Materials Science and Engineering Commons^™

Advanced Manufacturing Of Multifunctional Shape Memory Polymer Composites And Self-Healing Systems, John B. Konlan

LSU Doctoral Dissertations

The need for multifunctional light weight structures for engineering applications is on the rise. Multifunctional composites are desired because of their ability to combine multiple functionalities into one structure. The advantages of a high strength-to-weight ratio of multifunctional composites make them desirable and suitable for use in energy-efficient applications. Shape-memory polymers (SMPs) have attracted interest over the past several decades because of their multifunctional nature. They have found use in many applications such as aerospace, satellites, automobiles, textiles, and biomedical devices, where lightweight and multifunctionality are key. The self-healing nature of most SMPs makes them suitable for use in lightweight …

Bioactivity And Mechanical Performance Of Centrifugally Spun Poly(D,L-Lactide)/Poly(3-Hydroxybutyrate) Submicrometric Fibers Containing Zinc Oxide And Hydroxyapatite Nanostructures, Victoria Padilla-Gainza, Heriberto Rodríguez-Tobías, Karen Lozano, Cristobal Rodriguez, Robert Gilkerson, Antonio Ledezma-Pérez, Narcedalia Anaya-Barbosa, Graciela Morales

Mechanical Engineering Faculty Publications

This study investigates the morphological, thermal, mechanical, and bioactive properties of centrifugally spun fibrous composites made from poly(D,L-lactide)/poly(3-hydroxybutyrate) (PLA/PHB) blends with zinc oxide (ZnO) and hydroxyapatite (Hap) nanoparticles. A 75/25 PLA/PHB weight ratio was chosen to balance mechanical and thermal properties. The precursor solution viscosities ranged from 0.25 to 0.50 Pa s, increasing with nanoparticle incorporation probably due to polymer-nanoparticle interactions. SEM revealed a uniform fibrous morphology, with diameters of 1.21 for PLA/PHB, 2.65 for PLA/ZnO/Hap, and 1.80 μm for PLA/PHB/ZnO/Hap. TGA showed two-step degradation for PLA/PHB fibers, while PLA/PHB/ZnO/Hap degraded in a single step at 249°C, leaving a residue …

Impact Of Repeated Washing Cycles On Surface Integrity And Mechanical Properties Of Glass Bottles, Siwat Patamakam Mr., Thitisilp Kijchavengkul, Siriyupa Netramai, Gong Yaijam

Journal of Applied Packaging Research

Glass bottles are a top choice in the global beverage industry, but their inherent brittleness poses challenges in maintaining durability. This study focused on investigating the impact of numbers of washing processes from reusing on the surface quality and mechanical properties of glass bottles after each washing cycle. Contact angle technique was used to determine surface quality of glass bottles. It was found that mechanical integrity, as reflected in internal pressure resistance values, and surface quality of glass bottles exhibited an exponential decline with each washing cycle. Furthermore, a predictive model (R² = 0.8882) was developed to estimate its …

Numerical Simulation Of Heat Transfer In Self-Propagating High-Temperature Synthesis (Shs)-Based Calcination Of Limestone, Sayee Srikarah Volaity, Shubham Agrawal, Srinivas Kilambi, Patrick Phelan, Aditya Kumar, Narayanan Neithalath

Materials Science and Engineering Faculty Research & Creative Works

Calcination of limestone, a high temperature (∼900 °C) process that emits 44 % of the mass of limestone as CO₂, is a critical process in the production of many industrially important materials. To soften the CO₂-related impacts of traditional calcination, and to enable ultrafast synthesis of lime, a novel approach based on self-propagating high-temperature synthesis (SHS) has been put forward. SHS uses exothermic heat released by the combustion of fuel intermixed with the reactants to advance the reaction, and hence requires the provision of lower external temperatures. This study introduces a microstructure-guided modeling approach to understand …

Compositionally Complex Diborides: Competing Solubility During Sintering And Properties, Laura Silvestroni, Carlo Baldisserri, Jacopo Matteo Tabaglio, Nicola Gilli, Jeremy Watts, Steven M.I. Smith, Gregory E. Hilmas, William G. Fahrenholtz

Materials Science and Engineering Faculty Research & Creative Works

An ultra-high temperature ceramic based on ZrB2, TiB2, and SiC was hot pressed to full density at 1850 °C. Addition of 5 vol% of different metal-compounds, in the form of HfC, VC, NbC or CrB2, increased the densification temperature to 1910 °C. The resulting compositionally complex ceramics had homogeneous microstructures with boride grains exhibiting core-shell features. The shell was a solid solution containing variable amounts of the three metals. Notably, TiB2 remained as a discrete phase in the reference material and in the presence of the V- and Cr- based additions, whilst it dissolved into the main ZrB2-based grains for …

Effects Of Wetting Events On Mass Timber Surface Microbial Communities And Voc Emissions: Implications For Building Operation And Occupant Well-Being, Gwynne Á. Mhuireach, Susan Collins, Leslie Dietz, Patrick Finn Horve, Aurélie Laguerre, Dale Northcutt, Jason Stenson, Kevin Van Den Wymelenberg, Elliott Gall, Mark Fretz

Mechanical and Materials Engineering Faculty Publications and Presentations

IntroductionHumans have used wood as a construction material throughout history. Currently, mass timber products, such as cross-laminated timber (CLT), are becoming more popular as a structural material, since they are renewable and have a lower carbon footprint than concrete or steel. Nonetheless, some building types, such as healthcare, veterinary, and food manufacturing, avoid using structural mass timber due to concerns about microbial growth in the event of wetting. One solution is to use protective coatings on mass timber products to increase moisture resistance, although the coatings themselves may generate concerns about volatile organic compound (VOC) emissions. Natural uncoated wood also …

Atomistic Simulations Of Shape Memory Behavior And Negative Poisson's Ratio Effect Of Liquid Crystal Elastomers, Nanang Mahardika

Student Research Symposium

• LCEs are suitable materials for soft robotics application because it is programmable, responsive to various stimuli and has flexibility.

2024, A Landmark Year For Climate Change And Global Carbon Capture, Utilization, And Storage: Annual Progress Review, Shangli Shi, Yun Hang Hu

Michigan Tech Publications

This annual review outlines the progress of carbon capture, utilization, and storage (CCUS) technologies in 2024. As human-induced CO2 emissions continued to rise, the year presented critical challenges. Notably, 2024 was the hottest year on record and the first in which global temperatures exceeded preindustrial levels by more than 1.5°C, driving intensified efforts to advance CCUS. Scientific interest in CCUS grew significantly, with the annual number of related publications increasing by 11.4% compared to 2023, reaching 53,970. The total number of operational commercial CCUS facilities also expanded, rising by 16.3% to a total of 50. In the political area, governments …

Fabrication Of Ultra High-Temperature Compact Heat Exchanger By Extrusion-Based Ceramic Additive Manufacturing, Abid Hasan Rafi, David W. Lipke, Jeremy Lee Watts, Greg Hilmas, Ming-Chuan Leu

Miners Solving for Tomorrow Research Conference

No abstract provided.

Physical Characterization Of Copper Anode Slimes, Carter Glynn, Michael S. Moats

Miners Solving for Tomorrow Research Conference

No abstract provided.

Sustainable Solutions To Eutrophication: The Role Of Glass Fertilizers, Lucas Greiner, Charmayne Lonergan

Miners Solving for Tomorrow Research Conference

No abstract provided.

Additive Manufacturing Of Thermoplastic Composites, Matik Heskin, K. Chandrashekhara, Richard Billo, Ming-Chuan Leu, Thomas P. Schuman

Miners Solving for Tomorrow Research Conference

No abstract provided.

Microstructural Evolution Of High-Entropy Carbide Ceramics, Elizabeth Pritchett, William Fahrenholtz, Greg Hilmas, Steven Smith

Miners Solving for Tomorrow Research Conference

No abstract provided.

Polymerization Methods For Vinyl Phosphonate Monomers: Challenges And Perspectives, Sara Mccauley

Miners Solving for Tomorrow Research Conference

No abstract provided.

Preliminary Assessment Of Non-Volatile Particulate Matter And Gaseous Emissions From A Premixed Pre-Vaporized Combustor Designed For Civil Supersonic Transport, Ugochukwu Ewuzie, Godwin Ifeanyi Ogbuehi, Steven Achterberg, Monday Uchenna Okoronkwo, Philip D. Whitefield

Miners Solving for Tomorrow Research Conference

No abstract provided.

Innovative Design Methodology For Durable Open-Graded Friction Course Asphalt Mixtures, Anas Abualia

LSU Doctoral Dissertations

Open-graded friction course (OGFC) is a thin asphalt mixture surface layer with a high percentage of coarse aggregates and high interconnected air voids, which provides improved skid resistance, visibility, and decreased pavement-tire noise. However, construction personnel at DOTD reported that conventional OGFC mixtures have short service life (raveling distress). Further, their structural contribution to the pavement structure is commonly neglected and designed only for functionality purposes.

The objective of this study was to develop a rational mix design methodology to improve the durability of OGFC asphalt mixtures. Specific objectives are to: (1) conduct a rheological and chemical characterization of polymer-, …

Underlying Mechanisms Of The Effect Of Microfines Of Manufactured Sand On Non-Linear Structural Build-Up Of Cement Paste, Jiang Zhu, Jiaping Liu, Kamal H. Khayat, Xin Cheng, Wei Zhao, Zhen Li, Xin Shu, Yongbo Huang

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

The rheological properties of cement-based materials made with manufactured sand vary with the content and physio-chemical properties of microfines in the sand. However, the evaluation of rheological properties regarding the structural build-up at early-age hydration remains challenging for the cementitious materials prepared with different manufactured sands, due to complicated underlying structuration mechanisms. This paper studies the effect of disparate microfines of different manufactured sands on the non-linear growth of static yield stress of cement pastes at rest. The paste mixtures were prepared with 0.40 and 0.275 water-to-cement mass ratio (W/C) and had a fixed mini-slump flow of 240 ± 5 …

L.G. Twidwell Fifty-Six Years Of Research A Summary, Larry G. Twidwell

Metallurgical & Materials Engineering

Larry G. Twidwell, D.Sc. is Emeritus Professor in the Department of Metallurgical and Materials Engineering at Montana Technological University. He has fifty-six years of experience in teaching and directing research in Metallurgical and Materials Engineering at Montana Tech. Twidwell and his graduate students and coworkers have conducted research emphasizing extractive metallurgy and the application of extractive metallurgical engineering to the treatment of metallurgical wastes, process waters and byproducts. Four books, seventy-seven M.Sc. theses, one-hundred-thirty refereed publications and one hundred-eight national and international presentations have resulted from their research efforts. Twidwell has received several outstanding teacher/researcher awards during his tenure at …

Computational Modeling Of Astrophysical Systems, Leleya Iris Stallard

Spring Showcase for Research and Creative Inquiry

This research project focuses on the computational modeling of astrophysical systems using Femap with NX Nastran. The goal was to simulate and analyze the vibrational behavior and structural deformation of celestial bodies under different material compositions and collision conditions. Materials such as iron, granite, titanium, and models for white dwarf stars were used to investigate how varying physical properties affect the systems' dynamic responses. Both isotropic and anisotropic models were created to represent realistic astrophysical materials. Through static and modal analyses, the study explored how internal structure and material stiffness influence the reaction of celestial objects to applied forces and …

Josephson Junctions: Fabrication And Applications For The Axion Dark Matter Experiment, Jonah M. Sachs

Senior Honors Papers / Undergraduate Theses

The observation of axions could revolutionize the world of physics. Through microwave frequency cavity readout of the photons associated with these axions, the ADMX project at WashU utilizes multiple different forms of the Josephson junction (JJ), a superconductive circuit element. The physics behind the JJ are essential to understanding its operation for resonant cavity readout in addition to parametric amplification. Parametric amplifiers produced using JJs can approach the signal-to-noise ratio set by quantum mechanics, and prove essential for the amplification chain used by the ADMX experiment for axionic detection. The limits of these amplifiers are set by the noise tuning …