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Selective Laser Sintering; A Design Of Experiments, Philip David Hopkins, Victor Castillo PhD 2012 California Polytechnic State University - San Luis Obispo

Selective Laser Sintering; A Design Of Experiments, Philip David Hopkins, Victor Castillo Phd

STAR Program Research Presentations

Additive Manufacturing (AM), also commonly known as 3D Printing or Rapid Prototyping, is a method of manufacturing that provides for the ability to make intricate internal features and easily customizable parts. The concept is to break a Computer Aided Design (CAD) file into a series of thin layers that are sent to the machine and laid down one layer at a time. Just like any other form of processing, material properties can alter by undergoing this process. Manipulating various parameters of the AM process can allow for different properties to be achieved. For this reason, an in depth study will …


Development And Use Of A Simple Test Method To Evaluate Reheat Cracking Sensitivity In The Weld Deposit Region Of A Submerged Arc Weld, Maxwell Calder Trent 2012 University of Tennessee, Knoxville

Development And Use Of A Simple Test Method To Evaluate Reheat Cracking Sensitivity In The Weld Deposit Region Of A Submerged Arc Weld, Maxwell Calder Trent

Masters Theses

Several fabricators have recently noted the occurrence of reheat cracking in the weld deposits of 2¼[ two and one fourth]Cr‑1Mo‑¼[one fourth]V (22V) during the fabrication of pressure vessels used in the petrochemical industry. Due to increased oversight now required during fabrication of already expensive pressure vessels, studies have commenced worldwide in an effort to identify root causes and formulate mitigating actions to weld reheat cracking issues. The Materials Joining Group (MJG) at the University of Tennessee at Knoxville (UTK) have adapted an existing reheat cracking test originally developed for use with alloys similar to 22V. This original C‑Ring test was …


Dynamical Properties Of Ferroelectric Perovskites (Ba,Sr)Tio3 And Pb(Zr,Ti)O3 Systems From First Principles, Jeevaka Weerasinghe 2012 University of Arkansas, Fayetteville

Dynamical Properties Of Ferroelectric Perovskites (Ba,Sr)Tio3 And Pb(Zr,Ti)O3 Systems From First Principles, Jeevaka Weerasinghe

Graduate Theses and Dissertations

A first-principles-based effective Hamiltonian scheme which incorporates coupling between ferroelectric (FE) and antiferrodistortive (AFD) motions is applied to Pb(Zr,Ti)O3 alloys. It validates the existence of two modes of E symmetry (rather than the single E(1TO) soft mode) in the 50-75 cm-1 range for temperatures smaller than 200 K and for compositions falling within the Rhombohedral R3c phase. Coupling between long-range-ordered FE and AFD motions is shown to be the cause of the additional mode and more insight into its nature is provided. This scheme is further used to reveal a field-induced anticrossing involving FE and AFD degrees of …


Magnetic Properties Study Of The Mn-Al System With Additions Of B Or C And Mechanical Milling Techniques, Timothy E. Prost 2012 University of Nebraska-Lincoln

Magnetic Properties Study Of The Mn-Al System With Additions Of B Or C And Mechanical Milling Techniques, Timothy E. Prost

Department of Engineering Mechanics: Dissertations, Theses, and Student Research

Recently a shift in the focus of permanent magnetic research has moved from Rare Earth (RE)-based alloys to those made from more readily available elements. Because of their relatively large magnetocrystalline anisotropy, L10 compounds have the potential for use as permanent magnet materials. One particular alloy that is readily available and inexpensive is near equi-atomic manganese and aluminum (Mn50-Al50). First characterized in 1958, it did not receive much attention until more recently when RE supply chain issues made the alloy more attractive for commercial and research applications. The ferromagnetic (FM) τ-phase (L10) is …


Characteristic Study On Ni50mn45sn5 By Dsc & X-Ray Analysis, Ajit Behera 2012 Indian Institute of Technology - Kharagpur

Characteristic Study On Ni50mn45sn5 By Dsc & X-Ray Analysis, Ajit Behera

Ajit Behera

The Martensitic Transformation in Ferromagnetic shape memory alloys (FSMAs) can be triggered not only by changes in temperature and stress as that of paramagnetic conventional shape memory alloys, but also by changes in the applied magnetic field. It is well known that ferromagnetic shape memory alloy has diversified utilization, but not satisfactorily use, mainly because of high cost of processing and high cost of alloying elements. Among all Heusler alloy, Ni-Mn-Sn alloy have potential properties and exhibits lower cost. In this experiment Ni50Mn45Sn5 alloys characterize by using differential scanning calorimetric (DSC), optical microscope and X-Ray diffraction technique. The alloy undergoes …


Characterization And Analysis Of Low Room Temperature Ductility Nickel-Based Superalloy 718 Plus For Aircraft Engine Forgings, Jonathon Bracci 2012 California Polytechnic State University - San Luis Obispo

Characterization And Analysis Of Low Room Temperature Ductility Nickel-Based Superalloy 718 Plus For Aircraft Engine Forgings, Jonathon Bracci

Materials Engineering

Schlosser Forge Co. forges low pressure turbine (LPT) cases from the nickel based superalloy 718 Plus using the ring rolling forging process. Schlosser has been experiencing low room temperature ductility problems in a number of their 718 Plus LPT cases. LPT cases are required to pass a 4D tensile test at room temperature with a minimum of 15 percent elongation. The ductility problem was reduced by increasing the forging temperature from 1825˚F to 1850˚F. Analysis was performed on 718 Plus samples taken from forged LPT cases that failed the room temperature ductility requirement and ones that passed the requirement. The …


Effects Of Beta Stabilizers On Quench Delay Susceptibility Of Ti-6al-4v, Kyle Logan 2012 California Polytechnic State University - San Luis Obispo

Effects Of Beta Stabilizers On Quench Delay Susceptibility Of Ti-6al-4v, Kyle Logan

Materials Engineering

Tensile samples of Titanium 6Al-4V (Ti-6Al-4V) were machined from forgings containing rich and poor amounts of beta stabilizers in their compositions. The tensile samples were each heat treated two times. In the first round of heat treatments, the samples were either beta solution treated (BST), or solution treated (ST). Each sample was water quenched with varying quench delays of 10, 20, and 30 seconds. BST treated specimens were then overaged at 1350°F for 2 hours and air cooled (BSTOA); while the ST treated samples were aged at 990°F for 6 hours and air cooled (STA). Following heat treating, the tensile …


Discontinuous Grain Boundaries Of Forged René 41, Steven Crump 2012 California Polytechnic State University - San Luis Obispo

Discontinuous Grain Boundaries Of Forged René 41, Steven Crump

Materials Engineering

Forged components must pass a grain size specification (grain size, distribution) for acceptance in an application. The varying amounts of plastic deformation during forging can lead to abnormally large recrystallized grain sizes in certain regions of the part, which will not pass specification. The question exists whether these abnormally coarse grains are truly comprised of poly crystalline fine grains with grain boundaries resistant to etching techniques. To investigate this abnormal grain size effect, a cross section of a forged René 41 nickel-based superalloy aircraft engine ring was cut and sectioned into six segments. Those segments were then prepared for microstructural …


Effect Of Heating Temperature, Heating Time And Initial Microstructure On Recrystallization Of Waspaloy During Heating For Forging, Marissa Hill 2012 California Polytechnic State University - San Luis Obispo

Effect Of Heating Temperature, Heating Time And Initial Microstructure On Recrystallization Of Waspaloy During Heating For Forging, Marissa Hill

Materials Engineering

A fine, uniform grain size is required for creep limited Waspaloy in aircraft engine applications. Upon heating, Waspaloy does not always recrystallize in a uniform manner resulting in occasional large grains with a majority of the grains meeting the grain size requirements. Waspaloy’s microstructure was analyzed with different heat treatments and in the as-forged condition. The strengthening mechanism is the gamma prime phase. The gamma prime solvus temperature is 1908°F so the different heat treatments were determined around that temperature, as well as the forging temperature range of 1800-2150°F. At the 1850°F heat treatment, the microstructure recrystallized with small grains, …


Morphology And Roughness Of Al2o3 On Ferritic Stainless Steel Foil For Diesel Catalytic Converter Applications, Megan Butala 2012 California Polytechnic State University - San Luis Obispo

Morphology And Roughness Of Al2o3 On Ferritic Stainless Steel Foil For Diesel Catalytic Converter Applications, Megan Butala

Materials Engineering

The improved thermal properties of metal-substrate catalytic converters enable effective catalysis sooner after ignition than traditional ceramic monoliths, resulting in less harmful emissions. ACAT Global, a manufacturer of stainless steel catalytic converters, uses ferritic stainless steel substrates for low temperature catalytic converters for diesel automobiles. Production begins with an oxidizing heat treatment to increase surface roughness. The success of the second production step, the application of catalyst-containing ceramic slurry (washcoat), depends on the surface roughness that results from oxidation. Formation of the primary oxide of interest, alumina (Al2O3), is controlled by the stainless steel foil composition, …


Microstructural Characterization Of Ti-6al-4v And Its Relationship To Sample Geometry, Blake Gaspar 2012 California Polytechnic State University - San Luis Obispo

Microstructural Characterization Of Ti-6al-4v And Its Relationship To Sample Geometry, Blake Gaspar

Materials Engineering

A problem exists with a part produced by forging made by Shultz Steel of Ti-6Al-4V in the variance of properties throughout the part. There is one specific region that exhibits the most variance. The purpose of the report is to determine any microstructural differences within the region of interest in the part. When microstructures of the inner section and outer section of the part were looked at it was determined that they exhibited a martensitic structure. There was a noticeable difference in the lath structure between sections. The outer region contained larger more widely spread laths of an average length …


Effects Of Annealing/Solution Treating And Aging On Longitudinal And Transverse Properties Of Ti-6al-4v Forgings, Blake Reller 2012 California Polytechnic State University - San Luis Obispo

Effects Of Annealing/Solution Treating And Aging On Longitudinal And Transverse Properties Of Ti-6al-4v Forgings, Blake Reller

Materials Engineering

Forty-eight subsize round-bar tensile samples (ASTM E8) were machined from 3-in-thick forgings of Ti-6Al-4V. Half of these samples were cut so the axis aligned with the longitudinal (LG) direction of the forging, the other half were cut to align with the transverse (LT) direction. Four samples from each direction were subjected to one of six heat treatments so that a total of eight samples received each treatment. Annealed samples were held at 1350°F for two hours, then air cooled. Solution treated and aged (STA) samples were solution treated at one of five temperatures between 1785°F and 1435°F for one hour …


Analyzing The Corrosion Resistance Of Ni-Shield 200 Coatings At Different Temperatures When Exposed To Sulphuric Acid, Alex Hussinger 2012 California Polytechnic State University - San Luis Obispo

Analyzing The Corrosion Resistance Of Ni-Shield 200 Coatings At Different Temperatures When Exposed To Sulphuric Acid, Alex Hussinger

Materials Engineering

Six steel samples each were twin wire arc sprayed with Hastelloy C-276 or Nickel-Shield 200 coatings approximately 0.020″ thick. These samples were then cut into 3″ by 3″ squares. A 2″ diamond grit hole saw was used to abrade and polish to a smooth surface a ring in the middle in order to get an O-ring mechanical seal. The samples were then weighed and loaded into a jig that started from the bottom up with a stainless steel plate, then the sample, then a Viton O-ring, a ¾″ thick glass plate with a 1 3/4″ hole cut in it, another …


Characterization Of Positive Macrosegregation At The Subsurface Of Direct-Chill Cast 7050 Aluminum Forging Billets, Aaron Youril 2012 California Polytechnic State University - San Luis Obispo

Characterization Of Positive Macrosegregation At The Subsurface Of Direct-Chill Cast 7050 Aluminum Forging Billets, Aaron Youril

Materials Engineering

Segregation of alloying elements during casting of forging billets may persist to the final forged component leading to unacceptable surface appearance. Determination of the elements or compounds that segregate is the essential first step to solving this problem. Differential Scanning Calorimetry (DSC) was used to determine a composition profile of the macrosegregation occurring at the subsurface of an as-cast 7050 aluminum alloy billet. Data collection was carried out by separating 10 to 20 mg samples from the outer centimeter along the radius of the billet, as well as samples from the bulk interior of the billet for comparison with the …


Effect Of Oxidation On Weld Strengthof Dissimilar Resistance Weld Interface Between 304 Stainless Steeland Near Equiatomic Austenitic Nitinol Guide Wire, Matthew Rudow 2012 California Polytechnic State University, San Luis Obispo

Effect Of Oxidation On Weld Strengthof Dissimilar Resistance Weld Interface Between 304 Stainless Steeland Near Equiatomic Austenitic Nitinol Guide Wire, Matthew Rudow

Master's Theses

Abbott Vascular encountered strength and variability issues when attempting to resistively weld 304 Stainless Steel to equiatomic Nitinol. Initial observations suggested that passivation layer (Cr2O3, TiO2) formation affected the weld interface. One hundred 304 Stainless Steel/Nitinol pairs were allowed to oxidize in air at room temperature for allowed periods of time (.1, 1, 3, 5, 7, 12, 16, 24, 168, and 336 hours). Each pair was welded resistively with constant current. A Miyachi/Unitek Advanced Data Analysis Monitor (ADAM) recorded the peak resistance at the instance the weld was made. Resistances were compared to Instron …


Metallurgical Effects On Long-Term Creep-Rupture In A New Nickel-Based Alloy, John P Shingledecker 2012 University of Tennessee, Knoxville

Metallurgical Effects On Long-Term Creep-Rupture In A New Nickel-Based Alloy, John P Shingledecker

Doctoral Dissertations

A series of creep-rupture studies were conducted on a new nickel-based alloy, Inconel Alloy 740, for use in Advanced Ultrasupercritical (A-USC) Steam boiler applications. The research quantitatively showed, for the first time, that the formation of a small amount of eta phase during long-term creep testing at 750 degrees Celsius does not degrade the rupture strength or ductility of the alloy. A unique full-scale pressurized tubular creep test was conducted, and a new analysis methodology was developed to evaluate the effect of cold-straining on the creep performance of tube bends made from the alloy. The results showed that 15% cold-work …


Solar Cell Design Using Metamaterials, Yang Liu, Yitung Chen, Jichun Li 2012 University of Nevada, Las Vegas

Solar Cell Design Using Metamaterials, Yang Liu, Yitung Chen, Jichun Li

College of Engineering: Graduate Celebration Programs

Natural structure with simultaneous negative permittivity and permeability has not been discovered yet. However, using specially-designed metal embedded in dielectric bodies can achieve a kind of artificial negative index. This periodic structure which is smaller than the guided wavelength is known as a metamaterial. However, recent designs of metamaterials have some disadvantages when they are used in the application of solar cell. The perfect absorption is only within a narrow band, and for most of the solar spectrum, the absorption is no more than 10%. Here, a new kind of absorber for the solar spectrum has been designed and analyzed, …


Cellular Automaton For Simulation Of Oxide Layer Growth Influenced By Chromium Concentration Of Structure Material, Kuan-Che Lan, Yitung Chen, Ge-Ping Yu, Tzu-Chen Hung 2012 University of Nevada, Las Vegas

Cellular Automaton For Simulation Of Oxide Layer Growth Influenced By Chromium Concentration Of Structure Material, Kuan-Che Lan, Yitung Chen, Ge-Ping Yu, Tzu-Chen Hung

College of Engineering: Graduate Celebration Programs

Chromium, an important alloying element, has been added in ferrous and nickel based alloy such as stainless steels and Inconel alloy to improve the corrosion resistance. High corrosion resistance of structural materials in extremely high working temperature is one crucial R&D objective of Gen IV nuclear power plants which propose to raise the thermal efficiency via high working temperature. A cellular automaton (CA) model based on the stochastic approach was proposed to simulate the process of oxidation and corrosion of structural material in flowing fluid. The relation of chromium concentration against oxide layer thickness during a specific period was found. …


Investigation Of The Use Of Micro-Mechanical Testing To Analyze The Mechanical Anisotropy Of The Zr-2.5%Nb Pressure Tube Alloy, Richard O. Oviasuyi 2012 The University of Western Ontario

Investigation Of The Use Of Micro-Mechanical Testing To Analyze The Mechanical Anisotropy Of The Zr-2.5%Nb Pressure Tube Alloy, Richard O. Oviasuyi

Electronic Thesis and Dissertation Repository

Maintaining a safe operation of nuclear power plants is the primary requirement of nuclear power generating organizations worldwide. This necessitates the use of highly effective methods for assessing the mechanical properties of reactor materials and components. This is important since all components located in a nuclear reactor core experience high levels of neutron irradiation which cause defects to be formed in the metals’ crystal structure. The density of these crystal defects increases with increasing exposure to neutrons and cause the crystalline metal to become harder and simultaneously more brittle. This change in mechanical properties is potentially detrimental to the safe …


Modification Of Flow Structure Over A Van Model By Suction Flow Control To Reduce Aerodynamics Drag, Harinaldi Harinaldi, Budiarso Budiarso, Warjito Warjito, Engkos Achmad Kosasih, Rustan Tarakka, Sabar Pangihutan Simanungkalit, I Gusti Made Fredy Lay Teryanto 2012 Department of Mechanical Engineering, Faculty of Engineering, Universitas Indonesia, Depok 16424, Indonesia

Modification Of Flow Structure Over A Van Model By Suction Flow Control To Reduce Aerodynamics Drag, Harinaldi Harinaldi, Budiarso Budiarso, Warjito Warjito, Engkos Achmad Kosasih, Rustan Tarakka, Sabar Pangihutan Simanungkalit, I Gusti Made Fredy Lay Teryanto

Makara Journal of Technology

Automobile aerodynamic studies are typically undertaken to improve safety and increase fuel efficiency as well as to find new innovation in automobile technology to deal with the problem of energy crisis and global warming. Some car companies have the objective to develop control solutions that enable to reduce the aerodynamic drag of vehicle and significant modification progress is still possible by reducing the mass, rolling friction or aerodynamic drag. Some flow control method provides the possibility to modify the flow separation to reduce the development of the swirling structures around the vehicle. In this study, a family van is modeled …


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