Metallurgy Commons^™

Optimization Of Induction Quenching Processes For Hss Roll Based On Mmpt Model, Ligang Liu, Hui Yu, Zhiqiang Yang, Chunmei Zhao, Tongguang Zhai

Chemical and Materials Engineering Faculty Publications

To improve the comprehensive performance of high speed steel (HSS) cold rolls, the induction hardening processes were analyzed by numerical simulation and experimental research. Firstly, a modified martensitic phase transformation (MMPT) model of the tested steel under stress constraints was established. Then, the MMPT model was fed into DEFORM to simulate the induction quenching processes of working rolls based on an orthogonal test design and the optimal dual frequency of the induction quenching process was obtained. The results indicate that the depth of the roll’s hardened layer increases by 32.5% and the axial residual tensile stress also becomes acceptable under …

Erosion Resistance Of Tungsten-Carbide Coatings For Steel Pipes In Fluid Catalytic Cracking Units, Davis Vannasing, Jennifer Hulfachor

Materials Engineering

In petroleum processing, the flow of catalyst readily leads to erosion of piping in a fluid catalytic cracking unit. Advances in coating materials and processes necessitate a re-evaluation of current protection methods. Commercially available tungsten-carbide (WC) claddings and nanostructured WC-W CVD coatings were investigated as potential alternative erosion-resistant coatings. Erosion tests by solid particle impingement were conducted on 2 variations of claddings and 1 variation of WC-W coatings following ASTM standard G76. A36 steel coupons were used as reference samples. For statistical validation, 2-3 replications of the tests were performed for the claddings and WC-W coating. Testing was conducted using …

Investigation Of Copper Infiltration Alloys For Use In Metal Matrix Composite Drill Bits, Samuel J. Stueland, Timothy P. Markiewicz

Materials Engineering

A newly developed copper-based alloy, P98-X1 was tested for compressive strength to predict qualitative performance compared to MF53, F-Bronze, CuNiSn, and CuMnNi for use as the infiltration alloy in metal matrix composite (MMC) drill bits. Ingots of each alloy were cast using an arc furnace and cut into compression testing samples using wire electrical discharge machining (EDM). The alloys were selected for testing based on solid solution strengthening coefficient and melting point. Five of each alloy were compression tested to determine yield strength of the infiltration alloy. Yield strength was determined using a 0.002mm displacement offset from the linear elastic …

The Impact Of Preheat On 2205 Duplex Stainless Steel Welds, Angelee G. Q. Breuninger, Iris I. Li, Cristian V. Sion

Materials Engineering

The goal of this project is to determine the relationship between preheat temperature and phase balance of austenite and ferrite in the heat affected zone (HAZ) of a dissimilar thickness weld made of Sandvik SAF 2205 duplex stainless steel (DSS). Various preheat temperatures were applied (no preheat, 63°C, 98 °C, 141 °C, 181 °C, and 214 °C) to a 2-inch thick plate that was welded to a 0.072-inch thin sheet, with a 0.125-inch standoff, using manual gas tungsten arc welding (GTAW). Welding variables (voltage, amperage, and travel speed) were recorded and thermocouples were placed along the backside of the weld, …

Microstructural Transformation Of Cold-Sprayed Grcop-42 For Rocket Engine Combustion Chamber Liners, Mason Souther

Materials Engineering

Rocket engines have always relied on high-conductivity copper liners to protect structural components from extreme thermal loads produced by combustion. Forged NARloy-Z has been the material of choice for decades but increasing cost of its constituent silver and high waste in the machining process has reduced the alloy’s cost effectiveness. Aerojet Rocketdyne wants to determine the viability of cold-spray additively manufactured GRCop-42 as a replacement alloy to reduce liner cost. Screening tests were performed to observe the microstructural development and microhardness changes of cold-sprayed GRCop-42 after being subjected to multiple stages of the typical heat treatment of a combustion chamber …

Investment Cast C450 Microstructural Characterization In Golf Club Heads, Kenneth Yin-Fai Lau

Materials Engineering

Two types of tensile bars were observed in this study of golf iron heads for TaylorMade Golf. As-cast and as-cast then machined tensile bars. The tensile bars underwent tensile tests to observe tensile strength, percent elongation, and fracture mechanisms. Furthermore, the hardness of the tensile bars was also taken despite seeing no difference in sample types. However, the as-cast samples did not consistently meet the requirements of percent elongation > 10.00% as there was a sample with 0.00% and another with 1.26%. These samples also showed brittle fracture, instead of the desired cup-and- cone ductile fracture. To investigate further, transverse sections …

Modifying Casting Parameters To Improve The High Temperature Ductility Of Investment Cast Nickel-Based Superalloy Pwa 1455, Lars Alexander Hedin, Cole Magnum Introligator

Materials Engineering

PCC Structurals, an industry leader in superalloy investment castings, has observed inconsistencies in the stress rupture performance of polycrystalline nickel-based superalloy PWA 1455. PCC has changed their casting parameters to reduce the thermal gradient during cooling but have been unable to correlate these changes with an increase in stress rupture elongation. Metallographic examination of past samples indicated microstructures composed of non- equiaxed dendritic grains with mean diameter of .021 inches along the test axis. A similar study on polycrystalline superalloys has indicated that excessive superheat temperatures above the liquidus can result in large grains identical to those observed, limiting the …

Effect Of Overaging On Tensile Properties Of 2219-T852 Aluminum, Austin Bitter, Tristan Koyamatsu

Materials Engineering

This project investigated the overaging performance of aluminum alloy 2219-T852 for use in high temperature applications. 2219 aluminum is an alloy containing 5.8 to 6.8 percent copper, and is classified as a high strength age hardenable alloy. The sponsor for this project, Weber Metals, hopes to use 2219 Al to replace titanium in certain applications above the thermal limits of typical high strength Al. To test its performance, they manufactured round tensile samples and delivered them in peak aged, T852 condition. These samples were then overaged at a range of times and temperatures. The times in this experiment were one …

Weld Fracture Between C450 Stainless And C300 Maraging Steels In Golf Club Heads, Emily Oreste, Shea Costner

Materials Engineering

This project studied fractures along the weld on the face of TaylorMade metalwood golf clubs. The weld joint investigated was between investment cast C450 stainless steel and hot rolled C300 maraging steel that had been joined by plasma arc welding (PAW). Cracking in the welds between these two metals was discovered during in-house prototype testing. To understand the differences between the clubs with intact weld joints and clubs with fractured weld joints, the microstructures throughout the weld zones were imaged and a grid of microhardness values of the entire sample cross-section was generated. The images and hardness values were analyzed …

Rotating Beam Fatigue Of Forged 2219-T852 Aluminum Alloy, Julio Escamilla, Madison Reed

Materials Engineering

2219 aluminum has been used extensively in aerospace applications due to its ability to retain strength in large section thicknesses, thus making it ideal for large forgings. However, the Metallic Materials Properties Development and Standardization (MMPDS) handbook, a source of design data for aerospace industry applications, lacks information on 2219 in the T852 condition, particularly concerning the behavior of the alloy under cyclic loading conditions. Data was collected for forgings of 2219-T852 aluminum as produced by Weber Metals to determine the fatigue life of the alloy-temper combination and to assess the effects of forge thickness and orientation on fatigue life. …

Characteristics Of Bi-Metallic Interfaces Formed During Direct Energy Deposition Additive Manufacturing Processing, Ryan Anderson, Jordan Terrel, Judy Schneider, Sean Thompson, Paul Gradl

PRC-Affiliated Research

Various additive manufacturing processes are being evaluated to reduce the time and cost for fabrication of low volume, complex, and multifunctional assemblies. This study evaluated two direct energy deposition processes for the fabrication of large bi-metallic structures. The materials evaluated were Inconel 625 and copper alloy C18150, which are used in various high heat flux applications. Inconel was deposited onto the C18150 substrate using blown powder and wire-fed processes. Complete bonding was obtained in both processes and the resulting interfaces were evaluated using microscopy and indentation testing. Differences were observed in the interface region suggesting the kinetic energy of the …

Characteristics Of Bi-Metallic Interfaces Formed During Direct Energy Deposition Additive Manufacturing Processing, Ryan Anderson, Jordan Terrel, Judy Schneider, Sean Thompson, Paul Gradl

PRC-Affiliated Research

Various additive manufacturing processes are being evaluated to reduce the time and cost for fabrication of low volume, complex, and multifunctional assemblies. This study evaluated two direct energy deposition processes for the fabrication of large bi-metallic structures. The materials evaluated were Inconel 625 and copper alloy C18150, which are used in various high heat flux applications. Inconel was deposited onto the C18150 substrate using blown powder and wire-fed processes. Complete bonding was obtained in both processes and the resulting interfaces were evaluated using microscopy and indentation testing. Differences were observed in the interface region suggesting the kinetic energy of the …

Characteristics Of Bi-Metallic Interfaces Formed During Direct Energy Deposition Additive Manufacturing Processing, Ryan Anderson, Jordan Terrel, Judy Schneider, Sean Thompson, Paul Gradl

PRC-Affiliated Research

Various additive manufacturing processes are being evaluated to reduce the time and cost for fabrication of low volume, complex, and multifunctional assemblies. This study evaluated two direct energy deposition processes for the fabrication of large bi-metallic structures. The materials evaluated were Inconel 625 and copper alloy C18150, which are used in various high heat flux applications. Inconel was deposited onto the C18150 substrate using blown powder and wire-fed processes. Complete bonding was obtained in both processes and the resulting interfaces were evaluated using microscopy and indentation testing. Differences were observed in the interface region suggesting the kinetic energy of the …

The Influence Of Heat Treatment On Corrosion Behavior Of Martensitic Stainless Steel Uns 42670, Armen Kvryan

Boise State University Theses and Dissertations

Ceaseless demand for lighter, faster, and more efficient aircraft has been one of the greatest driving forces behind bearing steel innovations. Recent studies demonstrate that corrosion is one of the leading causes of bearing failure in both military and commercial aircraft. High-performing bearing steels are available but are not being used in US military applications due to high cost and security issues when steels are produced outside of the continental United States. One approach to address this issue is to engineer steels that are cost-efficient and heat treated for corrosion resistance, long wear life, etc.

This dissertation presents information on …

Mechanical Properties Of Heusler Alloys, Wesley Everhart, Joseph William Newkirk

Materials Science and Engineering Faculty Research & Creative Works

Heusler alloys have been a significant topic of research due to their unique electronic structure, which exhibits half-metallicity, and a wide variety of properties such as magneto-calorics, thermoelectrics, and magnetic shape memory effects. As the maturity of these materials grows and commercial applications become more near-term, the mechanical properties of these materials become an important factor to both their processing as well as their final use. Very few studies have experimentally investigated mechanical properties, but those that exist are reviewed within the context of their magnetic performance and application space with specific focus on elastic properties, hardness and strength, and …

A Study On Ultrasonic Energy Assisted Metal Processing : Its Correeltion With Microstructure And Properties, And Its Application To Additive Manufacturing., Anagh Deshpande

Electronic Theses and Dissertations

Additive manufacturing or 3d printing is the process of constructing a 3-dimensional object layer-by-layer. This additive approach to manufacturing has enabled fabrication of complex components directly from a computer model (or a CAD model). The process has now matured from its earlier version of being a rapid prototyping tool to a technology that can fabricate service-ready components. Development of low-cost polymer additive manufacturing printers enabled by open source Fused Deposition Modeling (FDM) printers and printers of other technologies like SLA and binder jetting has made polymer additive manufacturing accessible and affordable. But the metal additive manufacturing technologies are still expensive …

Iron-Containing Nanoparticles For The Treatment Of Chrionic Biofilm Infections In Cystic Fibrosis, Leisha M. A. Martin

Nanoscience and Microsystems ETDs

Cystic fibrosis (CF) is the most common genetic disease resulting in the morbidity and mortality of Caucasian children and adults worldwide. Due to a genetic mutation resulting in malfunction of the Cystic Fibrosis Transmembrane Conductance Regulator (CFTR) protein, CF patients produce highly viscous mucus in their respiratory tract. This leads to impairment of the mucociliary clearance of inhaled microbes. In addition to reduced microbial clearance, anoxic environmental conditions in the lungs promote biofilm-mode growth of the pathogenic bacterial species Pseudomonas aeruginosa. Chronic infections of P. aeruginosa begin in early childhood and typically persist until respiratory failure and death result. The …

Molecularly Conductive Behavior Of Blended Polymer Electrolyte-Based Cmc/Pva, Noor Saadiah Mohd Ali, Dishen Zhang, Yuki Nagao, Ahmad Salihin Samsudin

Makara Journal of Technology

This study investigated the electrical conduction and structural behavior of blended polymer electrolyte (BPE)-based carboxymethyl cellulose (CMC) and polyvinyl alcohol (PVA) in the development of solid-state electrochemical devices. Based on impedance spectroscopy and correlating Fourier transform infrared (FTIR) with thermogravimetric analysis, a framework was proposed to explain the structural enhancement of the BPE system. As revealed by FTIR, the optimum conductivity of CMC/PVA BPEs was 9.21 × 10−6 Scm−1 for 80:20 composition attributed to the intermolecular attraction between the polymers. Thermal stability of the CMC/PVA was influenced by the formation of a hydrogen bond between the hydroxyl (-OH), carboxylate (-COO-), …

Multistage Sonication Effect On The Composition And Properties Of Degraded Chitosan Product, Nurul Laili Arifin, Emma Savitri, Anjar Indah, Fesa Putra, Sumarno Sumarno

Makara Journal of Technology

The sonication method randomly breaks polymer chains to produce a varied distribution of products. A scheme with multi-stage sonication steps is proposed to identify oligomers and low molecular weight chitosan based on changes to the degrad-ed product. For each sonication level, 1% (w/v) chitosan in 1% (v/v) aqueous acetic acid was sonicated for 120 min at 60 °C. The products of the sonication treatment were deprotonized by adding an alkali solution, freeze dried and insoluble product re-sonicated until a low molecular weight was produced. Low molecular weight chitosan/insoluble products were character-ized with Fourier-transform infrared spectra (FT-IR) and X-ray diffraction (XRD) …

Study Of Zno Nanospheres Fabricated Via Thermal Evaporation For Solar Cell Application, Fatin Farisha Alia Azmi, Bouchta Sahraoui, Saifful Kamaluddin Muzakir

Makara Journal of Technology

A solar cell is a device that absorbs light energy to generate electrical energy. A typical example of a solar cell is the quantum dot solar cell (QDSC), which consists of three main components: (i) fluorophore: the component that absorbs light and generates excited state electrons and holes, (ii) photoelectrode: the component that transports the excited state electron and prevents recombination of excited state electrons and holes, and (iii) electrolyte: the component that re-plenishes the vacancy left by the excited electron in the hole. Despite the increasing number of research in the QDSC field, to date, a device with significant …