Metallurgy Commons^™

Minimizing Cr-Evaporation From Balance Of Plant Components By Utilizing Cost-Effective Alumina-Forming Austenitic Steels, Lingfeng Zhou

Graduate Theses, Dissertations, and Problem Reports (ETD)

A solid oxide fuel cell (SOFC) is a clean and efficient energy conversion device. The development of intermediate-temperature SOFCs has made it preferable to use metallic interconnects (MICs) to greatly reduce the cost and significantly increase the efficiency compared to ceramic interconnect materials. However, gaseous chromium species will evaporate from the chromium-containing layer formed on the surface of commonly used MICs and balance of plant (BoP) components. Volatile chromium species have been shown to form solid deposits which poison the cathodes of SOFCs, causing drastic cell performance degradation and thereby limiting commercialization. In order to alleviate the Cr poisoning and …

Calcite Depression In Bastnaesite-Calcite Flotation System Using Organic Acids, Emmy Muhoza

Graduate Theses, Dissertations, and Problem Reports (ETD)

Bastnaesite is the primary source of light REEs, namely cerium (Ce), lanthanum (La), praseodymium (Pr), neodymium (Nd), to name a few. Bastnaesite is typically concentrated using the froth flotation beneficiation method. Flotation of bastnaesite suffers from high reagent consumption due to the similar surface characteristics of bastnaesite and associated gangue minerals, including calcite. Additionally, complex stages of high-temperature conditioning are often required to suppress the detrimental impact of dissolved calcium ions on the flotation of bastnaesite. This research seeks to investigate the capabilities of organic acids in the bastnaesite-calcite flotation systems to selectively depress calcite minerals and effectively chelate calcium …

Study Of The Thermodynamic Properties Absorbation Sulfur Storage Gas Of Zinc And Copper Industry, Berdiyarov Tilovkabulovich Berdiyarov Dr., Sh. T. Khojiev, S. T. Matkarimov, Sh. Munosibov

Technical science and innovation

The article considers the problems of utilization of industrial gases formed in the production of copper and ore containing sulfur anhydrides. Currently, the composition of process gases entering the gas purification department is approximately 6-7% SO₂, 0.2-0.3% SO₃ and other gases, until sulfuric acid is obtained from these gases, the sulfate is treated in a counter-scheme with 8% sulfate acid. The aim is to first reduce the temperature of the exhaust gases and second to avoid flying components such as as As, F, Se. As a result of the studies, the amount of SO₂ in the …

Study Of Alloy And Process Modifications To Design Hydrogen Resilient High Hardness Steels, William R. Williams

Theses and Dissertations

High hardness steels (HHS) are vulnerable to hydrogen embrittlement, which can lead to rapid degradation of mechanical properties. Improved resistance to hydrogen embrittlement would be beneficial to many industries including construction, automotive, and military. A comparison study was performed to assess the hydrogen susceptibility of select commercially available and in-house designed HHS alloys. Slow strain rate tensile tests, performed with specimens charged with various levels of hydrogen, provided a macroscopic view of the onset of hydrogen embrittlement. Hydrogen permeation and thermal desorption spectroscopy tests determined the uptake and diffusivity of hydrogen through the material. The evaluation of hydrogen susceptibility for …

The Process-Structure-Property-Performance Of Aisi 1020​, Jonathan Wellman, Tate James, Robbie Christman, Brian Broom

ME 4133/6133 Mechanical Metallurgy

AISI 1020 is widely used in many different industries due to its high strength, high ductility, high machinability, and good weldability. AISI 1020 has a number of applications. Low carbon steel can be used on a macroscale to build bridges, and low carbon steel can be used on smaller scales such as Lawnmower blades. Low carbon steel is the material of choice for lawn mower blades because of its ability to bend before it breaks. The ductile attribute of low carbon steel also has many other benefits.

Ti-6al-7nb Utilization In Surgical Implants, Michael O. Fleming

ME 4133/6133 Mechanical Metallurgy

This presentation discusses the processing, structure, properties, and performance of Ti-6Al-7Nb in relation to use as a surgical implant.

Development Of Pspp Map For Stainless Steel Alloys Used In A Marine Environment, Jarrett D. Hawkins

ME 4133/6133 Mechanical Metallurgy

A process-structure-properties-performance map will be created for these alloys focusing on the modification of the structure or composition and outlining the processes required and the affected properties. A thorough review of different chemical alloys, grain refining methods, and grain boundary compositions for several alloys and their corresponding property effects. Also plan to review material treatment processes and standard refining methods for stainless steels. The performance of these metals will be evaluated for property requirements in regards to strength, toughness, with an emphasis on corrosion resistance.

Tungsten: The Strongest Natural Metal On Earth, Haley E. Holland, Razan Khadka, Lee Marble, Kaleb Tutor

ME 4133/6133 Mechanical Metallurgy

The overall objective of this project was to construct a process-structure-property-performance (PSPP) map for a chosen metallic material. The material chosen by the group is tungsten (W). Tungsten is a rare, naturally occurring element and is usually found in the form of ores. It is known predominantly for its ability to withstand extreme temperatures, as well as its high tensile strength. The PSPP map displays many specifications of tungsten in each of the four categories and further details regarding each specific linkage, or subcategory, within the map are written throughout the research paper.

Along with the four specific categories outlined …

Analysis Of Titanium Alloy Ti-6al-4v, Hunter C. Smith, Gordin Smith

ME 4133/6133 Mechanical Metallurgy

Titanium alloy Ti-6Al-4V was chosen for examination, more specifically, the Properties and Performance of the alloy. The students will share the responsibility of examining the attributes of the material. The team members participate evenly in performing research, producing calculations, and constructing the final report. Contained herein is the information gathered through research conducted thus far.

The performance of the material will be related to the processing methods of the material. This relationship forms the basis of cost analysis. The students will examine the atomic characteristics and crystalline structure to determine the effects of the alloyed materials on properties such as …

An Analysis Of The Effects Of Process, Structure, And Properties On The Performance Of The Ti6al4v Alloy, Brad Jay Sampson, Loubna Ifqir

ME 4133/6133 Mechanical Metallurgy

Ti6Al4V (pronounced Ti-64), is a titanium alloy used in a variety of engineering applications including the aerospace, automotive, and biomedical industries. Ti6Al4V is made up of a combined ɑ-β microstructure, which provides it with many valuable properties such as high strength, low weight, high melting point, corrosion resistance, and biocompatibility. [1] For years, casting and forging have been the traditional processes used for the manufacturing of Ti6Al4V components, but recent interest in the additive manufacturing of Ti6Al4V through the Electron Beam Melting (EBM), Selective Laser Melting (SLM), and Directed Energy Deposition (DED) methods has been gained. The goal of this …

Al 6061 Alloy, Will Mckelvey, Evan Robertson, Justin Yates

ME 4133/6133 Mechanical Metallurgy

We want to portray the Al 6061 manufacturing and machining processes and how these affect the mechanical properties of the material. We also want to portray the strength and weaknesses and the reasons why it is used in certain applications.

Duplex Stainless Steel 2205 In The Pulp And Paper Industry, Charlie S. Wilcher, Trevor Davus

ME 4133/6133 Mechanical Metallurgy

Duplex stainless steel’s durability, formability, and resistance to corrosion make it the primary steel option of the pulp and paper industry. The harsh environments found in certain aspects of this industry, such as in bleach plants, digesters, liquor vessels, and any piping where corrosive liquids may be passed, require the previously mentioned properties that duplex stainless steel 2205 offer. The structure and properties of duplex stainless steel, as well as the processes it undergoes, allow for it to withstand these environments. Research into the structure and properties of duplex stainless steel and the processes it undergoes will indicate how duplex …

Ar400 Wear Plates, Jase Tatum, Bryson Miller, John Howell, Aaron Alexander

ME 4133/6133 Mechanical Metallurgy

Wear resistance is an invaluable performance metric for most metallic components found in mechanical systems. Our research focused on AR400, a steel alloy known for its wear resistance capabilities, in an effort to determine what factors might be attributed to its performance in wear applications. After establishing the processing techniques and resulting material structures that give AR400 such an edge in extreme wear conditions, our goal is to determine indicators of wear resistance that can be used to distinguish excellent wear resistant alloys from average or subpar performers against wear.

Investigating Cobalt Chrome Alloy For Use In Biomedical Applications, Morgan Calhoun, Caitlin Cade

ME 4133/6133 Mechanical Metallurgy

Cobalt Chrome alloys, in particular cast Co-Cr ASTM-F75, are often used as the material for medical implants due to a combination of material properties: high strength, stiffness, temperature endurance, and wear / corrosion resistance. We aim to demonstrate and discuss what characteristics make it such a desirable material in the production of metallic biomedical implants

Titanium Ti-6al-4v, James Aaras Ross Brundege

ME 4133/6133 Mechanical Metallurgy

Titanium alloys, such as Ti-6A1-4V, used as biomaterials possess great characteristics compared to other alloys such as stainless steel alloys. Characteristics such as biocompatibility, enhanced corrosion, strain, and fatigue resistance provide amazing benefits from these alloys. Providing an understanding of Ti used in biomedical applications and production can provide insight into its benefits and limitations as well as the areas of potential improvement for future study.

3xx Aluminum Alloys For Ice Implementation, Kyle A. Taylor, Eric Cleckner, Jeffery Garrett

ME 4133/6133 Mechanical Metallurgy

The material to be explored for the purpose of this project relates to the Aluminum alloys used in the majority of modern engine “heads” and a number of engine “blocks”. The Aluminum used for these engine applications vary slightly across different manufacturers in their processing, structure and ultimate properties, despite their nearly identical performance applications. Part of the interest in this particular subject is the slight variations across manufacturing that result in different performance. Regardless of idiosyncrasies, these Al alloys are expected to perform under varying temperatures, with the ability to elastically deform and return to their original shape. They …

Stochastic Lightning Damage Prediction Of Carbon/Epoxy Composites With Material Uncertainties, S.Z.H. Shah, Juhyeong Lee

Mechanical and Aerospace Engineering Faculty Publications

This study presents a novel stochastic modeling framework predicting lightning thermal damage in carbon/epoxy composites. The stochastic lightning damage model (SLDM) was developed with random distributions of composite’s electrical conductivity and void. The Box-Muller transformation was applied to generate random in-plane and through-thickness electrical conductivities with Gaussian distributions. The SLDM suggested that the predicted lightning thermal damage to carbon/epoxy composites increased slightly with the use of stochastic electrical conductivity, but the presence of voids did not significantly affect the damage development. The predicted size and shape of lightning thermal damage agreed fairly well with experimental results. In addition, the proposed …

Ultra Low-Cycle Fatigue Behavior Comparison Between Additively Manufactured And Rolled 17-4 Ph (Aisi 630) Stainless Steels, David Gonzalez-Nino, Timothy Strasser, Gary S. Prinz

Civil Engineering Faculty Publications and Presentations

This study investigates the mechanical behavior of additively manufactured (AM) 17-4 PH (AISI 630) stainless steels and compares their behavior to traditionally produced wrought counterparts. The goal of this study is to understand the key parameters influencing AM 17-4 PH steel fatigue life under ULCF conditions and to develop simple predictive models for fatigue-life estimation in AM 17-4 steel components. In this study, both AM and traditionally produced (wrought) material samples are fatigue tested under fully reversed (R = −1) strain controlled (2–4% strain) loading and characterized using micro-hardness, x-ray diffraction, and fractography methods. Results indicate decreased fatigue life for …

Laser Surface Treatment And Laser Powder Bed Fusion Additive Manufacturing Study Using Custom Designed 3d Printer And The Application Of Machine Learning In Materials Science, Hao Wen

LSU Doctoral Dissertations

Selective Laser Melting (SLM) is a laser powder bed fusion (L-PBF) based additive manufacturing (AM) method, which uses a laser beam to melt the selected areas of the metal powder bed. A customized SLM 3D printer that can handle a small quantity of metal powders was built in the lab to achieve versatile research purposes. The hardware design, electrical diagrams, and software functions are introduced in Chapter 2. Several laser surface engineering and SLM experiments were conducted using this customized machine which showed the functionality of the machine and some prospective fields that this machine can be utilized. Chapter 3 …

Martensitic And Inter-Martensitic Transformations In Magnetocaloric Ni2.15mn0.85ga Heusler Alloy, A. Madiligama, P. Ari-Gur, Y, Ren, V, Shavrov, Y. Ge, J. George, I. Musabirov, V. Koledov

Mechanical and Aerospace Engineering Faculty Publications

The entropy changes of successive martensitic phase transformations in Ni-Mn-Ga Heusler alloys can be utilized to realize enhanced magnetocaloric properties. A detailed study of phase transformations of one such alloy, Ni2.15Mn0.85Ga, (ΔQ = 4900 J/kg at 343 K, under 140 kOe), is reported here. Upon cooling, the paramagnetic cubic (L21) austenitic phase transforms into a ferromagnetic 7M modulated monoclinic martensitic phase. This phase is stable in a narrow temperature range, and upon further cooling, transforms into a non-modulated ferromagnetic tetragonal (L10) phase. The separation between the equilibrium temperatures of the austenitic and tetragonal martensitic phases is only ~50 K. The …