiTi shape memory alloys. Besides, their lower density and higher work output than steels makes these alloys an excellent candidate for aerospace and automotive industry. Shape memory properties and phase transformation behavior of high Ni-rich Ni₅₄Ti₄₆ (at.%) polycrystals and Ni-rich Ni₅₁Ti₄₉ (at.%) single-crystals are determined. Their properties are sensitive …

Precipitation, Orientation And Composition Effects On The Shape Memory Properties Of High Strength Nitihfpd Alloys, Emre Acar

Theses and Dissertations--Mechanical and Aerospace Engineering

NiTiHf high temperature shape memory alloys are attractive due to their high operating temperatures (>100 ^oC) and acceptable transformation strain compared to NiTi. However, NiTiHf has limitations due to their lack of ductility and low strength, resulting in poor shape memory properties. In this study, Pd has been added to NiTiHf alloys in an attempt to improve their shape memory behavior. A combined approach of quaternary alloying and precipitation strengthening was used.

The characterization of a Ni_45.3Ti_29.7Hf₂₀Pd₅ (at. %) polycrystalline alloy was performed in compression after selected aging treatments. Transmission electron …

Thermodynamics And Crystallography Of The Γ→Ε→Α' Transformation In Femnalsic Steels, Scott Thomas Pisarik

Masters Theses

"FeMnAlSiC steels which exhibit two-stage transformation induced plasticity (TRIP) behavior characterized by the γ→ε→α' dual stage martensitic transformation promise to take a leading role in the development of 3rd generation advanced high strength steels. The crystallographic orientation relationship of the γ→α' and γ→ε athermal martensitic transformations in these steels has been determined as the Kurdjumov-Sachs and the Shoji-Nishiyama, respectively. Six crystallographic variants of α-martensite consisting of three twin-related variant pairs were observed in ε- bands. A planar parallelism of {0001}ε || {110}α' and a directional relation of α' lying within 1⁰ of ε existed for these variants. Two regular solution …

Crystallographic Orientation Of The Ε → Α' Martensitic (Athermal) Transformation In A Femnalsi Steel, S. T. Pisarik, D. C. Van Aken

Materials Science and Engineering Faculty Research & Creative Works

The presence of a thermal ε- and α-martensite (α') in the as-cast structure of a Fe-_0.08C-_1.95Si-_15.1Mn-_1.4Al-_0.017N alloy has been revealed by electron backscattered diffraction analysis. The alloy exhibited two a thermal martensitic transformation described by γ → α' and γ → ε → α'. The Shoji-Nishiyama orientation relationship was observed between γ-austenite and ε-martensite, while α-martensite nucleated from γ-austenite exhibited a Kurdjumov-Sachs orientation relationship. Six crystallographic variants of α-martensite consisting of three twin-related variant pairs were observed in ε-bands. A planar parallelism of {0001}ε || {110}α' and a directional relation …

A Preliminary Study Of Deformation Behavior Of Friction Stir Welded Ti-6al-4v, Jiye Wang, Jianqing Su, Rajiv S. Mishra, Ray Xu, John A. Baumann

Materials Science and Engineering Faculty Research & Creative Works

A preliminary study of deformation behavior of friction stir welded (FSW) Ti-6Al-4V was performed using two different tools with cylindrical and stepped spiral pin design for the welding process. The nugget regions experienced temperature above β transus and the matrix transformed to fine acicular α during cooling of the nugget. By using stepped spiral pin design, a local region with much refined grain structure and significant tool debris particles were observed. Room temperature tensile test showed increased strength and decreased ductility in the material from this region. Fractographic analysis revealed that tool debris particles served as void nucleation sites. Tensile …

An Evaluation Of Creep Behaviour In Friction Stir Welded Ma754 Alloy, Jiye Wang, Wei Yuan, Rajiv S. Mishra, Indrajit Charit

Materials Science and Engineering Faculty Research & Creative Works

Effect of friction stir welding (FSW) on microstructure and creep properties of oxide dispersion strengthened (ODS) alloy MA754 were investigated. Fine-grained microstructure developed in the weld zone. TEM results showed some degree of particle agglomeration as a result of intense material flow. Creep tests of the FSW material were carried out at 973 and 1073 K. Power law creep behavior was observed with stress exponent values of 6.9 and 6.3 at 973 and 1073 K, respectively. The results were compared to those of the as-received material. Creep resistance of FSW material was lower than that of as-received material associated with …

Practical Aspects Of Modern And Future Permanent Magnets, R.W. Mccallum, L. H. Lewis, Ralph Skomski, M. J. Kramer, I. E. Anderson

Ralph Skomski Publications

The mandate to reduce greenhouse gases will require highly efficient electric machines for both power generation and traction motor applications. Although permanent magnet electric machines utilizing Nd2Fe14B-based magnets provide obvious power-to-weight advantages over induction machines, the limited availability and high price of the rare earth (RE) metals make these machines less favorable. Of particular concern is the cost and supply criticality of Dy, a key RE element that is required to improve the high-temperature performance of Nd-based magnetic alloys for use in generators and traction motors. Alternatives to RE-based alloys do exist, but they currently lack the energy density necessary …

Magnesium-Titanium Alloys For Biomedical Applications, Ilona Hoffmann

Theses and Dissertations--Chemical and Materials Engineering

Magnesium has been identified as a promising biodegradable implant material because it does not cause systemic toxicity and can reduce stress shielding. However, it corrodes too quickly in the body. Titanium, which is already used ubiquitously for implants, was chosen as the alloying element because of its proven biocompatibility and corrosion resistance in physiological environments. Thus, alloying magnesium with titanium is expected to improve the corrosion resistance of magnesium.

Mg-Ti alloys with a titanium content ranging from 5 to 35 at.-% were successfully synthesized by mechanical alloying. Spark plasma sintering was identified as a processing route to consolidate the alloy …

Microgrid Development Using A Grid Tie Inverter, Hartono Budi Santoso, Budiyanto Budiyanto

Makara Journal of Technology

The use of renewable energy sources (RES), especially photovoltaic (PV), to meet the demand of electrical energy has been getting a great deal of attention as an alternative solution to electrical energy deficit problems. RES are being applied in power systems in a variety of configurations including microgrid systems. One of the characteristics of a microgrid is capability to supplying power to grid when there is an excess power to supply local load. This research examines the chances of saving power consumption from grid using power converters grid tie inverter (GTI) in a microgrid configuration. The test is done by …