Determination Of Mandipropamid Residues In Cucumber By Uplc-Ms,
2023
Nanchong Institute for Food and Drug Control, Nanchong, Sichuan 637000, China
Determination Of Mandipropamid Residues In Cucumber By Uplc-Ms, Zhang Zhouli, Li Dong, Luo Si, Luo Xingyu, Yong Ping, Yi Da
Food and Machinery
Objective： To establish a detecting method for mandipropamid residues in cucumber by UPLC-MS coupled with the positive ions mods of MRM. Methods： The cucumber samples were was extracted by ultrasonic acetonitrile and then were purified by dispersed solid phase extraction (QuEChERS). Cucumber solution diluted with ultrapure water, and filtered by 0.22 μm water phase. Then 0.1% formic acid water (A) and acetonitrile (B) were used as mobile phase for isocratic elution. Results： The results showed that a good linearity was obtained for the standard curve of the method, its correlation was high, R2=0.999 8. Its detection limit was …
Preparation Of Chitosan/Bentonite Composites By Impingement Flow-Hydraulic Cavitation And Its Application,
2023
Guangxi Key Laboratory of Green Processing of Sugar Resources 〔Guangxi University of Science and Technology〕, Liuzhou, Guangxi 545006, China;Province and Ministry Co-sponsored Collaborative Innovation Center of Sugarcane and Sugar Industry, Nanning, Guangxi 530004, China
Preparation Of Chitosan/Bentonite Composites By Impingement Flow-Hydraulic Cavitation And Its Application, Wang Ning, Huang Chengdu, Pang Xi, Huang Yongchun
Food and Machinery
Objective: In order to solve the problem that the preparation of chitosan/montmorillonite composites by traditional mechanical stirring was time-consuming and not conducive to scale-up production. Methods: Chitosan/montmorillonite composites were prepared by impinging stream hydrodynamic cavitation, the effects of four factors, namely chitosan dosage, chitosan molecular weight, reaction time and reaction temperature on the organic ignition loss were investigated, and then the optimum method of preparation was optimized by using the L9（34） orthogonal test. The structure of the composite was characterized by scanning electron microscopy, infrared spectroscopy, X-ray diffraction and Specific surface analyzer. Results: The optimal solution …
Modeling Analysis And Protection Study Of Vertical And Horizontal Vibrations In Hami Melon Logistics Packages,
2023
Tianjin University of Commerce, Tianjin 300134, China;Xinjiang Institute of Engineering, Urumqi, Xinjiang 830023, China
Modeling Analysis And Protection Study Of Vertical And Horizontal Vibrations In Hami Melon Logistics Packages, Zhang Lianwen, Xie Xiaoding, Wu Yuzhu, Zhang Chao, Gao Jia, Xu Bin
Food and Machinery
Objective: Optimized cushioning packaging. Methods: Taking Hami melon and its packaging as the research object, conducted sweep frequency vibration test on 5-layer stacked packaging, measured the natural frequency, maximum power Spectral density and peak acceleration of the vertical and horizontal vibration of each layer of packaging, and established the relational model between the maximum power spectral density, peak acceleration and stacking layer. Results: The higher the packaging, the larger the maximum power spectral density and peak acceleration in both vertical and horizontal directions. The maximum power spectral density and peak acceleration in the vertical direction of the same layer of …
Changes In Quality And Flavor Of Frozen Semi-Dried Pomfret Under Simulated Logistics And Transportation Conditions,
2023
College of Food Science and Engineering, Hainan University, Haikou, Hainan 570100, China
Changes In Quality And Flavor Of Frozen Semi-Dried Pomfret Under Simulated Logistics And Transportation Conditions, Duan Rubi, He Yanfu, Qiu Dan, Xia Guanghua, Li Yongcheng
Food and Machinery
Objective: This study aimed to investigate the changes in quality and flavor of semi-dried gold pomfret during the thawing process of logistics transportation. Methods: The logistics transportation process of frozen semi-dried gold pomfret was simulated at different temperatures. The thawing-loss rate, changes in myofibrillar protein conformation, physical and chemical indexes of protein, lipid oxidation and changes in flavor substances were determined. Results: The protein and lipid oxidation degrees of pomfret were significantly increased with the extension of transport time (P＜0.05). The oxidation degree was (P＜0.05) more significant as the temperature increased. During this process, protein aggregation …
Analysis On Quality In Three Kinds Of Basal Tea Of Noval-Jasmine Tea Beverage,
2023
Guangxi Subtropical Crops Research Institute, Nanning, Guangxi 530001, China;Guangxi Subtropical Agro-products Processing Research Institute, Nanning, Guangxi 530001, China
Analysis On Quality In Three Kinds Of Basal Tea Of Noval-Jasmine Tea Beverage, Zhang Fen, Chen Jiaxian, Yuan Dongyin, Zhang Xuhao, Wen Lixiang
Food and Machinery
Objective: This study aimed to explore the quality features of basal tea of noval-jasmine tea. Methods: Taking three kinds of basal tea（Fujian Xianghao, Yunnan Maojian, Sichuan Xiangming）of noval-jasmine tea beverage scenting tea dhool from Fujian, Yunnan and Sichuan as the research objects, the quality of the base tea including main biochemical components, taste, aroma were analyzed by electronic tongue, solid phase microextraction combined with gas chromatography-mass spectrometry (GC-MS), sensory evaluation and chemical analysis. Results: Water extracts of three kinds of basal tea was 49.40%~51.40%, tea polyphenols was 18.00%~23.20%, caffeine was 3.20%~4.30%, free amino acid was 3.32%~3.50%. The main biochemical components …
Study On The Effect Of Ultrasonic Aging Of Crude Baijiu After Second Distillation,
2023
College of Food and Chemical Engineering, Shaoyang University, Shaoyang, Hunan 422000, China
Study On The Effect Of Ultrasonic Aging Of Crude Baijiu After Second Distillation, Zhang Yingying, Chen Xuepeng, Yu Yougui, Tan Wenjun, Wu Jinlan, Dai Shan, Zheng Qing
Food and Machinery
Objective: Accelerated manmade aging of base liquor after heavy distillation. Methods: A single factor experimental design method was adopted based on the study of impurity removal in second distillation of Luzhou-flavor crude Baijiu. The changes in the content of total acids and total esters in the liquor were used as indicators to preliminarily explore the effect of ultrasonic treatment conditions on the crude Baijiu. Results: The results showed that: among the three single factors of ultrasonic treatment power, temperature and time, there were varying degrees of differences between the levels of each individual factor; At an ultrasonic frequency of 45 …
Purification And Comparison Of Enzymatic Properties Of Endogenous Transglutaminase Between Silver Carp And Black Carp,
2023
College of Food Science and Technology, Huazhong Agricultural University, Wuhan, Hubei 430070, China;National R & D Branch Center for Conventional Freshwater Fish Processing 〔Wuhan〕, Huazhong Agricultural University, Wuhan, Hubei 430070, China
Purification And Comparison Of Enzymatic Properties Of Endogenous Transglutaminase Between Silver Carp And Black Carp, Yi Lin, An Yueqi, Liu Ru, Hu Yang, Xiong Shanbai
Food and Machinery
Objective: This study aimed to investigate the differences in enzymatic properties of endogenous transglutaminase （TGase） in silver carp and black carp. Methods: STG and BTG were purified from the muscle of silver carp and black carp, respectively, by 80% ammonium sulfate precipitation, Q-Sepharose FF, and Sephacryl S-200 HR chromatographies. Two enzymes were analyzed for relative molecular weights, peptide sequences, secondary structures, optimal reaction conditions, and thermal inactivation kinetics. Results: The purified STG and BTG showed similar relative molecular weights, of which the enzyme activities were 14.34 U/mg and 12.67 U/mg, respectively. Both enzymes showed differences in peptide sequences. The secondary …
Screening And Identification Of Bifidobacterium Longum From Maternal Milk And Its Domestication Of Oxygen-Domestication,
2023
College of Food Science, South China Agricultural University, Guangzhou, Guangdong 510640, China;Institute of Food Biotechnology, South China Agricultural University, Guangzhou, Guangdong 510640, China;Research Center for Micro-Ecological Agent Engineering and Technology of Guangdong Province, Guangzhou, Guangdong 510640, China
Screening And Identification Of Bifidobacterium Longum From Maternal Milk And Its Domestication Of Oxygen-Domestication, Zhang Feng, Hou Xinyue, Guo Liqiong, Liu Chunhua, Lin Junfang
Food and Machinery
Objective: To screen Bifidobacterium from breast milk and improve its oxygen tolerance under aerobic conditions. Methods: Dilution and spread plate methods were performed to separate and screen Bifidobacterium from breast milk. Their Bifidobacterium identifications were characterized by 16S rDNA sequencing. The oxygen tolerant domestications were conducted through gradual increase of oxygen pressure and alternation of aerobic and anaerobic cultivations. Results: A novel Bifidobacterium strain was isolated from human milk and was identified as Bifidobacterium longum by 16S rDNA sequencing, which was named as MEFZ-2201. The homology between MEFZ-2201 and model strain (accession number in NCBI: ON631733.1) reached 100%. After oxygen …
Effect Of Different Processing Temperature On Texture Profile And Flavor Of The Edible Bird's Nest,
2023
School of Food Science and Technology, Jiangnan University, Wuxi, Jiangsu 214122, China
Effect Of Different Processing Temperature On Texture Profile And Flavor Of The Edible Bird's Nest, Shang Kexin, Qiu Shuang, Zhang Lan, Cheng Xiangrong, Wang Dongliang
Food and Machinery
Objective: This study aimed to investigate the effects of different processing temperature on texture profile and flavor of dried edible bird's nest. Methods: With dried edible bird's nest as the main raw material, the texture profile analysis of edible bird's nest at different processing temperature was carried out by physical property analyzer. The volatile components of edible bird's nest at different processing temperature were determined by electronic nose and solid phase microextraction gas chromatography-mass spectrometry (SPME-GC-MS). Results: It was found that the adhesion of cooked edible bird's nest decreased significantly (P<0.01), but its resilience increased significantly (P<0.05) with the increase of temperature. 12 kinds of effective flavor substances were detected in the cooked edible bird's nest by SPME-GC-MS, including: 3 alcohols, 2 aldehydes, 2 esters, 3 ketones, 1 acid, and 1 ether, accounting for 6.23%, 49.34%, and 54.85% of the total detected substances in the cooked edible bird's nest at 95 ℃, 105 ℃ and 115 ℃, respectively. Conclusion: Different processing temperature affects the taste of edible bird's nest and the overall odor profile after processing. Moreover, higher cooking temperature tends to make the egg white-like flavor stronger. The volatile substances in the bird's nest stew at 95 ℃ are mainly acids, the bird's nest cooked at 105 ℃ mainly produces alcohols, and the edible bird's nest cooked at 115 ℃ mainly produces ketones and alcohols.
Analysis Of Volatile Flavor Components And Characteristics Of Dough Fermented With Flavor Fermentation Liquid,
2023
Hubei Key Laboratory of Biologic Resources Protection and Utilization, Hubei Minzu University, Enshi, Hubei 445000, China;School of Forestry and Horticulture, Hubei Minzu University, Enshi, Hubei 445000, China
Analysis Of Volatile Flavor Components And Characteristics Of Dough Fermented With Flavor Fermentation Liquid, Zhang Yanmei, Zhu Yuchang, Yang Dandan, Pan Xufang, Bai Hui, Zhou Dazhai
Food and Machinery
Objective: This study aimed to investigate the varieties and contents of volatile components in fermented dough with flavor fermentation broth at different fermentation time. Methods: Headspace solid phase microextraction-gas chromatography (HS-SPME-GC-MS) was used to determine the volatile flavor substances in the dough of the flavor ferment at 12, 24, 36, 48 and 72 h. Also, sensory evaluation of the odor and determination of pH value, total acidity (TAA) and rheological properties of the dough were measured. Results: The strength of eight odors (frankincense, cheese, flower, fruit sweet, wine, malt, grass and sour) showed different performance, depending on the types and …
Effects Of Thawing Methods On The Quality, Physicochemical Properties And Microstructure Of Pork,
2023
College of Food Science and Technology, Hunan Agricultural University, Changsha, Hunan 410000, China
Effects Of Thawing Methods On The Quality, Physicochemical Properties And Microstructure Of Pork, Wang Li, Chen Wei, Wang Yuanliang, Li Zhongjun, Xia Di
Food and Machinery
Objective: To investigate the best defrosting method for frozen pork. Methods: Investigated the effects of three thawing methods, namely low-frequency electric field thawing, air thawing and hydrostatic thawing, on the juice loss rate, moisture content, water holding capacity, pH, colour difference, volatile saline nitrogen, total bacterial colony, textural characteristics, fat oxidation and protein oxidation of pork after thawing. Results: The low frequency electric field thawing resulted lower juice loss (1.09%), shear force (2 600.15 N), increase in thiobarbituric acid value (TBARS) (62.50%), good colour, pH close to that of fresh meat, less protein oxidation, richer taste material, less damage to …
Spin-Flash Drying Characteristics And Kinetic Model Of Antarctic Krill,
2023
Fishery Machinery and Instrument Research Institute, Chinese Academy of Fishery Science, Shanghai 200092, China;Key Laboratory of Ocean Fishing Vessel and Equipment, Ministry of Agriculture; Shanghai 200092, China
Spin-Flash Drying Characteristics And Kinetic Model Of Antarctic Krill, Tan Jiayu, Ouyang Jie, Ma Tiantian, Shen Jia
Food and Machinery
Objective: The purpose of this study was to investigate the drying characteristics and establish the kinetic model of Antarctic krill during spin-flash drying. The drying experiments were carried out at 120 ℃ to 180 ℃. Methods: Six common thin-layer drying models were selected to fit the experimental data. Further, the equations of drying model constant and temperature were established to obtain the model expression and validate the optimal drying model. The effective moisture diffusion coefficients were calculated by Fick's second law. Results: The results showed the drying temperature had a significant effect on drying thermal efficiency and drying rate. The …
Preparation Of Matrix Reference Material For Carbaryl Residues In Chinese Yam Flour,
2023
Chinese Academy of Inspection and Quarantine, Beijing 100176, China;CAIQ 〔Beijing〕 Science and Technology Co., Ltd., Beijing 100176, China
Preparation Of Matrix Reference Material For Carbaryl Residues In Chinese Yam Flour, Huo Siyu, Gen Xuhao, Yu Libo, Chen Dongdong, Peng Tao
Food and Machinery
Objective: This study aimed to establish a method for the Preparation of matrix reference material for carbaryl residues in Chinese yam flour. Methods: Yam powder containing menafyl was prepared by homogenized, freeze-dried, ground, sifted, mixed and packaged. A liquid chromatography-series mass spectrometer was used for detection, and the isotope internal standard curve method was used for quantification. Through the process of equalization stability evaluation, cooperative setting and uncertainty evaluation, the matrix reference material of the expected yam powder was obtained. Results: The property value and expanded uncertainty of carbaryl was (1.04±0.10) mg/kg (k=2). Conclusion: It could be used …
Determination Of Eight Anions In Liquid Milk,
2023
Guangzhou Inspection Testing and Certification Group Co. Ltd., National Quality Testing Center for Processed Food 〔Guangdong〕, Guangzhou, Guangdong 511447, China
Determination Of Eight Anions In Liquid Milk, Wu Ziling, Yao Xiaoqing, Shen Yingtao, Huang Jiale, He Minheng
Food and Machinery
Objective： A rapid method was established for the simultaneous determination of variety anions in liquid milk. Methods： The macromolecular protein in liquid milk was precipitated by acetonitrile, and a variety of anions were extracted. After purification by C18 column, the material was separated by Dionex IonPac AS19-HC ion column with gradient elution of potassium hydroxide and conductivity detection. Finally, a method for the determination of bromate, thiocyanate, nitrite, nitrate, chlorate, perchlorate, phosphate and iodine ion in liquid milk was established using ion chromatograph. Results： The results showed that the correlation coefficients （R2）of eight kinds of anion …
Determination Of 17 Aldehydes In Baijiu （Chinese Liquor） By Direct Injection Gas Chromatography,
2023
Sichuan Institute of Food Inspection, Chengdu, Sichuan 610000, China;Key Laboratory of Baijiu Supervising Technology for State Market Regulation, Chengdu, Sichuan 610000, China
Determination Of 17 Aldehydes In Baijiu （Chinese Liquor） By Direct Injection Gas Chromatography, Luo Yue, Zhong Ciping, Huang Ping, Chen Yanmei, Tang Jing, Yu Xiaoqin
Food and Machinery
Objective: To explore the content of aldehydes in Baijiu. Methods: A method for the determination of 17 aldehydes in Baijiu was established, and the methodological performance indexes were studied using statistics. Results: Through statistical analysis, the detection limit of 17 aldehydes in Baijiu was determined to be 0.7～5.9 mg/L, the limit of quantification was 1.9～14.6 mg/L, which passes the quality inspection of the calibration curve within the range of 0.6～320.0 mg/L, and the linear relationship meets the requirements. The recovery rate of intermediate standard addition in Baijiu was 73%～114%, the coefficient of variation in the laboratory was ≤11%, and the …
Solid Phase Extraction-Gas Chromatography-Flame Ionization Detection （Spe-Gc-Fid） For The Detection Of Mineral Oil Saturated Hydrocarbons （Mosh） In Infant Formula,
2023
Hunan Provincial Institute of Product and Goods Quality Inspection, Changsha, Hunan 410017, China
Solid Phase Extraction-Gas Chromatography-Flame Ionization Detection （Spe-Gc-Fid） For The Detection Of Mineral Oil Saturated Hydrocarbons （Mosh） In Infant Formula, Tang Wanli, Feng Yanying, Xiang Jun, Qin Haijiao, Hu Lingli
Food and Machinery
Objective: To establish a new accurate method for the determination of mineral oil saturated hydrocarbon （MOSH） in infant formula by solid phase extraction combined with gas chromatography-Flame Ionization Detection （SPE-GC-FID）. Methods: Different extraction methods such as soaking extraction, oscillating extraction, ultrasonic assisted extraction, liquid-liquid extraction were used to extract MOSH from infant formula milk powder, and different extraction solvents such as n-hexane, isooctane, benzene, mixed solvents were used to extract MOSH. The optimal extraction method and extraction solvent were determined based on the extraction amount of MOSH. The target compounds purified by AgNO3 SPE column, and finally detected by …
Determination Of 5 Kinds Of Biogenic Amines In Cheeses By High Performance Liquid Chromatography-Tandem Mass Spectrometry,
2023
School of Biological and Chemical Engineering, ZheJiang University of Science ＆ Technology, Hangzhou, Zhejiang 310023, China
Determination Of 5 Kinds Of Biogenic Amines In Cheeses By High Performance Liquid Chromatography-Tandem Mass Spectrometry, Zhang Hui, Cao Hui, Wang Jin, Xiao Gongnian, Jiang Kan
Food and Machinery
Objective: A new technical idea was provided for the study of biogenic amine formation mechanism and food safety risk assessment. Methods: An analytical method was established for determination of tyramine, phenylethylamine, tryptamine, octopamine and cadaverine in cheeses with high performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS). Biogenic amines were extracted by ultrasonic-assisted solvent extraction from cheeses, and were separated by HILIC column, determined by positive electrospray ionization (ESI) with multiple reaction monitoring (MRM) mode, quantified by the internal standard method. The effect of extraction solvent type, ultrasonic time and matrix effect on the peak area was studied, and the performance of …
Numerical Simulation Of Factors Affecting Flow Characteristics Of Double-Circular-Arc Gear Pump,
2023
College of Mechanical and Electrical Engineering, Henan University of Science and Technology, Luoyang, Henan 471003, China
Numerical Simulation Of Factors Affecting Flow Characteristics Of Double-Circular-Arc Gear Pump, Huang Cheng, Xu Kai, Wei Zhibo, Li Geqiang
Food and Machinery
Objective: Analyzed the influencing factors of the internal flow field pulsation characteristics of the new double circular arc gear pump, and adopt reasonable parameters to improve the output efficiency of the gear pump. Methods: The two-dimensional flow field simulation model of the gear pump was established, and the computational fluid dynamics software Fluent was used for simulation analysis to study the influence of different tip clearance, different gear eccentricity, load and speed on the instantaneous flow, flow pulsation and flow field characteristics of the oil outlet of the gear pump. Results: As the tooth tip clearance increased, the outlet flow …
Simulation Analysis Of Influence Of Pitch Variation On Flow Field Of Twin Screw Extruder With Different Direction,
2023
School of Artificial Intelligence, Being Technology and Business University, Beijing 100048, China;Plastic Beijing Municipal Key Laboratory of Health and Safety Quality Evaluation Technology, Beijing 100048, China
Simulation Analysis Of Influence Of Pitch Variation On Flow Field Of Twin Screw Extruder With Different Direction, Zhang Yiming, Huang Zhigang, Xu Zhen, Cheng Yuanyuan
Food and Machinery
Objective: Taking polylactic acid （PLA） as an example, the flow channel distribution of twin-screw extrusion under different pitch was studied. Methods: In Solidworks, two 3D models with variable pitch and constant pitch were drawn according to the theoretical end curve equation and modified. Workbench software was used to generate the required analysis models with the swept mesh method for the two screw configurations, and then Polyflow fluid simulation software was used to simulate the actual situation. After obtaining the post-processing results, FieldView software was used to analyze the final results. The pressure, shear rate and viscosity of polylactic acid fluid …
Research On Trajectory Planning Method For Camellia Oleifera Fruit Sorting Robot Based On Multi-Objective Optimization,
2023
JiangsuJinhu Secondary Professional School, Huai'an, Jiangsu 223001, China
Research On Trajectory Planning Method For Camellia Oleifera Fruit Sorting Robot Based On Multi-Objective Optimization, Fu Mingdi, Li Zhong, Wang Qianru, Zhao Fei
Food and Machinery
Objective: Solved the problems of poor motion stability and accuracy in the food sorting process of parallel robots. Methods: Based on the analysis of the three degree of freedom food sorting robot system, a method proposed which combined polynomial interpolation and improve multi-objective particle swarm optimization algorithm for Delta robot trajectory optimization. As a parallel robot, the optimization of the shortest operation time, lowest energy consumption, and minimal motion impact were taken as multiple objectives. The improved multi-objective particle swarm optimization algorithm was applied to optimize the polynomial interpolation method, and its performance was validated. Results: The planning trajectory of …
