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Full-Text Articles in Manufacturing

Temperature Gradient Effect On Solid-Liqid Interface Properties Of Al-Cu Alloy: A Molecular Dynamics Study, Prashant Kumar Jha Dec 2023

Temperature Gradient Effect On Solid-Liqid Interface Properties Of Al-Cu Alloy: A Molecular Dynamics Study, Prashant Kumar Jha

All Theses

Aluminum-copper (Al-Cu) alloys are widely used in the aerospace industry due to their favorable strength-to-weight ratio, good fatigue resistance, and corrosion resistance. These properties make Al-Cu alloys an excellent choice for aircraft structural components that require high strength and low weight. Additive manufacturing (AM), also known as 3D printing, has emerged as a promising processing method for Al-Cu alloys in aerospace manufacturing. AM enables the production of lightweight optimized geometries difficult to manufacture through conventional subtractive methods. AM also reduces material waste by only depositing material where needed in the part geometry. The rapid solidification conditions in AM processes motivate …


Analyzing The Effects Of Ultrafast Laser Processing On Mechanical Properties Of 3d-Printed Pla Parts, Darshan Pramodbhai Yadav Dec 2023

Analyzing The Effects Of Ultrafast Laser Processing On Mechanical Properties Of 3d-Printed Pla Parts, Darshan Pramodbhai Yadav

Theses and Dissertations

Recent advances in additive manufacturing technologies have already led to wide-scale adoption of 3D-printed parts in various industries. The expansion in choice of materials that can be processed, particularly using Fused Deposition Modeling (FDM), and the steady advancements in dimensional accuracy control have extended the range of applications far beyond rapid prototyping. However, additive manufacturing still has considerable limitations compared to traditional and subtractive manufacturing processes. This work addresses limitations associated with the as-deposited surface roughness of 3D-printed parts. The effects of roughness-induced stress concentrations were studied on ultimate tensile strength and fatigue life. The samples were manufactured using a …


Implementation Of Experimental Static Recrystallization Of High Strength Steel Into Computational Simulation Of Multi-Pass Slab Hot Rolling, S. K. Dasari, S. Ganguly, A. Abutunis, K. Chandrashekhara, M. F. Buchely, S. N. Lekakh, R. J. O'Malley, T. Natarajan Nov 2023

Implementation Of Experimental Static Recrystallization Of High Strength Steel Into Computational Simulation Of Multi-Pass Slab Hot Rolling, S. K. Dasari, S. Ganguly, A. Abutunis, K. Chandrashekhara, M. F. Buchely, S. N. Lekakh, R. J. O'Malley, T. Natarajan

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Microstructural changes and softening due to static recrystallization have a critical influence on thermo-mechanical behavior of high strength steels during industrial multi-pass hot rolling. Numerical simulation using finite element analysis (FEA) can be used to accurately predict the softening behavior during the hot rolling process. Therefore, the implementation of an experimentally defined static recrystallization model into FEA is necessary to get realistic simulation prediction. in this study, the extent of softening during static recrystallization in Si and Mn alloyed high strength steel was measured using double hit tests. a Gleeble™ thermo-mechanical simulator was used to perform the double hit tests …


An Investigation Into The Challenges Of Contemporary Additive Manufacturing: Insights Into The Metallurgical Response Of Materials And Relevant Solution, Huan Ding Nov 2023

An Investigation Into The Challenges Of Contemporary Additive Manufacturing: Insights Into The Metallurgical Response Of Materials And Relevant Solution, Huan Ding

LSU Doctoral Dissertations

Additive Manufacturing (AM) has gained attention in recent years due to its unique capabilities in the fabrication of complex parts. As with any new research, there is still a lack of sufficient understanding in the field of additive manufacturing, and further investigation is needed to solve existing problems. Ultimately, the aim is to enable the widespread use of AM components across various industries.

Chapter One provides a brief introduction to the background and current bottlenecks of additive manufacturing technology. Chapter two focuses on the development of high-strength 7075 aluminum alloy (Al7075) for Fused Deposition Modeling and Sintering (FDMS) technology. Al7075 …


Additive Manufacturing For Medical Education, Michael Noon Oct 2023

Additive Manufacturing For Medical Education, Michael Noon

College of Engineering Summer Undergraduate Research Program

A growing body of evidence is suggesting that anatomical knowledge, the keystone of many medical specialties, is suffering among new graduates. While a host of reasons are provided, one common thread that many point to is the decline of cadaver dissections in the classroom. Many virtual audio-visual tools are used to address this gap, yet evidence has shown their ineffectiveness. Given this gap, the high degree of flexibility found in additive manufacturing (AM), and the many uses AM has already found in the medical field, we propose its use to fill this gap, allowing for students to learn with touch …


Optimizing Mn-Al Permanent Magnet Performance Through Control Of The Phase Transformation, Ternary Element Addition, And Advanced Processing, Thomas R. Keller Sep 2023

Optimizing Mn-Al Permanent Magnet Performance Through Control Of The Phase Transformation, Ternary Element Addition, And Advanced Processing, Thomas R. Keller

Dartmouth College Ph.D Dissertations

The growing need for electrical power in machines and vehicles brings with it a growing need for critical materials. The current high-performance permanent magnets (PMs) based on rare-earth (RE) elements Nd and Sm cannot escape the problem of raw material cost, geographic scarcity in the earth’s crust, and lack of circular global supply chains. This poses a problem of industrial ecology: can PMs be made from inexpensive, more abundant materials while still meeting sufficient performance criteria? PMs based on the magnetic τ phase of Mn-Al offer a possible alternative to REPMs. However, years of innovation have not yet achieved real-world …


Fatigue And Fracture Of Electron Beam Melting Ti-6al-4v, William A. Grell Aug 2023

Fatigue And Fracture Of Electron Beam Melting Ti-6al-4v, William A. Grell

Electronic Theses and Dissertations

For applications in the aerospace field, selection of materials for a given design requires an understanding of critical properties, like fatigue and fracture, in addition to static mechanical and physical properties. With the ongoing advancements in metallic additive manufacturing techniques and the interest in applying the process to aerospace applications, there is a clear need to fully characterize properties. Arguably, the most attractive alloy for applications in aerospace is the Ti-6Al-4V alloy. The current dissertation examines the mechanical properties of the alloy, made by the Electron Beam Melting (EBM) Powder Bed Fusion (PBF) method. As illustrated in this work, the …


Life Cycle Energy Assesment Of Advanced Fiber Reinforced Composite Design And Manufacturing Methodologies, Urjit Lad Aug 2023

Life Cycle Energy Assesment Of Advanced Fiber Reinforced Composite Design And Manufacturing Methodologies, Urjit Lad

All Theses

Automotive industry at large is focused on vehicle light-weighting since a 6%-8% increase in fuel efficiency can be achieved with a 10% reduction in vehicle weight [1]. With the growing demand for cost-effective and sustainable light weighting of automobile structures, interest has increased in the application of fiber reinforced plastic (FRP) composites for use in the Body-in-White (BiW), which can account for up to 40% of the total vehicle weight. Traditional FRP composite manufacturing processes like vacuum assisted resin transfer molding, autoclave consolidation or use of automated fiber placement have been successfully used for marine and aerospace applications. However, these …


Characterization Of Mechanically Recycled Polylactic Acid (Pla) Filament For 3d-Printing By Evaluating Mechanical, Thermal, And Chemical Properties And Process Performance, Mahsa Shabani Samghabady Aug 2023

Characterization Of Mechanically Recycled Polylactic Acid (Pla) Filament For 3d-Printing By Evaluating Mechanical, Thermal, And Chemical Properties And Process Performance, Mahsa Shabani Samghabady

All Theses

Polylactic acid (PLA) is a biopolymer made from renewable resources such as sugar and corn. PLA filament is a popular material used in Fused Deposition Modeling (FDM) 3D-printing. While this material has many advantages, all the failed parts, support structures, rafts, nozzle tests, and the many prototype iterations during the 3D-printing process contribute to the plastic pollution and release of greenhouse gases. Although PLA is biodegradable, it can take years to degrade in landfills. Instead of throwing away PLA waste and buying new filaments, PLA can be recycled. Amongst the different recycling technologies, mechanical recycling is the most environmentally friendly. …


Optimization Of Alti Pld Coating By Increasing Ti Content, N2 And Annealing Which Used For Skd61 Pins In Aluminum Die Casting, Rusman Kosasih, Maria Margaretha Suliyanti Prof, Dedi Priadi, Wisnu Usni Jul 2023

Optimization Of Alti Pld Coating By Increasing Ti Content, N2 And Annealing Which Used For Skd61 Pins In Aluminum Die Casting, Rusman Kosasih, Maria Margaretha Suliyanti Prof, Dedi Priadi, Wisnu Usni

Journal of Materials Exploration and Findings

The Alumunium Titanium Nitrogen (AlTiN) coating is known as one of the best coating materials for protective coating, while Pulsed Laser Deposition (PLD) is a laser coating process used for electric layer and superconductor applications, producing thin films up to 20 µm in thickness. The combination of these two matters has already been researched and is still in progress. One major challenge in the aluminium casting industry is to minimize the damage caused to tool steel pins made from SKD61, when aluminium material sticks to the pin, and halting production. Therefore, research on effective coatings for tool steels and testing …


The Effect Of Current Density And Hard Chrome Coating Duration On The Mechanical And Tribological Properties Of Aisi D2 Steel, Indah Uswatun Hasanah, Dedi Priadi, Donanta Dhaneswara Jul 2023

The Effect Of Current Density And Hard Chrome Coating Duration On The Mechanical And Tribological Properties Of Aisi D2 Steel, Indah Uswatun Hasanah, Dedi Priadi, Donanta Dhaneswara

Journal of Materials Exploration and Findings

The effect of hard chromium coating on AISI D2's mechanical properties and wear resistance has been investigated using the electrolysis technique with varying current and coating duration. The variations of current used are 0.8 A, 1.2 A, and 1.6 A, while the coating duration used are 300, 600 and 900 seconds. Characterization of the films was conducted using SEM-EDS, and XRD. It can be observed from SEM characterization that the chrome grains resulted from the electroplating process are fine. The XRD identify chrome compund on the surface coating. The highest hardness value was 520.6 HV on a sample with a …


A Strong And Ductile Cobalt-Free Solid-Solution Fe30ni30mn30cr10 Multi-Principal Element Alloy From Hot Rolling, Hans Pommerenke, Jiaqi Duan, Nathan Curtis, Victor Delibera, Adam Bratten, Andrew Hoffman, Mario Buchely, Ronald O'Malley, Haiming Wen Jul 2023

A Strong And Ductile Cobalt-Free Solid-Solution Fe30ni30mn30cr10 Multi-Principal Element Alloy From Hot Rolling, Hans Pommerenke, Jiaqi Duan, Nathan Curtis, Victor Delibera, Adam Bratten, Andrew Hoffman, Mario Buchely, Ronald O'Malley, Haiming Wen

Materials Science and Engineering Faculty Research & Creative Works

Most of the face-centered cubic (FCC) multi-principal element alloys (MPEAs) developed thus far contain cobalt. for many applications, it is either required or beneficial to avoid cobalt, since cobalt has long-term activation issue (for nuclear applications), is expensive, and is considered a critical material. in addition, FCC structured solid-solution MPEAs tend to have relatively low strength. an FCC solid-solution Fe30Ni30Mn30Cr10 (at %) MPEA was fabricated via arc melting, followed by homogenization at 1100 °C for 12 h. the alloy was hot rolled at 1100 °C with a total reduction of up to 97 %. the microstructure was characterized, and mechanical …


Additive Manufacturing Of Stretchable Strain Sensors: Fabrication, Optimization And Application, John Nady Shihat Bastawrous Jun 2023

Additive Manufacturing Of Stretchable Strain Sensors: Fabrication, Optimization And Application, John Nady Shihat Bastawrous

Theses and Dissertations

In this project, a novel strain sensor design is fabricated employing different additive manufacturing techniques. The spring sensor's primary material is PLA-Like resin with a nanocomposite encapsulation layer as the functional material. The main principle of Straining the sensors results in a change in resistivity as the distances among the conductive carbon particles change according to the strain applied.

Sensor fabrication consists of two parts: spring manufacturing and development of nanocomposite encapsulation The nanocomposite matrix is developed through the dispersion of Graphene and Carbon nanotubes in Thermoplastic Polyurethane through sonication and magnetic hotplate stirring. While the spring itself is manufactured …


Fungi In Flux | Designing Regenerative Materials And Products With Mycelium, Arvind Bhallamudi Jun 2023

Fungi In Flux | Designing Regenerative Materials And Products With Mycelium, Arvind Bhallamudi

Masters Theses

As the world grapples with the escalating crisis of climate threats and environmental degradation, this research delves into the synergistic potential of design and biology, developing safe and sustainable materials for applications in prototyping, furniture and interior design. Harnessing the power of a unique organism - fungi, the study proposes an accessible, efficient, and resilient material resource system. It utilizes local waste streams and mycelium (the vegetative part of fungi) to grow functional structures. An experimental and small-scale protocol is modeled by testing bio-fabrication and bio-printing methods. The composites' performance qualities and characteristics are evaluated through mechanical testing and a …


3d Printed Aircraft, Matthew Nagy, Charles D'Amico, Alexis Salgado Medina Jun 2023

3d Printed Aircraft, Matthew Nagy, Charles D'Amico, Alexis Salgado Medina

Mechanical Engineering

This project is to design, build, and test a 3D-printable aircraft. The goal is to create a final design that will be able to fly for the longest duration possible, around 20 seconds. To determine the correct preliminary design and manufacturing process for a 3D printed RC aircraft, an analysis of multiple design options and manufacturing materials was performed. This allowed for a variety of choices for aircraft type, airfoil design, structure, among other topics to be narrowed down to the most promising option. It has been found that the aircraft will follow a design similar to industry motor-gliders, with …


Thermal Transport And Physical Characteristics Of Silver-Reinforced Biodegradable Nanolubricant, Jaime Taha-Tijerina, Karla Aviña, Nicolás Antonio Ulloa-Castillo, Dulce Viridiana Melo-Maximo May 2023

Thermal Transport And Physical Characteristics Of Silver-Reinforced Biodegradable Nanolubricant, Jaime Taha-Tijerina, Karla Aviña, Nicolás Antonio Ulloa-Castillo, Dulce Viridiana Melo-Maximo

Informatics and Engineering Systems Faculty Publications

In this investigation, the thermal transport behavior of biodegradable lubricant reinforced with silver nanostructures (AgNs) at various filler fractions of 0.01, 0.05, 0.10, and 0.20 weight percent was evaluated over a temperature scan analysis, ranging from room temperature up to 60 °C. The experimental results revealed significant gradual enhancements in thermal conductivity as AgNs concentration and evaluating temperatures were increased. These improvements showed the important role of nanostructures’ interaction within the biodegradable lubricant. The thermal conductivity performance improved for nanolubricants ranging from 6.5% at 30 °C and 0.20 wt.% AgNs content up to a maximum 32.2%, which was obtained at …


Exploring Methods For Recycling Filament Waste In 3d Printing, Max Rios Carballo May 2023

Exploring Methods For Recycling Filament Waste In 3d Printing, Max Rios Carballo

Publications and Research

The goal of the current study is to investigate cutting-edge techniques for recycling filament waste from 3D printing procedures. Appropriate waste management techniques are required to reduce this trash's harmful environmental consequences. The goal of the project is to look at new methods for recycling filament waste in order to minimize disposal and encourage reuse. To acquire data from pertinent papers and research, a thorough literature review methodology was used. The findings show that this issue may be resolved utilizing a variety of recycling techniques, including shredding, melting, and re-extrusion. The type of filament waste and the intended goal will …


Effects Of Tempering Temperature On Gas Turbine Fan Cases, Seth Utter Apr 2023

Effects Of Tempering Temperature On Gas Turbine Fan Cases, Seth Utter

Honors Scholar Theses

The project aimed to investigate the effects of tempering temperature on metals used for gas turbine engine fan cases as a major relevant concern is containing blades in during blade-out events. There are three ways to accomplish this: using a thicker metal, incorporating different materials into the case, or heat treating the metal. This project focused on the third solution: reviewing the impact toughness and hardness of fractured samples and their equivalent ductile-to-brittle transition shear faces. Given its availability, 1045 steel, as opposed to aerospace grade metals, was used for in-house testing. The data obtained from these experiments were then …


Mechanical Characterization Of Additively Manufactured Alloys Compared To Their Wrought Counterparts, Laith A. Alqawasmi Apr 2023

Mechanical Characterization Of Additively Manufactured Alloys Compared To Their Wrought Counterparts, Laith A. Alqawasmi

Mechanical Engineering ETDs

Additive manufacturing is a method of manufacturing based on building parts layer by layer, allowing for more control over shape of the product, therefore reducing machining costs, reducing material waste, faster production times and the ability to build complex engineering design that other manufacturing technologies won’t be able to produce. This research is on the tensile and indentation testing (following ASME standards) of 3D printed Ti-6Al-4V and Inconel 718 built by powder-based direct energy deposition technology. Ti-6Al-4V is an attractive material for the aerospace and aviation industry, and Inconel 718, a nickel-chromium based superalloy, is an attractive material for usage …


A High-Strength Precipitation Hardened Cobalt-Free High-Entropy Alloy, Matthew Luebbe, Jiaqi Duan, Fan Zhang, Jonathan Poplawsky, Hans Pommeranke, Maalavan Arivu, Andrew Hoffman, Mario Buchely, Haiming Wen Apr 2023

A High-Strength Precipitation Hardened Cobalt-Free High-Entropy Alloy, Matthew Luebbe, Jiaqi Duan, Fan Zhang, Jonathan Poplawsky, Hans Pommeranke, Maalavan Arivu, Andrew Hoffman, Mario Buchely, Haiming Wen

Materials Science and Engineering Faculty Research & Creative Works

Recent studies on precipitation-hardened high-entropy alloys (HEAs) demonstrate their high strength and thermal stability, making them promising materials for high-temperature structural applications such as nuclear reactors. However, many existing HEAs contain cobalt (Co), which is unsuitable for nuclear applications because of the long-term activation issue of Co. Co is also expensive and considered a critical material for other applications. Therefore, it is desired to exclude Co from the composition. a Co-free (Fe0.3Ni0.3Mn0.3Cr0.1)88Ti4Al8 HEA was developed and studied in this work. in contrast to previous Co-free HEAs, this alloy is close to Equi atomic in its composition and promises a more …


Fast-, Light-Cured Scintillating Plastic For 3d-Printing Applications, Brian G. Frandsen, Michael Febbraro, Thomas Ruland, Theodore W. Stephens, Paul A. Hausladen, Juan J. Manfredi, James E. Bevins Mar 2023

Fast-, Light-Cured Scintillating Plastic For 3d-Printing Applications, Brian G. Frandsen, Michael Febbraro, Thomas Ruland, Theodore W. Stephens, Paul A. Hausladen, Juan J. Manfredi, James E. Bevins

Faculty Publications

Additive manufacturing techniques enable a wide range of possibilities for novel radiation detectors spanning simple to highly complex geometries, multi-material composites, and metamaterials that are either impossible or cost prohibitive to produce using conventional methods. The present work identifies a set of promising formulations of photocurable scintillator resins capable of neutron-gamma pulse shape discrimination (PSD) to support the additive manufacturing of fast neutron detectors. The development of these resins utilizes a step-by-step, trial-and-error approach to identify different monomer and cross-linker combinations that meet the requirements for 3D printing followed by a 2-level factorial parameter study to optimize the radiation detection …


Material Property Dependence Of Nanoparticle Silicon Carbide Alloying In Additively Manufactured Molybdenum, Andrew P. Mason Mar 2023

Material Property Dependence Of Nanoparticle Silicon Carbide Alloying In Additively Manufactured Molybdenum, Andrew P. Mason

Theses and Dissertations

The structural performance of additively manufactured Mo printed by LPBF can be significantly improved by nanoparticle alloying. Previous AFIT studies of SiC nanoparticle addition conducted by Ellsworth (2022) et al. demonstrated increased powder consolidation, leading to reduced porosity, increased microhardness, and a shift in atomic defect concentrations. The addition of defected SiC particles is proposed to reduce in situ oxidation by acting as a sacrificial oxidizing agent and contributing to the formation of Mo disilicide secondary phases. This study investigated the relationship between laser powder bed fusion Mo microscale and nanoscale properties with varying SiC particle size while maintaining a …


Development Of Novel Turbomachinery Manufacturing Methods, Timothy P. Winkler Mar 2023

Development Of Novel Turbomachinery Manufacturing Methods, Timothy P. Winkler

Theses and Dissertations

Compact turbine engines are of increasing interest as a means of propulsion for small, lightweight, low cost, unmanned aerial systems. This study looks to leverage advancements in novel manufacturing technology to produce turbomachinery components while simultaneously reducing costs and manufacturing time. To determine the feasibility of drop-in replacements for stock components this study focused on several research areas. This included materials research on both polymer-reinforced and ceramic materials, specimen tensile testing to determine temperature-dependent material properties, finite element analysis of multiple candidate materials, design and fabrication of a spin test rig, and physical spin testing of manufactured components to predict …


Launching A 3d Printing Program For Students: Recommendations And Best Practices For Libraries, Wilhelmina Randtke, Lee Bareford Feb 2023

Launching A 3d Printing Program For Students: Recommendations And Best Practices For Libraries, Wilhelmina Randtke, Lee Bareford

Georgia Library Quarterly

The Georgia Southern University Libraries launched a 3D printing program for students in July 2022. Prior to launch, library employees at two of Georgia Southern University’s campuses investigated options for implementing safe, affordable, and sustainable 3D printing in existing academic libraries without retrofitting costly ventilation systems into existing facilities. This article describes the reasons why the Georgia Southern University Libraries thought that a 3D printing program could fulfill a service need for students across university colleges and departments and outlines some of the challenges, best practices, and unique innovations that the library’s employees experienced throughout the program launch process. The …


Effect Of Austenization And Repeated Quenching On The Microstructures And Mechanical Properties Of Wear-Resistant Steel, Yanuar Nugraha, Myrna Ariati Mochtar Jan 2023

Effect Of Austenization And Repeated Quenching On The Microstructures And Mechanical Properties Of Wear-Resistant Steel, Yanuar Nugraha, Myrna Ariati Mochtar

Journal of Materials Exploration and Findings

This study was focused on determining the effect of repeated austenitization and quenching on mechanical properties and microstructure. The experiment was carried out in a rolled quencher facility with a heat treatment process of one to two times, with parameters of an austenizing temperature of 9500C and quenching at a temperature of 8500C with pressurized water media. Testing of specimens, including microstructure observations and hardness testing. The repeated heat treatment process showed an increase in hardness of 0.79% on one-time repeated heat treatment and 1.65% on two repeated heat treatments. This occurs due to the presence accompanied by refinement of …


Advanced Microstructural Characterization Of Functionally Graded Dental Ceramic Material For Materials-Informed Finishing, Angani Vigneswaran Jan 2023

Advanced Microstructural Characterization Of Functionally Graded Dental Ceramic Material For Materials-Informed Finishing, Angani Vigneswaran

Theses and Dissertations--Manufacturing Systems Engineering

Yttria-stabilized tetragonal zirconia polycrystal (Y-TZP) has gained popularity as the choice of material for dental prosthetics. Ivoclar Vivadent’s IPS e.max ZirCAD Prime dental ceramic incorporates a unique gradient technology that varies the yttria content over the thickness of the material. The top layer is composed of 5Y-TZP which is desired for its optical properties while the bottom layer is composed of a much stronger 3Y-TZP. In between the two layers, 5Y-TZP and 3Y-TZP are mixed to form a transition layer. Varying the amount of yttria allows for more esthetically pleasing translucency in the visible areas of the restoration without compromising …


Recycling Metal Chips Into Usable Materials, Alex Mortensen, Ben Mortensen Jan 2023

Recycling Metal Chips Into Usable Materials, Alex Mortensen, Ben Mortensen

Williams Honors College, Honors Research Projects

This report entails the scope, design considerations, and plans for creating a metal chip converter into metal briquettes. The construction is a set of machines with multiple processes to make the conversion happen. The process includes washing fine metal chips, drying them off, compressing them, and melting them down into usable briquettes. This project is intended to make a simple process to recycle metal chips into usable material for reuse. The project's objective is to reduce the costs of storage and recycling waste by offering a solution to recycle it into materials the shop can reuse.


Dome Tester, Clark Bates, Nikolas M. Kulin Jan 2023

Dome Tester, Clark Bates, Nikolas M. Kulin

Williams Honors College, Honors Research Projects

We are reconfiguring and modifying the previously built dome tester to be more user friendly and mechanically applicable. This has a long-term goal of being a usable teaching tool for manufacturing education within the college of engineering and polymer sciences. The dome tester pushes a metal dome into a clamped sheet of metal to test its forming limits and where necking occurs. We have implemented a better method of viewing the sheet sample as it is being deformed, and improved measuring methods for the distance a sample is deformed. By introducing these changes in conjunction with improved documentation of the …


Investigation Of Microstructurally Dependent Mechanical Properties Of Cold Sprayed Copper Using Correlative Microscopy, Quintin Otto Jan 2023

Investigation Of Microstructurally Dependent Mechanical Properties Of Cold Sprayed Copper Using Correlative Microscopy, Quintin Otto

UNF Graduate Theses and Dissertations

This project employs multi-instrument materials characterization to analyze material made with the “Cold Spray” additive manufacturing process. Cold spray is an emerging additive manufacturing technique with unique benefits resulting from its low temperature adhesion process induced by plastic deformation. Metallic powder collides at high speeds creating three dimensional materials and coatings without the need for melting. Copper cold sprayed specimens were analyzed using a series of imaging techniques to characterize the microstructure at varying levels of detail and magnification. Scanning electron microscopy and electron back scattered diffraction were paired with microhardness testing to generate a correlative comparison between microstructure and …


Modified Reactive Sputter Deposition Of Titanium Nitride Thin Films Via Hipims With Kick-Pulse And Improvement Of The Structure-Zone Model, Andrew Miceli Jan 2023

Modified Reactive Sputter Deposition Of Titanium Nitride Thin Films Via Hipims With Kick-Pulse And Improvement Of The Structure-Zone Model, Andrew Miceli

UNF Graduate Theses and Dissertations

Direct current (DC) and radio frequency (RF) sputtering methods have been commonplace in industry for several decades and widely studied in literature. Hard films of nitrides, such as titanium nitride (TiN), have been deposited using reactive DC sputtering onto cutting tools and medical devices extensively as well. For these applications, the films require excellent adhesion, high density, and high hardness. High-Power Impulse Magnetron Sputtering (HIPIMS) has emerged over the last several years as a method to produce films with increased density and mechanical properties. Process-structure-property relationships for reactive HIPIMS are not yet well developed. Additionally, conventional HIPIMS suffers from relatively …