Condensed Matter Physics Commons^™

Effects Of Radiation Type On Charge Transport In Aged Polymers, Zachary J. Gibson, Jr Dennison, Virginie Griseri

Journal Articles

Spacecraft charging issues are often investigated with simulated space environments and evaluated on pass–fail criteria that may yield little or no information about materials’ properties. It is far more effective to understand and mitigate spacecraft charging issues through investigations of material properties. However, material properties are dynamic in the harsh environment of space. Approximations must be made to simulate the space environment in the laboratory. This article reports on the investigation of the approximation that energy deposition causes the same aging effects in materials irrespective of the type of radiation sources. Samples of polytetrafluoroethylene (PTFE) and polyether-etherketone (PEEK) were irradiated …

Effect Of Space Radiation On The Mechanical Properties Of High-Strength Polyethylene Nanocomposite Films, Seunghyun Moon, Achal Duhoon, Zhongtian Gu, Jr Dennison, Tengfei Luo

Journal Articles

This study experimentally investigates the effects of prolonged radiation exposure on mechanical properties of high-strength, highly crystalline polyethylene (PE)/thermally reduced graphene oxide (TrGO) nanocomposite films for space applications. Prior to irradiation, PE/TrGO films were found to have tensile strengths up to ~4 GPa, more than 40 times that of conventional space-deployed membrane films (e.g., those used in solar sails) and over 59× the specific tensile strength. The PE/TrGO films were subjected to three radiation conditions to simulate space environmental conditions: ⁹⁰Sr beta radiation (0.2 to 2.5 MeV), 80 keV electron beam irradiation, and 4.9 eV ultraviolet (254 nm) exposure. …

Electron Yields Of Lunar Regolith Simulant Layers, Christopher Vega, Matthew Robertson, Thomas Keaton, Heather Allen, Jr Dennison

Journal Articles

The charging of bulk lunar regolith has been recognized since the Apollo era as an immediate and critical issue facing our return to the moon. Accurate electron yield (EY) measurements of bulk highly insulating granular materials—which largely determine how such particles charge through interactions with space environments—are lacking due to many experimental complexities that have led to a critical knowledge gap. Such knowledge is essential for addressing fundamental science and myriad important lunar applications and simulations related to lunar dust and regolith electrostatic charging. The few prior EY studies of lunar dust were limited due to severe charging effects and …

Time-Dependent Radiation Induced Conductivity Of Polyimide: Effects Of Dose Rate And Temperature On Dynamic Ric, Tyler Heggenes, Jenny R. Whiteley, Jodie Gillespie, Jr Dennison

Journal Articles

Radiation induced conductivity (RIC) can impact charge dissipation within highly insulating materials used in spacecraft in harsh space plasma environments. Previous Utah State University (USU) research analyzed only the equilibrium portions of an extensive RIC database for polymeric materials, including Kapton HN (Trademark). This confirmed that equilibrium RIC follows a standard theoretical model that is temperature and dose rate dependent. The current study provides a new analysis of RIC’s time-dependent behavior of the Kapton HN data from this database. With the onset of radiation, the material response is characterized by an exponential increase in conductivity, while a hyperbolic inverse time-dependent …

Time-Evolved Constant Voltage Conductivity Measurements Of Common Spaceborne Polymeric Materials, Brian Wood, David King, Jr Dennison

Journal Articles

Long-duration current measurements were made for low-density polyethylene (LDPE), polyimide (PI), polyether ether ketone (PEEK), and biaxially oriented polypropylene (BOPP) to determine their bulk conductivity near room temperature as a function of time. These common thin-film spacecraft material samples were vacuum baked to remove moisture and volatile contaminants to better simulate space conditions. The constant voltage conductivity (CVC) method used a very stable, low-noise dc voltage source and measured the resulting current in a parallel plate geometry. Due to the extremely low conductivity of these four polymeric materials, extended experiments of up to ten days were necessary to establish equilibrium …

Young Professionals, Zachary Gibson

Journal Articles

Like many of us, I have attended numerous panels, seminars, and workshops geared toward helping young professionals and students. The more senior professionals are gathered for us to question and tap them for wisdom and anecdotes. One such question that inevitably comes up in one form or another is, “How did you get to where you are?” A thinly veiled question intending to ask how can one get to the same or similar position. The response often begins with a soft chuckle and a “well … ” Their answers are caveated by “my path was not the typical path.”

Modeling Permittivity Measurements Of Thin Film Materials Versus Film Thickness, Jr Dennison, Cameron Eggleston

Journal Articles

Measured permittivity of thin film polymeric samples were substantially less for thin samples, asymptotically approaching bulk values above ~500 μm. For ~25 μm samples the observed permittivities were as much as 50% less than for bulk measurements. This behavior has been studied for four common homogeneous polymeric materials for sample thickness in the range of ~10 μm to > 1000 μm. To quantify these observations, an empirical single-parameter model was developed to correct measured permittivity of thin samples based on an effective stray capacitance in series with the samples to compensate for effects attributed to instrumentation.

Effects Of Differing Radiation Methods On Charge Transport In Polymers, Zachary Gibson, Jr Dennison, Virginie Griseri

Presentations

The mitigation of deleterious arcing and sparking onboard spacecraft depends upon a thorough understanding of the electrical properties of the materials involved. This includes not only understanding steady-state parameters such as dark conductivity, but responses to the space environment as well. For example, radiation-induced conductivity drastically changes the conductivity of a material due to the presence of radiation. However, this change in conductivity diminishes away once the radiation is no longer present. There may also be permanent changes, or aging, in the material properties. The physical processes of aging can be complicated and are often difficult to model. Therefore, empirical …

Radiation Induced Conductivity Of Peek: Effects Of Temperature And Total Ionizing Dose, Joshua Boman, Brian Wood, Jordan Lee, Jr Dennison, Kim M. Aaron, Wousik Kim

Conference Proceedings

Radiation induced conductivity (RIC) plays a critical role in space charge dissipation with insulating materials used in spacecraft. Ionizing radiation present in harsh space plasma environments deposits energy into materials via inelastic scatter, exciting electrons into the conduction band without depositing charge for penetration radiation. RIC is expected to be affected by temperature and total ionizing dose (TID); temperature primarily affects the rate of promotion of electrons in localized trap states within the band gap to the conduction band, while TID can create additional traps states thereby increasing trap density and reducing mean trap separation.

RIC was measured in a …

Temperature Dependent Radiation Induced Conductivity Of Polymeric Spacecraft Materials, Jodie Corbridge Gillespie, Jr Dennison

Conference Proceedings

Temperature dependent radiation induced conductivity (RIC) data applicable to conditions experienced by spacecraft are presented for low density polyethylene (LDPE) and poylimide (PI, Kapton^HN, along with summaries for five other common polymeric spacecraft mateials: polyimide (PI; Kapton HN^TM, and Kapton E^TM), polytetraflouroethylene (PTFE; Teflon^TM), expanded PTFE (ePTFE), ethylene-tetrafluoroethylene and (ETFE; Tefzel^TM). Data were measured over approximately 105 K to 330 K and incident dose rates, D, of 10^-4 Gy/s to 10^-1Gy/s. Theoretical expressions proposed by Rose/Fowler/Vissenberg predict equilibrium RIC behavior according to a general expression σ …

Time-Dependent Behavior Of Radiation Induced Conductivity In Polymers, Tyler Heggenes, Jenny R. Whiteley, Jodie Corbridge Gillespie, Joshua Boman, Jr Dennison

Conference Proceedings

Ionizing radiation can induce conductivity in polymers via inelastic scattering which imparts energy to electrons in the valence band and trapped states, exciting them into the conduction band without depositing charge into the material. This radiation-induced conductivity (RIC) can impact space charge dissipation within highly insulating materials used in spacecraft in harsh space plasma environments. Previous USU research analyzed only the equilibrium portions of an extensive RIC database for polymeric materials, including Kapton HN^TM. This confirmed that equilibrium RIC follows a standard theoretical model that is temperature and dose-dependent. The current study provides a new analysis of RIC's …

Comparison Of Absolute Electron Emission Yields Of Extreme Insulators: Round Robin Tests Of Polyimide And Low Density Polyethylene, Jr Dennison, Matthew Robertson, Christopher Vega, Mohamed Belhaj, Juste Sarah Dadouch, Isabel Montero, María E. Dávila, Kazuhiro Toyoda

Posters

No abstract provided.

Temperature Dependent Radiation Induced Conductivity Of Polymeric Spacecraft Materials, Jodie Corbridge Gillespie, Jr Dennison

Posters

No abstract provided.

Analysis Of The Effects Of Surface Modifications And Other Extrinsic Factors On Electron Yield With A “Patch” Model, Matthew Robertson, Christopher Vega, Trace Taylor, Jr Dennison

Presentations

Electron yield (EY) is a material attribute of central importance to understanding and modeling spacecraft charging. EY is defined as the ratio of emitted electrons to incident electrons, when irradiated with an electron beam. It depends on incident energy and is unique for each material as determined by its chemical composition, crystal structure, and electronic configurations. Dynamic surface modifications and other extrinsic factors—including surface morphology, composition, contamination, oxidation, and charging— can significantly affect EY and consequently spacecraft charging. This research proposes a “patch” model to provide a simple theoretical framework to model more complex materials comprised of any number of …

Time-Dependent Behavior Of Radiation Induced Conductivity Of Polymers, Tyler Heggenes, Jenny R. Whiteley, Jodie Corbridge Gillespie, Joshua Boman, Jr Dennison

Presentations

The conductivity of insulating materials can be enhanced above the baseline dark conductivity by incident radiation via inelastic scattering that imparts energy to electrons in trapped states and excites them into the conduction band, without depositing charge. Such radiation-induced conductivity (RIC), caused by ionizing radiation present in harsh space plasma environments, can play a critical role in space charge dissipation within highly insulating materials used in spacecraft. An equilibrium value for RIC, 𝜎_RIC, is attained after prolonged exposure to an incident dose rate; this follows a standard theoretical power law model proposed by Rose/Fowler/Vissenberg, 𝜎_RIC(T …

Analysis Of The Effects Of Surface Modifications And Other Extrinsic Factors On Electron Yield With A “Patch” Model, Matthew Robertson, Christopher Vega, Trace Taylor, Jr Dennison

Conference Proceedings

Electron yield (EY) is a material property of central importance to understanding and modeling spacecraft charging. It depends on incident energy and is unique for each material. Dynamic surface modifications and other extrinsic factors—including composition, surface morphology, contamination, oxidation, and charging— can significantly affect EY and consequently spacecraft charging. This research proposes a “patch” model to provide a simple theoretical framework to model more complex materials comprised of any number of different types of constituent materials in terms of the EY contribution of each constituent material or extrinsic factor. The “patch” model merges the unique EY curve contribution of each …

Effects Of Differing Radiation Methods On Charge Transport In Polymers, Zachary J. Gibson, Jr Dennison, Virginie Griseri

Conference Proceedings

Spacecraft charging issues are understood and mitigated through an understanding of material properties. Material properties are dynamic in the harsh environment of space. Approximations must be made to simulate the space environment in the laboratory. This paper reports on the investigation of the approximation that energy deposition causes the same aging effects in the materials regardless of the radiation source. Samples of polytetrafluoroethylene (PTFE) and polyether-etherketone (PEEK) were irradiated with x-rays, γ-rays, or electrons at total ionizing dose (TID) of either 2 x 10⁴, 2 x 10⁵, or 2 x 10⁶ rad. Charge was then …

Young Professionals: Fireside Chat With Jacques Lewiner And J. Keith Nelson At The Ieee Conference On Electrical Insulation And Dielectric Phenomena, Mattewos Tefferi, Allen Andersen, Sneha Hedge, Moein Borghei

Journal Articles

At the IEEE Conference on Electrical Insulation and Dielectric Phenomena (CEIDP), the Dielectrics and Electrical Insulation Society’s Young Professionals (DEIS-YP) Committee has initiated a YP luncheon event. This event aims to feature keynote speakers who share insights into their career trajectories with young professionals. In the current CEIDP edition, we had the privilege of hosting two distinguished speakers: Jacques Lewiner, the 2023 Whitehead Memorial Lecturer, and J. Keith Nelson, the 2022 recipient of the Dakin Award who also presented his award lecture at the CEIDP 2023. The fire- side chat was moderated by Allen Andersen, who began with initial questions …

A Simple Method For Determining Shallow Charge Distributions In Dielectrics Via Pulsed Electroacoustic Measurements, Zachary Gibson, J. R. Dennison

Journal Articles

The understanding of charge dynamics in dielectric materials is paramount in mitigating electrostatic discharge events for spacecraft. The most critical spacecraft charging events are found to result from incident electrons in the energy range of 10 keV to 50 keV. The charge embedded in dielectric materials in this energy range are deposited a distance into the material on the order of a few to tens of microns. One way to measure and understand the deposited charge is via pulsed electroacoustic measurements (PEA). However, the typical PEA spatial resolution of ~ 10 μm is not sufficient to resolve or discern charge …

Methods For Preparing And Characterizing Granular Materials For Electron Yield Measurements, Tom Keaton

All Graduate Plan B and other Reports, Spring 1920 to Spring 2023

This work presents a systematic study on sample preparation methods and accuracy of electron yield (EY) measurements of highly insulating, granular materials. EY measurements of highly insulating materials, especially those with high EY, are challenging due to the effects of sample charging even for very low fluence electron probe beams. EY measurements of particulates are complicated by: (i) roughness effects from particulate size, shape, coverage, and compactness; (ii) particle adhesion; (iii) substrate contributions; and (iv) electrostatic repulsion and potential barriers from charged particles and substrates. Numerous methods were explored to rigidly affix particles on conducting substrates at varying coverages for …

Relevancy Of Pulsed Electroacoustic Measurements For Investigating Spacecraft Charging, Zachary Gibson, J. R. Dennison

Journal Articles

The magnitude and spatial distribution of charge embedded in dielectric materials and the evolution of the charge distributions with time are paramount for the understanding and mitigation of spacecraft charging. Spacecraft materials are charged primarily by incident fluxes of low-energy electrons, with electron fluxes in the 10–50 keV range often responsible for the most deleterious arcing effects. While the pulsed electroacoustic (PEA) method can provide sensitive nondestructive measurements of the internal charge distribution in insulating materials, it has often been limited for spacecraft charging applications by typical spatial resolutions of ≤ 10 μm , with a 10- μm …

Space Environment Effects On The Electron Yields Of Ldef Thermal Control Coatings, Trace Taylor, Matthew Robertson, Heather Allen, Jr Dennison, Michael Guy, Emily Willis

Journal Articles

Space-environment-induced degradation of white thermal control coatings from the Long Duration Exposure Facility (LDEF) was investigated. Much of the exterior of the LDEF was painted with a white thermal control coating, Aeroglaze A276; and most of the interior was coated with a black thermal control coating, Aeroglaze Z306. Outgassing from these coatings and other LDEF materials interacted with the white surface when exposed to sunlight after volatile materials condensed on the LDEF surfaces. Surface morphology was characterized by optical and scanning electron microscopies. Fourier-transform infrared spectroscopy and energy-dispersive x-ray spectroscopy were used to identify the chemical compounds and elements present …

Comparison Of Pulsed Electroacoustic Measurements And Af-Numit3 Modeling Of Polymers Irradiated With Monoenergetic Electrons, Zachary Gibson, J. R. Dennison, Brian Beecken, Ryan Hoffmann

Journal Articles

Successful spacecraft design and charging mitigation techniques require precise and accurate knowledge of charge deposition profiles. This paper compares models of charge deposition and transport using a venerable deep dielectric charging code, AF-NUMIT3, with direct measurements of charge profiles via pulsed electroacoustic (PEA) measurements. Eight different simulations were performed for comparison to PEA experiments of samples irradiated by 50 or 80 keV monoenergetic electrons in vacuum and at room temperature. Two materials, polyether-ether ketone (PEEK) and polytetrafluoroethylene (PTFE), were chosen for their very low conductivities so that minimal charge migration would occur between irradiation and PEA measurements. PEEK was found …

Spacecraft Charging Test Considerations For Composite Materials, Allen Andersen, Wousik Kim, J. R. Dennison, Brian Wood, Todd A. Schneider, Jason Vaughn, Kenneth H. Wright Jr., Nelson W. Green, Eric Suh, Joel Schwartz, Abdul-Majeed Azad

Journal Articles

Composite materials present a growing challenge for spacecraft charging assessments. We review some recent lessons learned for charging tests of composite materials using both parallel-plate and electron beam test geometries. We also discuss examples of materials that exhibit significant variations between samples, despite them all having the same trade name.

Effects Of Volatile Compounds On Breakdown Field Strength Measurements Of Polymers, Megan Loveland Dewaal, Jr Dennison

Journal Articles

This study investigates the effects of absorbed water and volatile compounds on measurements of the electrostatic breakdown field strength. Comparisons are made between sets of pristine samples, ones that underwent a thorough vacuum bake out, and ones subsequently exposed to humid conditions to determine how quickly the samples reverted to an unbaked state. Specifically, we compared signatures related to an electrostatic breakdown (electrostatic breakdown field strength, frequency of pre-breakdown arcing, and flashover) and images of the arc damage sites. The work reports results for three prototypical polymeric dielectric materials: low density polyethylene (LDPE), polyether-etherketone (PEEK), and Nylon 66, listed in …

Modeling The Effects Of Surface Roughness On Electron Yield, Trace Taylor, Matthew Robertson, Jr Dennison

Conference Proceedings

Surface conditions—including surface morphology, composition, contamination, and oxidation—can significantly affect electron yields and consequently spacecraft charging. The effects of surface roughness on electron yield are modeled in this study by considering four aspects of electron yield calculations: (i) simple models of rough surface geometry, (ii) the angular distributions of electrons emitted from various points on these surfaces, (iii) the likelihood of these emitted electrons escaping the rough surface, and (iv) the relative fractions of smooth and rough surfaces. Three simple periodic one-dimensional surface profiles were considered—namely rectangular, triangular, and sawtooth features; each surface profile was characterized by an aspect ratio …

Laboratory Simulations Of Simultaneous Reduced Gravity And Ionizing Radiation Environments, Achal Duhoon, Jr Dennison

Conference Proceedings

A novel system has been developed to simulate the combined effects of reduced gravity and ionizing radiation present during spaceflight on biological and particulate samples. The miniature rotary cell culture system (mRCCS) was designed to synchronously rotate up to five independent vessels containing particulate samples suspended in fluid media, constructed using radiation tolerant, biocompatible, and vacuum compatible materials. Reduced gravity conditions were achieved when particles (e.g., 200 µm polystyrene microcarrier beads with or without adhered cell clusters) were suspended inside the vessels moving near terminal velocity in viscous fluid media with densities matched to the suspended …

Ion Beam-Treated Space Polymers: Long-Term Stability In Geo-Simulated Environments, Jacob Kleiman, Zelina Iskanderova, Leonid Krishtein, J. R. Dennison, Brian Wood, Anatoly Grigorievsky, Carl Best

Journal Articles

As part of a large program conducted between years 2010 and 2018, a number of ion beam surface treatments and proprietary coatings formed on advanced space polymers by direct ion beam deposition were developed at Integrity Testing Laboratory (ITL) Inc, in Canada. Thistechnology allowed producing surfaces with controlled surface resistivity in a wide range of charge dissipation values, with negligibly low additional RF losses and other important functional properties, that allowed using such treated materials and products in modern space antennae, solar arrays and other external applications on spacecrafts in GEO environment. This paper will present an overview of results …

Electron Emission And Transport Properties Database For Spacecraft Charging Models, Phil Lundgreen

Theses and Dissertations

Modeling the rate and likelihood of spacecraft charging during spacecraft mission is critical to determine mission length, proposed spacec­raft attitude, and spacecraft design. The focus of this work is the creation and utilization of a database of secondary electron yield (SEY) measurements for a host of materials to increase accuracy in spacecraft modeling. Traditional methods of SEY data selection for input into spacecraft charging codes typically include the use of compiled materials databases incorporated in charging codes or selecting values from a specific scientific study. The SEY database allows users to select data inputs based upon the details associated with …

Experimental Investigation Of The Secondary And Backscatter Electron Emission From New Spacecraft Surface Materials, Millan F. Diaz-Aguado, John W. Bonnell, Stuart D. Bale, Justin Christensen, Phillip Lundgreen, Jordan Lee, Jr Dennison, Justin Dekany, Brian Wood, Mike Gruntman

Journal Articles

The emission of secondary and backscattered electrons influences spacecraft surface potentials and the surrounding plasma. Modern spacecraft use new materials for which secondary emission properties have been unavailable. In this work, the total electron yield (i.e., the sum of secondary and backscattered electron yields) was measured for niobium-C103 alloy, molybdenum Titanium, Zirconium, Molybdenum (TZM) alloy, tantalum-tungsten alloy, Elgiloy®, graphite lubricant (DAG 213®), and titanium nitride. The surface properties of tungsten were also measured for comparison with past test data. The materials were readied as spacecraft flight materials and temperature-treated ("annealed") to predicted peak flight temperatures. The yield properties for 10 …