Metallurgy Commons^™

Analysis Of The Interfacial Reaction Between Bulk Metallic Glass Coated Copper, Nickel, And Titanium With Lead-Free Solders, Andromeda Dwi Laksono, Yee-Wen Yen, Rifqi Aulia Tanjung, Teodoro A. Amatosa, Ruki Harwahyu

Makara Journal of Technology

Bulk metallic glass (BMG) has good mechanical strength, high hardness, wear resistance, and corrosion resistance with promising application in various industries. However, for the industrial production of BMG, the main issue is how to overcome limitations of joining with other materials. The present study focuses on solder processing at low operating temperature to avoid exceeding the recrystallization temperature. A feasible joining process for BMG was developed using lead-free solders. The BMG surface is pre-plated with copper, nickel, or titanium as a wetting layer. The reaction temperature is set between the glass transition temperature of BMG and the melting point of …

Design Of Ac Microgrid Topology With Photovoltaic Uncertainties In A Rural Village, Vannak Vai

Makara Journal of Technology

Energy needs are increasing day by day, especially for developing countries, due to population growth and changing lifestyles. A suitable microgrid topology with renewable energy integration is considered to fulfill the people and society’s needs. This paper focuses on the design of AC microgrid topology for a nonelectrified village with the integration of PV uncertainties in both sitting and sizing. The development of an optimal algorithm based on the conductor use minimization and unbalanced load improvement is proposed. The shortest path is proposed to search for the minimum conductor use. Then, the algorithm for improving the unbalanced load with two …

Mean-Shift Object Tracking Algorithm With Systematic Sampling Technique, Yoanes Bandung, Aris Ardiansyah

Makara Journal of Technology

Mean shift is a fast object tracking algorithm that only considers pixels in an object area, hence its relatively small computational load. This algorithm is suitable for use in real-time conditions in terms of execution time. The use of histograms causes this algorithm to be relatively resistant to rotation and changes in object size. However, its resistance to lighting changes is not optimal. This study aims to improve the performance of the algorithm under lighting changes and reduce its processing time. The proposed technique involves the use of sampling techniques to reduce the number of iterations, optimization of candidate search …

Analysis Of Correlation And Mapping Of Chlorophyll-A Concentrations And Sea Surface Temperatures In Coastal Areas Based On Terra Modis Satellite Image Data, Hendrata Wibisana, Bangun Muljo Sukotjo, Umboro Lasminto

Makara Journal of Technology

Ecosystems in aquatic environments are distinct from ecosystems on land. Changes that occur in ecosystems in aquatic environments affect the lives of biota in these waters, including the fish used as a food source in fishing communities in coastal areas. This study aims to determine the role of remote sensing in mapping and analyzing the relationship between the parameters of sea surface temperature and chlorophyll-a concentrations on the coast. The correlation of sea surface temperature with chlorophyll-a concentrations is modeled via linear regression. An analysis of variance test is performed to establish the suitability of the temperature data for the …

Experimental Study Of Hollow-Core Slab Containing Waste Pet Bottles, Mulia Orientilize, Josia Irwan Rastandi, R. M. Dimas Aries C., Marsha Niken P., Krisna Adi S.S., Abimantrana Abimantrana

Makara Journal of Technology

This study investigated the utilization of plastic-waste concrete as an effort to reduce urban waste problems. The waste plastic bottles were utilized to form the hollows of the hollow-core slabs (HCSs). The bottles were made of polyethylene terephthalate (PET). As a part of green research to reuse waste material, shredded PET was also added to the concrete mixture to improve the HCS strength. The cast-in-site HCS could be constructed without any difficulties. Three parameters were investigated: the effects of void content, shredded PET content, and steel-fiber (SF) content on the HCS ultimate bending capacity (Mu). Fifteen specimens were tested under …

Numerical Study Of A Buckling Restrained Brace (Brb) In Steel Structures And Comparison With A Convergent Ordinary Brace (Ocb) Under Static And Dynamic Loading, Fatemeh Habibpour

Makara Journal of Technology

Bulk metallic glass (BMG) has good mechanical strength, high hardness, wear resistance, and corrosion resistance with promising application in various industries. However, for the industrial production of BMG, the main issue is how to overcome limitations of joining with other materials. The present study focuses on solder processing at low operating temperature to avoid exceeding the recrystallization temperature. A feasible joining process for BMG was developed using lead-free solders. The BMG surface is pre-plated with copper, nickel, or titanium as a wetting layer. The reaction temperature is set between the glass transition temperature of BMG and the melting point of …

Study Of Laser Based Additive Manufacturing For Titanium And Copper Alloys, Congyuan Zeng

LSU Doctoral Dissertations

Material processing by laser is increasingly applied in industrial applications for its outstanding characteristics, such as localized heating, high efficiency, and high manufacturing precision. In this study, two kinds of laser material processing strategies were investigated, namely laser surface engineering and laser-powder-bed fusion additive manufacturing, with pure titanium and copper alloys as target materials, respectively.

For laser surface engineering related studies, the work includes the investigation of the dynamic interactions between titanium and pure nitrogen or ambient air under transient laser processing conditions. Thanks to the in-situ synchrotron X-ray diffraction tests, the high-temperature reaction steps between titanium and pure nitrogen/ambient …

Absorption Of Nitrogen During Pulsed Wave L-Pbf Of 17-4 Ph Steel, Ben Brown, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

In the fabrication of 17-4 PH by laser powder bed fusion (L-PBF) the well-documented occurrence of large amounts of retained austenite can be attributed to an elevated concentration of nitrogen present in the material. While the effects of continuous wave (CW) laser processing on in-situ nitrogen absorption characteristics have been evaluated, power modulated pulsed wave (PW) laser processing effects have not. In this study the effects of PW L-PBF processing of 17-4 PH on nitrogen absorption, phase composition, and mechanical performance are explored using commercially available PW L-PBF equipment and compared to samples produced by CW L-PBF. PW L-PBF samples …

Thermodynamic Prediction And Experimental Verification Of Multiphase Composition Of Scale Formed On Reheated Alloy Steels, Richard Osei, Semen Naumovich Lekakh, Ronald O'Malley

Materials Science and Engineering Faculty Research & Creative Works

The structure, phase, and composition of scale formed on a continuously cast steel slab during reheating depend on intrinsic factors (steel chemistry, microstructure, and as-cast surface condition) and extrinsic parameters (temperature, time, composition, and velocity of combustion gas atmosphere). The scale that forms on a slab normally has several layers with differing compositions and phases and knowledge of this scale structure is important in subsequent descaling and hot rolling processing steps. Formation of multiphase scale structures on steel during high temperature oxidation in reheat furnace proceeds according to a local thermodynamic equilibrium, while thickness of layers depends on kinetic conditions …

The Investigation Of The Underlying Microstructure Associated With Fracture Features In 6061 Cold Sprayed Aluminum, Justin White

UNF Graduate Theses and Dissertations

Cold gas dynamic spraying commonly known as cold spray is a process currently used for restoration, re-tolerancing, and application of coatings. With additional resources allocated towards the development of a through process model aimed at predicting the properties of bulk material produced via the Cold Spray process, more lab testing and investigation must be done to capture the effects of the varying microstructure in CS materials. The properties of ultra-fine-grained materials are derived from data collected from coarse grained materials and processes that do not accurately capture the effects as elevated strain rates and ultra-fine-grained materials. The lack of property …

Morphology Control Of One-Dimensional Gallium Nitride Nanostructures By Modulating The Crystallinity Of Sacrificial Gallium Oxide Templates, Yun Taek Ko, Mijeong Park, Jingyeong Park, Jaeyun Moon, Yong Ho Choa, Young In Lee

Mechanical Engineering Faculty Research

In this study, we demonstrated a method of controllably synthesizing one-dimensional nanostructures having a dense or a hollow structure using fibrous sacrificial templates with tunable crystallinity. The fibrous ga2o3 templates were prepared by calcining the polymer/gallium precursor nanofiber synthesized by an electrospinning process, and their crystallinity was varied by controlling the calcination temperature from 500oC to 900oC. gaN nanostructures were transformed by nitriding the ga2o3 nanofibers using NH3 gas. All of the transformed gaN nanostructures maintained a one-dimensional structure well and exhibited a diameter of about 50 nm, but their morphology was clearly distinguished according to the crystallinity of the …

Direct Energy Deposition Of Mo Powder Prepared By Electrode Induction Melting Gas Atomization, Goo Won Roh, Eun Soo Park, Jaeyun Moon, Hojun Lee, Jongmin Byun

Mechanical Engineering Faculty Research

Molybdenum (Mo) is used to form a barrier layer for metal wiring in displays or semiconductor devices. Recently, researches have been continuously attempted to fabricate Mo sputtering targets through additive manufacturing. in this study, spherical Mo powders with an average particle size of about 37 um were manufactured by electrode induction melting gas atomization. Subsequently, Mo layer with a thickness of 0.25 mm was formed by direct energy deposition in which the scan speed was set as a variable. According to the change of the scan speed, pores or cracks were found in the Mo deposition layer. Mo layer deposited …

Modeling Of Rare Earth Solvent Extraction Process For Flowsheet Design And Optimization, Vaibhav Kumar Srivastava

Theses and Dissertations--Mining Engineering

The separation and purification of rare earth elements (REEs) into individual products has been a topic of significant interest for researchers and engineers for many decades. The prime reason for such sustained interest is due to REEs’ demand and application in modern technology, as well as the challenges associated with their separation and purification. The chemical similarity of rare earth group elements is responsible for difficult separability which makes purification of individual elements challenging. Despite associated complications, processes such as solvent extraction (SX) and ion-exchange have been successfully utilized in the separation and production of REEs on pilot and commercial …

New Horizons For Processing And Utilizing Red Mud, M. Archambo

Dissertations, Master's Theses and Master's Reports

Red mud is an industrial slurry waste that is produced as a byproduct of the Bayer process for alumina. The waste is generated in large quantities, up to a ratio of 2:1 against the valued product alumina. Red mud exhibits many chemical and physical properties that categorize it as a hazardous material. Due to the addition of sodium hydroxide in processing, the pH is typically at values close to 13. Small particle size discourages separation from water for disposal, so drying red mud happens over many years.

The pH of red mud can be reduced with inexpensive reagents. Carbon dioxide …

Anaerobic Reductive Bioleaching Of Manganese Ores, Neha Sharma

Dissertations, Master's Theses and Master's Reports

The increasing demand of manganese in the industries and various hindrances in its production from low grade ores by conventional method has made it imperative for researchers around the world to develop a method of manganese extraction from low grade ores that is both environment friendly and economical. Bioleaching has shown significant potential in manganese extraction and efficiencies of extraction have been found to be 70-98% with the help of various bacteria and fungi.

This study focuses on extraction of manganese with the help of mixed bacterial strains that have been collected from their natural anaerobic environment. The extraction of …

Thermomechanical Mechanisms That Cause Adhesion Of Aluminum High Pressure Die Castings To The Die, Alex Monroe

Dissertations, Master's Theses and Master's Reports

In high pressure die casting (HPDC) of aluminum, cast material adhering to die is a significant defect. Adhesion occurs in two primary ways. The casting may stick preventing its removal from the die. Aluminum can also adhere to the die and buildup in local areas on the die surface with additional casting cycles. This second form of adhesion is called soldering. Lubricant is the best technology to control all forms of adhesion, but it comes at the cost of casting porosity, blisters, reduced die life, and increased die casting machine wear. New strategies to prevent adhesion are desired to eliminate …

Atomistic Monte Carlo Simulation Study Of Phase Transitions In Metal Alloys, Xiaoxu Guo

Dissertations, Master's Theses and Master's Reports

The atomic-scale Monte Carlo simulation study focuses on the intrinsic behaviors of a defect-free crystal that undergoes a cubic-to-tetragonal martensitic transformation. The quasi-spin variable associated with the lattice sites characterizes the local unit cells of the orientation variants of the ground-state martensite phase, which interact with each other through long-range elastic interactions. It is shown that the diffuse scattering in the premartensitic austenite state results from the spatial correlation of the atomic-scale heterogeneous lattice displacements and manifests the displacement short-range ordering. The effects of temperature, elastic anisotropy, and shear modulus softening on the diffuse scattering and displacement short-range ordering are …

Role Of Eta Phase Evolution On Creep Properties Of Nickel Base Superalloys Used In Advanced Electric Power Generation Plants, Ninad Mohale

Dissertations, Master's Theses and Master's Reports

Advanced fossil energy power generation plants require materials that withstand high temperatures and corrosive environments. One such material that is used in steam turbines is Nimonic 263. It is a nickel-base superalloy that is principally strengthened by gamma primephase (Ni₃(Ti, Al)) and has an L1₂structure. At extended times and at turbine operating temperatures however, eta (Ni₃Ti) phase is known to form at the expense of gamma prime. Eta has a complex DO₂₄structure and is the stable phase between 750°C and 900°C, but with slow kinetics of formation. Little is understood about eta …

Analyzing Variation In Dispersoid Formation In Aluminum Alloys By Minor Changes In Homogenization Temperature, Brendan Treanore

Dissertations, Master's Theses and Master's Reports

The homogenization of billets in the aluminum extrusion industry is a critical step that removes chemical segregation from casting, dissolves low melting point phases, forms nanoscale dispersoid phases, and promotes the beta to alpha transformation of iron particles in the matrix. With ever increasing use of aluminum extrusion in the automotive industry there is a constant need for increased efficiency and consistency in processing of extruded aluminum. The work in this thesis explores the effects of 10°C differences in the homogenization temperature on the formation of dispersoids in 6082 alloys used in the automotive industry. The role of dispersoids is …

Analysis Of Post-Deposition Recrystallization Processing Via Indium Bromide Of Cu(In,Ga)Se2 Thin Films, Deewakar Poudel, Benjamin Belfore, Tasnuva Ashrafee, Shankar Karki, Grace Rajan, Angus Rockett, Sylvain Marsillac

Applied Research Center Publications

Cu(In,Ga)Se₂ (CIGS) thin films were deposited at low temperature (350 °C) and high rate (10 µm/h) by a single stage process. The effect of post-deposition treatments at 400 °C and 500 °C by indium bromide vapor were studied and compared to the effect of a simple annealing under selenium. Structural, electrical, and chemical analyses demonstrate that there is a drastic difference between the different types of annealing, with the ones under indium bromide leading to much larger grains and higher conductivity. These properties are associated with a modification of the elemental profiles, specifically for gallium and sodium.