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2011

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Articles 91 - 120 of 373

Full-Text Articles in Materials Science and Engineering

Synthesis And Development Of Boron Nanotubes And Metal/Ceramic-Carbon Nanotube Composites, Jinwen Liu Aug 2011

Synthesis And Development Of Boron Nanotubes And Metal/Ceramic-Carbon Nanotube Composites, Jinwen Liu

Dissertations

The first part of this thesis will be focused on developing a facile and scalable solid — solid chemical vapor deposition (CVD) process using a solid boron precursor to synthesize crystalline boron nanotubes (BNTs) mixed with small amounts of boron nanofibers (BNFs). The synthesis involves the use of solid boron precursors - magnesium boride and magnesium borohydride, magnesium and nickel boride as co-catalysts, and porous MCM-41 zeolite as the growth template. Experimental parameters, such as temperature, grinding of constituents and starting precursor-catalyst-template compositions, were studied and optimized. Detailed characterization have been carried out using field-emission scanning electron microscopy (FE-SEM), transmission …

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Study On The Fluorescent Carbon Nanodots With Electrochemical Methods, Bao-Ping Qi, Yan-Min Long, Lei Bao, Cui Liu, Zhi-Ling Zhang, Dai-Wen Pang Aug 2011

Study On The Fluorescent Carbon Nanodots With Electrochemical Methods, Bao-Ping Qi, Yan-Min Long, Lei Bao, Cui Liu, Zhi-Ling Zhang, Dai-Wen Pang

Journal of Electrochemistry

Carbon nanodots are a new class of fluorescent nanoparticles with a carbon-based core, which possess wavelength-tunable luminescence, high photostability, resistance to photobleaching, water-solubility, and ease of bioconjugation. Owing to their attractive merits, carbon nanodots like other carbon nanomaterials such as fullerene, carbon nanotubes and graphene, have attracted much attention. In addition, carbon nanodots can be inexpensively produced by electrochemical methods with simple post-processing under mild conditions. Electrochemical approaches have unique advantages in the analysis of surface structures and luminescence mechanism of materials. In this review, recent advances in electrochemical methods used for the synthesis and luminescence mechanism of fluorescent carbon …

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Brief Introduction To Metal Corrosion And Protection, Hou-Yi Ma, Cong-Ying Cui, Ting Chen Aug 2011

Brief Introduction To Metal Corrosion And Protection, Hou-Yi Ma, Cong-Ying Cui, Ting Chen

Journal of Electrochemistry

This paper explains why corrosion processes are usually electrochemical in nature, describes the significance of electrochemical kinetic parameters of corrosion process, and briefly introduces the principles of corrosion protection, the most common corrosion protection methods and some special application of corrosion processes.

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Study On Residual Powders Of Lithium-Ion Batteries With Different Voltages After Explosion, He Li, Zhi-Kui Chen, Ji-Na Cao, Guang-Chuan Liang Aug 2011

Study On Residual Powders Of Lithium-Ion Batteries With Different Voltages After Explosion, He Li, Zhi-Kui Chen, Ji-Na Cao, Guang-Chuan Liang

Journal of Electrochemistry

The residual powders of lithium-ion batteries at different voltages after explosion were obtained by using the battery impact testing machine. And these powders have been investigated by weighing, water solution and X-ray diffraction (XRD). The results showed that the integrity status of copper current collector and weight of residual powders decreased gradually with increasing of battery voltage, rising of burning temperature and releasing of burning duration time. The residual powders could be separated to insoluble powders and soluble powders by the water solution. The proportion of the insoluble powders is more (about 90%) including C, Co and CoO, while the …

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Electrochemical Performance Of Tin Dioxide/Carbon Xerogel Composites As Anode Materials For Lithium-Ion Batteries, Xiao-Jing Liu, Lin-Lin Qin, Yi-Ning Shi, Ming-Sen Zheng, Quan-Feng Dong Aug 2011

Electrochemical Performance Of Tin Dioxide/Carbon Xerogel Composites As Anode Materials For Lithium-Ion Batteries, Xiao-Jing Liu, Lin-Lin Qin, Yi-Ning Shi, Ming-Sen Zheng, Quan-Feng Dong

Journal of Electrochemistry

The tin dioxide/carbon xerogel composites were synthesized by using vacuum infiltration method. Structural characterization and morphology of the composites were investigated by using XRD, TEM and SEM techniques. BET test was performed to determine the pore size distributions of carbon xerogels and the composites. The results showed that the nano-sized SnO2 particles (5~10 nm) were encapsulated in the pores of carbon xerogels. During the electrochemical tests the SnO2 in the composites exhibited capacity retention of 61.9% after 100 cycles of charge-discharge tests at 100 mA/g.

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Study On The Electrochemical Behaviors Of Gc Electrode Modified With Carbon Nanotube-Polyelectrolytes And Its Application For Rutin Detection, Liang Hua, Xia-Qin Wu, Rong Wang Aug 2011

Study On The Electrochemical Behaviors Of Gc Electrode Modified With Carbon Nanotube-Polyelectrolytes And Its Application For Rutin Detection, Liang Hua, Xia-Qin Wu, Rong Wang

Journal of Electrochemistry

The electrochemical behaviors of rutin and ascorbic acid at single-wall carbon nanotube and polyelectrolytes (dimethyl-diallylammonium chloride, PDDA) film modified glassy carbon electrode was investigated. The cyclic voltammetric results showed that electron transfer of rutin at PDDA/SWCNTs/GC modified electrode is an adsorption-controlled process. The separation of oxidation peak potentials of rutin and ascorbic acid was more than 200 mV. The rutin concentration in the presence of AA were detected by differential pulse voltammetry (DPV). The experimental results indicated that the PDDA/SWCNTs/GC modified electrode can be used for the detection of rutin in the presence of high concentration of AA. The DPV …

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Effects Of Graphene On Electrochemical Behaviors Of Ni(Oh)2 As Supercapacitor Material, Zhen-Zhen Zhao, Wen-Bin Ni, Neng-Yue Gao, Hong-Bo Wang, Jian-Wei Zhao Aug 2011

Effects Of Graphene On Electrochemical Behaviors Of Ni(Oh)2 As Supercapacitor Material, Zhen-Zhen Zhao, Wen-Bin Ni, Neng-Yue Gao, Hong-Bo Wang, Jian-Wei Zhao

Journal of Electrochemistry

The enhanced electrochemical properties of Ni(OH)2 by the oxidation defected graphene were studied by both experimental method and theoretical calculation. The composite material of nano-Ni(OH)2/graphene was prepared by potentiostatic deposition on the graphene substrate. Observed by TEM, the Ni(OH)2 nanoparticles were well dispersed on the graphene substrate with the diameter of 5.0±0.5 nm. The capacitance of the system measured by the electrochemical test was 1928 F·g-1. As indicated by the theoretical calculations, the composite material becomes conductive since Ni(OH)2 is combined with surface functional groups of the graphene through the strong chemical interaction. …

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Surface Diffusion Of Adsorptive Species On Gold Nanoelectrodes, Bao-Fa Su, Wei Wang, Dong-Ping Zhan, Bin Ren, Zhong-Qun Tian Aug 2011

Surface Diffusion Of Adsorptive Species On Gold Nanoelectrodes, Bao-Fa Su, Wei Wang, Dong-Ping Zhan, Bin Ren, Zhong-Qun Tian

Journal of Electrochemistry

Gold nanoelectrodes were prepared successfully by a programmed laser puller. The Faraday adsorptions of oxygen and iodine, and the underpotential deposition of lead on the gold nanoelectrodes were investigated. The results showed that the active areas of nanoelectrodes were dramatically higher than their appearant geometry areas, which is caused by the surface diffusion of adsorptive species from the nanoscale gold/electrolyte interface to the adjacent gold surface.

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Synthesis Of Limnpo4/C Used As Cathode Material For Lithium Ion Batteries, Xin Yang, Xue-Wu Liu, Gui-Chang Liu, Zhi-Cong Shi, Xin Li, Guo-Hua Chen Aug 2011

Synthesis Of Limnpo4/C Used As Cathode Material For Lithium Ion Batteries, Xin Yang, Xue-Wu Liu, Gui-Chang Liu, Zhi-Cong Shi, Xin Li, Guo-Hua Chen

Journal of Electrochemistry

The LiMnPO4/C composites were prepared using a solid-state reaction with addition of the resorcinol formaldehyde resin as the carbon source. The effects of reaction temperature and time on the crystal structure, morphology and electrochemical properties of the LiMnPO4/C composites were investigated. The results show that the best performance was achieved with the LiMnPO4/C composites synthesized at 600 oC for 12 h which had the particle sizes about 100~200 nm. The initial discharge capacities were 121.6 mAh·g-1 at 0.02C, 110 mAh·g-1 at 0.1C and more than 60 mAh·g-1 at 1C. An …

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Photogenerated Cathodic Protection Of Stainless Steel, Cheng-Gang Lin, Ze-Quan Lin, Jing Li, Chang-Jian Lin Aug 2011

Photogenerated Cathodic Protection Of Stainless Steel, Cheng-Gang Lin, Ze-Quan Lin, Jing Li, Chang-Jian Lin

Journal of Electrochemistry

A highly ordered Co-doped TiO2 nanotube layers were fabricated by potentiostatic anodization of pure titanium in fluorinated electrolyte solutions followed by ion-exchange method. The structure and composition of the as-prepared Co-doped TiO2 nanotube layers were characterized by SEM, XRD, UV-Vis, and XPS. The effects of dopant content on the morphologies, structural and photochemical properties of the TiO2 nanotube arrays were investigated. The performances of photogenerated cathodic protection and the photoelectrochemical response for the Co-doped TiO2 nanotube arrays under illumination and dark conditions were evaluated through the electrochemical measurements. The Co-doped TiO2 nanotubes showed a stronger …

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Synthesis And Electrochemical Behaviors Of Li2Coxmn1-XSio4 As A Cathode Material For Lithium-Ion Batteries, Lin Wang, Dong-Ping Lv, Yong Yang Aug 2011

Synthesis And Electrochemical Behaviors Of Li2Coxmn1-XSio4 As A Cathode Material For Lithium-Ion Batteries, Lin Wang, Dong-Ping Lv, Yong Yang

Journal of Electrochemistry

We have successfully synthesized Li2CoxMn1-xSiO4/C (x=0, 0.1, 0.3, 0.5, 1)/C composites using hydrothermal assisted sol-gel process and ball-milling method. The results of X-ray diffraction show that the solid solutions of Li2CoxMn1-xSiO4 can be achieved when x≤0.3. The initial capacities increase from 70 mAh·g-1 of Li2MnSiO4/C to 105 mAh·g-1 of Li2Co0.3Mn0.7SiO4/C. Cyclic Voltammetry (CV) curves show that the replacement of Mn with Co can reduce the electrochemical polarization, making the insertion-extraction reaction …

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Corrosion Characteristics Of Galvanized Flat Steel For Power Grounding In Nacl Solution Medium, Yong Li, Gao-Lin Wu, Bang-Fei Deng, Ping Yang, Xue-Ming Li, Qing-Bin Zong Aug 2011

Corrosion Characteristics Of Galvanized Flat Steel For Power Grounding In Nacl Solution Medium, Yong Li, Gao-Lin Wu, Bang-Fei Deng, Ping Yang, Xue-Ming Li, Qing-Bin Zong

Journal of Electrochemistry

The corrosion behavior of power grounding galvanized flat steel was studied by polarization measurement, electrochemical impedance spectroscopy and neutral salt spray test in 5% NaCl solutions. The surface morphologies of galvanized coating and structural properties of corrosion products were observed with scanning electron microscope and X-ray diffraction spectrometer, respectively. Results showed that under the temperatures of 20~60℃, the corrosion currents of galvanized flat steel increased with the temperature rising. The corrosion rate at 60℃ was 0.8408 mA·cm-2, which is 2.9 times larger than that at 20℃. The corrosion rate dropped after reaching the maximal value of 1.95 mg·cm …

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Simultaneous Determination Of Dopamine(Da)And Epinephrine (Ep) At Ca/Gc Electrode, Wang Ren, Ying Zhang, Min-Jiao Li Aug 2011

Simultaneous Determination Of Dopamine(Da)And Epinephrine (Ep) At Ca/Gc Electrode, Wang Ren, Ying Zhang, Min-Jiao Li

Journal of Electrochemistry

The citric acid modified glassy carbon electrode (CA/GC) was prepared by potentiostatic technique and was used for detections of dopamine (DA), epinephrine (EP), and their mixtures by differential pulse voltammetry (DPV). The modified electrode shows the enhanced sensitivity and excellent electrochemical discrimination to DA and EP. The cathodic potential difference between DA and EP was about 380 mV, while no cathodic reduction of ascorbic acid (AA) was observed because the oxidation of AA is an irreversible reaction at the sensor. As a result, DA and EP could be determined simultaneously with the interferences of high concentrations of AA being eliminated. …

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Energy - Activities, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Energy - Activities, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

The document contains activities for students in higher education. These activities are focused on energy issues related to sustainability. It is designed for the general engineering or science audience. Its design is based on the framework of the Fink Taxonomy of Significant Learning. Each activity includes a profile that indicates whether the activity involves direct or indirect information sources, whether the experience is doing or observing and whether it involves individual or group reflection. The profile also includes notes for faculty, an estimate of the time investment, a graphic of the developmental aims with respect to the six areas of …

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Fink Taxonomy Of Significant Learning, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Fink Taxonomy Of Significant Learning, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

This document is graphical summary of the framework within the Fink Taxonomy of Significant Learning and the definition of each of the six areas of significant learning.

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Sustainable Development, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Sustainable Development, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

This document is a set of learning materials to support the teaching of Sustainable Development issues particularly related to sustainability in engineering. It is designed for the general engineering or science audience. Its design is based on the framework of the Fink Taxonomy of Significant Learning. The document is a fully-editable set of slides in open source format (pptx) that includes references to targeted learning objectives on each slide and annotations in the notes section of each slide.

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Water - Activities, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Water - Activities, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

The document contains activities for students in higher education. These activities are focused on water issues related to sustainability. It is designed for the general engineering or science audience. Its design is based on the framework of the Fink Taxonomy of Significant Learning. Each activity includes a profile that indicates whether the activity involves direct or indirect information sources, whether the experience is doing or observing and whether it involves individual or group reflection. The profile also includes notes for faculty, an estimate of the time investment, a graphic of the developmental aims with respect to the six areas of …

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Population, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Population, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

This document is a set of learning materials to support the teaching of population issues particularly related to sustainability in engineering. It is designed for the general engineering or science audience. Its design is based on the framework of the Fink Taxonomy of Significant Learning. The document is a fully-editable set of slides in open source format (pptx) that includes references to targeted learning objectives on each slide and annotations in the notes section of each slide.

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Sustainable Development - Learning Objectives, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Sustainable Development - Learning Objectives, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

This document is a list of learning objectives based on the framework of Fink’s taxonomy of significant learning: foundational knowledge, application, integration, human dimension, caring, and learning how to learn. It represents the aspirations for learning that the sustainable development is based on.

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Systems Thinking - Assessment, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Systems Thinking - Assessment, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

The document contains an assessment activity for an individual or team project in higher education. These assessments are focused on systems thinking issues related to sustainability. It is designed for the general engineering or science audience. Its design is based on the framework of the Fink Taxonomy of Significant Learning. Each assessment consists of a scenario in which the student is an actor who must address some design dilemma. The assessment also includes an estimate of the time investment, a detailed list of learning objectives with respect to the six areas of development within the Fink Taxonomy, and a suggested …

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Materials - Learning Objectives, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Materials - Learning Objectives, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

This document is a list of learning objectives based on the framework of Fink’s taxonomy of significant learning: foundational knowledge, application, integration, human dimension, caring, and learning how to learn. It represents the aspirations for learning that the materials is based on.

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Sustainable Development - Activities, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Sustainable Development - Activities, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

The document contains activities for students in higher education. These activities are focused on sustainable development issues related to sustainability. It is designed for the general engineering or science audience. Its design is based on the framework of the Fink Taxonomy of Significant Learning. Each activity includes a profile that indicates whether the activity involves direct or indirect information sources, whether the experience is doing or observing and whether it involves individual or group reflection. The profile also includes notes for faculty, an estimate of the time investment, a graphic of the developmental aims with respect to the six areas …

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Systems Thinking - Learning Objectives, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Systems Thinking - Learning Objectives, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

This document is a list of learning objectives based on the framework of Fink’s taxonomy of significant learning: foundational knowledge, application, integration, human dimension, caring, and learning how to learn. It represents the aspirations for learning that the systems thinking is based on.

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Systems Thinking - Activities, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Systems Thinking - Activities, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

The document contains activities for students in higher education. These activities are focused on systems thinking issues related to sustainability. It is designed for the general engineering or science audience. Its design is based on the framework of the Fink Taxonomy of Significant Learning. Each activity includes a profile that indicates whether the activity involves direct or indirect information sources, whether the experience is doing or observing and whether it involves individual or group reflection. The profile also includes notes for faculty, an estimate of the time investment, a graphic of the developmental aims with respect to the six areas …

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Energy - Learning Objectives, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Energy - Learning Objectives, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

This document is a list of learning objectives based on the framework of Fink’s taxonomy of significant learning: foundational knowledge, application, integration, human dimension, caring, and learning how to learn. It represents the aspirations for learning that the energy is based on.

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Population - Learning Objectives, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Population - Learning Objectives, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

This document is a list of learning objectives based on the framework of Fink’s taxonomy of significant learning: foundational knowledge, application, integration, human dimension, caring, and learning how to learn. It represents the aspirations for learning that the population is based on.

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Materials, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Materials, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

This document is a set of learning materials to support the teaching of materials issues particularly related to sustainability in engineering. It is designed for the general engineering or science audience. Its design is based on the framework of the Fink Taxonomy of Significant Learning. The document is a fully-editable set of slides in open source format (pptx) that includes references to targeted learning objectives on each slide and annotations in the notes section of each slide.

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Water, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Water, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

This document is a set of learning materials to support the teaching of water issues particularly related to sustainability in engineering. It is designed for the general engineering or science audience. Its design is based on the framework of the Fink Taxonomy of Significant Learning. The document is a fully-editable set of slides in open source format (pptx) that includes references to targeted learning objectives on each slide and annotations in the notes section of each slide.

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Materials - Activities, Jane Qiong Zhang, Linda Vanasupa Aug 2011

Materials - Activities, Jane Qiong Zhang, Linda Vanasupa

Materials Engineering

The document contains activities for students in higher education. These activities are focused on materials issues related to sustainability. It is designed for the general engineering or science audience. Its design is based on the framework of the Fink Taxonomy of Significant Learning. Each activity includes a profile that indicates whether the activity involves direct or indirect information sources, whether the experience is doing or observing and whether it involves individual or group reflection. The profile also includes notes for faculty, an estimate of the time investment, a graphic of the developmental aims with respect to the six areas of …

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Study Of Novel Materials For Organic Photovoltaics And Organic/Inorganic Hybrid Solar Cells, Viney Saini Aug 2011

Study Of Novel Materials For Organic Photovoltaics And Organic/Inorganic Hybrid Solar Cells, Viney Saini

Theses and Dissertations

As the human race evolves and continues to progress in the future, we will face some obstacles during the advancement. Challenges like water, food, and poverty crisis, pollution, population explosion, and diseases are impediments in the development of mankind. Above all, with the development arises the need to fulfill the energy requirements. There are number of technologies available to answer the present energy needs, e.g. coal, nuclear, oil/natural gas, hydropower, etc. All these technologies have their advantages and disadvantages, with disadvantages being greenhouse gas emissions and other environmental impacts. One technology which has lagged behind due to high cost is …

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