Engineering Commons^™

Separation Of Copper And Zinc On Synthetic Resins, Ernest Joseph Breton

Masters Theses

"It was desired to know whether ion exchange resins could be of value to the metallurgist in the recovery and separation of metals. The recovery and separation of copper and zinc from dilute solutions on Amberlite IRC-50, a carboxylic resin, and Amberlite IR-120, a nuclear sulfonic resin, were investigated. It was found that Amberlite IRC-50 could effectively remove copper ions from a solution of copper and zinc. Amberlite IR-120, due to the strong sulfonic acid groups, exhibited only a slight preference for copper as compared to zinc. It would seem that a judicious choice of resins coupled with appropriate chemistry …

Construction And Operation Of A Vacuum Retort Pilot-Plant For Distillation Of Alloys, Robert Frederick Doelling

Masters Theses

"The widespread appearance of large scale vacuum systems operating commercially in the micron range of pressures has initiated a new field of industrial endeavor, vacuum engineering. The ever increasing number of applications of vacuo in commercial processes and laboratory research has stimulated the design and improvement of vacuum equipment, and at the present time equipment may be obtained to meet practically any need. In turn, the variety of available tools has directed the engineers attention to improving old processes and developing new ones through the utilization of vacuum techniques ... The possibility of producing a relatively high purity silver in …

The Nature Of Molecular Films Of Oleic Acid On Quartz, Kenneth Lee Keating

Masters Theses

"The purpose of this research was to show the nature of oleic acid on quartz mineral by transferring calcium oleate films, known to be monomolecular and of a definite orientation, to the surface of a piece of quartz, and measuring the resulting coated mineral by contact angle technique"--Introduction, page 1.

A Study Of Missouri Flint Clay, Edmond Preston Hyatt

Masters Theses

"The problem is one of attempting to explain the peculiar nature of Missouri Flint Clay and to expand the knowledge concerning it. Among the questions for which answers are sought are: What makes Missouri Flint Clay so hard? What happens to Missouri Flint Clay when it is ground? What is the mineralogical constitution of Missouri Flint clay?"--Introduction, The Problem, page 1.

The Volatility Of Metallic Sulfides And Their Treatment By Vacuum Metallurgy, Chi-Mei Hsiao

Doctoral Dissertations

"The purpose of this investigation is to determine the vapor pressure or volatility of the sulfides of the following metals by Langmuir's method: a) Zinc b) Cadmium c) Mercury d) Manganese e) Tin f) Lead g) Arsenic h) Antimony i) Molybdenum J) Iron k) Cobalt l) Nickel m) Copper n) Silver o) Calcium p) Aluminum.

The relation of this property to the position of the metals in the periodic table will be discussed, thus the vapor pressure or volatility of the remaining metals can be predicted as to the order of magnitude if the law of periodicity holds.

The possible …

A Study Of The Dissolution Of Titanium In Acids With Emphasis On Hydrofluoric Acid, Ping-Chao Chen

Doctoral Dissertations

"Titanium is practically a new metal. Although it was discovered by W. Gregor in 1791, the pure metal was not prepared until 1910 by M. A. Hunter, and it is only very recently that tremendous interest has been focused on this new metal, as evidenced by the activities of numerous leading laboratories and pilot plants.

The reasons that Ti is gaining increasing attention may be attributed to the natural abundance of Ti ores in reasonable concentration and, what is more important, to its unusual combination of physical and chemical properties. According to F. W. Clark’s classical geochemical data, Ti amounts …

Solid Solution In The Series Sodium Tungsten Bronze, Lithium Tungsten Bronze And Tungstic Oxide, Godrej F. Doctor

Masters Theses

"The tungsten bronzes are a series of anionic substitutional solid solutions of alkali metal metatungstates and tungstic oxide. They are neither alloys nor intermetallic compounds, the term tungsten bronzes was adopted because of their remarkable metallic properties, e.g. luster, specific gravity and especially high electrical conductivity, which resembles to that of graphite. Due to its chemical inactivity and beautiful shades of color, it is used as a coating, especially in the plastic industry and for other ornamental products. The properties and the structure of these bronzes have not been investigated entirely satisfactory; within the last twenty years, only a few …

Measurement Of Flotation Rate As A Function Of Particle Size, Thomas Martin Morris

Doctoral Dissertations

“The Problem. The rate of flotation of solid particles determines the percentage recovery of these particles which can be obtained during a given time interval. An examination of operating data from a flotation plant shows that percentage recovery varies with the size of particle.

Many investigators have explored the problem of measuring flotation rate. In most cases the results obtained were expressed qualitatively. The results obtained by one worker were often at variance with results reported by another worker.

This investigation was undertaken with the object of (1) quantitatively measuring the rate of flotation of various sizes of particles and …

A Study Of Cast Eutectic Structures By Means Of Optical And X-Ray Microscopy, John Stanton Winston

Masters Theses

"The present research is the result of interest in two rather broad, and at first thought, seemingly entirely separate topics: the structure of eutectics and x-ray microscopy. D. Hanson in 1923 in his correspondence with Albert M. Portevin in regard to his article on the structure of eutectics states, "A point that always stuck him (D. Hanson) in examining eutectics was that one of the constituents always formed a continuous phase round the other one. The orientation of one constituent was either constant or varied in a uniform manner. What, however, was the condition of the 'enveloped' constituent, which formed …

An Experimental Study Of Crystallization In Opal Glass, William C. Rous

Masters Theses

"Opal glasses are well known from use in such forms as ointment jars, lighting globes, wall panelling [sic], and decorative effects in glass vases. Cryolite, fluorspar, and sodium fluosilicate are used in varying proportions in most glasses of this type. Since little is known of the mechanism of crystallization in opal glass, there is a definite need of gathering further information on this subject. This information is of particular interest to the manufacturers whose products consist of this type of glass. Further information would aid in control of the characteristics desired and perhaps would allow a more economical control"--Introduction, page …

The Transformation Of The Aluminum-Zinc Eutectoid Alloy At Subcritical Temperatures, Thomas Joseph Burke

Masters Theses

"Interest in the mechanism of the austenite eutectoid transformation in iron-carbon alloys, especially as produced by the isothermal sub-critical techniques introduced by Davenport and Bain, has resulted in the application of similar heat treatment studies to the eutectoid transformations in other alloy systems. The study of the eutectoid transformation is of both fundamental and industrial interest because past experience has shown that these studies yielded much information concerning the nature and mechanism of the changes in eutectoid alloys during the decomposition of the phase stable at high temperatures and has also contributed much toward the development of new properties to …

Separation Of Cobalt From Zinc Sulfate Solutions By Synthetic Cation Exchange Resins, Wen-Hsiang Chang

Masters Theses

"The purpose of the present research is primarily to investigate the possibility of the separation and recovery of cobalt from zinc sulfate solutions by means of cation exchange resins. It is thought that such an investigation, seemingly of academic interest, might throw some light on determining the possibility of processing some industrial solutions containing both cobalt and zinc. Cobalt, for instance, has been well known as one of the most detrimental impurities in zinc electrolytic solutions. In spite of various purification treatments, small amounts of cobalt are often present in the electrolytic solution, causing a reduction in current efficiency and …

A High-Temperature X-Ray Diffraction Camera And Its Application To Copper And Titanium, Robert R. Penman

Masters Theses

"The purpose of this research was threefold, and consists of the following sections: 1. Effective use of a high temperature x-ray camera, capable of reaching temperatures of 1000 ºC. 2. Investigation of the thermal dilation of certain cubic metals. 3. Accurate determination of the lattice constant (aₒ) of Beta Titanium at 900 ºC "--Introduction, page 1.

A Study Of Relative Ionic Mobility Of Alkali Ions In Dilute Alkali-Boron Trioxide Glasses As Deduced From Space Charge Considerations, Theodore J. Planje

Doctoral Dissertations

"The extensive investigations in the past have conclusively established that the alkali ions are responsible for the electrical conductivity of glass in both the brittle and viscous states; however, with the exception of one investigation in the brittle state, little consideration has been given to determination of the mobility of the alkali ion in such glassy systems. A review of the literature pertaining to the electrical conductivity of glass is presented.

A method, based on the rate of development of the ionic space charge responsible for polarization of conductivity cell employing direct current voltages, is proposed as a means for …

The Potassium Tungsten Bronzes, Ching Hou Ma

Masters Theses

"The tungsten bronzes are a series of substitutional solid solutions of alkali or alkaline earth metatungstates and tungstic oxides. They are not really metallic alloys or intermetallic compounds but they possess some marked metallic properties such as metallic luster, good electric conductivity, high specific gravity, etc. For this reason the name of "bronzes" is applied to them"--Introduction, page 1.

Purification Department Of Zinc Leaching Division At Anaconda, Montana, J. L. Brown

Bachelors Theses and Reports, 1928 - 1970

The original smelter, known as the Upper Works smelter, was located on the north side of the Warm Springs Creek, just 2 miles east of the city of Anaconda and 26 miles from the city of Butte. By the year 1894 this smelter had a capacity of 500 tons of ore a day.

The Vanadium Plant Of The Anaconda Reduction Works, Tom Liss

Bachelors Theses and Reports, 1928 - 1970

No complete history of mining and smelting will ever be written that does not include a major discussion of the Butte district. The colorful tale of this area plays a major role in the interesting stories of mining. In the fields of mining methods, labor relations end financial manipulations, the Butte area has set a standard.

A Study Of The Differential Seperation Of Galena And Sphalerite, Wilfred E. Nagel

Bachelors Theses and Reports, 1928 - 1970

The smelting of complex lead ores is a difficult operation, especially when they contain considerable amounts of iron and zinc. When these ores are smelted, all of the zinc, which is valuable and well worth recovering, goes into the slag. With the advent of the flotation processes, and the ability of these processes to concentrate the lead and zinc minerals into separate products, the smelting of complex lead ores was to a great extent simplified.

The Christensen Sillimanite Deposit Southeast Of Dillon, Montana, Everett O. Bracken

Bachelors Theses and Reports, 1928 - 1970

The minerals sillimanite, kyanite, andalusite, dumortierite, and topaz comprise a group of minerals whose high alumina content and physical properties are particularly desirable in the manufacture of refractory products. Sillimanite is the least plentiful of the minerals of this group, and for this reason it is not used extensively at the present time. However, it would be very desirable to the refractory industry if a suitable domestic source of supply could be established.

A Mineral Dressing And Economic Study Of A Complex Arsenical Ore, Luigi D. Piana

Bachelors Theses and Reports, 1928 - 1970

The factors that influence the choice of a method for treat­ment of an ore comprise the technical and economic limitations and advantages, derived in detail and balanced according to the exigencies of the particular situation.

Separation Of Cadmium From Zinc In The Purification Step Of The Leaching Cycle, L. C. Powell

Bachelors Theses and Reports, 1928 - 1970

The purpose of this investigation is to determine the effect of the factors listed previously by conducting a series of tests that will indicate the ex­tent to which the purification is influenced by time, temperature, zinc oust size, zinc dust quantity, iron concentration, two stage precipitation, and aeration.

An Investigation Of The Precipitation Of Cobalt With Zinc Dust, Lyle Hallberg

Bachelors Theses and Reports, 1928 - 1970

Cobalt, as well as copper, cadmium, and other impurities, is removed by selective precipitation with zinc during the zinc electrolyte purification cycle, and the purification residue may be treated by a Cadmium Plant for the recovery of cadmium.

Construction And Operation Of A Laboaratory Size Thum Cell, Raymond Dugdale

Bachelors Theses and Reports, 1928 - 1970

Electrolytic silver refining was not perfected until the end of the nineteenth century. During the process of development, two systems of silver refining have come into prominence: the Moebius and the Thum types.

An Investigation Into The Precipitation Of Copper From Mine Water, Using Sulfur Dioxide To Reduce The Ferric Ion Content, David S. Gleason

Bachelors Theses and Reports, 1928 - 1970

The experiments which were preformed showed that sulfur dioxide would reduce the ferric ion content of the mine waters to a very low figure. The reduction in the ferric ion content would improve the efficiency of the precipitation process, and also increase the recovery of copper.

Application Of The Electric Furnace To The Melting Of Cathode Copper At The Tacoma Smelter, Alvin H. Nelson

Bachelors Theses and Reports, 1928 - 1970

In the field of copper metallurgy, the major chang­es effected in the original metallurgical scheme have been based largely upon the lowering in grade of copper ores, and the more particular demands of the fabricators of the metal. The former trend fostered the development of mineral beneficiation, which in turn caused the con­version from blast furnace to reverberatory furnace smelting.

An Investigation Of Silicon Impregnation Of Low-Carbon Steels, Thomas E. Groce

Bachelors Theses and Reports, 1928 - 1970

A problem of metallurgy during the last part of the Nineteenth and the early Twentieth Century, and one that stood very near the front, was investigations of methods to produce a non-corrosive surface on iron and steel without affecting the physical properties of these base metals.

Aluminum - Bronze Compacts And Their Possible Use As A Bearing Material, Donald J. Mcmaster

Bachelors Theses and Reports, 1928 - 1970

In the modern aspect of powder metallurgy, the first use of a sintering process was in making filaments for incandescent electric lamps.In the short while from the day of Edison to the pres­ent, the science of working with metal powders has advanced by leaps and bounds.

A Study Of The Transformation Of A Twenty-Eight Per Cent Tin Bronze, Perry A. Boukind

Bachelors Theses and Reports, 1928 - 1970

In this investigation, attention is directed to the phases covered by a 28 per cent tin alloy. When the investigation was started, consideration was given to the possibility of making a Time - Temperature - Transformation curve for this parti­cular alloy. As the work progressed and further research was carried on, this phase of the work was abandoned.

Caustic Leaching Of Montana Chromite, Chester Freshour

Bachelors Theses and Reports, 1928 - 1970

Chromite is the most important ore used for the production of chromium and chromium alloys. At present, the domestic production is insignificant as compared with the amount of chromite consumed in the United States.

The Characteristics Of The Electrolyte In The Series System Of Electrolytic Copper Refining, Carl W. Howald Jr.

Bachelors Theses and Reports, 1928 - 1970

Almost everyone is familiar with the tremendous importance of copper in our everyday life. One of the pro­perties of copper which determines its great usefulness to mankind is its electrical conductivity. This property alone has more to do with the prominence of copper among useful metals then does any other.