Engineering Commons^™

The Influence Of Aluminium Dross Residue And Coal Fly Ash On The Properties Of Geopolymers, Haswanee Phungpha, Pitak Laoratanakul, Benya Cherdhirunkorn

Journal of Metals, Materials and Minerals

In this research, aluminium dross residue (AD) and coal fly ash (FA) were used for the production of geopolymers. The illegal dumping of AD and the high cost for AD waste disposal have been problems for long time in Thailand. Therefore, the feasibility of using AD (0 wt% to 100 wt%) in the geopolymer production had been carried out to find the alternative way to resolve these problems. The alkaline solution of NaOH 7 M and Na2SiO3 with the ratio of 1:3 was used for the geopolymerization reaction. It was found that the addition of AD caused the ammonia gas …

Tin Oxide Nanoparticle Extraction From Waste Solder Dross Via Low-Temperature Hydrometallurgical Process, Tanongsak Yingnakorn, Sirunya Somla, Thanapon Chandakhiaw, Ethan Cheung, Sakhob Khumkoa

Journal of Metals, Materials and Minerals

This study proposes a hydrometallurgical approach to valorising industrial waste by producing SnO2 nanoparticles (NPs) from waste solder dross obtained by skimming off of tin solder baths from electronic dipping processes. The process involves leaching the dross with aqueous hydrochloric acid solution and hydrogen peroxide, followed by precipitation with ammonium hydroxide and purification with aqueous nitric acid solution. The optimised leaching conditions were determined to be 4 mol∙ L‒1 HCl, 11% v/v H2O2, 25℃, and a leaching time of 15 min. SnO2 NPs were successfully precipitated at pH 4 using 25% v/v NH4OH and purified with 1 mol∙ L‒1 HNO3. …

Investigation Of Pressure And Temperature Distributions In Aerofoils Using Cfd Simulation, Ramesh Krishnan L., Jasgurpreet Singh Chohan, S. Vijayakumar, N. Beemkumar, Sriram Desikan, V. Nagabhushana Rao, M.Naga Swapna Sri, Mayank Kundlas

Journal of Metals, Materials and Minerals

Most aircraft derive the design of their wings, fins, and horizontal stabilizers from this construction approach, incorporating curved surfaces to enhance the lift-to-drag ratio during flight. Over the past decade, Computational Fluid Dynamics (CFD) has become the leading tool for designing components and processes involving fluid or gas movement across industries such as aviation, automotive, and manufacturing. This study examines the aerodynamic characteristics—including pressure, density, and temperature distribution, as well as lift and drag forces—of two different angles of attack based on the M13 and Eppler 1233 airfoils. The analysis considers an airfoil with varying chord thickness while maintaining a …

Photocatalytic Behaviour Of (Biybo3)0.5-(Batio3)0.5, Yasaswi Priyadarshini Samal, Subhalaxmi Patra, Tapan Das, Minakshi Padhy

Journal of Metals, Materials and Minerals

Different organic compounds like dyes and pharmaceutical contaminants pollute a large amount of water which can increase the chemical oxygen demand in water bodies. The photodegradation of dyes has been widely studied using TiO2-based nanomaterials, which are typical photocatalysts. TiO2 is highly effective in reducing pollutants when exposed to UV light and does not cause secondary pollution. However, TiO2 is only functional when exposed to UV light, which is not ideal for real-world use. This drawback of TiO2 pulls the research towards modified photocatalysts for better yield. In this study, the (BiYbO3)0.5 - (BaTiO3)0.5 material was formulated by solid state …

Synergistic Effects Of Co-Ni Nanoalloys On Sio2@Tio2: A Novel Approach To Photocatalytic Tetracycline Degradation, Pratyush Kumar Sahu, Alaka Rath, Aslisha Champati, Ashish Madual, Pravat Manjari Mishra, Abanti Pradhan, Brundabana Naik

Journal of Metals, Materials and Minerals

To develop a cost-effective alternative to noble metal catalysts for photocatalysis, we synthesized a series of bimetallic Co-Ni nanoalloys on core-shelled SiO2@TiO2 nanostructures via a chemical reduction approach. The research demonstrates the photocatalytic behaviour of the Co-Ni alloy-enhanced SiO2@TiO2 (ST-Co, Ni) hybrid nanocatalyst, focusing on its crystalline structures, morphological shapes, chemical conditions, and optical properties, utilizing techniques such as X-ray diffraction, field emission scanning electron microscopy, UV-visible diffuse reflectance spectroscopy, photoluminescence spectroscopy, transmission electron microscope, and electrochemical analysis. The catalyst was evaluated for its effectiveness in degrading tetracycline, an overused antibiotic that persists in aquatic environments and is known for …

Studies Of Structural, Microstructural, Dielectric, And Electrical Characterization Of Binaznmoo6 Double Perovskite, Swati Panda, Supriya Barik, Ritu Purna Sahu, Adwit Prasad Sahu, S. Mishra, S. K. Parida

Journal of Metals, Materials and Minerals

This study investigates the structural, microstructural, dielectric, and electrical properties of BiNaZnMoO₆ (BNZM) ceramic synthesized using a conventional solid-state reaction method. Preliminary structural analysis using X-ray diffraction (XRD) suggests orthorhombic crystal symmetry. Scanning electron microscopy (SEM) micrographs reveal a uniform distribution of well-grown grains with well-defined grain boundaries, which may contribute to the enhanced dielectric properties. Energy dispersive X-ray spectroscopy (EDX) analysis confirms the presence of all constituent elements Bi, Na, Zn, Mo, and O in the studied sample. Dielectric spectra analysis as a function of frequency and temperature indicates the formation of high-quality dielectric materials, evidenced by a high …

Graphitic Carbon Nitride Loaded Bi4o5i2 For Elevated Photocatalytic Tetracycline Degradation, Subhasish Mishra, Barsha Marandi, Kali Sanjay, Rashmi Acharya

Journal of Metals, Materials and Minerals

As a robust photocatalyst, Bi4O5I2 have has attracted significant scientific interest owing to its narrow bandgap energy, escalated electronic properties and high stability. Nonetheless, the unfavourable band structure and higher recombination of excitons have restricted its diversified photocatalytic applications. In this context, binary heterojunction construction using Bi4O5I2 could be considered an effective strategy for spatial charge carrier separation across the hetero-interface, leading to an enhanced activity. In this study, we have prepared Bi4O5I2/g-C3N4 Z-scheme hetero-structures via a wet impregnation strategy that preserves the spherical structure of Bi4O5I2. The phase purity, chemical bonding, morphology and microstructure of the composite were confirmed …

Oxidation Of Sn-1 Wt.% Bi In Air And In Oxygen Deprived Environment, Pakawat Polmanee, Benjie Fernandez, Patama Visuttipitukul, Ittipon Cheowanish, Tachai Luangvaranunt

Journal of Metals, Materials and Minerals

Oxidation of Sn-1wt% Bi in air and in oxygen deprived environment is studied in this research. Electrochemical process with SERA technique was used to determine oxide film thickness and rate of oxidation of tin alloy. The thickness of oxide film at 72 hours of the specimens that is tested in air, in vacuum, in argon environment, and wrapped with plastic film are 16, 10, 18, and 13 Å respectively. XPS was used to determine the type of oxides in the oxide layer. Result after signals deconvolution shows that SnO and SnO2 compounds were formed on the Sn-1wt% Bi surface.

Solar Radiation Assisted Photocatalytic Degradation Of Congo Red Using Ce Doped Lacoo3, Rishabh Kamal, Rasmirekha Pattanaik, Debapriya Pradhan, Suresh Kumar Dash

Journal of Metals, Materials and Minerals

A viable sol-gel synthesis technique was used to synthesize LaCoO3 and Ce doped LaCoO3 for degradation of congo red dye taking a renewable source of light i.e solar radiation. The crystalline structure, morphology, and optical properties of the synthesized catalysts were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) analysis of Ce-doped LaCoO₃ confirmed the presence of La (3d), Ce (3d), Co (2p), C (1s), and O (1s) and their valence states in the perovskite matrix, Fourier-transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and ultraviolet diffuse reflectance spectroscopy (UV-DRS). The XRD analysis with a prominent diffraction peak detected …

Optimization And Characterization Of Carrageenan/Alginate Ratio And Seaweed Waste To Develop Composite Bioplastics From Kappaphycus Alvarezii, Ali Ridlo, Retno Hartati, Agus Sabdono

Journal of Metals, Materials and Minerals

Carrageenan and alginate, derived from seaweed, offer potential as alternatives to traditional plastics. This study aims to assess the properties of biodegradable bioplastics made from a composite of carrageenan, alginate, and waste from K. alvarezii seaweed carrageenan extraction. A mixture of carrageenan and alginate was added with a ratio of 4:6 and K. alvarezii extraction waste 0, 20, 40, 60, and 80 % waste concentration,  in the carrageenan-alginate-waste mixture. The process involves blending carrageenan, alginate, waste, glycerol, and distilled water until uniform at 90o C and 1000 rpm for 45 minutes, followed by molding, immersion in a 4% CaCl2 solution, …

Green-Synthesized Yttrium-Doped Cerium Oxide Nanoparticles: A Promising Optical Material, Sasmita Sarangi, Nibedita Nayak, Binita Nanda, Tapas Sahoo

Journal of Metals, Materials and Minerals

This work focuses on the green synthesis, characterization, and optical properties of yttrium-doped cerium dioxide (CeO2) nanoparticles. A green approach was adopted using Acacia concinna fruit extract as surfactant and stabilizing agent. Their structural, morphological, and physical-chemical properties were characterized using different analytical techniques, like XRD, FE-SEM, FTIR, PL, Raman, UV-Visible Spectroscopy. XRD study validated the structure of cubic fluorite-type structure of CeO2 nanoparticles, with the average crystallite size ranging between 7-15 nm. Raman spectroscopy validated this structure with F2g band observed at 463 cm−1. FESEM images showed irregular spherical morphologies with grain sizes in the range of 50-60 nm. …

Pyrolysis And Modification Of Coconut Shell Into Sulfonated Biochar And Its Catalytic Activity On Cellobiose Conversion, Addy Rachmat, Yessi Eka Wahyu, Poedji Loekitowati Hariani, Fahma Riyanti, Fatma Fatma

Journal of Metals, Materials and Minerals

Coconut shell was successfully valorized into sulfonated biochar through carbonization in various temperatures and duration. This work aims to provide suitable solid acid carbonaceous catalyst for cellobiose conversion into valuable product. Sulfonated biochar is characterized to evaluate its crystallinity, sulfonate, and oxygenated functional groups by XRD method and FTIR spectroscopy. The resulting solid acid carbonaceous material was tested toward cellobiose hydrolysis to assess its catalytic activity in various time, temperature, and catalyst weight. FTIR spectra reveals some of the biochar product has sulfonate group as indicated by absorbance band at 1234 cm‒1, 1070 cm‒1 and 1180 cm‒1, which belongs to …

Macro-Encapsulation Of Polyethylene Glycol And Magnetite (Fe3o4) In Concrete As Phase Change Materials For Building Thermal Management, Muhammad Fauzi, Budhy Kurniawan, Anggito Pringgo Tetuko, Timbangen Sembiring, Fanna Nilam, Amdy Fachredzy, Perdamean Sebayang

Journal of Metals, Materials and Minerals

Thermal management technology is a crucial strategy for reducing energy consumption in buildings by utilizing stored solar energy. This study developed a polyethylene glycol (PEG)-based phase-change material (PCM), selected for its superior physicochemical stability, high latent enthalpy, and environmental compatibility. To enhance thermal conductivity, 20 vol% magnetite (Fe₃O₄) was incorporated into the PEG matrix. The composite was synthesized via an ultrasonic-assisted method (37 kHz, 80°C, 1 h). X-ray diffraction (XRD) confirmed the crystalline structure of PEG and the cubic phase of Fe3O4, while Fourier-transform infrared spectroscopy (FTIR) validated the synthesis by identifying Fe–O, C–H, and O–H functional groups. Scanning electron …

The Effect Of Pt And Pd Decoration On Sno2 Slant Nanorods Fabricated Using Dc Magnetron Sputtering With Oad Technique For Co Gas Sensing Applications, Nampueng Pangpaiboon, Thitiporn Kaewyou, Sethavut Duangchan, Kata Jaruwongrungsee, Manatsawee Srirak, Tossaporn Lertvanithphol, Viyapol Patthanasettakul, Tawee Pogfay, Mati Horprathum, Saksorn Limwichean

Journal of Metals, Materials and Minerals

This research investigates the effect of Pt and Pd decoration on the structure of SnO2 slant nanorods (SNRs) films produced using DC magnetron sputtering with Oblique Angle Deposition (OAD), as well as their impact on the films' physical properties and gas sensing applications. Pt and Pd were deposited onto the SnO2 SNRs for the same duration of 20 s each. Following deposition, all the films were heat-treated temperature at 400℃ for 2 h. The characterization of both as-deposited and annealed films involved analyzing the physical morphology using FE-SEM and the crystal structure using GI-XRD. It was observed that the structure …

Microwave Absorption Properties Of Porous Activated Carbon/Nickel Oxide Composites Derived From Coconut Husks, Mohamad Zul Aqiman Shukeri, Nor Zakiah Yahaya, Ezzan Afifah Zainuddin, Nazri Mahmud, Liyana Zahid, Hasliza A. Rahim

Journal of Metals, Materials and Minerals

Porous Activated Carbon (AC) is a promising material for microwave absorbing materials, showing potential in communication and modern warfare. The study explores the process of creating porous AC from coconut husks using hydrochloric acid and carbonization at varying temperatures, followed by doping AC with nickel oxide to create an AC/NiO polymer composite with varying thicknesses. These composites are compared to AC composites loaded in a paraffin matrix. The dielectric and microwave (MW) properties of the AC/NiO and AC polymer composites at various thicknesses were analyzed using a Performance (PNA)-X Network Analyzer. The study also examines the carbon content and porosity …

Improvement In Electrical And Energy Storage Properties Of Lead-Free Bnkt-Bt Piezoceramics, Manlika Kamnoy, Supalak Manotham, Pichitchai Butnoi, Sukum Eitssayeam, Piewpan Parjansri

Journal of Metals, Materials and Minerals

The electrical characteristics and energy storage performance of BNKT-BT lead-free piezoceramics were examined. All ceramics were produced via the mixed oxide technique. The findings indicated that the density of this ceramic system varied between 5.61 and 5.83 g/cm3. Conditions with 2.0 mol% (BT=0.02) and 6.0 mol% (BT=0.06) exhibited the largest dielectric constant (er) at both ambient temperature and elevated temperature, with values of 1307 and 4272, respectively. The ceramic sample with BT = 0.06 exhibited the highest values of %strain ~0.13 and a d*33 ~179.65 pm/V. Furthermore, BT-doped ceramics yielded optimal energy storage densities compared to undoped BNKT ceramics. The …

Optimization Of Indigo Dyeing On Modal Fabrics Using Thiourea Dioxide As An Environmentally Friendly Reducing Agent, Monthon Nakpathom, Buppha Somboon, Nootsara Narumol, Rattanaphol Mongkholrattanasit, Pisutsaran Chitichotpanya, Nattaya Vuthiganond

Journal of Metals, Materials and Minerals

This investigation examines the potential of thiourea dioxide as an environmentally reducing agent for dyeing of natural indigo on modal fabrics. Although traditional sodium dithionite is effective, its sulfur by-products generate environmental concerns. Thiourea dioxide, which provides a more environmentally friendly alternative, was studied under various dyeing conditions. In this study, six dyeing parameters, including thiourea dioxide and sodium hydroxide concentrations, reduction temperature, reduction duration, dyeing time, and reduction-oxidation cycles, were optimized to enhance color strength. Results indicated that the most favorable reduction conditions were achieved when 80 g/L of thiourea dioxide and 2 g/L of sodium hydroxide were heated …

Eco-Friendly Synthesis Of Flower-Like Hierarchical Structure Of Cuo Nps For Advancing Photocatalytic Efficiency And Antibacterial Applications, Yodchai Tangjaideborisut, Shanmugam Shanmugam, Supakorn Boonyuen, Govindasamy Siva, Prema Yugala, Joon Ching Juan, Choowin Phanawansombat, Atchariya Pitintharangkul, Seerangaraj Vasantharaj, Pornpan Pungpo, Pariya Na Nakorn

Journal of Metals, Materials and Minerals

In recent decades, environmental pollution caused by organic dyes and pathogenic microorganisms has posed significant challenges to both ecological and public health. Therefore, the development of multifunctional materials capable of simultaneously degrading dyes and exhibiting antibacterial properties is crucial for effective environmental remediation. Combining photocatalytic dye degradation with antibacterial activity offers a promising approach to address these dual concerns in a single process. The present study investigates the copper oxide nanparticles (CuNPs) were prepared by green synthetic method using bamboo extract for degradation of methylene blue and in inactivation of biological pathogens. The green synthesized CuONPs were characterized various spectroscopic …

Enhancing Efficiency And Productivity Of Microbial Fuel Cells For Optimization Of Wastewater Treatment With Bioenergy Production, Diptimayee Pradhan, Krishna Pada Bauri, Debarpita Ghosal, Satchidananda Mishra, Abhijeet Das, Aditya Raj Singh, Akhil Gedela, Kumbhakarna Mallik, Mohammed Hassan Ali Hbag

Journal of Metals, Materials and Minerals

The primary objective is to remove the pollutants from the wastewater streams and reintegrate them into the water cycle, therefore safeguarding the environment and promoting public health. The utilization of membrane fuel cells (MFCs) enables the conversion of organic molecules present in wastewater into electrical energy, while concurrently generating potable water. To optimize the process, it is essential to understand the parameters that affect the performance and the relevant techniques such as electrode materials, microbial collectives, and operating settings to improve the efficiency and performance of MFC. Thus, it aims to present novel ideas that support the real-world deployment of …

A Review On Recent Progress In Supported Magnetic Nanoparticles: From Synthetic Methods To Applications, Khushboo Dhiman, Ayashkanta Nanda, Navneet Kaur, Manvinder Kaur, Harvinder Singh Sohal, Himanshi Sharma, Meenakshi Verma

Journal of Metals, Materials and Minerals

Magnetic nanoparticles supported on various materials have recently gained significant attention due to their wide range of applications across multiple fields such as catalysis, biomedicine, environmental remediation, and magnetic separation. The support materials are essential for stabilizing magnetic nano-particles and enhancing their properties, thereby improving their performance and versatility. This review presents a comprehensive summary of recent advancements and key developments in supported magnetic nanoparticles, focusing on various support materials including silica, alumina, cellulose, charcoal, polymeric materials, and carbon nanotubes. We also discussed why we needed a shift from conventional nanoparticles to magnetic nanoparticles and from magnetic nanoparticles to supported …

Comprehensive Study On The Structural And Optical Properties Of Bismuth Manganese Oxide Composite Ceramic For Optoelectronic Applications, P. P. Nayak, B. Swain, R. R. Patro, S. S. Hota, O. P. Das, S. Bhuyan

Journal of Metals, Materials and Minerals

This work assessed the potential of bismuth manganese oxide composite ceramic for optoelectronic applications by methodically examining its structural, vibrational, and optical characteristics. X-ray diffraction (XRD) spectroscopy provided the coexistence of Bi12MnO20 (sillenite-type) and Bi2Mn4O10 (mullite-type) phases, indicating a deviation from the ideal perovskite structure and suggesting a complex crystallographic nature influencing its functional properties. Fourier transform infrared (FTIR) spectroscopy confirmed the modes of vibration of Bi–O and Mn–O bonds that were contained, supporting the structural composition. UV-Vis-NIR spectroscopy demonstrated strong optical absorption in the 300 nm to 800 nm range, affirming the suitability of the material for optoelectronic applications. …

Fem Modeling And Comparative Study Of Graphite Lubricants In The Hot Forging Of Aisi 1045 Medium Carbon Steel, Raschanan Poungprasert, Nattarawee Siripath, Naiyanut Jantepa, Surasak Suranuntchai

Journal of Metals, Materials and Minerals

This study investigates the performance of water-based and oil-based graphite lubricants in the hot forging of AISI 1045 medium carbon steel, aiming to enhance product quality while minimizing die wear. Utilizing Finite Element Method (FEM) simulations and experimental analysis, we examined key factors including flow lines, dimensional accuracy, forging load, and die wear. Results indicate that oil-based graphite lubricants significantly outperform water-based options, achieving a lower average error of 0.26% in dimensional accuracy compared to 0.99% for water-based lubricants. Additionally, oil-based lubricants resulted in reduced forming loads, leading to improved energy efficiency and longer die life. Microstructural analysis revealed that …

Effect Of Compaction Pressure On The Structure And Mechanical Properties Of Functionally Graded Aluminium-Glass Microsphere (Fgagm) Foams Produced By Powder Metallurgy Process, Vicheka Moeun, Seksak Asavavisithchai

Journal of Metals, Materials and Minerals

Functionally graded aluminium-glass microsphere (FGAGM) foams were successfully fabricated via powder metallurgy. The influence of compaction pressure on the structural and mechanical properties of the foams was systematically investigated. The study observed that increasing compaction pressure enhanced the green (pre-sintering) density of FGAGM foam, while post-sintering densities exhibited a decreasing trend with higher compaction pressures. The mechanical examination indicated that mechanical properties improved significantly with higher compaction pressures. While higher compaction pressures generally improve mechanical properties, the study identified that excessive pressures could lead to the fracture of GM particles, introducing defects that compromise the foam's structural integrity. Therefore, determining …

Structural Tuning Of Bioi Toward Bi O /Agi Heterostructures Via Room-Temperature Ion Exchange For Improved Photocatalytic Activity, Varunya Atimayulerd, Sorawit Thueanbangyang, Kittiyaporn Singsumphan, Ganyaporn Wongwaen, Cheewita Suwanchawalit, Montri Aiempanakit

Journal of Metals, Materials and Minerals

In this work, a bismuth oxide/silver iodide (Bi2O3/AgI) heterojunction photocatalyst was successfully fabricated via a room-temperature ion exchange process using bismuth oxyiodide (BiOI) as a morphology-directing precursor. Building upon our previous work on solvent-modulated BiOI nanostructures, this study employs a chemical transformation route to develop interfacially connected heterostructures while preserving key morphological features. Structural, morphological, and optical characterizations, including X-ray diffraction, field-emission scanning electron microscopy, energy-dispersive X-ray spectroscopy, Fourier-transform infrared spectroscopy, and ultraviolet–visible diffuse reflectance spectroscopy, provided supporting evidence for the successful formation of Bi2O3/AgI heterojunctions with likely close interfacial contact. The optimized Bi2O3/AgI composite with a 50:50 mass ratio …

Optically Stimulated Luminescence Dating Of Earthenware From The Nam Tok Khao Pang Archaeological Site, Kanchanaburi, Thailand, Thananan Phetkongtong, Peerasak Klubket, Santi Pailoplee, Pichet Limsuwan, Voranuch Thongpool

Journal of Metals, Materials and Minerals

The Nam Tok Khao Pang archaeological site, located in Tha Sao subdistrict, Sai Yok district, Kanchanaburi province, Thailand, is a limestone cave where numerous artifacts, including black-burnished earthenware fragments with in-curving rims, out-curving rims, and carinated bodies, have been discovered. Mineralogical and microstructural analyses using X-ray diffraction (XRD), energy-dispersive X-ray spectroscopy (EDS), and scanning electron microscopy (SEM) identified quartz (SiO₂) as the dominant mineral phase within a partially sintered silicate matrix. The absence of vitrification and the presence of mineral impurities indicate that the earthenware was fired at temperatures between 900°C and 1000°C. To determine the age of these ceramics, …

Facile Bio-Synthesis Of Cerium Oxide Nanoparticles, Characterization And Their Photocatalytic Potential In The Degradation Of Real Tannery Wastewater, Ganeshkumar Govindasamy, A. Babu Ponnusami

Journal of Metals, Materials and Minerals

The sustainable metal oxide photocatalysts using plant extract presents a viable alternative to conventional chemical synthesis techniques. In this study, spherical shaped cerium oxide nanoparticles were synthesized using ammonium ceric nitrate and Peepal Leaves (PL) extracted and used as a photocatalyst to remove hexavalent chromium and chemical oxygen demand from actual tannery wastewater. The characterization of cerium oxide nanoparticles was carried out using UV-Visible spectroscopy, X-ray diffraction, Fourier-transform infrared spectroscopy, Brunauer-Emmett-Teller surface area analysis, Field Emission-Scanning Electron Microscopy with energy-dispersive X-ray spectroscopy, Raman analysis, High Resolution-Transmission Electron Microscopy and Zeta potential analysis. The band gap energy of 3.25 eV was …

Reuse Of Calcium Carbonate (Caco3) Recovered From Discarded Carpets As Filler In Fiber-Reinforced Polymer (Frp) Composites, Roshan Devkota

Graduate Theses, Dissertations, and Problem Reports (ETD)

Over four billion pounds of carpet are discarded annually in the United States, making carpet waste a significant environmental concern. Calcium carbonate (CaCo₃) constitutes up to 45% of the mass of most synthetic carpets. Reusing this CaCo₃ as a filler in the rapidly growing fiber-reinforced polymer (FRP) industry, which is projected to reach USD 10.38 billion, presents a low-cost, practical approach to developing a market-based solution to post-consumer carpet waste.

This study investigates the reuse of CaCo₃ recovered from discarded carpet backing as a filler in FRP composites, focusing on its mechanical viability in comparison to virgin CaCo₃. The methodology …

Electrochemical And Nanomaterial Based Strategies For Nonenzymatic Glucose Detection: A Review, Reagan Aviha, Gymama Slaughter

Center for Bioelectronics Publications

Electrochemical glucose sensing technologies have undergone significant evolution, with continual advancements aimed at improving sensitivity, selectivity, and user convenience. This review systematically explores the development of emerging nonenzymatic glucose sensor designs. Nonenzymatic sensors are critically evaluated for their ability to overcome enzymatic limitations, leveraging novel materials and catalytic mechanisms. Additionally, the emergence of smartphone-integrated glucose monitoring systems is highlighted as the fifth generation, representing a paradigm shift toward personalized, real-time healthcare management. Emphasis is placed on the strategies employed to reduce the working electrode potential and enhance analytical performance. Key analytical metrics and real-sample applicability are evaluated, and persistent challenges …

Electro-Mechanical Behavior Of Core-Shell Carbon Grease-Silicone Fibers Fabricated Via Coaxial Direct Ink Writing, Fahrettin Kilic

Graduate Theses, Dissertations, and Problem Reports (ETD)

Highly stretchable strain sensors are essential components in soft electronics, enabling integration of sensing and signal transmission into deformable systems. This thesis explores the fabrication and characterization of coaxial core–shell fibers composed of a conductive carbon grease core and an elastomeric silicone shell. These fibers were produced using coaxial direct ink writing (DIW), a versatile additive manufacturing technique that allows continuous deposition of multi-material filaments. The goal was to achieve mechanically compliant yet electrically stable fibers capable of withstanding large deformations, suitable for applications in wearable electronics and soft robotics.
The printed fibers were systematically examined through mechanical tensile testing, …

Development Of Group Iii-V Quantum Confinement-Enabled Detectors: Bias-Tunable Quantum Well Infrared Photodetector (Qwip) And Quantum Dot Scintillation Detector (Qdsd), Gyana R. Biswal

Electronic Theses & Dissertations (2024 - present)

This dissertation discloses the physics, fabrication, characterization, and analysis of two novel types of group III-V semiconductor detectors relying on quantum confinement of carriers, namely voltage-tunable quantum well infrared photodetectors (QWIP) and a high-yield ultrafast quantum dot scintillation detector (QDSD). Both QWIP and QDSD heterostructures presented here were grown on 3” GaAs (001) substrates using molecular beam epitaxy (MBE).

A major part of the dissertation focuses on development of the voltage-tunable QWIPs targeting detection in the mid-wave infrared region (MWIR) (3μm -5μm) and long-wave infrared region (LWIR) (8μm -12μm) with control of sensitivity by the applied bias. The QWIPs utilize …