Metallurgy Commons^™

Investigating Microalloying Elements To Accelerate Zirconium Trialuminide Precipitation In Aluminum Alloys, Philip D. Staublin

Dissertations, Master's Theses and Master's Reports

Precipitation of the L1₂-structured coherent Al₃Zr trialuminide phase in aluminum-zirconium alloys increases the alloy strength. Precipitation of a more refined dispersion of Al₃Zr can further increase the strength of these alloys. The addition of microalloying elements which bind to zirconium may accelerate the precipitation kinetics, allowing for nucleation of a greater number of precipitates and faster precipitate growth. Zirconium binding energies are computed for a wide range of elements, based on which the elements tin, antimony, and tellurium were selected for investigation. Ternary Al-Zr-X alloys (X = Sn, Sb, Te) were cast and heat …

Conversion Of Heat Energy From Cooling Water Of Diesel Engine To Electrical Energy Using Thermoelectric Generator, Muhammad Hasan Albana

Makara Journal of Technology

This research objective is to convert heat from the radiator fluid of a diesel engine to electrical energy by utilizing a thermoelectric generator (TEG). The TEG consists of 20 semiconductors (TE modules) and is equipped with a heat sink. The research shows that using the TEG, the heat of radiator fluid can be converted to electrical energy, although the electricity generated is small. The maximum electrical voltage generated by the TEG when modules were connected in series was 10 volts. When the TE modules were connected in parallel and series-parallel, the maximum voltages generated were 2.11 and 2.53 volts, respectively. …

Immittance Response On Carboxymethyl Cellulose Blend With Polyvinyl Alcohol- Doped Ammonium Bromide-Based Biopolymer Electrolyte, Norfatihah Mazuki, Yuki Nagao, Ahmad Salihin Samsudin

Makara Journal of Technology

The blended carboxymethyl cellulose (CMC) and polyvinyl alcohol (PVA) doped with various compositions of ammonium bromide (NH4Br)-based solid biopolymer electrolytes (SBEs) were prepared by using the casting method. In this present work, CMC/PVA–NH4Br SBE thin film was used to investigate the electrical conductivity via electrical impedance spectroscopy. The maximum conductivity obtained was 3.21 X 10−4 S cm−1 for sample AB20 at ambient temperature (303 K), and this result might be due to the increased number of charge carrier. A dielectric study was conducted to understand the conductivity behavior. The electrical properties have been measured as a function of frequency of …

Transition Metal Dichalcogenide For High-Performance Electrode Of Supercapacitor, Saifful Kamaluddin Muzakir, Ahmad Salihin Samsudin, Bouchta Sahraoui

Makara Journal of Technology

Molybdenum dichalcogenides have been reviewed from the perspectives of bandgap, conductivity, and oxidation states of transition metal. Researchers have concluded that a narrow-bandgap transition metal dichalcogenide with high conductivity could be achieved for the high-performance electrode of a supercapacitor.

Automated Compilation Test System For Embedded System, Mohamad Khairi Ishak, Ooi Jun Hwan, Teh Jiashen, Nor Ashidi Mat Isa

Makara Journal of Technology

Embedded system testing involves testing an integration of software and hardware. It is increasingly difficult to evaluate the functionality of each module within a short time because of the increasing number of tests required. In this paper, a novel stepwise methodology involving the use of an automated compilation test system (ACTS) is proposed, to improve the quality of testing and optimize the testing time using automation. Using the proposed method, the testing coverage can be maximized, while minimizing the manual work and testing time required. This ACTS was used to automate the test code compilation and execution for different hardware …

Activated Carbon Fixed-Bed Adsorber Design For Treating Chromium Hexavalent Wastewater, Tedi Hudaya, Velicia Rachmat

Makara Journal of Technology

Pollution caused by industrial wastewater containing heavy metals is a major issue, primarily due to its toxic nature. A cheap yet effective method to deal with such wastewater is activated carbon adsorption. The purpose of this research is to evaluate and design a fixed bed adsorber with granular activated carbon as an adsorbent to process wastewater-containing chromium hexavalent (Cr 6+). Experiments show that the Langmuir isotherm fits the equilibrium data as effectively as the Freundlich isotherm. Activated carbon used in this research is Jacobi 2000® derived from bituminous coal. The lab scale inlet volumetric flow is 100 mL/h with different …

A 2.3/3.3-Ghz Dual Band Low Noise Amplifier Using Switchable Load Inductor In 0.18-Um Cmos Technology, Taufiq Alif Kurniawan, Hsiao-Chin Chen

Makara Journal of Technology

In this paper, the dual band low noise amplifier is designed in 0.18-μm CMOS technology. By combining the proposed switchable load inductor for gain controlling and the conventional inductive source degeneration topology, narrow band gain and good impedance matching are achieved at 2.3/3.3-GHz frequency bands. The new mathematical analysis of low noise amplifier design is derived to define the component parameters of the proposed circuits. The proposed low noise amplifier exhibits gain of 17.18 dB and 15.5 dB, and noise figure of 2.67 dB and 2.52 dB at the two frequency bands, respectively.

Ascorbic Acid Degradation In Cut Lemon Packaged Using Oxygen Scavenging Active Film During Storage, Kurniawan Yuniarto, Setyo Purwanto, Bruce Ari Welt, Anang Lastriyanto

Makara Journal of Technology

Oxygen scavenging active film can be used to prevent diffusion of free oxygen due to the action of permeation mechanism. In this study, biodegradable oxygen scavenging plastic film was designed by incorporating an antioxidant agent into plasticized polylactic acid or PLA-PEG (PPLA). Butylated hydroxytoluene (BHT) was added at different concentrations into the matrix of the PPLA film using a direct casting method to produce oxygen scavenging active film. The antiradical activity of the oxygen scavenging active film was observed, which could be applied for preventing vitamin C degradation in cut lemon during storage. The antiradical activity of the active film …

The Importance Of Usability Aspect In M-Commerce Application For Satisfaction And Continuance Intention, Yassierli Yassierli, Vinsensius Vinsensius, M. S. Syed Mohamed

Makara Journal of Technology

There has been a rapid growing of m-commerce application in recent years due to the development of mobile communication technology and e-commerce business. However, only about 30% of online users, who conduct online searching, make online purchases. The low conversion rate seems to be correlated with poor usability aspect of most m-commerce applications and poor satisfaction reported by users. Research has reported that satisfaction and continuance intention in using m-commerce applications have relationships with service quality and information quality. In this study, a new model of user satisfaction and continuance intention in the context of mobile application was proposed by …

Optimization Of The Practice Of Slow Cooling Steel Bars: A Redesign And Modernization Of Materials, Eryn Johnston

Mechanical Engineering Undergraduate Honors Theses

Throughout the process of steel making, certain grades of steel are a higher risk for defects caused by the inability to quickly diffuse hydrogen through the steel when cooled to room temperature at a normal rate based on the ambient air temperature. To reduce the hydrogen flaking defects that are caused due to hydrogen entrapment in the steel, the process of slow cooling is utilized. This process reduces the cooling rate of steel bars by keeping them at a higher temperature for extended periods and in turn gives the hydrogen a chance to fully dissipate from the steel. In many …

Compensation Of Vertical Position Error Using A Force–Deflection Model In Friction Stir Spot Welding, Jinyoung Yoon, Cheolhee Kim, Sehoon Rhee

Mechanical and Materials Engineering Faculty Publications and Presentations

Despite increasing need for friction stir spot welding (FSSW) for high-temperature softening materials, system deflection due to relatively high plunging force remains an obstacle. System deflection results in the vertical position error of a welding tool and insufficient plunge depth. In this study, we used adaptive control to maintain plunge depth, the plunging force was coaxially measured, and the position error was estimated using a force–deflection model. A linear relationship was confirmed between the force and deflection; this relationship is dependent on the stiffness of the welding system while independent of process parameters and base materials. The proposed model was …

Process-Property-Microstructure Relationships In Laser-Powder Bed Fusion Of 420 Stainless Steel., Subrata Deb Nath

Electronic Theses and Dissertations

Laser-powder bed fusion (L-PBF) is an additive manufacturing technique for fabricating metal components with complex design and customized features. However, only a limited number of materials have been widely studied using L-PBF. AISI 420 stainless steel, an alloy with a useful combination of high strength, hardness, and corrosion resistance, is an example of one such material where few L-PBF investigations have emerged to date. In this dissertation, L-PBF experiments were conducted using 420 stainless steel powders to understand the effects of chemical composition, particle size distribution and processing parameters on ensuing physical, mechanical and corrosion properties and microstructure in comparison …

Prediction Of Metal Sample Failure From Scanning Electron Microscope Images Using Deep Learning Neural Network, Lawrence Madriaga, Ivan Novikov, Morteza Nurcheshmeh

Posters-at-the-Capitol

We present the preliminary results on using a deep learning neural network to predict a metal sample failure based on a set of images obtained with a Scanning Electron Microscope.

Various metal alloy samples were prepared according to ASTM E8/E8M-11 standards for a tensile test. Each sample was prepared for circle grid analysis and then stressed on a tensile machine. Stress and strain values were obtained for each position along the sample by measuring dimensions of each elongated circle. Increasing stress and strain values were found closer to the breakage of the sample with low values found at the holding …

Surface Chemistry And Modelling Of Salicyl Hydroxamic Acid Adsorption At The Surface Of Rare Earth Oxides, Carbonates And Phosphates, Marc F. Sime

Graduate Theses & Non-Theses

The adsorption mechanism of salicyl hydroxamic acid (SHA, C7H7O3N) on rare earth minerals was investigated using two complementary methods: precipitation studies and modelling. Precipitation studies showed that SHA adsorption occurs through a displacement of the hydroxide ion at the surface in an ion exchange mechanism, leading to surface precipitation and/or chemisorption. Surface precipitation predominates in the light rare earth oxides (LREOs), while chemisorption predominates in the heavier REOs. Modelling revealed that adsorption of SHA on the REM surface is dependent upon the orientation of SHA on the surface as well as the distance between rare earth elements sites on the …

Comparison Of Salicyl Hydroxamate Adsorption On Rare Earth Phosphates To Oxides And Carbonates, Stephanie Trant

Graduate Theses & Non-Theses

Adsorption behavior of the anionic collector salicyl hydroxamic acid (SHA) on a group of selected rare earth phosphates (REPs) was studied by means of experimental methods and modeling software. These REPs were then compared to rare earth carbonates (RECs) and rare earth oxides (REOs) to develop a trend. A suite of rare earth elements (REE) were studied that included light (LREE) and middle (MREE). Results for heavy (HREE) were inferred. Synthetic phosphate, oxide and carbonate powders of the rare earth elements Lanthanum (La), Cerium (Ce), Europium (Eu) and Dysprosium (Dy) were tested for these studies. Dysprosium phosphate was the only …

A Study Of The Diffusion Characteristics Of Tungsten Bar Stock And Tungsten Produced Via Direct Metal Laser Sintering (Dmls), Jonathan Robert Bruss

Master's Theses (2009 -)

Using a vacuum hot extraction method diffusivity and concentration of hydrogen were measured in samples of tungsten bar stock and direct metal laser sintered (DMLS) tungsten. It was found that the tungsten bar stock closely adhered to the model established by Frauenfelder. The DMLS samples approximately follow a downward sloping trend over the 500K-1200K temperature range. The trend is opposite of what is expected suggesting processing has a major effect on diffusion behavior. A CFD model was created using ANSYS Fluent to simulate the diffusion behavior. The model functions by separating out diffusion mechanisms and solving Fick’s law with each …

Effect Of Wall Thickness And Build Quality On The Compressive Properties Of 304l Thin-Walled Structures Fabricated By Slm, Myranda Spratt, Sudharshan Anandan, Rafid M. Hussein, Joseph William Newkirk, K. Chandrashekhara, Heath Misak, Michael Walker

Materials Science and Engineering Faculty Research & Creative Works

The specific strength of lightweight lattice structures built with SLM is of interest to the aerospace industry. Honeycombs were manufactured with increasing wall thicknesses (which increases density) and tested under compression. The optimal strength to density ratio was determined from the resulting data. The build quality was also evaluated to determine how/if the results were influenced by the specimen quality. Differences between the nominal and as-built geometry were identified, but considered to be minimal. Microstructural evaluation of the specimens revealed a possible dependence on the ‘border scan’ properties, as the thickness of the specimens was such that the board scan …

Fast Prediction Of Thermal History In Large-Scale Parts Fabricated Via A Laser Metal Deposition Process, Lei Yan, Tan Pan, Joseph William Newkirk, Frank W. Liou, Eric E. Thomas, Andrew H. Baker, James B. Castle

Materials Science and Engineering Faculty Research & Creative Works

Laser metal deposition (LMD) has become a popular choice for the fabrication of near-net shape complex parts. Plastic deformation and residual stresses are common phenomena that are generated from the intrinsic large thermal gradients and high cooling rates in the process. Finite element analysis (FEA) is often used to predict the transient thermal cycle and optimize processing parameters; however, the process of predicting the thermal history in the LMD process with the FEA method is usually time-consuming, especially for large-scale parts. Herein, multiple 3D FEA models with simple assumptions on the heat source and its loading methods are compared and …

Development Of An Engineering Diagram For Additively Manufactured Austenitic Stainless Steel Alloys, Zachary T. Hilton, Joseph William Newkirk, Ronald J. O'Malley

Materials Science and Engineering Faculty Research & Creative Works

Austenitic stainless steels are the most widely applied types of stainless steels, due to their good weldability and high corrosion resistance. A number of engineering diagrams exist for the purpose of providing insight into the behavior of these steels. Examples of these diagrams are constitution diagrams (aka Schaeffler Diagrams) which are used to approximate the solidification path of the alloy and the amount of retained ferrite in the solidified matrix. Other diagrams are the Suutala diagram, which approximates cracking susceptibility, and microstructural maps, which predict the solidification path by varying a processing parameter, such as cooling rate. By combining these …

Internet Traffic Forecasting Model Using Self Organizing Map And Support Vector Regression Method, Enrico Laoh, Fakhrul Agustriwan, Chyntia Megawati, Isti Surjandari

Makara Journal of Technology

Internet traffic forecasting is one of important aspect in order to fulfill the customer demand. So, the service quality of internet service provider (ISP) can be maintained at the good level. In this study self-organizing map (SOM) and support vector regression (SVR) algorithm are used as forecasting method. SOM is first used to decompose the whole historical data of traffic internet into clusters, while SVR is used to build a forecasting model in each cluster. This method is used to forecast ISPs traffic internet in Jakarta and surrounding areas. The result of this study shows that SOM-SVR method gives more …