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Articles 151 - 180 of 483
Full-Text Articles in Food Biotechnology
Optimization Of Extraction Process Of Polyphenols From Different Parts Of Trifolium Pretense Linn And Its Antioxidant Activity, Li Xin-Ran, Wang Xu-Ying, Xu Zi-Yi, Pan Yong-Qi, Weng Gui-Ying
Optimization Of Extraction Process Of Polyphenols From Different Parts Of Trifolium Pretense Linn And Its Antioxidant Activity, Li Xin-Ran, Wang Xu-Ying, Xu Zi-Yi, Pan Yong-Qi, Weng Gui-Ying
Food and Machinery
Objective: The present study aimed to optimize the extraction process of polyphenols from Trifolium pratense Linn and evaluate the antioxidant activity in vitro. Methods: Ultrasonic-assisted extraction of total polyphenols from stems, leaves, and flowers was firstly performed, and the parts with higher polyphenol content were selected for further investigation. Then the response surface methodology was used to optimize the extraction process, and its antioxidant activity was evaluated by scavenging rate of hydroxyl radical and superoxide anion radical. Results: The results showed that the content of polyphenols in the leaves is relatively high. The optimal extraction process is as follows: the …
Effects Of Ultra-Fine Green Tea Powder On Noodle Quality And Optimization Of Green Tea Noodle Formula, Cai Xi-Xi, Chen Xu, Chen Xuan, Chen Meng-Shi, Gao Xue-Ling, Wang Shao-Yun
Effects Of Ultra-Fine Green Tea Powder On Noodle Quality And Optimization Of Green Tea Noodle Formula, Cai Xi-Xi, Chen Xu, Chen Xuan, Chen Meng-Shi, Gao Xue-Ling, Wang Shao-Yun
Food and Machinery
Objective: The study aimed to explore the effect of ultra-fine green-tea powder on the quality of noodles, and develop a kind of noodles rich in superfine powder of green tea. Methods: The effects of ultra-fine green tea powder on the texture characteristics, water migration and sensory flavor of noodles were comprehensively analyzed, and the formula of ultra-fine green tea noodles was optimized by response surface design. Results: The addition of ultra-fine green-tea powder had adverse effect on the cooking characteristics of noodles. Adding 2%~4% superfine green tea powder could improve the sensory and texture properties of noodles, including hardness, chewability …
Study On Western Style Of Rabbit Meat Ham Rich In Corn Germ Oil And It's Quality Analysis, Zhang Xue-Quan, Li Xiang-Hui, Wu Guang-Hui
Study On Western Style Of Rabbit Meat Ham Rich In Corn Germ Oil And It's Quality Analysis, Zhang Xue-Quan, Li Xiang-Hui, Wu Guang-Hui
Food and Machinery
Objective: A western-style rabbit meat ham rich in corn germ oil was developed, and the corn germ oil was used to replace animal fat in traditional ham. Methods: Using corn germ oil, rabbit and starch as the main raw materials, through single factor test and L9 （34） orthogonal test, the types of starch and the best addition amount of corn germ oil, rabbit and starch were determine, and the quality indexes of western-style rabbit meat ham were tested according to relevant national standards. Results: The western-style rabbit meat ham, which was rich in corn germ oil, made …
Analysis Of Edible Areca Products Based On Electronic Tongue Technology, Chao Yu-Zhou, Liu Yi, Zhao Zhi-You, Xia Yan-Bin
Analysis Of Edible Areca Products Based On Electronic Tongue Technology, Chao Yu-Zhou, Liu Yi, Zhao Zhi-You, Xia Yan-Bin
Food and Machinery
Objective: Electronic tongue technology was used to analyze the taste of edible areca and compared with sensory evaluation to provide a more objective and accurate evaluation method. Methods: The taste of 12 different areca products from 8 enterprises was analyzed using electronic tongue, sensory evaluation, and multivariate statistical methods. Results: There were significant differences in the areca taste index between different brands; the samples were divided into three groups by principal component analysis, factor analysis and cluster analysis, and each cluster had its unique taste characteristics. Combined with the electronic tongue and sensory evaluation, the results were consistent except for …
Research Progress On The Mechanism Of Dietary Polyphenols In Improving Inflammatory Bowel Disease, Lin Peng-Cheng, Cao Jun-Han, Xie Wan-Cui
Research Progress On The Mechanism Of Dietary Polyphenols In Improving Inflammatory Bowel Disease, Lin Peng-Cheng, Cao Jun-Han, Xie Wan-Cui
Food and Machinery
This article summarizes the mechanism by which dietary polyphenols improve inflammatory bowel disease by regulating oxidative stress, protecting the intestinal mucosal barrier, regulating intestinal flora and metabolites, highlights the regulatory effect of dietary polyphenols on inflammatory bowel disease inflammatory signaling pathways, and prospects to the research direction of dietary polyphenols in the nutritional intervention field of inflammatory bowel disease and other diseases.
Nutrition Misunderstanding Of Competitive Athletes And Its Improvement, Zeng Jia
Nutrition Misunderstanding Of Competitive Athletes And Its Improvement, Zeng Jia
Food and Machinery
At present, the main problems in athletes' diet include imbalance in the proportion of nutrients, unreasonable distribution of nutrients and calories, insufficient intake of trace elements, lack of awareness of nutrition matching, etc. Therefore, a few measures such as scientific nutrition matching, rational distribution of calories for three meals, paying attention to the intake and distribution of trace elements, and strengthening nutrition education for athletes were proposed, and this is the healthy basis for maintaining the best competitive state of competitive athletes.
Research Progress On Management Of Athletes’ Dietary Nutrition, Jing Xi-Min
Research Progress On Management Of Athletes’ Dietary Nutrition, Jing Xi-Min
Food and Machinery
By systematically selecting, combing and analyzing the published papers on the literature retrieval websites, such as SCI、CNKI, etc., this review summarized the current research progress of foreign and domestic sports dietary nutrition of athletes, and explored the metabolic laws and nutrition management strategies of energy, carbohydrates, protein and fat, in order to provide some references for theoretical development of sports nutrition and the research and manufacturing of sports nutrition food in China.
Research On Development Model Of Gastronomy Tourism, Liu Cang
Research On Development Model Of Gastronomy Tourism, Liu Cang
Food and Machinery
The value and significance of food tourism were analyzed from two aspects including consumer satisfaction and economic development. The development model of food tourism was classified into three categories, i. e., regional food tourism, festival food tourism and theme food tourism, and the development status of the three kinds of modes in and outside China was also enumerated. Finally, suggestions are given for the development of food tourism in the future.
Research Progress On Application Of Compound Edible Gum In Meat Products, Zhang Gen-Sheng, Zhao Jin-Na, Yu Shi-You, Wang Jun-Ru
Research Progress On Application Of Compound Edible Gum In Meat Products, Zhang Gen-Sheng, Zhao Jin-Na, Yu Shi-You, Wang Jun-Ru
Food and Machinery
The application of compound edible gum in meat processing and its effect on the quality of meat products were reviewed. The compound edible glue plays an important role in protein protection, gel water, emulsion stability, quality improvement and preservation. However, the proportion of species and distribution of edible gum and its action mechanism of improving the meat quality remains to be further studied.
Seaweed Polysaccharide In Food Contact Materials (Active Packaging, Intelligent Packaging, Edible Films, And Coatings), Kalpani Y. Perera, Shubham Sharma, Amit K. Jaiswal, Swarna Jaiswal
Seaweed Polysaccharide In Food Contact Materials (Active Packaging, Intelligent Packaging, Edible Films, And Coatings), Kalpani Y. Perera, Shubham Sharma, Amit K. Jaiswal, Swarna Jaiswal
Articles
Food contact materials (FCMs) are materials that come in contact with food products such as food packaging which play a significant role in the food quality and safety. Plastic, which is a major food packaging material, harms the eco-system, wildlife, and the environment. As a result, numerous researches have been in progress on alternative polymers, which has similar properties as plastic but is also environmentally friendly (biodegradable). In recent years, the utilization of seaweed polysaccharides has piqued interest due to its biodegradability, non-toxicity, antioxidant capabilities, and excellent film formation ability. However, it has a number of drawbacks such as low …
Optimization Of Ethanol Production From Enzymatically Saccharified Biomass Of Acid-Pretreated Rice Straw, Muzammal Mateen Azhar, Qurban Ali, Arif Malik, Elham Khalili, Muhammad Arshad Javed, Shinawar Waseem Ali, Muhammad Saleem Haidar
Optimization Of Ethanol Production From Enzymatically Saccharified Biomass Of Acid-Pretreated Rice Straw, Muzammal Mateen Azhar, Qurban Ali, Arif Malik, Elham Khalili, Muhammad Arshad Javed, Shinawar Waseem Ali, Muhammad Saleem Haidar
The Philippine Agricultural Scientist
The substrate of rice (Oryza sativa) straw employed in this study was procured from local market and stored in polyethene bags until needed. The study was conducted to find out the effects of process optimization of ethanol production from enzymatically saccharified biomass of acid-pretreated rice straw. The results indicated that acid pretreatment has reduced lignin content about 50%. Resultantly, pretreatment raised cellulose contents up to 52% making it suitable for enzymatic saccharification. Optimization of saccharification illustrated that parameters such as biomass, enzyme concentration, temperature, incubation time and agitation indeed affected the action of cellulase on pretreated biomass releasing …
Isolation And Characterization Of The Total Protein In ’Lakatan’ Banana (Musa Acuminata Colla) With Bioactive Peptides Exhibiting Antioxidative And Antihypertensive Activities, David Mangussad, Ana Teresa Sucgang, Mia Clare Marie Clemencia, Marlo Manalo, Lawrence Yves Uy, Mary Ann Torio
Isolation And Characterization Of The Total Protein In ’Lakatan’ Banana (Musa Acuminata Colla) With Bioactive Peptides Exhibiting Antioxidative And Antihypertensive Activities, David Mangussad, Ana Teresa Sucgang, Mia Clare Marie Clemencia, Marlo Manalo, Lawrence Yves Uy, Mary Ann Torio
The Philippine Agricultural Scientist
Hypertension is a leading cause of disease burden in developing countries. Leading factors are obesity, increased cholesterol levels, and long-term oxidative stress. Since commercially available drugs for cardiovascular diseases such as antioxidants and ACE receptor blockers are expensive, preventive cheaper alternatives derived from foods are sought after. Lakatan, one of the most abundant and cheap food sources in the Philippines has been proven to have antioxidant and antihypertensive properties but studies exploring the proteins and bioactive peptides responsible for its health benefits are very limited. In this study, proteins from Lakatan (Musa acuminata Colla) have been studied to understand …
An Evaluation Of The Hargreaves-Samani Method For Estimating Evapotranspiration Under Semi-Arid Conditions, Yusuf Aydin
An Evaluation Of The Hargreaves-Samani Method For Estimating Evapotranspiration Under Semi-Arid Conditions, Yusuf Aydin
The Philippine Agricultural Scientist
It is suggested by the Food and Agriculture Organization of the United Nations (FAO) to use the FAO56-Penman-Monteith (FAO56-PM) model as the standard model in reference crop water consumption studies. However, the climate parameters required by the standard model cannot be fully and reliably obtained in under developed or developing countries. Hence, the Hargreaves-Samani (HS) equation is used as an alternative to the FAO56-PM model since it can be used for calculations with less climate data. In this study, ETo-PM and ETo-HS values calculated at 8 provinces in Southeastern Turkey using the IAM-ETo software were evaluated and …
Dual Real-Time Fluorescence Quantitative Pcr Method For The Detection Of Orange And Citrus Components In Orange Juices, Chen Yin-Yin, Li Juan, Zhou Lu, Chen Dan-Xia, Han Zhi-Jie, Ding Qing-Long
Dual Real-Time Fluorescence Quantitative Pcr Method For The Detection Of Orange And Citrus Components In Orange Juices, Chen Yin-Yin, Li Juan, Zhou Lu, Chen Dan-Xia, Han Zhi-Jie, Ding Qing-Long
Food and Machinery
Objective: To establish a dual real-time PCR method for the detection of orange and citrus components in orange juices. Methods: Through the design and screening of primers and probes for orange and citrus components. Through the detection of fruits, found the rule of fluorescence amplification of orange and citrus. Using the ratio difference of orange and citrus in FAM/VIC two fluorescence channels to determine the composition of orange and citrus. The lowest doping ratio detected by the method was verified by the experiment of orange juice adulteration, tested the commercial orange juice and verify the feasibility of the method. Results: …
Empirical Analysis And Enlightenment Of American Nuval Scoring Labeling Development, Huang Ze-Ying, Huang Bei-Xun
Empirical Analysis And Enlightenment Of American Nuval Scoring Labeling Development, Huang Ze-Ying, Huang Bei-Xun
Food and Machinery
NuVal scoring labeling that was based on overall nutritional quality index, adopted 1 to 100 to show the nutritional value of packaged food and fresh agricultural products. The higher was the score, the better was the nutritional status of food. The labeling was integrated with food prices to make it easier for consumers to compare the nutritional value of what they pay. Therefore, FOP labeling in China could be attempted to integrate nutrition evaluation information with food price, and promote in fresh agricultural products, and adjust its algorithm in accordance with the national nutritional needs.
Simultaneous Determination Of 10 Kinds Of Amide Herbicide Residues In Dark Tea By Quechers With Gas Chromatography-Triple Quadrupole Mass Spectrometry, Yi Shou-Fu, Liang Feng, He Qing-Ke, Song Yang, Liao Yan-Zhi
Simultaneous Determination Of 10 Kinds Of Amide Herbicide Residues In Dark Tea By Quechers With Gas Chromatography-Triple Quadrupole Mass Spectrometry, Yi Shou-Fu, Liang Feng, He Qing-Ke, Song Yang, Liao Yan-Zhi
Food and Machinery
Objective: A method for simultaneous determination of 10 amide herbicide residues in dark tea was developed by QuEChERS method coupled with gas chromatography-triple quadrupole mass spectrometry （GC-MS/MS）. Methods: After being extracted by acetonitrile and purified by QuChERS, the samples were separated by TG-5 SIL MS column （30 m×0.25 mm×0.25 μm）, then detected bymultiple reaction monitoring mode （MRM）. Blank matrix matching standard curve was used in quantitative analysis. Results: The calibration curves had a good liner relationship in the range of 0.001~0.500 mg/L with the correlation coefficients greater than 0.999. The limits of detection （LODs） and limits of quantitation （LQDs） of …
The Design Of The Sweeping And Collecting Device For The Residual Grain At The Bottom Of The Flat Warehouse, Wang Ming-Xu, He Ying-Zhen, Zhao Zi-Yan, He Wen-Bin, Ding Le-Le
The Design Of The Sweeping And Collecting Device For The Residual Grain At The Bottom Of The Flat Warehouse, Wang Ming-Xu, He Ying-Zhen, Zhao Zi-Yan, He Wen-Bin, Ding Le-Le
Food and Machinery
Objective: Aiming at the low degree of mechanization, automation and intelligence in the cleaning and collecting process of the surplus grain at the bottom of the granary, a cleaning and collecting device for the surplus grain at the bottom of the silo was designed and manufactured. Methods: Based on simulation and numerical calculation, the structural strength analysis and optimization of the reliability of the key components of the cleaning and collection device were carried out, and verification experiments were also carried out through the manufacturing prototype. Results: The cleaning device designed in the experiment can clean the surplus grain of …
Research On Jujube Defect Recognition Method Based On Improved Convolution Neural Network, Zhang Zhong-Zhi, Xue Huan-Qing, Fan Guang-Ling
Research On Jujube Defect Recognition Method Based On Improved Convolution Neural Network, Zhang Zhong-Zhi, Xue Huan-Qing, Fan Guang-Ling
Food and Machinery
Objective: An automatic identification method of jujube defects based on improved convolution neural network was established. Methods: Using the dual branch convolution neural network structure, branch 1 combined with the transfer learning strategy for pre training, analysis 2 extracted the feature information from the jujube image based on the lightweight network fusion feature map. The superiority of this method was verified by comparative experiments. Results: Compared with the improvement before, the improved defect recognition method optimized the structure of the convolutional neural network, and the detection accuracy was further improved, from 96.02% to 99.50%. Conclusion: This method improved the network …
Effects Of Static Deposition Method And Koh Treatment Of Zeolite On Separation Of Wheat Gliadin, Wang Dan-Li, Liu Lu, Zhang Yi-Fan, Lian Xi-Jun
Effects Of Static Deposition Method And Koh Treatment Of Zeolite On Separation Of Wheat Gliadin, Wang Dan-Li, Liu Lu, Zhang Yi-Fan, Lian Xi-Jun
Food and Machinery
Objective: To study the technology of extracting gliadin from gluten and separating different gliadin components. Methods: The solution of gluten dissolved in 65% ethanol was settled at 4, 10, 20 and 30 ℃ for 1, 2, 4, 8, 10, 20 and 40 hours respectively, and the mass of the precipitated gliadin was measured. Further, the gliadin prepared by static deposition at 4 ℃ for 12 hours was used as raw material to study the separation of gliadin component by modified zeolite with KOH in different conditions. The zeolite was modified in three different mass fractions （20%, 50% and 80%）, three …
Study On Preparation Technology And Properties Of Dietary Fiber Ultrafine Powders From Okra Fermented Wine Pomace, Luo Xin, Zhou Yan-Qiang, Wu Guang-Bin, Chen Fa-He
Study On Preparation Technology And Properties Of Dietary Fiber Ultrafine Powders From Okra Fermented Wine Pomace, Luo Xin, Zhou Yan-Qiang, Wu Guang-Bin, Chen Fa-He
Food and Machinery
Objective: This study aimed to effectively utilize a large amount of dietary fiber andpectic polysaccharides in okra fermented wine pomace and turn waste into treasure. Methods: The processing technology and related characteristics of okra dietary fiber ultrafine powder were studied by wet ultrafine grinding and spray drying technology. Results: The results showed that okra fermented wine pomace was treated by colloid mill three times; then homogenized by high-pressure homogenizer for three times with 40 MPa of the homogenization pressure; after homogenization, spray drying was made with 210 ℃ in the inlet air temperature, 40 Hz of the fan frequency, solids …
Research Progress On Wall-Breaking Technology Of Rape Bee Pollen, Zheng Hui, Yang Si-Qi, Sun Yan, Li Shun-Xiang
Research Progress On Wall-Breaking Technology Of Rape Bee Pollen, Zheng Hui, Yang Si-Qi, Sun Yan, Li Shun-Xiang
Food and Machinery
This paper summarized the cell structure, wall breaking morphology and wall-breaking methods of rape bee pollen, analyzed and compared the advantages and disadvantages of various wall-breaking methods, summarized the application and development status of wall breaking rape bee pollen, and prospected the research on wall-breaking technology of rape bee pollen in the later stage.
Application Of Magnetic Covalent Organic Frameworks In Food Safety Analysis, Yang Da-Yu, Chen Zi-Ying, Pang Jie, Yan Zhi-Ming
Application Of Magnetic Covalent Organic Frameworks In Food Safety Analysis, Yang Da-Yu, Chen Zi-Ying, Pang Jie, Yan Zhi-Ming
Food and Machinery
In this paper, the application of magnetic covalent organic frameworks （MCOFs） in food safety analysis is reviewed by combining with the domestic and foreign literature, and the common preparation methods of MCOFs are briefly introduced. The application examples of MCOFs in pesticide residues, veterinary drug residues, organic pollutants, toxins and harmful substances in packaging were discussed, and the practical detection application of MCOFS in the future is prospected.
Analysis Of The Main Chemical And Volatile Components Of Xianggan Tea, Xiang-Style Ganpu Tea, Li Xiang, Fu Fu-Hua, Pan Zhao-Ping, Wang Chen, He Shuang
Analysis Of The Main Chemical And Volatile Components Of Xianggan Tea, Xiang-Style Ganpu Tea, Li Xiang, Fu Fu-Hua, Pan Zhao-Ping, Wang Chen, He Shuang
Food and Machinery
Objective: Xianggan tea, was made from Hunan Anhua dark tea, i. e. Tianjian tea and the mandarin peel of Yueyang Jinpen pomelo, based on the preparation method of Ganpu tea, and this contributed to ascertaining the quality of Xianggan tea. Methods: The main chemical components, mineral element content and volatile components were analyzed in the Tianjian tea, mandarin peel and Xianggan tea. Results: The moisture content of Tianjian tea, mandarin peel, and Xianggan tea were all less than 20%, and made them easy for storage. The content of crude polysaccharides, total flavonoids, and total phenols was in the order of …
Active Components, Antioxidant Capacity And Quality Evaluation Of Sichuan Dark Tea, Zhu Bo-Yu, Xia Chen, Luo Ke-Bin, Zhu Yong-Qing, Tang Xiao-Bo, Chen Jian
Active Components, Antioxidant Capacity And Quality Evaluation Of Sichuan Dark Tea, Zhu Bo-Yu, Xia Chen, Luo Ke-Bin, Zhu Yong-Qing, Tang Xiao-Bo, Chen Jian
Food and Machinery
Objective: The contents of tea polyphenol monomer, caffeine (CAF), total polyphenols acid (TPC) and total flavonoids (TFC) in 26 kinds of commercial Sichuan dark tea (S1～S26) were analyzed, and the in vitro antioxidant activities were investigated, to provide a theoretical basis for the quality evaluation of Sichuan dark tea. Methods: Gradient elution was used to analyze the content of tea polyphenol monomer and caffeine. The contents of TPC and TFC were determined by the folin phenol method and chemical analysis method, respectively. The antioxidant activity was evaluated by DPPH and ABTS radical scavenging capacity. Results: The content of gallic acid …
Adsorption Of Caffeic Acid In Sucrose Solution By Magnetic Chitosan Modified Kaolin, Pan Yan-Mei, Wu Hai-Ling, Wei Qiao-Yan, Su Long, Liu Fu-Jie
Adsorption Of Caffeic Acid In Sucrose Solution By Magnetic Chitosan Modified Kaolin, Pan Yan-Mei, Wu Hai-Ling, Wei Qiao-Yan, Su Long, Liu Fu-Jie
Food and Machinery
Objective: Studied the adsorption characteristics of magnetic chitosan modified kaolin on caffeic acid in simulated sugarcane juice, and provided the reference for the removal of phenolic pigments in sugarcane juice. Methods: Magnetic chitosan modified kaolin was prepared by coprecipitation of chitosan, nano ferric oxide and kaolin. The surface structure and group changes of kaolin before and after modification were characterized by FT-IR, VSM and SEM; The adsorption characteristics of caffeic acid were studied by adsorption test. Results: the modified chitosan and nano-Fe3O4 were successfully loaded on kaolin, and the adsorption performance of caffeic acid was improved. The …
Effects Of Milling Degree And Cooking Method On The Cooked Rice Quality Of High-Quality Indica Rice, Li Liu-Yan, Zhan Zhan, Zhang Wei, Shu Zai-Xi, Wang Ping-Ping
Effects Of Milling Degree And Cooking Method On The Cooked Rice Quality Of High-Quality Indica Rice, Li Liu-Yan, Zhan Zhan, Zhang Wei, Shu Zai-Xi, Wang Ping-Ping
Food and Machinery
Objective: To investigate the effects of milling degree and cooking method on cooked rice quality of high-quality Indica rice. Methods: Paddy rice （variety Longliangyou 1813） were dehulled and milled for 20, 35, and 50 s, respectively. Rice milled for different durations were cooked with electric pressure cooker and ordinary rice cooker, respectively. Quality attributes of cooked rice were compared by texture analyzer, gas chromatograph-ion mobility spectrometer （GC-IMS）, and sensory judgement. Results: For rice milled for 20 s, the cooked product of ordinary rice cooker had higher hardness than that of electric pressure cooker. However, for rice milled for 35 or …
Effect Of Jet Milling On The Physical And Chemical Properties Of Tartary Buckwheat Powder, Zhang Xue, Zhang Dong-Jie, Zhang Ai-Wu
Effect Of Jet Milling On The Physical And Chemical Properties Of Tartary Buckwheat Powder, Zhang Xue, Zhang Dong-Jie, Zhang Ai-Wu
Food and Machinery
Objective: The effect of superfine grinding on the physicochemical properties of tartary buckwheat powder in different parts was studied, aiming to provide a certain theoretical reference for the food industry to use superfine grinding to prepare tartary buckwheat food. Methods: Tartary buckwheat skin powder, core powder and whole powder were used as materials to prepare tartary buckwheat ultrafine powder by superfine grinding combined with a fluidized bed jet mill. The superfine powder was studied by measuring the particle size, specific surface area, comprehensive powder characteristics, swelling property, water solubility and other indicators. Results: The particle size of the three kinds …
Determination Of 10-Hydroxy-2-Decenoic Acid In Honey By Ultra High-Performance Liquid Chromatography-Tandem Mass Spectrometry, Hu Li-Li, Li Ying, Wang Hui, Pi Lu-Lu, Chen Xian-Gui, Jiang Li
Determination Of 10-Hydroxy-2-Decenoic Acid In Honey By Ultra High-Performance Liquid Chromatography-Tandem Mass Spectrometry, Hu Li-Li, Li Ying, Wang Hui, Pi Lu-Lu, Chen Xian-Gui, Jiang Li
Food and Machinery
Objective: This study aimed to establish a method using ultra-high-performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS) to determine 10-hydroxy-2-decenoic acid in honey. Methods: The samples were extracted with methanol-water and cleaned up by a PLS solid-phase extraction column. The separation was performed on an Agilent ZOXBAR SB-C18 column (2.1 mm×50 mm, 1.8 μm) and methanol -5 mmol/L ammonium acetate solution was used as the mobile phase for gradient elution. Mass spectrometry was carried out under the multiple reaction monitoring (MRM) mode with negative electrospray ionization (ESI-) and standard external method for quantitative analysis. Results: Good linearity of the developed analytical method …
Simultaneous Rapid Determination Of 18 Quinolones Residues In Raw Milk By Liquid-Liquid Extraction And Ultra Performance Liquid Chromatography Tandem Mass Spectrometry, Zhou Yan-Hua, Li Tao, Pan Xiao-Hong, Xiang Jun
Simultaneous Rapid Determination Of 18 Quinolones Residues In Raw Milk By Liquid-Liquid Extraction And Ultra Performance Liquid Chromatography Tandem Mass Spectrometry, Zhou Yan-Hua, Li Tao, Pan Xiao-Hong, Xiang Jun
Food and Machinery
Objective: A rapid method for simultaneous determination of 18 quinolones residues in raw milk was established. Methods: The raw milk was pretreated by liquid-liquid extraction, and the residues of 18 quinolones in raw milk were analyzed by ultra-performance liquid chromatography-tandem mass spectrometry. Results: The linearity of all the 18 quinolones from 2.0 to 100.0 ng/mL had correlation coefficients greater than 0.992. The limits of detection (LOD) of this method ranged from 0.02 to 0.50 μg/kg, and the limits of quantification (LOQ) were 0.06 to 1.50 μg/kg. The average recoveries of the 18 quinolones were 74.0% to 106.5%, with the relative …
Rapid Determination Simultaneously Of Twelve Kinds Of Nitrophenolic Compounds In Water By Modified Quechers-Gc-Ms, Wu Jian-Qiang, Zhao Zhong-Jing, Hong Xia, He Hai-Ning, Yuan Cai-Xia
Rapid Determination Simultaneously Of Twelve Kinds Of Nitrophenolic Compounds In Water By Modified Quechers-Gc-Ms, Wu Jian-Qiang, Zhao Zhong-Jing, Hong Xia, He Hai-Ning, Yuan Cai-Xia
Food and Machinery
Objective: A simple, efficient, rapid, sensitive, reproducible, accurate and rapid method was established for the simultaneous determination of 12 nitrophenols in water. Methods: Magnetic Fe3O4 nanoparticles loaded with bifunctional octadecylamine functionalized carbon nanotube composites were synthesized by coprecipitation and hydrothermal methods. The sample pretreatment method of QuEChERS was optimized and combined with gas chromatography-mass spectrometry to establish a method for the simultaneous determination of 12 kinds of nitrophenols in water quality. Results: The optimized QuEChERS sample pretreatment method gave the advantages of magnetic nanoparticles and carbon nano materials. Under the control of these conditions, high efficiency of …