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Articles 241 - 244 of 244
Full-Text Articles in Physical Sciences and Mathematics
The Synthesis Of N-Chlorosulfonyl Β-Lactams And Their Rearrangements, Lihua Zhang
The Synthesis Of N-Chlorosulfonyl Β-Lactams And Their Rearrangements, Lihua Zhang
Masters Theses
The synthesis of several N-chlorosulfonyl-β-lactams and their rearrangements have been carried out via CSI (chlorosulfonylisocyanate) reaction. The mechanism of β-lactam synthesis as well as its rearrangements were also studied. The characterization of β-lactams was performed with IR, 1H and 13C NMR, and HRMS. β-lactams 2-chlorosulfonyl-1-methyl-2-azabicyclo[4.2.0]octan-3-one (71), 1-chlorosulfonyl-4-methyl-4- (phenylmethyl)azetidin-2-one (74) and 1-chlorosulfonyl-4,4- (diphenylmethyl)azetidin-2-one (75) were synthesized for the first time. β-lactam 4-chlorosulfonyl-3, 9, 9-trimethyl-4-azatricyclo [6.1.0.03,6] nonan-5-one (73) was obtained as crystalline solid instead of liquid.
Different effects, such as temperature, solvents and catalysts, on the rearrangement of the …
Acid Dissociation Of Chloroguaiacols And Ph Dependent Sorption To Estuarine Sediments, Jennifer Lisa Gundersen
Acid Dissociation Of Chloroguaiacols And Ph Dependent Sorption To Estuarine Sediments, Jennifer Lisa Gundersen
Dissertations, Theses, and Masters Projects
Chloroguaiacols are common components of bleached kraft pulp mill effluent known to bioaccumulate in aquatic organisms, and sorb onto particulate material and sediments. Ionization properties of the chloroguaiacols must be known in order to explain their sorptive behavior in aquatic systems. to obtain this information, thermodynamic acid dissociation constants (p&K\sb{lcub}\rm a{rcub})& of guaiacol (o-methoxyphenol) and nine chloroguaiacols have been determined by spectrophotometric methods. These experimental p&K\sb{lcub}\rm a{rcub}& values have been compared with literature values, values predicted by the Hammett equation and predictions by quantum chemical calculations using MOPAC 6.0 with AM1 and MNDO Hamiltonian operators. Experimental and predicted acidities were …
Designing Chemical Education Hypermedia For The World-Wide Web, Brian Tissue, Ching-Wan Yip, Yue-Ling Wong, Mark Anderson
Designing Chemical Education Hypermedia For The World-Wide Web, Brian Tissue, Ching-Wan Yip, Yue-Ling Wong, Mark Anderson
Mark R. Anderson
No abstract is currently available.
Determination Of Plasma Parameters In A Dc Arcjet Part Ii, Scott Reeve, Wayne Weimer
Determination Of Plasma Parameters In A Dc Arcjet Part Ii, Scott Reeve, Wayne Weimer
Scott Reeve
No abstract provided.