Engineering Commons^™

An Investigation Of Initially Delaminated Composite Sandwich With Delamination Arrest Mechanism Under Buckling Loading, Tony D. Tran

Master's Theses

This thesis involves the development of a fiberglass-foam composite sandwich structure with the introduction of delamination arrestment keys; therefore, a study of an initially delaminated composite sandwich structure was the experimental analysis on multiple configurations in how the arrestment keys are placed.

The first part of this thesis research was to the experimental design and manufacturing of the composite sandwich plates. These plates were later cut down to the specific test dimensions and manufacturing processes for the composite sandwich plates and test specimens were created. The composite sandwich plates were manufactured using a vacuum resin infusion process. The dimensions of …

Analyzing The Impact Of Reactive Transport On The Repository Performance Of Triso Fuel, Gregory Schmidt

UNLV Theses, Dissertations, Professional Papers, and Capstones

One of the largest determiners of the amount of electricity generated by current nuclear reactors is the efficiency of the thermodynamic cycle used for power generation. Current light water reactors (LWR) have an efficiency of 35% or less for the conversion of heat energy generated by the reactor to electrical energy. If this efficiency could be improved, more power could be generated from equivalent volumes of nuclear fuel. One method of improving this efficiency is to use a coolant flow that operates at a much higher temperature for electricity production. A reactor design that is currently proposed to take advantage …

Chemical And Electronic Structure Of Surfaces And Interfaces In Compound Semiconductors, Sujitra Pookpanratana

UNLV Theses, Dissertations, Professional Papers, and Capstones

The interface formation between two different materials is important in applications for optoelectronic devices. Often, the success or performance of these devices is dependent on the formation of these heterojunctions. In this work, the surface and interfaces in such materials for optoelectronic devices are investigated by a suite of X-ray analytical techniques including X-ray photoelectron (XPS), X-ray excited Auger electron (XAES), and X-ray emission (XES) spectroscopies to provide novel insight.

For the group III-nitrides (e.g., AlxGa1-xN) used in many light emitting devices, a significant challenge exists to form an Ohmic contact. The electron affinities and band gaps of GaN and …

Electrochemical Detection For The Corrosion Of Reinforcing Steel In Concrete During Immersion And Drying Cycles, Bing-Li Jia, Fa-He Cao, An-Na Chen, Jian-Qing Zhang

Journal of Electrochemistry

The corrosion behavior of reinforcing steel in concrete under dry-wet cycle condition has been studied by electrochemical noise(EN) compared with the electrochemical impedance spectroscopy(EIS),SEM micrographs and EDS.The statistical method has been employed to analyze the EN data of reinforcing steel in concrete,which revealed three different corrosion stages of reinforcing steel in concrete,including the dissolution of the passive film,the active corrosion and the cumulation of corrosion product.The wavelet transform has also been employed,which indicated that steel in concrete with pH 1 is associated with uniform corrosion,while steel in concrete with pH 3 and pH 7 are associated with localized corrosion,such as …

Preparation And Characterization Of The Silane-Phosphonic Acid Composite Passivation Coating For Electrogalvanized Steel, Yong Guan, Jian-Guo Liu, Chuan-Wei Yan

Journal of Electrochemistry

A new silane-phosphonic acid composite passivation coating process has been developed for the protection of electrogalvanized steel based on N-(β-aminoethyl)-γ-aminopropyltrimethoxysilane(AAPTMS),γ-(2,3-epoxypropoxy)propyltrimethoxy-silane(GPTMS) and 1-hydroxy ethylidene-1,1-diphosphonic acid(HEDP).The results of X-ray photoelectron spectroscopy(XPS),Fourier transform infrared spectroscopy(FTIR),potentiodynamic polarization scan,electrochemical impedance spectroscopy(EIS) and neutral salt spray(NSS) tests indicated that the major structure of the prepared silane-phosphonic acid composite passivation coating consisted mainly of Si—O—Si and Si—O—P bonds.The area of white rust was not more than 5% of the total panal after 120 h NSS test,which could be compared favourably with the chromate colour passivation coating.However,the corrosion reaction on the anode of the silane-phosphonic acid composite passivation …

Initial Stage Of Atmospheric Corrosion Of Ndfeb(M35) In A Simulated Marine Atmosphere, Chun-Ling Li, Yuan-Tai Ma, Ying Li, Fu-Hui Wang

Journal of Electrochemistry

This study detailed the atmospheric corrosion behaviour of sintered NdFeB(M35) in a simulated marine atmosphere with 80% relative humidity(RH).The dissolution and subsequent reaction of NaCl particles cause the attack of NdFeB.The corrosion presented three representative types:if the electrolyte covered magnetic phase and Nd-rich phase,the Nd-rich phase was corroded firstly due to galvanic effect;if the electrolyte covered magnetic phase,magnetic phase was corroded along the grain boundary;if the electrolyte located near the position of defects,corrosion progressed along with the defect because of low concentration of oxygen inside the defect.With corrosion progressing,local corrosion areas were mutually connected,with Nd-rich phase and grain boundary being …

Electrodeposition Of Lead Dioxide From Dluoroborate Solutions, Chun-Mei Kong, Yong-Ming Tang, Wen-Zhong Yang, Xiao-Yuan Yang

Journal of Electrochemistry

The PbO2 anodes were prepared on platinum from fluoroborate media and its doped solutions by electrodeposition technique.Elecchemical and pysicochemical properties of these PbO2 films were studied by cyclic voltammetry methods,XRD and SEM.The results showed that the presence of BF4-increased PbO2 electrodeposition rate;the prepared lead dioxide consisted of β-PbO2;the preferential orientation of crystals and surface morphology were affected a lot by doping F-and Fe3+.The FB/F-Fe-PbO2 electrode exhibited regular-shaped layers with compact morphology.Furthermore,increasing current density also change the preferential orientation of PbO2 crystals.

The Sol-Gel Synthesis And Electrochemical Performance Of Li_3v_2(Po_4)_3/C Cathode Material For Lithium Ion Battery, Li-Ying Liu, Lian Chen, Hai-Yan Zhang, Yu-Chun Zhai

Journal of Electrochemistry

Li3V2(PO4)3/C was synthesized by sol-gel method with citric acid as chelate and C sources.Physical and electrochemical performances of as-prepared materials were characterized through XRD,SEM and galvanostatic charge-discharge tests,etc.The results showed that products produced by calcining at 800 ℃ for 12 h had a single phase crystal structure and relatively small particle sizes with uniform distribution.At 0.1 C,0.5 C and 1 C,the initial specific discharge capacities were 153.0,143.1 and 130.6 mAh·g-1,respectively,and capacity efficiencies were 93.1%,85.4% and 77.3% after 50 cycles,respectively.Charge efficiencies were all above 80% and discharge voltages were higher.

Study On Preparing Technology And Corrosion Resistance Of Ti/Zr Based Chromium-Free Chemical Conversion Coating On Zinc Electroplating Layer, Yong Guan, Jian-Guo Liu, Chuan-Wei Yan

Journal of Electrochemistry

In this paper,we obtained environmental-friendly chromium-free chemical conversion coating on the non-cyanide alkaline zinc electroplating layer by employing the optimized Ti/Zr based conversion technique.At the same time,the performances of the Ti/Zr based conversion coating were compared with chromate colour passivation coating.The corrosion resistances of the conversion coatings were investigated by using neutral salt spray(NSS) test,potentiodynamic polarization and electrochemical impedance spectroscopy(EIS).The results showed that the white rust appeared after 96 hours when the NSS test was performed on the Ti/Zr based conversion coating,which was close to the corrosion resistance rating of chromate colour passivation coating.Compared with the chromate passivation coating,the Ti/Zr …

The Roles Of The Width Of Gas/Liquid/Solid Three-Phase Boundary Zone Of Dispersion Water Films In Atmospheric Corrosion Of Metals, Wang Jia, Jing Jiang

Journal of Electrochemistry

The roles of TPB(Three-Phase Boundary) width in the corrosion processes of metals under dispersed water films were investigated by electrochemical techniques combined with contact angle measurement.It is found that both cathodic limiting current density and corrosion current density linearly increases with increasing the TPB width,confirming the important role of TPB width in gas/liquid/solid multiphase corrosion systems.Based on above results,the effect of water film thickness on atmospheric corrosion rate was quantitatively evaluated by the TPB width.

Hydrothermal Reduction Synthesis Of Lifepo_4 And Its Electrochemical Performance, Hong-Li Zou, Guang-Hui Zhang, Pei-Kang Shen

Journal of Electrochemistry

The cathode materials of LiFePO4 were prepared via a hydrothermal reduction method using FeCl3 as Fe source and iron as a reducing agent.The results showed that ferric salt could be reduced to ferrous salt completely under the hydrothermal condition and pure-phase LiFePO4 was obtained based on the test results of XRD and FTIR.Carbon-coated LiFePO4 was synthesized by pyrolysisng glucose at high temperature.The morphologies of pure LiFePO4 displayed cluster-like while the LiFePO4/C displayed sphere-like particles.The electrochemical test showed that the LiFePO4/C had good rate performance,while LiFePO4 delivered much lower discharge capacity.

Effects Of Solvents And Electrolyte Salts On The Electrochemical Reduction Of Oxygen In Non-Aqueous Electrolytes, Yan-Yan Tian, Wei Wu, Jun Gao, Yong Yang

Journal of Electrochemistry

The electrochemical reduction processes of oxygen in different non-aqueous solvents such as acetonitrile(MeCN),propylene carbonate(PC) and their mixtures were investigated by cyclic voltammetry method.The results indicated a one electron reduction of oxygen to O2-occured in these systems as a first step reduction,no matter whether in tetrabutylammonium hexafluorophosphate(TBAPF6)/MeCN or TBAPF6/PC electrolyte.However,the CV curves in 0.1 mol·L-1 TBAPF6/MeCN showed a couple of reversible redox peaks,indicating that the reduction process of oxygen was irreversible in the 0.1 mol·L-1 TBAPF6/PC electrolyte.In the PC-based electrolyte,the reduction current peak reduced largely and the oxidation peak of O2-almost disappeared as compared to that of the former electrolytes.The possible …

Effect Of Cldh On Rebar Corrosion Behavior In Chloride Contaminated Neutral Pore Solutions, Yu-Ming Tang, Le Niu, Yu Zuo

Journal of Electrochemistry

The effect of calcined LDH-MgAl-CO3 on rebar corrosion behavior in chloride ion contaminated neutral concrete pore solutions was investigated in this paper.Corrosion potentials of rebars in pore solutions after treatment with CLDH were higher than before treatment.According to polarization tests,passivated region of rebars in pore solutions after treatment with CLDH was found apparently instead of activation.EIS tests showed that CLDH made the impedance of specimens increase.The measurements of pH and chloride ion concentration after treatment indicated that / of pore solutions decreased by 4～5 magnitude orders.

Photoelectrochemical Properties Of N,S,And Cl Modified Nano Tio_2 Thin Films, Hong Yun, Chang-Jian Lin, Jing Li, Rong-Gui Du

Journal of Electrochemistry

The nitrogen(N),sulfur(S) and chlorine(Cl) modified nano TiO2 thin films were prepared by adding Ti(O-n-Bu)4 as the precursor into concentrated HNO3,H2SO4 and HCl Solutions,respectively,on different substrates in a sol-gel process.The photoelectrochemical performances of N,S and Cl modified nano TiO2 thin films have been studied by UV-vis(DRS),photocurrent curves,EIS and OCP-time curves.N-modified TiO2 nano films show better surface structure,which helps to improve the quantum efficiency of nano TiO2 thin films.

Corrosion Electrochemical Behavior Of Am60 Magnesium Alloys In Automobile Engine Coolants, Ling-Jie Li, Sha Wang, Yin Xiao, Jun Lan, Jing-Lei Lei, Sheng-Tao Zhang, Fu-Sheng Pan

Journal of Electrochemistry

The polarization measurements and electrochemical impedance spectroscopy(EIS) were used to study the corrosion electrochemical behavior of AM60 magnesium alloys in three kinds of commercial coolants for automobile engine.Results show that the tested commercial coolants are slightly corrosive to AM60 magnesium alloys and their corrosivity varies from coolant to coolant.The coolant C is the least corrosive among the studied commercial coolants and the coolant A is more corrosive than the coolant B and C.The coolant C appears to be the most promising coolant for automobile engine made by magnesium alloys.The coolant resistivity plays an important role in the corrosion of AM60 …

Research On Nafion/Sio_2 Composite Membrane In All Vanadium Redox Flow Battery, Dong-Dong Liu, Mao-Cai Lin, Tao Guan, Qing-Chun Yu

Journal of Electrochemistry

The Nafion117/SiO2 composite membrane was prepared by sol-gel method.The results showed that,during composite membrane preparation process,the ratio of MeOH and TEOS did not affect the penetration rate of VO2+ basically,however,the lowest permeability of 427×10-9cm2/s in the membrane was achieved while hydrolysis time was 10 min and natural drying for 24 h after hydrolysis,which reduced by 52 times than that in Nafion117 membrane.The SEM tests proved that SiO2 grains grew bigger in the composite membrane during the natural drying,and most of the holes in Nafion117 were filled.Single cell test showed the battery power efficiency was improved by 2.7 %.

Virtual Coatings Application System, Jason M. Ebsensberger, Michael J. Bolick, Richard J. Klein Ii, Eric C. Peterson, Chad J. Zalkin, James B. Fisher, Leslie C. Hughes

Patents (University of Northern Iowa)

A virtual coatings application system has several features to enhance the realism of simulated spray painting. The system generally includes a display screen on which is defined a virtual surface (such as a truck door) that is intended to be virtually painted or coated by the user. Alternatively, the system includes a head-mounted display unit that displays a virtual spray painting environment in which the virtual surface is defined. The user operates an instrumented spray gun controller that outputs one or more signals representing data as to the status of the controls on the spray gun controller. The system also …

Virtual Coatings Application System, Jason M. Ebensberger, Michael J. Bolick, Jeremiah G. Treloar, Richard J. Klein Ii, Eric C. Peterson, Chad J. Zalkin, James B. Fisher, Leslie C. Hughes

Patents (University of Northern Iowa)

A virtual coatings application system has several features to enhance the realism of simulated spray painting. The system generally includes a display screen on which is defined a virtual surface (such as a truck door) that is intended to be virtually painted or coated by the user. The user operates an instrumented spray gun controller that outputs one or more signals representing data as to the status of the controls on the spray gun controller. The system also has a motion tracking system that tracks the position and orientation of the spray gun controller with respect to the virtual surface …

The Relationship Between Induced Fluid Structure And Boundary Slip In Nanoscale Polymer Films, Nikolai V. Priezjev

Mechanical and Materials Engineering Faculty Publications

The molecular mechanism of slip at the interface between polymer melts and weakly attractive smooth surfaces is investigated using molecular dynamics simulations. In agreement with our previous studies on slip flow of shear-thinning fluids, it is shown that the slip length passes through a local minimum at low shear rates and then increases rapidly at higher shear rates. We found that at sufficiently high shear rates, the slip flow over atomically flat crystalline surfaces is anisotropic. It is demonstrated numerically that the friction coefficient at the liquid-solid interface (the ratio of viscosity and slip length) undergoes a transition from a …

Plant Ecophysiology Of Mycorrhizal Fungi, Gregory Keith Bartley Jr.

Gregory Keith Bartley Jr.

No abstract provided.

Synthesis Of Mild–Hard Aao Templates For Studying Magnetic Interactions Between Metal Nanowires, Jin-Hee Lim, Aurelian Rotaru, Seong-Gi Min, Leszek Malkinski, John B. Wiley

Physics Faculty Publications

The sequential application of mild and hard anodization techniques in the fabrication of porous aluminamembranes allows one to decrease the number of continuous pores in anodized aluminium oxide (AAO) templates. Initially, standard mild anodization techniques were used to create porous templates with 100 nm interpore distances and 70 nm pore diameters. Hard anodization treatment on the same membrane then produced interpore distances of about 265 nm with diameters of 110 nm. At the interface between the two anodization steps, many of the mild-side pores were terminated to create a mild–hard membrane (Mi–Ha AAO) where the functional interpore distances were 200–300 …

Dye Sensitized Solar Cell With Conventionally Annealed And Post-Hydrothermally Treated Nanocrystalline Semiconductor Oxide Tio2 Derived From Sol-Gel Process, Akhmad Herman Yuwono, Badrul Munir, Alfian Ferdiansyah, Arif Rahman, Wulandari Handini

Makara Journal of Technology

Dye-sensitized solar cell (DSSC) is one of the very promising alternative renewable energy sources to anticipate the declination in the fossil fuel reserves in the next few decades and to make use of the abundance of intensive sunlight energy in tropical countries like Indonesia. In the present study, TiO2 nanoparticles of different nanocrystallinity was synthesized via sol−gel process with various water to inorganic precursor ratio (Rw) of 0.85, 2.00 and 3.50 upon sol preparation, followed with subsequent drying, conventional annealing and post-hydrothermal treatments. The resulting nanoparticles were integrated into the DSSC prototype and sensitized with an organic dye made of …

Remote Sensing And Geographical Information System To Identify Drought Potency, Puguh Dwi Raharjo

Makara Journal of Technology

Remote Sensing and Geographical Information System to Identify Drought Potency. Kebumen regency was drought in year 2008, community clean water shortages and irrigation water following a decline in water resources. The use of remote sensing data and GIS can be used to identify the potential for drought-prone areas. Transformation of Landsat TM satellite imagery to obtain the brightness index, wetness index and vegetation index used to determine surface conditions in relation to drought. Brightness index and wetness index derived from the tasseled cap modifications, while the vegetation index derived from normalized difference vegetation index (NDVI) values. Other parameters such as …

Immobilization Of Saccharomyces Cerevisiae In Rice Hulls For Ethanol Production, Edita Martini, Dian Andriani, Sriramulu Gobikrishnan, Kyeong Eop Kang, Surn-Teh Bark, Changshin Sunwoo, Bambang Prasetya, Don-Hee Park

Makara Journal of Technology

The whole cell immobilization in ethanol fermentation can be done by using natural carriers or through synthetic carriers. All of these methods have the same purpose of retaining high cell concentrations within a certain defined region of space which leads to higher ethanol productivity. Lignocellulosic plant substance represents one of highly potential sources in ethanol production. Some studies have found that cellulosic substances substances can also be used as a natural carrier in cell immobilization by re-circulating pre-culture medium into a reactor. In this experiment, rice hulls without any treatment were used to immobilize Saccharomyces cerevisiae through semi solid state …

Simulation On The Use Of Losat Data For Rice Field Mapping, Bambang H. Trisasongko, Dyah R. Panuju, Boedi Tjahjono, Baba Barus, Hari Wijayanto, Mahmud A. Raimadoya, Irzaman Irzaman

Makara Journal of Technology

Simulation on the Use of LOSAT Data for Rice Field Mapping. Since the launch of LAPAN-TUBSAT satellite in 2007, Indonesia has been developing mission on earth observation missions for various applications. The next generation mission, called LAPAN-ORARI Satellite (LOSAT), is currently under development and expected to be launched in 2011. In order to facilitate the applications, a thorough assessment of the sensor should be made. This paper presents an examination of simulated LOSAT data for rice monitoring and mapping purposes coupled with QUEST statistical tree. We found that three-band simulated LOSAT data were suitable for the task with reasonably high …

Shaft Torsional Vibration Response Of Vertical Axis Ocean Current Turbine Model Due To Torque Excitation, Adi Wirawan Husodo, I Ketut Aria Pria Utama, I Made Ariana

Makara Journal of Technology

Shaft Torsional Vibration Response of Vertical Axis Ocean Current Turbine Model Due to Torque Excitation. The current research aimed to study the torsional vibration response of Vertical Axis Ocean Current Turbine due to randomly torque excitation pattern, owing to the variety of ocean current velocity. The turbine model is composed of 3 aluminum blades of NACA 0018 connected to steel shaft. Turbine dimensions are 10 cm of chord, 1.8 cm of chamber and 100 cm of span. The variation of ocean current velocity is 0.5 m/s, 1.0 m/s, 1.5 m/s, 2.0 m/s, 2.5 m/s and 3.0 m/s. The Model has …

The Stability Characteristics Of Sandbag Submerged Breakwater, Ferry Fatnanta, Widi Agoes Pratikto, Haryo Dwito Armono, Wahyudi Citrosiswoyo

Makara Journal of Technology

The Stability Characteristics of Sandbag Submerged Breakwater. Breakwater is one of coastal structures to overcome problems of abrasion. Due to difficulties in obtaining rock material at the coastal area. The using of sandbags as a breakwater provides advantages in utilizing local materials. A Sandbag has a smooth surface, so the internal shear forces are relatively small. According to these phenomena, the research for parameters that are expected to affect the stability of the sand bags. These parameters are a slope, shape and formation of sand bags. This experimental research conducted in two dimensional physical model and took place on the …

Static Hand Gesture Recognition Of Indonesian Sign Language System Based On Backpropagation Neural Networks, Farida Asriani, Hesti Susilawati

Makara Journal of Technology

Static Hand Gesture Recognition of Indonesian Sign Language System Based on Backpropagation Neural Networks. The main objective of this research is to perform pattern recognition of static hand gesture in Indonesian sign language. Basically, pattern recognition of static hand gesture in the form of image had three phases include: 1) segmentation of the image that will be recognizable form of the hands and face, 2) feature extraction and 3) pattern classification. In this research, we used images data of 15 classes of words static. Segmentation is performed using HSV with a threshold filter based on skin color. Feature extraction performed …

The Effect Of Enzymatic Hydrolysis On The Properties Of Protein Hydrolysate From Paddy Mushroom, Niken Widya Palupi, Wiwik Siti Windrati, Tamtarini Tamtarini

Makara Journal of Technology

Protein hydrolysate was prepared from Paddy (Volvariella volvaceae) mushroom. Hydrolysis uses commercially protease available Protamex ™ with enzyme concentration of 0.1% (w/w). Hydrolysis was performed at three different temperatures (room temperature, 40 °C, and 50 °C) with different incubation periods (60, 90, and 120 minutes). Enzyme inactivation was done in 90 °C for 3 minutes. Yield and degree of hydrolysis ranged from 94.76% to 99.55% and 19.06% to 24.59%. Protein solubility was about 89–11,8%. The longer time of hydrolysis, the darker the color of protein hydrolysate. Protein hydrolysate which has hydrolysis at 50 °C for 120 minutes has the highest …

Plant Growth Modeling Using L-System Approach And Its Visualization, Atris Suyantohadi, Alfiyan Alfiyan, Mochamad Hariadi, Mauridhi Hery Purnomo

Makara Journal of Technology

The visualization of plant growth modeling using computer simulation has rarely been conducted with Lindenmayer System (L-System) approach. L-System generally has been used as framework for improving and designing realistic modeling on plant growth. It is one kind of tools for representing plant growth based on grammar sintax and mathematic formulation. This research aimed to design modeling and visualizing plant growth structure generated using L-System. The environment on modeling design used three dimension graphic on standart OpenGL format. The visualization on system design has been developed by some of L-System grammar, and the output graphic on three dimension reflected on …