Synthesis And Electrochemical Property Of Li2Fesio4/C Cathode Material By Solid State Method,
2013
School of Chemistry and Material Science, Guizhou Normal University, Guiyang 550001, Guizhou, China;
Synthesis And Electrochemical Property Of Li2Fesio4/C Cathode Material By Solid State Method, Jiao-Li Sun, Zhi-Jiao Chen, Yi-Xiao Li, Hu Cheng
Journal of Electrochemistry
Li2FeSiO4/C cathode material was synthesized using Li2SiO3 and FeC2O4 as raw materials by solid state method. The structure and morphology of the material were characterized by XRD and SEM. The electrochemical properties of the material were studied by constant-current cyclic testing. The results show that Li2FeSiO4/C has a good electrochemical performance. The first discharge capacity of Li2FeSiO4/C cathode material at 30oC reached 167 mAh∙g-1 when cycled at 10 mA∙g-1 between 1.5 and 4.8 V.
Electrochemical Na-Storage Materials And Their Applications For Na-Ion Batteries,
2013
1. Department of Chemistry, Wuhan University, Wuhan, 430072, Hubei, China
Electrochemical Na-Storage Materials And Their Applications For Na-Ion Batteries, Jiang-Feng Qian, Xue-Ping Gao, Han-Xi Yang
Journal of Electrochemistry
Oncoming large scale electric energy storage (EES) requires battery systems not only to have sufficient storage capacity but also to be cost-effective and environmentally friendly. Li-ion batteries for widespread EES applications may be limited due to the constraint of global lithium resource. From the considerations of available resources and environmental impact, Na-ion batteries have potential advantages as next generation secondary batteries and an alternative to Li-ion batteries. However, in the present state of the art, the Na-storage cathodes reported so far are still deficient both in energy density and power capability, while the carbon and alloy anodes for Na-ion batteries …
Surface Composition Structure And Electrochemical Performance Of Aluminum Doped Lifepo4,
2013
College of Environmental and Energy Engineering, Beijing University of Technology, Beijing 100022, P. R. China;
Surface Composition Structure And Electrochemical Performance Of Aluminum Doped Lifepo4, Huai-Fang Shang, Wei-Feng Huang, Wang-Sheng Hu, Ding-Guo Xia, Zi-Yu Wu
Journal of Electrochemistry
Despite there are many successful reports about the preparation of electrode materials with surface coating for lithium ion batteries, the study in surface self-coating of cathode materials using segregation of doping elements and their electrochemical properties is still very rare. The LiFePO4 particles with rich-Al on the surface were synthesized by one step solvothermal route. TEM results demonstrated that the surface of the obtained LiFePO4 particles was well-covered by the amorphous coating. The soft X-ray absorption spectroscopy (XAS) and Auger electron spectroscopy (AES) component analyses revealed that the amorphous coating was composed of LiFe1-xAlxPO …
Free-Troposphere Ozone And Carbon Monoxide Over The North Atlantic For 2001-2011,
2013
Michigan Technological University
Free-Troposphere Ozone And Carbon Monoxide Over The North Atlantic For 2001-2011, Aditya Kumar, S. Wu, M. F. Weise, R. Honrath, R. C. Owen, D. Helmig, L. Kramer, M. Val Martin, Q. Li
Michigan Tech Publications, Part 1
In situ measurements of carbon monoxide (CO) and ozone (O3) at the Pico Mountain Observatory (PMO) located in the Azores, Portugal, are analyzed together with results from an atmospheric chemical transport model (GEOS-Chem) and satellite remote sensing data (AIRS (Atmospheric Infrared Sounder) for CO, and TES (Tropospheric Emission Spectrometer) for O3) to examine the evolution of free-troposphere CO and O3 over the North Atlantic for 2001-2011. GEOS-Chem captured the seasonal cycles for CO and O3 well but significantly underestimated the mixing ratios of CO, particularly in spring. Statistically significant (using a significance level of 0.05) decreasing trends were found for …
Enhanced Dna Sensing Via Catalytic Aggregation Of Gold Nanoparticles,
2013
Boise State University
Enhanced Dna Sensing Via Catalytic Aggregation Of Gold Nanoparticles, Herbert M. Huttanus, Elton Graugnard, Bernard Yurke, William B. Knowlton, Wan Kuang, William L. Hughes, Jeunghoon Lee
Materials Science and Engineering Faculty Publications and Presentations
A catalytic colorimetric detection scheme that incorporates a DNA-based hybridization chain reaction into gold nanoparticles was designed and tested. While direct aggregation forms an inter-particle linkagefrom only one target DNA strand, catalytic aggregation forms multiple linkages from a single target DNA strand. Gold nanoparticles were functionalized with thiol-modified DNA strands capable of undergoing hybridization chain reactions. The changes in their absorption spectra were measured at different times and target concentrations and compared against direct aggregation. Catalytic aggregation showed a multifold increase in sensitivity at low target concentrations when compared to direct aggregation. Gelelectrophoresis was performed to compare DNA hybridization reactions …
Synthesis Of Tungsten Oxide Nanowires Onto Ito Glass Using T-Cvd,
2013
Graduate Institute of Electro-Optical Engineering, National Taiwan University of Science and Technology, Taipei 106, Taiwan, R.O.C.
Synthesis Of Tungsten Oxide Nanowires Onto Ito Glass Using T-Cvd, Tomy Abuzairi, Bohr-Ran Huang, Tzu-Ching Lin
Makara Journal of Technology
Tungsten oxide is an n-type semiconductor with interesting physical and chemical properties that make it suitable for various technological applications. Tungsten oxide nanowires were synthesized not only at low temperature but also without the use of any catalysts. The tungsten oxide nanowires were synthesized at 550 °C with tungsten layers onto the ITO glass using thermal chemical vapor deposition (T-CVD). The SEM image shows that the tungsten oxide nanowires are effectively grown with the 200 nm tungsten film. The Raman spectra shoulder at ~690 cm-1 proves the synthesized of tungsten oxide nanowires.
Radiation Characteristics Of A Planar Strip Dipole Antenna And A Slot Dipole Antenna For Thz Applications,
2013
Antenna Propagation and Microwave Research Group (AMRG), Department of Electrical Engineering, Faculty of Engineering, Universitas Indonesia, Depok 16424, Indonesia
Radiation Characteristics Of A Planar Strip Dipole Antenna And A Slot Dipole Antenna For Thz Applications, Catur Apriono, Eko Tjipto Rahardjo
Makara Journal of Technology
The development of a THz system often requires a device that is used to radiate or detect THz waves. One way to fulfill this requirement is to use an antenna. Therefore, we need to consider the radiation characteristics of an antenna working in the THz region. In this paper, we present simulation study of two dipole antennas, i.e. a planar strip dipole antenna and a slot dipole antenna. The simulation results show that a planar strip dipole antenna has a better radiation efficiency (more than 95%) compared to the slot dipole. It also shows that an efficiency of more than …
The Effect Of Pressing Temperature And Time On The Quality Of Particle Board Made From Jatropha Fruit Hulls Treated In Acidic Condition,
2013
Major of Forestry, Faculty of Agriculture, North Sumatera University, Medan 20155, Indonesia
The Effect Of Pressing Temperature And Time On The Quality Of Particle Board Made From Jatropha Fruit Hulls Treated In Acidic Condition, Apri Heri Iswanto, Fauzi Febrianto, Yusuf Sudo Hadi, Surdiding Ruhendi, Dede Hermawan
Makara Journal of Technology
The high of pH of jatropha fruit hulls causes the negative properties of particleboard made from this material. Adjusting the particle acidity and pressing conditions (temperature and time) is among the technical modifications available to improve this particleboard’s properties. Particle acidity has been adjusted in a previous research project, and immersing the particles in acetic acid was found to be the best treatment in this preliminary research. In order to improve the particleboard’s properties, an experiment was conducted to determine the best pressing temperature and time. The objective of the research was to evaluate the influence of pressing temperature and …
Nd–Fe–B Nanoparticles Through Surfactant Assisted Mechanical Milling And Alloy Design,
2013
University of Nebraska-Lincoln
Nd–Fe–B Nanoparticles Through Surfactant Assisted Mechanical Milling And Alloy Design, Jordann M. Bornhoft
Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research
Surfactant-assisted mechanical milling has been used to produce discrete nanoparticles of both Nd-Fe-B and Sm-Co amenable for bottom-up production of nanostructured or nanocomposite permanent magnets. However, in Nd-Fe-B the comminution of the material proceeds by transgranular fracture, which influences both the morphology of the nanoparticles and the magnetic properties. This paper utilizes alloy design to alter the fracture behavior from transgranular fracture to intergranular fracture. Nd-rich Nd2Fe14B alloys were produced by melt spinning in an overquenched state. The melt spun ribbons were annealed at 700°C and 800°C to ensure complete crystallization and to form different grain …
Microgrid Development Using A Grid Tie Inverter,
2013
Faculty of Engineering, Universitas Indonesia, Depok 16424, Indonesia
Microgrid Development Using A Grid Tie Inverter, Hartono Budi Santoso, Budiyanto Budiyanto
Makara Journal of Technology
The use of renewable energy sources (RES), especially photovoltaic (PV), to meet the demand of electrical energy has been getting a great deal of attention as an alternative solution to electrical energy deficit problems. RES are being applied in power systems in a variety of configurations including microgrid systems. One of the characteristics of a microgrid is capability to supplying power to grid when there is an excess power to supply local load. This research examines the chances of saving power consumption from grid using power converters grid tie inverter (GTI) in a microgrid configuration. The test is done by …
Surface Treatment Of Fly Ash For Improving The Tensile Strength Of Fly Ash/Unsaturated Polyester Composites,
2013
Department of Mechanical Engineering, Faculty of Engineering, University of Mataram, Mataram 83125, Indonesia
Surface Treatment Of Fly Ash For Improving The Tensile Strength Of Fly Ash/Unsaturated Polyester Composites, Sugiman Sugiman, Paryanto Dwi Setyawan
Makara Journal of Technology
The paper presents the surface treatment of fly ashes using acid and alkali solution on the tensile strength of the fly ash/unsaturated polyester (UP) composites. Sulfuric acid (H2SO4), hydrofluoric acid (HF) and sodium hydroxide (NaOH) solution with concentration of 0%, 5%, 10%, 15%, and 20% (by weight) were used for surface treatment of fly ashes. Generally, the tensile strength of the treated fly-ash/UP composites shows a significant increase compared to the untreated fly ash. Of all surface treatments studied, the optimum tensile strength was obtained at a concentration of 10%. At this concentration, at a fly ash content of 30% …
Recycling Roof Tile Waste Material For Wall Cover Tiles,
2013
Interior Design Department, Letters and Visual Arts Faculty, Sebelas Maret University, Surakarta 57126, Indonesia
Recycling Roof Tile Waste Material For Wall Cover Tiles, Ambar Mulyono, Silfia Mona Aryani, Joko Lulut
Makara Journal of Technology
Prior research on roof tile waste treatment has attempted to find the appropriate technology to reuse old roof tile waste by create wall cladding materials from it. Through exploration and experimentation, a treatment method has been discovered to transform the tile fragments into artificial stone that resembles the shape of coral. This baked clay artificial stone material is then processed as a decorative element for vertical surfaces that are not load-bearing, such as on the interior and exterior walls of a building. Before applying the fragments as wall tiles, several steps must be taken: 1) Blunting, which changes the look …
Semiconductor Thermal Neutron Detector,
2013
Research Institute of Electronics, Shizuoka University, Hamamatsu, Shizuoka 432-8011, Japan
Semiconductor Thermal Neutron Detector, Toru Aoki, Aki Miyake, Takayuki Nakano, Akifumi Koike, Hisashi Morii, Hidenori Mimura
Makara Journal of Technology
The CdTe and GaN detector with a Gd converter have been developed and investigated as a neutron detector for neutron imaging. The fabricated Gd/CdTe detector with the 25 mm thick Gd was designed on the basis of simulation results of thermal neutron detection efficiency and spatial resolution. The Gd/CdTe detector shows the detection of neutron capture gamma ray emission in the 155Gd(n, g)156Gd, 157Gd(n, g)158Gd and 113Cd(n, g)114Cd reactions and characteristic X-ray emissions due to conversion-electrons generated inside the Gd film. The observed efficient thermal neutron detection with the Gd/CdTe detector shows its promise in neutron radiography application. Moreover, a …
Corrosion Behavior Of Tialn Film On Aisi 4140 Steel,
2013
Chulalongkorn University
Corrosion Behavior Of Tialn Film On Aisi 4140 Steel, T Wongpinij, P Wongpanya, C Euaruksakul, P Photongkam, N Witit-Anun
Journal of Metals, Materials and Minerals
The corrosion behavior of uncoated and TiAlN coated on AISI 4140 steel were studied by an electrochemical technique in 3.5 wt% NaCl solution at pH value of 2, 7 and 10 at room temperature. The corrosion potential (Ecorr), pitting potential (Epit), corrosion rate (Rmmy) and passive region in polarization curves were analyzed and compared.After electrochemical testing, samples surface was characterized by scanning electron microscopy (SEM) with energy dispersive X-ray analysis (EDX) and X-ray photoemission electron microscopy (X-PEEM). The results indicated that the TiAlN coated samples yielded better corrosion resistance than the uncoated samples. The coated samples had lower corrosion rate …
Dolomite Stabilized Zirconia For Refractory Application : Part-I Phase Analysis, Densification Behavior And Microstructure Of Partial Stabilized Zirconia,
2013
Chulalongkorn University
Dolomite Stabilized Zirconia For Refractory Application : Part-I Phase Analysis, Densification Behavior And Microstructure Of Partial Stabilized Zirconia, R Prasad Rana, P Kumar, A Suvrajit Bal
Journal of Metals, Materials and Minerals
In the continuous casting of steel, Zircon and Zirconia based products are used due to its high thermal stability, excellent erosion resistance, self-opening, consistent casting speed and resistance to oxygen lancing during casting for removal of inclusion clogging and to streamline the flow. Higher casting sequences of molten steel CaO or MgO stabilized zirconia nozzles were being used and for industrial application point of view, dolomite stabilized zirconia (DSZ) could be a better substitute for the stabilization of zirconia. DSZ samples were prepared having 3,4,5,6 and 7 mole % of dolomite by solid state route using high purity monoclinic zirconia …
Mineralogical Characterization Of Pozuzo District's Soils Through Physical Techniques,
2013
Chulalongkorn University
Mineralogical Characterization Of Pozuzo District's Soils Through Physical Techniques, M L Cerón Loayza, J B. Cabrejos, F Reyes Navarro
Journal of Metals, Materials and Minerals
We introduce a study on soils in three different fields of plantations in Pozuzo District, Oxapampa province, Peru. Two of the fields are cultivated and the third one has a degradation problem. In situ, in all, we collected 29 samples in the three plantations. We utilized analytical and physical techniques, namely, energy dispersive X-ray fluorescence, X-ray diffractometry, and transmission Msbauer spectroscopy; we complemented our research with a physical-chemical analysis to determine texture, pH, content of organic matter and cation interchange capacity. For all analyzed samples, the results of the analysis by energy dispersive X-ray fluorescence show the presence of the …
Friction And Wear Of Polytetrafluoroethylene/Graphene Oxide Composite Thin Films,
2013
University of Arkansas, Fayetteville
Friction And Wear Of Polytetrafluoroethylene/Graphene Oxide Composite Thin Films, Justin Kyle Carter
Graduate Theses and Dissertations
Polytetrafluoroethylene (PTFE) is a commonly used solid lubricant due to its low coefficient of friction and chemical inertness. As a polymer, PTFE suffers from high wear and low adhesion to substrates limiting its use as a thin film. Thin PTFE films are ideal candidates for solid lubrication in micro-machines and bearing applications. The main goal of this work is to enhance the durability of thin PTFE films through the addition of few layered graphene oxide (GO) as filler. In order to address adhesion issues, the addition of an adhesive layer of polydopamine (PDA) between stainless steel substrates and thin PTFE …
Crack Growth Behavior Under Creep-Fatigue Conditions Using Compact And Double Edge Notch Tension-Compression Specimens,
2013
University of Arkansas, Fayetteville
Crack Growth Behavior Under Creep-Fatigue Conditions Using Compact And Double Edge Notch Tension-Compression Specimens, Santosh B. Narasimha Chary
Graduate Theses and Dissertations
The American Society for Testing and Materials (ASTM) has recently developed a new standard for creep-fatigue crack growth testing, E 2760-10, that supports testing compact specimens, C(T), under load controlled conditions. C(T) specimens are commonly used for fatigue and creep-fatigue crack growth testing under constant-load-amplitude conditions. The use of these specimens is limited to positive load ratios. They are also limited in the amount of crack growth data that can be developed at high stress intensity values due to accumulation of plastic and/or creep strains leading to ratcheting in the specimen. Testing under displacement control can potentially address these shortcomings …
Au-Based Core-Shell Nanoparticles For Direct Formic Acid Fuel Cells,
2013
University of Texas at Arlington
Au-Based Core-Shell Nanoparticles For Direct Formic Acid Fuel Cells, Chiajen Hsu
Material Science and Engineering Dissertations - Archive
Unique Au/Pd core-shell nanoparticles were synthesized via galvanic replacement of Cu by Pd on hollow Au nanoparticles. Au/PtCu core-shell nanoparticles were also synthesized using this method. These core-shell nanoparticles exhibited unique electrochemical properties - the Au/Pd nanoparticles demonstrated superior electrochemical activity for formic acid oxidation and the Au/PtCu nanoparticles improved the kinetics in oxygen reduction reaction, when compared to their corresponding pure metal particles. In this dissertation, we aim at investigating catalytic abilities of these core-shell nanoparticles and understanding electrochemical reactions in direct formic acid fuel cells.Different Pd thicknesses on hollow Au nanoparticles in the core-shell configuration have been investigated. …
Grain Structure Evolution Of Tin-Based Lead-Free Solder Joints In Electronic Packaging Assembly And Its Impact On The Fatigue Reliability,
2013
University of Texas at Arlington
Grain Structure Evolution Of Tin-Based Lead-Free Solder Joints In Electronic Packaging Assembly And Its Impact On The Fatigue Reliability, Huili Xu
Material Science and Engineering Dissertations - Archive
Solder is one of the main joints materials used in the electronics for decades of years. It is not only the mechanical support but also conducts the electric signals in the electronics. However, the regulation of lead content in electronic devices has driven the transition from lead-tin solder to the lead-free solder that requires lots of research to fill the knowledge gap in the lead-free solder property. At the same time, the reliability issues due to solder failure are of great interest as the miniaturization and mobilization trend of the electronic devices continues. A lot of works have been done …
