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Determination Of 72 Antibiotics Residues In Raw Milk By Ultra-Performance Liquid Chromatography-Tandem Mass Spectrometry, WANG Chengping, QIN Yu, HOU Beibei, LEI Tao, YU Chenghua, GE Yu 2019 Shanghai Institute of Quality Inspection and Technical Research, Shanghai 200233, China; National Quality Supervision and Inspection Center for Food Products, Shanghai 200233, China

Determination Of 72 Antibiotics Residues In Raw Milk By Ultra-Performance Liquid Chromatography-Tandem Mass Spectrometry, Wang Chengping, Qin Yu, Hou Beibei, Lei Tao, Yu Chenghua, Ge Yu

Food and Machinery

The pretreatment method of antibiotic residues in fresh milk was established and optimized. At the same time, 72 kinds of compounds were effectively extracted and purified, and analyzed by ultra performance liquid chromatography-tandem mass spectrometry. In this paper, the effects of different extraction solvents and purification methods on the recovery rate of the target were investigated and the conditions were optimized. 72 antibiotics were linearly good in the range 1.0䥺[email protected] μg/L. The LOD of the five compounds was 10.0 μg/kg, the LOD of the 15 compounds was 5.0 μg/kg, and the LOD of the remaining 52 compounds was no more …


Hplc Analysis Of Flavonoids In Apocynumvenetum Tea And Its Antioxidation In Vitro, ZHANG Jing, REN Xiaoli, LI Xixi, YI Sha, LI Chong, ZHAO Xin 2019 Environment and Quality Inspection College, Chongqing Chemical Industry Vocational College, Chongqing 401228, China

Hplc Analysis Of Flavonoids In Apocynumvenetum Tea And Its Antioxidation In Vitro, Zhang Jing, Ren Xiaoli, Li Xixi, Yi Sha, Li Chong, Zhao Xin

Food and Machinery

In this study, the contents of rutin and isoquercetin in flavonoids of Apocynumvenetum tea was determined by high performance liquid chromatography (HPLC), and the antioxidant effect in vitro was evaluated. A good separation of rutin and isoquercetin from flavonoids of Apocynumvenetum tea was achieved by vacuum heating reflux combined with macroporous adsorption. Rutin and isoquercetin were separated effectively in the extract of Apocynum venetum teaflavonoids. The results showed good linear relationship, the range of rutin was 0.453 1~9.062 5 μg (r=0.999 55) and that of isoquercetin ranged from 0.258 3 to 5.166 5 μg (r=0.999 65). The recoveries of rutin …


Recognition Of Plant Diseases And Insect Pests In Potato Based On Machine Vision Image Extraction, WANG Yi 2019 Shijiazhuang University of Applied Technology, Shijiazhuang, Hebei 050081, China

Recognition Of Plant Diseases And Insect Pests In Potato Based On Machine Vision Image Extraction, Wang Yi

Food and Machinery

In order to improve the detection and recognition ability of potato internal diseases and insect pests, image visual feature recognition method was used to detect potato diseases and insect pests, and a method of potato internal diseases and insect pests feature recognition based on machine vision image was proposed. A two-dimensional visual image acquisition model of potato internal diseases and insect pests was constructed, and the visual images of potato internal diseases and insect pests were detected by block fusion, and the characteristics of diseases and insect pests were detected according to the distribution of potato green leafin texture. The …


Study On Antioxidant Components And Antioxidant Activities Of Peels Extracts From Sweet Orange In Hunan Province, LI Juan, NIU Zeyu, YUE Xiangqi, XIE Xuan, FU Xinjing, LU Jun 2019 Hunan Key Laboratory of Processed Food for Special Medical Purpose, Changsha, Hunan 410004, China; College of Food Science and Technology, Central South University of Forestry and Technology, Changsha, Hunan 410004, China

Study On Antioxidant Components And Antioxidant Activities Of Peels Extracts From Sweet Orange In Hunan Province, Li Juan, Niu Zeyu, Yue Xiangqi, Xie Xuan, Fu Xinjing, Lu Jun

Food and Machinery

Eight kinds of sweet orange peels extracts were investigated to compare their antioxidant active ingredients and antioxidant capacity. The results showed that the highest level of the content of polyphenols, flavonoids, tannins and vitamin C were found in Mayang Bingtang sweet orange peel extracts, which reached 7.60 mg gallic acid equivalent (GAE)/per gram dried sample (g·md), 4.57 mg rutin equivalent (RE)/g·md, 17.90 tannin (TAE) mg/g·md, 17.86 mg vitamin c (VC)/g·md, respectively. Meanwhile, Mayang Bingtang orange peel also showed the highest ferric reducing power (81.50±0.93 μmol Trolox equivalent (TE)/g·md), and very …


Research Progress On The Effects Of Ozone Treatment On The Structuraland Processing Characteristics Of Food Starches, XIA Rui, LIU Lijun, CAO Mengling, ZHAO Guohua, YE Fayin 2019 College of Food Science, Southwest University, Chongqing 400715, China

Research Progress On The Effects Of Ozone Treatment On The Structuraland Processing Characteristics Of Food Starches, Xia Rui, Liu Lijun, Cao Mengling, Zhao Guohua, Ye Fayin

Food and Machinery

This review introduces the chemical properties of ozone and the ways of starch ozonation, and then summarizes the effects of ozone treatment on the molecular structure, granular characteristics and processing properties of the starches. The factors effecting the starch ozonation are also reviewed. Further research directions on utilizing ozone reasonably to improve the starch functionalities are also suggested.


Development Of A Dna Mini-Barcoding Protocol Targeting Coi For The Identification Of Elasmobranch Species In Shark Cartilage Pills, Rowena J. Zahn, Anthony J. Silva, Rosalee S. Hellberg 2019 Chapman University

Development Of A Dna Mini-Barcoding Protocol Targeting Coi For The Identification Of Elasmobranch Species In Shark Cartilage Pills, Rowena J. Zahn, Anthony J. Silva, Rosalee S. Hellberg

Food Science Faculty Articles and Research

Many elasmobranch (shark and ray) species are considered threatened and their identification in processed products is important for conservation and authentication purposes. However, identification of elasmobranch species in shark cartilage pills has proven difficult using existing methodologies. The objective of this study was to develop a DNA mini-barcoding protocol using a ~130 bp region of the cytochrome c oxidase subunit I (COI) gene for species identification in shark cartilage pills. A total of 22 shark cartilage products underwent DNA extraction in duplicate using the DNeasy Blood and Tissue Kit (Qiagen). The effectiveness of a clean-up step following DNA extraction was …


Seaweeds As Nutraceuticals For Health And Nutrition, Emer Shannon, Nissreen Abu-Ghannam 2019 Technological University Dublin

Seaweeds As Nutraceuticals For Health And Nutrition, Emer Shannon, Nissreen Abu-Ghannam

Articles

Throughout human history, seaweeds have been used as food, folk remedies, dyes, and as mineral-rich fertilisers. Seaweeds as nutraceuticals or functional foods with dietary benefits beyond their fundamental macronutrient content are now a major research and industrial development concept. The occurrence of dietary and lifestyle related diseases, notably type 2 diabetes, obesity, cancer, and metabolic syndrome has become a health epidemic in developed countries. Global epidemiological studies have shown that countries where seaweed is consumed on a regular basis have significantly fewer instances of obesity and dietary-related disease. This review outlines recent developments in seaweed applications for human health from …


Evaluation Of Chilling Efficiency, Meat Tenderness, And Microbial Analysis Of Broiler Carcasses Using Sub-Zero Saline Solutions, Samira Viliani 2019 California Polytechnic State University, San Luis Obispo

Evaluation Of Chilling Efficiency, Meat Tenderness, And Microbial Analysis Of Broiler Carcasses Using Sub-Zero Saline Solutions, Samira Viliani

Master's Theses

The poultry industry is seeking an advanced chilling system that can improve chilling efficiency, microbial safety, and water consumption without compromising meat quality. The objective of this study was to evaluate the effects of sub-zero saline chilling methods on chilling efficiency, breast fillet tenderness and microbial reduction of broiler carcasses. Following evisceration and rinsing, broiler carcasses were randomly assigned to one of three chilling solutions: 1) 0% salt or ice water control (0% NaCl/0.5oC), 2) 3% salt (3% NaCl/-1.8oC), and 3) 4% salt (4% NaCl/-2.41oC) solutions. Broiler carcasses in sub-zero saline solutions reached the …


Correlation Of The Water-Interacting Property Of Dietary Fiber Powder With Its Composition And Particle Structure, TAO Jianming, YAN Caizhi, ZHAO Guohua 2019 College of Food Science, Southwest University, Chongqing 400715, China

Correlation Of The Water-Interacting Property Of Dietary Fiber Powder With Its Composition And Particle Structure, Tao Jianming, Yan Caizhi, Zhao Guohua

Food and Machinery

As one of the most important physicochemical properties of dietary fiber powders, the water-interacting property is closely related to their technological properties and physiological functions in the food system. However, systematic research is unavailable on the relationship between the water-interacting properties and the composition and particle structure of dietary fiber powders. Therefore, the water-interacting properties of dietary fiber powder and these dependence on composition and particle structure by correlation analysis were investigated, based on the determinations of the hydration properties (water holding capacity, swelling capacity), hygroscopicities (initial absorption rate, absorption time, maximum absorption rate), dietary fiber contents (total dietary fiber, …


Inhibition Of Punicalagin On The Expression Of Virulence Factors Of Staphylococcus Aureus, XU Yunfeng, WU Qian, FAN Qiuxia, WANG Xin, XIA Xiaodong 2019 College of Food and Bioengineering, Henan University of Science and Technology, Luoyang, Henan 471023, China; College of Food Science and Engineering, Northwest A&F University, Yangling, Shaanxi 712100, China

Inhibition Of Punicalagin On The Expression Of Virulence Factors Of Staphylococcus Aureus, Xu Yunfeng, Wu Qian, Fan Qiuxia, Wang Xin, Xia Xiaodong

Food and Machinery

Hemolysis test, coagulase titer assay, and enzyme-linked immunoreaction method were used to detect the expression changes of hemolysin, plasma coagulase, and total enterotoxins after treating with punicalagin. Reverse transcription real-time fluorescence quantitative PCR was used to detect the expression of virulence-related genes. The results showed that punicalagin could significantly reduce the production of α-hemolysin, but the inhibition effect was not concentration-dependent. At the concentrations of higher than 1/4 MIC, punicalagin could decrease the expression of plasma coagulase. At the concentrations of higher than 1/2 MIC, punicalagin significantly reduced the production of total enterotoxins. Punicalagin also significantly reduced the transcription of …


Isolation, Identification And Tolerance To Simulated Gastrointestinal Environment Of Lactococcus Lactis From Soy Sauce Residue, HUANG Guidong, TANG Suting, CHENG Yunhui, SUN Zhangle, CHEN Ziqi, JIAO Ye, ZHANG Can, ZHONG Xianfeng 2019 College of Food Science and Engineering, Foshan University, Foshan, Guangdong 528231, China; Guangdong Engineering Reseach Center for Traditional Fermentational Food, Foshan, Guangdong 528231, China; Guangdong Engineering Reseach Center for Safety Control

Isolation, Identification And Tolerance To Simulated Gastrointestinal Environment Of Lactococcus Lactis From Soy Sauce Residue, Huang Guidong, Tang Suting, Cheng Yunhui, Sun Zhangle, Chen Ziqi, Jiao Ye, Zhang Can, Zhong Xianfeng

Food and Machinery

In order to enrich lactic acid bacteria resource from soy sauce residue, Lactococcus lactis from soy sauce residue were screened and identified by physiological and biochemical tests and 16S rRNA gene sequence analysis, and their tolerance to gastrointestinal environment were further studied. Four strains of lactic acid bacteria were isolated from soy sauce residue. Three of them were identified as Lactococcus lactis subsp. hordniae, HT127, HT223 and HT227, respectively. One was identified as Lactococcus lactis subsp. lactis and named HT122. The results of growth curve showed that the growth of four strains were similar, and the logarithmic growth period was …


Preparation And Structural Characterization Of Silkworm Pupa Peptides Chelated Calcium, ZHAO Ziyue, WANG Siyuan, LIAO Sentai, MU Lixia, ZOU Yuxiao 2019 Sericultural & Agri-Food Research Institute Guangdong Academy of Agricultural Sciences, Guangzhou, Guangdong 510610, China; Guangdong Key Laboratory of Agricultural Products Processing, Guangzhou, Guangdong 510610, China; Key Laboratory of Functional Food

Preparation And Structural Characterization Of Silkworm Pupa Peptides Chelated Calcium, Zhao Ziyue, Wang Siyuan, Liao Sentai, Mu Lixia, Zou Yuxiao

Food and Machinery

Preparation of peptides chelated calcium from silkworm pupa peptides, taking the soluble calcium content as the main index, and considering the chelation and yield rate, the effects of reaction pH, temperature, time, and peptide-calcium ratio were examined. On the basis of single factor experiment, Box-Behnken central composite design was utilized, and the optimal conditions were as followed: reaction time 80 min, reaction temperature 73 ℃, pH 10, peptide calcium ratio 3.4∶1.0. Under this condition, the soluble calcium content of the silkworm pupa peptide chelated calcium was 14.51%. Through the UV absorption and infrared spectroscopy and SEM analysis, it showed that …


Effect Of The Heater Temperature On The Aroma Components Of Finished Tobacco, LI Chao, YUAN Xiangyun, LI Da, GE Wen, WANG Jiashou 2019 Technology Center of China Tobacco Yunnan Industrial Co., Ltd., Kunming, Yunnan 650024, China

Effect Of The Heater Temperature On The Aroma Components Of Finished Tobacco, Li Chao, Yuan Xiangyun, Li Da, Ge Wen, Wang Jiashou

Food and Machinery

Head space solid-phase microextraction (HS-SPME) coupled with chromatography-mass spectrometry (GC-MS) method was developed to study the effects of different tempera-ture of the heater on the composition and content of aroma components in the test samples of different batches of cigarettes. The results were as follows: ① A total of 35 core aroma components were detected in two batches of finished cut tobacco, of which batches X and Y contained 30 and 34 kinds respectively; ② 3-methyl-3-buten-2-one, 2-hexene-1-alcohol, 2-(butoxyethoxy)ethanol, Methyl palmitate and 3,5-dimethylphenol were undetected components in X, while 3-methyl-1,2-cyclopentadione was undetected components in Y. 1,2-propanediol was the highest content of …


Analysis Of Taste Substances Of Cooked Pork Based On Electronic Tongue And Chromatographic Techniques, GUO Jinying, LI Jie, WU Ying, REN Guoyan, CUI Guoting, WANG Ping, LIU Jianxue 2019 College of Food and Bioengineering, Henan University of Science and Technology, Luoyang, Henan 471023, China; Henan Engineering Research Center of Food Material, Luoyang, Henan 471023, China; National Demonstration Center for Experimental Food Processing

Analysis Of Taste Substances Of Cooked Pork Based On Electronic Tongue And Chromatographic Techniques, Guo Jinying, Li Jie, Wu Ying, Ren Guoyan, Cui Guoting, Wang Ping, Liu Jianxue

Food and Machinery

To analyze the taste substances of cooked Tibetan pork, Sanmenxia black pork and Du changda white pork, the three raw materials were separately cooked, and then the free amino acids and nucleotides were determined by liquid chromatography, and the fatty acid content was determined by gas chromatography. The taste substances were tested by electronic tongue. SPSS 19 was used to analyze the taste substance difference of the three porks. The results showed that the free glutamic acid content of cooked Sanmenxia black pork was the highest, and the inosinic acid content of cooked Tibetan pork was the highest. Compared with …


Analysis Of Quality Characteristics Of Yunnan Broken Black Tea By Color, Fragrance And Tasty, ZHANG Yangbo, LIU Zhonghua, RAO Tiantian, LI Shi, OU Xingchang, AN Huimin, XIONG Yifan, LI Wenxiong, JIANG Hongjian, HUANG Jianan 2019 Key Laboratory of Tea Science of Ministry of Education, Hunan Agricultural University, Changsha, Hunan 410128, China

Analysis Of Quality Characteristics Of Yunnan Broken Black Tea By Color, Fragrance And Tasty, Zhang Yangbo, Liu Zhonghua, Rao Tiantian, Li Shi, Ou Xingchang, An Huimin, Xiong Yifan, Li Wenxiong, Jiang Hongjian, Huang Jianan

Food and Machinery

In order to explore the color, fragrance and taste quality of Yunnan broken black tea, it provides a reference of the quality characteristics of domestic broken black tea in this study. This study collected 14 Yunnan broken black tea and analyzed the quality from sensory evaluation, color difference, aroma components, and physical and chemical ingredients. The results showed that the 14 sample tea soups were mainly red and bright, and the color differences L*, a*, and b* were -22.50 to -12.28, 9.09~23.80, 62.09~164.40, respectively. The amounts of TF, TF-3G, TF-3'G and TFDG were 0.146%~0.209%, 0.108%~0.225%, 0.041%~0.109%, 0.056%~0.177%; respectively. The aroma …


Correlation Between Physical Moisture Retention Propertyin Tobacco Samples And Its Pore Structure, GUO Huacheng, LI Qiang, SUN Xueping, HOU Pengjuan 2019 China Tobacco Henan Industrial Co., Ltd., Zhengzhou, Henan 450016, China

Correlation Between Physical Moisture Retention Propertyin Tobacco Samples And Its Pore Structure, Guo Huacheng, Li Qiang, Sun Xueping, Hou Pengjuan

Food and Machinery

In order to understand the relationship between the moisture content of tobacco and its microporous structure, and to provide a theoretical basis for the preservation of tobacco, the dehydration rate over 4 000 min of 26 Tobacco samples including flue-cured tobacco, burley tobacco, oriental tobacco, reconstituted tobacco leaf and expanded cut stems were measured (1 time/min) at a temperature of (22±1) ℃ and a relative humidity of 30% using a tobacco dynamic moisture content monitoring device. The α and β values in the thermodynamic Weibull model were calculated from the dehydration rate. Results: At the same storage temperature, humidity and …


Moisture Retention Properties Of Polygonatum Polysaccharide In Tobacco And Its Mechanism, LEI Sheng, LIU Xiuming, LI Yuandong, JIANG Juxing, ZENG Yicheng, WANG Huijuan, LIN Chao, WANG Xuejiao, YANG Qianxu 2019 Technology Center, China Tobacco Yunnan Industrial Co., Ltd., Kunming, Yunnan 650231, China

Moisture Retention Properties Of Polygonatum Polysaccharide In Tobacco And Its Mechanism, Lei Sheng, Liu Xiuming, Li Yuandong, Jiang Juxing, Zeng Yicheng, Wang Huijuan, Lin Chao, Wang Xuejiao, Yang Qianxu

Food and Machinery

The moisture absorption and moisture retention properties of polygonatum polysaccharides, fenugreek polysaccha-rides, chlorella polysaccharides and ganoderma lucidum polysaccharides were investigated as compared with propylene glycol and water. The results showed that polygonatum polysaccharides had similar moisture absorption properties as propylene glycol, but its moisture retention was significantly better than that of propylene glycol. Therefore, the desorption process of tobacco under low humidity conditions was fitted nonlinearly by common thin-layer drying models. It was found that the tobacco added with polygonatum polysaccharides have the lowest drying rate constant and the slowest moisture retention rate. Low field nuclear magnetic (LF-NMR) results showed …


Establishment And Application Of Prediction Model For Content Determination Of Mashed Potato In Noodles By Nir Spectroscopy, LV Du, DONG Nan, WANG Mei, WANG Hui, LIU Yongxiang, LI Fei, LIU Jia 2019 Biotechnology Institute of Guizhou Province, Guiyang, Guizhou 550006, China; Food Processing Institute of Guizhou Province, Guiyang, Guizhou 550006, China

Establishment And Application Of Prediction Model For Content Determination Of Mashed Potato In Noodles By Nir Spectroscopy, Lv Du, Dong Nan, Wang Mei, Wang Hui, Liu Yongxiang, Li Fei, Liu Jia

Food and Machinery

A fast determination method was established for content determination of mashed potato in noodles. Studied 170 potato noodles by near infrared spectroscopy and stoichiometry to establish prediction model by PLS. The result indicated that the prediction model based on wave number of 9 403.6~5 446.2 cm-1, and spectral pretreatment by the standard normal variate transformation (SNV) showed an excellent prediction accuracy. The external validation determinants was 0.956 4, the root mean square error of prediction was 3.73%, the slope was 1.029, and relative prediction deviation was 2.04. The results indicate that near infrared spectroscopy can be used as …


Uncertainty Evaluation For The Determination Of Neotame Content In Roasted Seeds And Nuts By Uplc-Ms/Ms Method, HUANG Kun, WANG Huixia, FAN Xiaolong, GUO Jia 2019 Hubei Provincial Institute for Food Supervision and Test, Wuhan, Hubei 430075, China; Hubei Provincial Engineering and Technology Research Center for Food Quality and Safety Test, Wuhan, Hubei 430075, China

Uncertainty Evaluation For The Determination Of Neotame Content In Roasted Seeds And Nuts By Uplc-Ms/Ms Method, Huang Kun, Wang Huixia, Fan Xiaolong, Guo Jia

Food and Machinery

To analyse and evaluate the uncertainty in the determination of neotame content in roasted seeds and nuts by UPLC-MS/MS. A mathematical model of uncertainty in the determination of neotame content in roasted seeds and nuts was established, various factors of uncertainty in the whole determination process were studied and evaluated, the components of uncertainty in the method were confirmed and composed. The results showed that the expanded uncertainty was 0.71 mg/kg(k=2) when the neotame content was 7.69 mg/kg, which was greater caused by preparation of standard stock solution and repeatability of determination.


Quantitative Analysis Of Glycine Solutions By Terahertz Attenuated Total Reflection (Thz-Atr) Spectra, CHENG Li, MA Wei, LIU Qi, OGAWA Yuichi 2019 Engineering Research Center of Agricultural Microbiology Technology, Ministry of Education, Heilongjiang University, Harbin, Heilongjiang 150500, China

Quantitative Analysis Of Glycine Solutions By Terahertz Attenuated Total Reflection (Thz-Atr) Spectra, Cheng Li, Ma Wei, Liu Qi, Ogawa Yuichi

Food and Machinery

Terahertz attenuated total reflection spectroscopy was employed to investigate the terahertz absorption spectra of different concentration glycine solutions within 20~450 cm-1 at room temperature. There are four clear absorption peaks at 65.56, 127.28, 173.56, 308.55 cm-1 respectively. The 2nd derivative spectra and the multiple linear regressions were employed to perform the quantitative analysis of the glycine solution concentr-ation. Randomly combine different wave numbers, the optimum ternary linear regression equation was gained. The R2 Adj was 0.990 3, the Root Mean Square Error (RMSE) was 0.005 7, the Root Mean Squares Error of Prediction (RMSEP) was 1.658 …


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