Materials Science and Engineering Commons^™

Metallurgical And Thermal Processing Investigation Of Additively Manufactured Superalloys Jbk-75 And Nasa-Hr-1, Allyse Birken, Derek Noel

Materials Engineering

Aerojet Rocketdyne is investigating the use of directed energy deposition (DED), an additive manufacturing process, to reduce cost and lead time for manufacturing complex rocket engine components for their RS-25 engines. JBK-75 and NASA-HR-1, two Fe-Ni-base, age-hardenable (γ′) superalloys, are used for nozzle structural jackets and hot gas manifolds. Currently, these parts are produced using traditional forging or casting methods followed by intensive machining operations. Additionally, these alloys were designed for use in the wrought condition and require a different set of post-processing heat treatments when produced using DED due to their dendritic, segregated microstructure in the as-built condition. Homogenization …

The Corrosion Of Stainless Steel Made By Additive Manufacturing: A Review, Gyeongbin Ko, Wooseok Kim, Kyungjung Kwon, Tae-Kyu Lee

Mechanical and Materials Engineering Faculty Publications and Presentations

The advantages of additive manufacturing (AM) of metals over traditional manufacturing methods have triggered many relevant studies comparing the mechanical properties, corrosion behavior, and microstructure of metals produced by AM or traditional manufacturing methods. This review focuses exclusively on the corrosion property of AM-fabricated stainless steel by comprehensively analyzing the relevant literature. The principles of various AM processes, which have been adopted in the corrosion study of stainless steel, and the corrosion behaviors of stainless steel depending on the AM process, the stainless steel type, and the corrosion environment are summarized. In this comprehensive analysis of relevant literature, we extract …

Absorption Of Nitrogen During Pulsed Wave L-Pbf Of 17-4 Ph Steel, Ben Brown, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

In the fabrication of 17-4 PH by laser powder bed fusion (L-PBF) the well-documented occurrence of large amounts of retained austenite can be attributed to an elevated concentration of nitrogen present in the material. While the effects of continuous wave (CW) laser processing on in-situ nitrogen absorption characteristics have been evaluated, power modulated pulsed wave (PW) laser processing effects have not. In this study the effects of PW L-PBF processing of 17-4 PH on nitrogen absorption, phase composition, and mechanical performance are explored using commercially available PW L-PBF equipment and compared to samples produced by CW L-PBF. PW L-PBF samples …

Tailoring Texture, Microstructure, And Shape Memory Behavior Of Niti Alloys Fabricated By L-Pbf-Am, Sayed Ehsan Saghaian N.E.

Theses and Dissertations--Mechanical and Aerospace Engineering

Laser Powder Bed Fusion (L-PBF) is one of the most promising Additive Manufacturing (AM) methods to fabricate near net-shape metallic materials for a wide range of applications such as patient-specific medical devices, functionally graded materials, and complex structures. NiTi shape memory alloys (SMAs) are of great interest due to a combination of unique features, such as superelasticity, shape memory effect, high ductility, work output, corrosion resistance, and biocompatibility that could be employed in many applications in automotive, aerospace, and biomedical industries. Due to the difficulties with traditional machining and forming of NiTi components, the ability to fabricate complex parts, tailor …

Study On The Viability Of Preparing Plaster Molds For Rapid Prototyping Of Complex Ceramic Parts Using The Lost Pla Method, Shelton F. Fowler Iv

Honors College Theses

In the field of metal casting, cast parts often require an internal cavity to be made to meet design requirements. Frequently, these interior surfaces are not manufacturable through standard machining processes, and even when possible, they would most likely involve expensive and time-consuming operations. In order to avoid these machining costs, expendable ceramic or sand cores are manufactured and placed into the mold to allow the direct casting of complex internal geometries. This research seeks to use relatively inexpensive plastic 3D printing technology and the lost PLA casting process for the production of low-cost and rapidly producible ceramic cores. A …

Additive Manufacturing And How 3d Printing Is Fighting Covid-19, Raghavan Srinivasan, Ahsan Mian, Joy Gockel, Laura M. Luehrmann

Mechanical and Materials Engineering Faculty Publications

This is the fourth installment in the Shelter in Place (SiP) Lecture series. This installment covers the creative ways that 3D printing has supported efforts to combat the pandemic. It covers the basics of what 3D printing is, some of the various creative projects that have used 3D printing to combat the pandemic, among other topics and questions by the pandemic.

Thermal Modeling Of Additive Manufacturing Using Graph Theory: Validation With Directed Energy Deposition, Jordan Severson

Department of Mechanical and Materials Engineering: Dissertations, Theses, and Student Research

Metal additive manufacturing (AM/3D printing) offers unparalleled advantages over conventional manufacturing, including greater design freedom and a lower lead time. However, the use of AM parts in safety-critical industries, such as aerospace and biomedical, is limited by the tendency of the process to create flaws that can lead to sudden failure during use. The root cause of flaw formation in metal AM parts, such as porosity and deformation, is linked to the temperature inside the part during the process, called the thermal history. The thermal history is a function of the process parameters and part design.

Consequently, the first step …

Investigation Of Selective Laser Melting Fabricated Internal Cooling Channels, Colin Jack

Masters Theses

Channels where coolant is run to cool a system are common in injection mold tooling. Conventionally, these channels are machined into the mold. This has limited the design of mold cooling systems to the constraints of traditional machining processes, where straight circular channels machined from cast material are typical. The transfer of heat away from the part cavity into these cooling channels has a large effect on the cooling time of the injection mold cycle. In this investigation, laser powder bed fusion processes were used to create non-circular cooling channels. To compare cooling performance, elliptical and circular channels of equal …

Characterization Of Directed Energy Deposition Additively Manufactured Grcop-42 Alloy, Scott Landes

Electronic Theses and Dissertations

GRCop is an alloy family constructed of copper, chromium, and niobium and was developed by NASA for high heat flux applications. The first of its kind, GRCop-84, was specifically designed for the environments seen by channel cooled main combustion chamber liners. To further increase thermal conductivity while maintaining material strength characteristics, the percentage of alloying elements were cut in half and GRCop- 42 was developed. In recent years, NASA has successfully additively manufactured GRCop with comparable material characteristics to wrought GRCop using a Laser Powder Bed Fusion (L-PBF) process. Benefits of this process include fabrication of intricate cooling channels as …

Performance Evaluation Of Alsi10mg Fabricated By A Selective Laser Melting Process, David Michael Murphy

Masters Theses

“Selective laser melting is becoming a widely used additive manufacturing technique that melts metal powder in a layer by layer process in order to build a desired part or geometry. Like many additive processes, selective laser melting allows for fabrication of parts with complex geometries. In order to fabricate a fully dense part there are a number of variables to take into account including: powder characteristics, laser parameters, and environmental parameters. Each of these variables can affect the microstructure and thus the mechanical performance of an additively manufactured part. In this work, the aluminum alloy AlSi10Mg was investigated. AlSi10Mg is …

Development Of Lightweight Materials By Meso- And Microstructure Control, Myranda Shea Spratt

Doctoral Dissertations

”In this work, two lightweight structures – lattice structures and metal matrix syntactic foams (MMSF) – were studied. Honeycomb lattices were manufactured by powder bed selective laser melting (SLM) from 304L stainless steel. The wall thicknesses of these structures ranged from 0.2 to 0.5 mm. Surface roughness was the primary cause of dimensional mismatch between the expected and as-built structures with an average wall thickness increase of 0.12 mm. The strength of the honeycombs increased with increasing wall thickness. A feature of the SLM microstructure, the melt pool boundary, was also studied as a part of this work. 3D models …

Grain Size Effects In Selective Laser Melted Fe-Co-2v, Wesley Everhart, Joseph William Newkirk

Materials Science and Engineering Faculty Research & Creative Works

The material science of additive manufacturing (AM) has become a significant topic due to the unique way in which the material and geometry are created simultaneously. Major areas of research within inorganic materials include traditional structural materials, shape memory alloys, amorphous materials, and some new work in intermetallics. The unique thermal profiles created during selective laser melting (SLM) may provide new opportunities for processing intermetallics to improve mechanical and magnetic performance. A parameter set for the production of Fe-Co-2V material with additive manufacturing is developed and efforts are made to compare the traditional wrought alloy to the AM version of …

A Displacement Controlled Fatigue Test Method For Additively Manufactured Materials, Mohammad Masud Parvez, Yitao Chen, Sreekar Karnati, Connor Coward, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

A novel adaptive displacement-controlled test setup was developed for fatigue testing on mini specimens. In property characterization of additive manufacturing materials, mini specimens are preferred due to the specimen preparation, and manufacturing cost but mini specimens demonstrate higher fatigue strength than standard specimens due to the lower probability of material defects resulting in fatigue. In this study, a dual gauge section Krouse type mini specimen was designed to conduct fatigue tests on additively manufactured materials. The large surface area of the specimen with a constant stress distribution and increased control volume as the gauge section may capture all different types …

Process Parameter Development Of Additively Manufactured Af9628 Weapons Steel, Erin M. Hager

Theses and Dissertations

The manufacture of components in Additive Manufacturing processes is limited by the range of materials available. Qualification of materials for Additive Manufacturing is time intensive, and is often specific to a single type of machine. In this study, an approach to selecting power, speed, and hatch spacing values for a newly powderized material, AF9628 weapons steel, is described that results in highly dense (>99.9%) parts on an MLab 200R Cusing. Initial power and speed values used in a weld track study were selected based on a survey of parameters used on similar materials, with a focus on the energy …

Direct Laser Metal Deposition Of Nickel Based Superalloys, Abhishek Ramakrishnan-Sudha

Wayne State University Dissertations

Nickel-based superalloys are substantially used in the manufacturing of boilers for ultra-supercritical power plants and gas turbine hot-section as this grade of alloys provide higher yield strength with the rise in operating temperature and pressure owing to the presence of γʹ second phase precipitates. Conventionally, casting techniques such as centrifugal casting, investment casting, vacuum molding and several other casting based methods are used to fabricate the hot-section components. Nevertheless, a need for designing advanced materials with complex designs such as geometry, microstructure control, compositional changes, microstructure and property varying with the location as in functionally graded materials is not viable …

Direct Write 3d Printing Of Functional Ceramics, Jorge Angel Diaz

Open Access Theses & Dissertations

Humidity sensors are used in many industries and are important for ensuring quality and safety. Ceramic sensors are preferred because of their quick response time, ability to withstand high temperatures and excellent Chemical and mechanical stability. The manufacturing world has been moving toward additive manufacturing which is a form of synthesizing 3D tangible layer by layer in witch minimal waste is produced. Additive manufacturing also is known as 3D printing has opened new possibilities to design engineers by giving them design freedom and access to the layers of a part to allow embedded sensors. There is a category of ceramics …

Investigating Using Titanium Zirconium Molybdenum For Additively Manufacturing Aerospace Components, Justin Hunter Vanhoose

Open Access Theses & Dissertations

Mankind throughout history has possessed an innate characteristic to explore, migrating to new frontiers.The requirement for this travel is most broadly associated with the need to pursue more resources. Rockets have been used as a means of weapons since the Sung Dynasty in the thirteenth empire and have now been integrated for travel/transport. The sophistication of rocketry and propulsion has reached a level to where it is plausible that mankind will be a multi-planetary species. The space industry has grown significantly with the advancement of the sophistication of these rocket technologies. However, a specific challenge to overcome in the space …

The Influence Of Build Parameters On The Compressive Properties Of Selective Laser Melted 304l Stainless Steel, Okanmisope Fashanu, Mario F. Buchely, R. Hussein, S. Anandan, Myranda Spratt, Joseph William Newkirk, K. Chandrashekhara, H. Misak, M. A. Walker

Materials Science and Engineering Faculty Research & Creative Works

Process parameters used during Selective Laser Melting (SLM) process have significant effects on the mechanical properties of the manufactured parts. In this study, the influence of two build parameters (build orientation and hatch angle) on the compressive properties of 304L stainless steel was evaluated. SLM 304L samples were manufactured using three hatch angles, 0°, 67°,105° and two orientations, z-direction and x-direction, and tested using a compression frame according to ASTM E9-09. Bulk density was measured according to ASTM C373-17 before compression. Properties evaluated were the bulk density, yield strength, strength at 15% plastic-strain and strength at 30% plastic-strain. Results showed …

Design Of Lattice Structures With Graded Density Fabricated By Additive Manufacturing, Wenjin Tao, Yong Liu, Austin T. Sutton, Krishna C. R. Kolan, Ming-Chuan Leu

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Lattice structures fabricated by Additive Manufacturing (AM) processes are promising for many applications, such as lightweight structures and energy absorbers. However, predicting and controlling of their mechanical behaviors is challenging due to the complexity of modeling and the uncertainties exist in the manufacturing process. In this paper, we explore the possibilities enabled by controlling the local densities. A set of lattice structures with different density gradients are designed using an implicit isosurface equation, and they are manufactured by Selective Laser Melting (SLM) process with 304L stainless steel. Finite element analysis and compression test are used to evaluate their mechanical properties. …

Material Properties Of Laser Powder Bed Fusion Processed 316l Stainless Steel, Steven Keckler

Graduate Theses & Non-Theses

Laser powder bed fusion additive manufactured 316L stainless steel specimens were evaluated to establish a baseline for future research in determining an optimized energy density and build orientation. Test specimens were printed at various energy densities. At each energy density, tensile and fatigue specimens were printed at 0o (longitudinal), 45o, and 90o (transverse) orientation to the build plate. Tensile and high cycle fatigue tests were performed then representative fracture surfaces were analyzed. The apparent melt track and dendrite size were evaluated using grain analysis software. Static loading of the tensile specimens showed a marginal difference in UTS for specimens with …

An Evaluation Of Ultrasonic Shot Peening And Abrasive Flow Machining As Surface Finishing Processes For Selective Laser Melted 316l, Rhys Gilmore

Master's Theses

Additive Manufacturing, and specifically powder bed fusion processes, have advanced rapidly in recent years. Selective Laser Melting in particular has been adopted in a variety of industries from biomedical to aerospace because of its capability to produce complex components with numerous alloys, including stainless steels, nickel superalloys, and titanium alloys. Post-processing is required to treat or solve metallurgical issues such as porosity, residual stresses, and surface roughness. Because of the geometric complexity of SLM produced parts, the reduction of surface roughness with conventional processing has proven especially challenging. In this Thesis, two processes, abrasive flow machining and ultrasonic shot peening, …

Mechanical Characterization Of Selectively Laser Melted 316l Stainless Steel Body Centered Cubic Unit Cells And Lattice Of Varying Node Radii And Strut Angle, Christopher James Hornbeak

Master's Theses

An experimental study of several variants of radius and strut angle of the body centered cubic unit cell was performed to determine the mechanical properties and failure mechanisms of the mesostructure. Quasi static compression tests were performed on an Instron® universal testing machine with a 50kN load cell at 0.2mm/min. The test samples were built using a SLM Solutions 125 selective laser melting machine with 316L stainless steel. Test specimens were based on 5mm cubic unit cells, with a strut diameter 10% of the unit cell size, with skins on top and bottom to provide a cantilever boundary constraint. Specimens …

The Effects Of Varying Composition And Build Direction On Direct Metal Deposition Fabricated Inconel 718, Abigail P. Nilan, Jessica M. Fordham

Materials Engineering

Inconel 718 (IN718) is a popular wrought superalloy, and is currently being investigated for additive manufacturing (AM) applications in the aerospace industry. However, overaging and the presence of microcracks have caused a significant reduction in properties. The purpose of this study is to meet or exceed the mechanical properties of wrought IN718 by varying the composition and build direction of the AM alloy. Alternative compositions were selected with Oerlilon Metco’s Rapid Alloy Development (RAD) software, and differ in niobium content, which increases the fraction of the primary strengthening phase (γʺ). Direct metal deposition (DMD) was used to fabricate the samples, …

Characterization Of Process Induced Defects In Laser Powder Bed Fusion Processed Alsi10mg Alloy, Edward Stugelmayer

Graduate Theses & Non-Theses

Additive manufacturing using laser powder bed fusion (AM-LPBF) methods have recently experienced rapid growth and development, having the potential to replace manufacturing by plastic deformation, precision machining, or casting. AM offers advantages such as the freedom to design highly complex geometries, time and cost savings through material usage efficiency and shortened production cycles, and the potential for improved mechanical properties. Process induced defects, however, result in degradation and scattering of mechanical properties and hinder the widespread adoption of AM-LPBF in industry. This investigation focuses on the effects of varying energy density and build orientation on the evolution of process induced …

Evaluation Of Metallurgical And Mechanical Properties Of Alsi10mg Produced By Selective Laser Melting, Luke J. Suttey

Graduate Theses & Non-Theses

Selective laser melting (SLM) additive manufacturing (AM) of metal powders has long been a focus in the study of AM due to the possibility of weight reduction, complex shape formation, and production cost savings. Although applicable to a variety of metals SLM AM of the AlSi10Mg alloy was studied in an attempt to characterize the effect of processing parameter and build angle variation on the final microstructural, fractographic, and mechanical properties of parts produced without any thermal post-processing techniques. Research was conducted on five build angles (0°, 30°, 45°, 60°, and 90°), and three Global Energy Densities (GED) (37.15, 45.39, …

Equibiaxial Flexural Strength Testing Of Advance Ceramics, Ryan T. Jordan

Honors Undergraduate Theses

Ceramics are very important materials with many unique properties used in numerous industrial applications. Ceramics could be very hard and very strong in comparison to metals; however, they are very brittle, thus they are prone to instantaneous and catastrophic failure. Therefore, their reliability is compromised and it is very important to have advanced techniques that allow evaluating their mechanical behavior in many unusual stress states. One of such testing methods is biaxial strength method, that allows to measure properties not only unidirectional, but also in a biaxial way. The research work for this thesis will be built on design and …

Development Of Material For 3d Printed Habitats With Extraplanetary Applications, Taylor Wait

Electronic Theses and Dissertations

3D printing, also called Additive Manufacturing, has increasingly become a focus for research because of the potential to replace complicated assemblies or complex parts with a single printed item. The space industry is very interesting in studying 3d printing with parts being tested and used on rockets, a 3D printer being installed at the International Space Station and is being developed for use in manned exploration of extraplanetary bodies to build habitats. To encourage teams from around the world to develop technologies and materials for autonomous habitat construction using minimal Earth exports, NASA created the 3D Printed Habitat Challenge. NASA …

Designed Extrudate For Ceramic Additive Manufacturing, Devin Mcmillen

Masters Theses

"The objective of this thesis work was to design ceramic paste systems that assist in achieving a high theoretical density ( > 95%) after deposition by a novel additive manufacturing process, i.e. Ceramic On-Demand Extrusion (CODE). The work is encompassed in five main sections: Sections 1 and 2 provide an introduction and literature review of relevant topics for the following sections of experimentation. Section 3 provides an analysis of a reaction chemistry to identify three discrete materials that could be combined via CODE and result in zirconium diboride (ZrB₂) post-sintering. Section 4 describes the development of a high solids …

A New Approach To Multiplanar, Real-Time Simulation Of Physiological Knee Loads And Synthetic Knee Components Augmented By Local Composition Control In Fused Filament Fabrication, Joshua Taylor Green

Open Access Theses & Dissertations

Despite numerous advances in biomedical engineering, few developments in surgical simulation have been made outside of computational models. Cadavers remain the primary media on which surgical research and simulation is conducted. Most attempts to quantify the effects of orthopedic surgical methods fail to achieve statistical significance due to limited quantities of cadaver specimen, large variations among the cadaver population, and a lack of repeatability among measurement techniques. The general purpose of the research covered in this dissertation is to develop repeatable simulation of physiological loads and develop techniques to fabricate a synthetic-based replacement of cadaver specimens. Future work applying this …

Investigation Of 2195 And 2219 Post Weld Heat Treatments For Additive Friction Stir Lap Welds, Matthew Champagne

LSU New Orleans Theses and Dissertations

To evaluate potential uses for friction stir welding in additive manufacturing, two separate parts were fabricated, one of 2195-T84 and the other 2219-T87, utilizing fixed pin techniques and additive lap welds. The parts were cut into samples, artificially aged and subjected to Rockwell hardness (HRB), Vickers hardness, micrographic photography, and metallographic imaging on both pre- and post- heat treatment. Additionally, tensile testing was performed on the heat-treated samples. A comparisons of test results showed a minimal increase in the yield strength of the 2195-T84 samples compared to as-welded tensile results obtained from a previous project. The ultimate tensile strength was …