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Articles 61 - 90 of 2617

Full-Text Articles in Materials Science and Engineering

Reduced Order Approach For Peening Stress Field Variability, Langdon Feltner, Paul Mort Sep 2025

Reduced Order Approach For Peening Stress Field Variability, Langdon Feltner, Paul Mort

15th International Conference on Shot Peening

A common goal in shot peening research is to connect operational parameters to resultant residual stress fields, providing a means to control and optimize the effectiveness of surface treatment. In practice, experimental measurements of residual stresses are often averaged values over regions that are large in comparison to an impact dimple. In fact, the stochastic nature of impact locations leads to residual stress fields that are distributed. Finite element peening simulations confirm this observation. The goal of this report is to connect operational parameters to localized fluctuations in residual stress through probabilistic reasoning (Figure 1). In particular, the development of …


The Effect Of Surface Treatment On The Fatigue Strength Of Sus316l Additive Manufactured Products, Hitoshi Nishijima, Yuji Kobayashi, Toshiya Tsuji, Kiyotaka Masaki Sep 2025

The Effect Of Surface Treatment On The Fatigue Strength Of Sus316l Additive Manufactured Products, Hitoshi Nishijima, Yuji Kobayashi, Toshiya Tsuji, Kiyotaka Masaki

15th International Conference on Shot Peening

Rotating bending fatigue tests were conducted to investigate the effect of shot peening and barrel finishing on fatigue properties of SUS316L made by laser PBF which was one of additive manufacturing processes. Surface roughness, residual stress, and fatigue strength were investigated for each specimen. As a result, the fatigue strength of the barrel finished specimens was almost same or better than that of the shot peened specimens. Barrel finished specimens increased 4.1 times higher fatigue strength than as-built specimens. The surface roughness of the specimens after barrel finishing was reduced by up to 96% compared to the as-built specimens. On …


Dynamic Flowsheet Modeling Of Shot Peening Processes, Langdon Feltner, Paul Mort Sep 2025

Dynamic Flowsheet Modeling Of Shot Peening Processes, Langdon Feltner, Paul Mort

15th International Conference on Shot Peening

Process flowsheet modeling is used to map and predict performance by integrating sub-models within a system. This paper presents a dynamic flowsheet for shot peening used to track the effects of media characteristics, removal of worn media, and replenishment thereof. Input parameters include media characteristics, media feed rate, velocity (i.e., air pressure), effective impact area (i.e., nozzle setup), and recharge replenishment. The media working mix is described dynamically using tri-modal size and shape characteristics: as-manufactured, conditioned, and worn modes, each having impact-dependent rate coefficients for transition to the next mode, i.e., as-manufactured > conditioned > worn > debris. The flowsheet includes the effect …


Evaluating The Effectiveness Of Localized Masking To Prevent Changes In Residual Stress When Shot Peening, James R. Harrison, James Pineault, Tom Mills Sep 2025

Evaluating The Effectiveness Of Localized Masking To Prevent Changes In Residual Stress When Shot Peening, James R. Harrison, James Pineault, Tom Mills

15th International Conference on Shot Peening

When shot peening components, it is common practice to mask certain localized regions where peening roughness is not desirable. For example, surfaces that have been highly machined such as bearing races or areas of interference-fit may require masking to protect them from the cold working effects of shot peening. Oftentimes shot peening the grip sections of fatigue test coupons can prevent cracking and failures due to fretting fatigue in the grip area but could affect the outcome of the test if applied to the gauge section of the coupons. Thus, maintaining an “as machined” surface roughness is the most common …


Improving Fatigue Strength And Life Of Single Crystal Cmsx-4, Jochen Peter Fuhr, Lloyd Hackel, Nicolau I. Morar, Noah Holtham, Keivan Davami, Montu Sharma, Rajkumar Roy Sep 2025

Improving Fatigue Strength And Life Of Single Crystal Cmsx-4, Jochen Peter Fuhr, Lloyd Hackel, Nicolau I. Morar, Noah Holtham, Keivan Davami, Montu Sharma, Rajkumar Roy

15th International Conference on Shot Peening

The deep penetration of laser peening (LP) and retention of residual stress at high temperature by LP is significant in improving fatigue life and strength of superalloys exposed to high temperature and corrosion. Single crystal CMSX-4, was evaluated for stress relaxation and both fatigue life and fatigue strength of material that was LP-treated compared to non-LP and shot-peened (SP) specimens. LP was done with multiple layers using a 20 J/pulse laser where the laser high energy enabled using a 5 mm spot size on the metal surface. Stress measurements by the slitting technique showed the plastic penetration depth exceeded SP …


First Principles Materials Discovery And Design For Photovoltaic And Solar Thermal Alloys Using High Throughput Methods, Andrew Pike Aug 2025

First Principles Materials Discovery And Design For Photovoltaic And Solar Thermal Alloys Using High Throughput Methods, Andrew Pike

Dartmouth College Ph.D Dissertations

Materials selection has been a challenge since the dawn of time. With the advent of computational methods and high throughput databases, materials can be discovered and assessed before they are even synthesized. In this thesis I will discuss my work towards designing new materials for clean energy uses, especially alloys which have been underexplored from computational methods. To begin, I present a case study explaining the synthesis of the Yb14ZnSb11 thermoelectric material. Next, I explore the class of AM2Pn2 Zintl materials. From the previously identified BaCd2P2, it is suspected that …


Recent Progress And Scientific Challenges In Wire-Arc Additive Manufacturing Of Metallic Multi-Material Structures, Sainand M. Jadhav, Sambhaji Kusekar, Akash Belure, Satyavan Digole, Abhijeet Mali, Muralimohan Cheepu, Manoj Mugale, Suhas Alkunte, Duckbong Kim Aug 2025

Recent Progress And Scientific Challenges In Wire-Arc Additive Manufacturing Of Metallic Multi-Material Structures, Sainand M. Jadhav, Sambhaji Kusekar, Akash Belure, Satyavan Digole, Abhijeet Mali, Muralimohan Cheepu, Manoj Mugale, Suhas Alkunte, Duckbong Kim

Faculty Articles

Metallic multi-material structures are heterogeneous structures characterized by changing composition, microstructures, and site-specific characteristics, advantageous for numerous applications where multifunctionality is desired. Metallic multi-material structures are known as bimetallic structures (BSs), which are functionally graded materials (FGMs). In recent years, wire-arc additive manufacturing (WAAM) advanced as a promising additive manufacturing process to realize the fabrication of these structures due to its high deposition rate, cost-effectiveness, and material utilization efficiency. This review presents a comprehensive overview of the recent progress, processing strategies, and scientific challenges in WAAM of multi-material structures. The paper begins with an introduction to multi-material structures, followed by …


A Study Of Wear Measurement And Life Prediction Of Insert Chute Liner On Gold Ore Processing, Ferry Ardika Natanael, Nony Maulidya, Dedi Priadi Aug 2025

A Study Of Wear Measurement And Life Prediction Of Insert Chute Liner On Gold Ore Processing, Ferry Ardika Natanael, Nony Maulidya, Dedi Priadi

Journal of Materials Exploration and Findings

Chutes are critical materials handling assets to transport solid particles from one process step to another in mineral processing, coal mining and cement industries. The material transport, because of material characteristics, cause severe wear on internal lining of chutes or bins’ structure. The wear problem on internal lining of bins or chutes needs to be checked to keep production efficiency. Therefore, not checked wear rate causes liner replacement schedule becomes unpredictable. It leads to production loss and highly cost maintenance in industry. This study shows that condition-based maintenance through regular thickness measurement using Ultrasonic Transducer (UT) to predict life service …


Correlation Between Microstructure And Hardfacing Properties With Welding Current Intensity In Reconditioned Low-Alloy Steel Material Using Submerged Arc Welding (Saw) : A Comprehensive Review, Iman Nugraha Asmara, Winarto Winarto Aug 2025

Correlation Between Microstructure And Hardfacing Properties With Welding Current Intensity In Reconditioned Low-Alloy Steel Material Using Submerged Arc Welding (Saw) : A Comprehensive Review, Iman Nugraha Asmara, Winarto Winarto

Journal of Materials Exploration and Findings

This review studying the correlation between microstructural transformations and mechanical properties in reconditioned low-allow steel material, focusing on the impact of Submerged Arc Welding (SAW) parameters, especially current, on microstructure . The study highlights how variation on welding parameters, especially current intensity variation, affecting microstructural transformations, hardness, and wear resistance of hardfaced layers. Key aspects such as dilution effect, phases distribution, and carbide formation are reviewed to understanding their impact on mechanical properties. By reviewing insights from existing literature and experimental findings, this review underscores the role of Submerged Arc Welding in enhancing mechanical properties and microstructural of low-alloy steel …


Wear Of High Entropy Alloys: Understanding Effects Of Cryogenic Temperatures And Surface Nitriding On Wear Behavior, Aubrey Yu Tang Aug 2025

Wear Of High Entropy Alloys: Understanding Effects Of Cryogenic Temperatures And Surface Nitriding On Wear Behavior, Aubrey Yu Tang

Dartmouth College Ph.D Dissertations

Cryogenic tribological applications have become increasingly important with the development and innovation of advanced equipment in aerospace, polar regions, superconductivity, and more. Traditional lubrication methods are not viable under these harsh environments, so metallic materials must be able to maintain excellent mechanical properties and withstand the constant impact and wear alone. High entropy alloys (HEAs) have emerged as potential candidates for these applications because of their wide variety of excellent room temperature properties and apparent improvement of mechanical properties of some HEAs at extremely low temperatures. Despite their promising nature, very limited work has been done on understanding the wear …


Crevice Corrosion Mechanisms Of Cocrmo Alloys In Orthopedic Implants: Retrieval Analysis, Nano-Tribocorrosion And Cellular Responses, Hwaran Lee Aug 2025

Crevice Corrosion Mechanisms Of Cocrmo Alloys In Orthopedic Implants: Retrieval Analysis, Nano-Tribocorrosion And Cellular Responses, Hwaran Lee

All Dissertations

Mechanically assisted corrosion and non-mechanically (chemically) driven corrosion in modular junctions of orthopedic implants using cobalt-chromium-molybdenum (CoCrMo) alloys remain clinical concerns and may contribute to implant failure. The underlying corrosion mechanisms are not yet fully understood, leaving a critical research gap. We hypothesized that corrosion in modular junctions may be driven by aggressive local environments, including fretting, metal ion release (cobalt ion, Co2+), low pH and reactive oxygen species (ROS). This dissertation aims to (1) analyze corrosion modes and potential causes in modular junctions; (2) identify chemically driven corrosion modes on CoCrMo alloys using simulated inflammatory modular taper …


Ferroelectricity And Multiferroicity In Ultrathin Films Of Unconventional Transition Metal Oxide, Xin Li Aug 2025

Ferroelectricity And Multiferroicity In Ultrathin Films Of Unconventional Transition Metal Oxide, Xin Li

Department of Physics and Astronomy: Dissertations, Theses, and Student Research

Ferroic orders of transition metal oxides, such as ferroelectricity and ferromagnetism, are determined by the intercoupling between spin, charge, lattice. Consequently, ferroic epitaxial thin films have attracted wide interest due to the profuse novel phenomena and the great application potentials for modern electronics. However, the mainstream of the study for transition metal oxides has focused on perovskite structure, limiting the understanding and discovery of novel phenomena associate with ferroic orders. In this thesis, the epitaxial films of hexagonal rare-earth ferrites (h-RFeO3) and fluorite-structure hafnia oxide (HfO2) are studied comprehensively, providing new experimental and theoretic …


Shape Memory Behavior In Medium To High Entropy Shape Memory Alloys: Design, Prediction, And Experimental Analysis, Hatim Raji Aug 2025

Shape Memory Behavior In Medium To High Entropy Shape Memory Alloys: Design, Prediction, And Experimental Analysis, Hatim Raji

Theses and Dissertations

This dissertation provides a data-driven system integrating synthetic data generation and machine learning (ML) techniques to create multicomponent SMA compositions with specific transformation temperatures (TTs). Models were trained to represent the nonlinear dependencies influencing martensitic transformation behavior by using elemental, thermodynamic, and process-related aspects. The capacity of the ML models on medium entropy NiTiHfPd and high entropy NiTiHfZrCu systems accuracy was confirmed by experimental validation showing TTs closely matched with model outputs.


Grain Boundary Migration And Radiation Induced Segregation In Fe-Cr Alloys, Mohit Dhoriya Aug 2025

Grain Boundary Migration And Radiation Induced Segregation In Fe-Cr Alloys, Mohit Dhoriya

All Theses

Radiation-induced segregation (RIS) is a significant phenomenon that occurs in alloys subjected to irradiation, particularly in environments such as nuclear reactors. This thesis investigates RIS in ferritic Fe- Cr alloys through the use of Atomic Kinetic Monte Carlo (AKMC) simulations, focusing on the interaction between solute atoms and migrating grain boundaries. The study explores the influence of temperature, solute concentration, and grain boundary velocity on solute drag, a critical process driving RIS. The results show that solute migration is strongly influenced by the presence of vacancies and interstitials generated under irradiation, which are absorbed by grain boundaries and other defect …


Material Extrusion 3d Printing Of Metal Alloy: Material, Methods And Application., Sihan Zhang Aug 2025

Material Extrusion 3d Printing Of Metal Alloy: Material, Methods And Application., Sihan Zhang

Electronic Theses and Dissertations

Material extrusion (MEX) additive manufacturing presents a promising pathway for producing metal components with complex geometries while avoiding the safety hazards associated with loose powder handling in conventional metal additive manufacturing processes. This dissertation investigates the development and optimization of MEX processes for aluminum alloys, addressing critical challenges in feedstock formulation, printing parameter optimization, and post-processing strategies. Three distinct approaches were explored to advance the capabilities of aluminum MEX: filament-based processing of 6061 aluminum, paste-based extrusion of 6061 aluminum, and development of a novel aluminum-magnesium-tin alloy system for space manufacturing applications. The filament-based approach successfully demonstrated the production of 6061 …


Magnetically Impelled Arc Butt Welding And Straight Tube Butt Welding Analysis Of Boiler Grade Tube Joints, Santhosh Kumar S Jul 2025

Magnetically Impelled Arc Butt Welding And Straight Tube Butt Welding Analysis Of Boiler Grade Tube Joints, Santhosh Kumar S

Theses and Dissertations

Boiler-graded tubes of T11, T12, T91, and T92 materials with a thickness of 4.5 mm thick and 44.5 mm outer diameter were selected for the Straight Tube Butt Welding process using Hot Wire (STBW-HW) and Cold Wire (STBW-CW) conditions. Moreover, the research investigates and compares the welding characteristics of dissimilar T11 and T91 boiler-graded tubes using STBW - HW & Magnetically Impelled Arc Butt (MIAB) welding techniques. Similar and dissimilar welding was performed in STBW – HW & CW conditions.

In dissimilar welding, the tensile strength was higher in the T11-T91 STBWHW joints of 663 MPa than in the T12-T92 …


Measurement And Process Relation For Cast Surface Defects, Nachiket Laxman Shinde Jun 2025

Measurement And Process Relation For Cast Surface Defects, Nachiket Laxman Shinde

Masters Theses

This thesis presents an in-depth investigation into the classification and prediction of surface defects in aluminum sand castings using a combination of experimental trials and machine learning techniques. Key process variables such head height, pouring temperature, resin %, sand type and process were systematically varied to study their influence on defects like veining, and burn-on. Comparative analysis indicated superior performance of the deep learning model in handling nonlinear interactions between process parameters. The study emphasizes the importance of integrating data-driven models with foundry practices to enhance surface quality, reduce rework, and support intelligent decision-making in casting operations.


Ni-Mn-In Heusler Alloy Ribbon For Magnetocaloric Application, Bao Nguyen Jun 2025

Ni-Mn-In Heusler Alloy Ribbon For Magnetocaloric Application, Bao Nguyen

Masters Theses

A traditional cooling system, which applies compression technology within the working fluid, has had a lot of negative impacts on the environment and has low efficiency. They have almost reached the thermodynamic efficiency; there is little room for further improvement. Therefore, solid-state cooling systems, especially those that use the magnetocaloric effect (MCE), have drawnmuch interest as an alternative solution for the vapor-compression system. The Heusler alloy, especially Ni-Mn-In in this research, can be an excellent candidate for this application due to its unique properties, such as the shape memory effect and giant MCE. Their giant MCE results from a first-order …


Exploring Metal Additive Manufacturing In Martian Atmospheric Environments, Zane Mebruer May 2025

Exploring Metal Additive Manufacturing In Martian Atmospheric Environments, Zane Mebruer

Mechanical Engineering Undergraduate Honors Theses

On-surface manufacturing is key to the success of a planetary colonization, especially that of Mars. However, traditional subtractive manufacturing processes are equipment, energy, and material intensive, meaning novel additive manufacturing (AM) processes must be pursued for this end. Selective laser melting, one of the most effective and versatile AM methods, would be incredibly beneficial to a Martian mission but requires an artificial argon atmosphere to create effective parts. The purpose of this study was to examine if carbon dioxide, the gas that makes up over 95% of Mars’ surface atmosphere, would be a sufficient substitute for argon in SLM fabrication. …


Developing Reduced Order Models For Gas Bubble Formation In Irradiated Metals Using Integrated Phase Field Modeling And Koopman Operator Theory, John M. Eggemeyer V May 2025

Developing Reduced Order Models For Gas Bubble Formation In Irradiated Metals Using Integrated Phase Field Modeling And Koopman Operator Theory, John M. Eggemeyer V

All Theses

Irradiation damage in materials is prevalent in nuclear components, posing significant risks in the safety and reliability of nuclear reactors. Phase field models offer a versatile framework for modeling irradiation damage in materials at mesoscales. Such high fidelity method has been used to model the formation of fission gas bubbles superlattice, a microstructure array occurs at certain irradiation conditions (dose, dose-rate, and temperature). To overcome the high computational cost of phase field modeling, Koopman operator theory is applied to create reduced order models, allowing for instantaneous simulations of fission gas bubble behaviors. These low fidelity models are integrated into machine …


Manipulating Martensitic Transformation And Residual Stress Development In Stress Superposed Incremental Forming Of Ss304, Elizabeth M. Mamros, Fabian Maaß, Thomas Gnaupel-Herold, A. Erman Tekkaya, Brad L. Kinsey, Jinjin Ha May 2025

Manipulating Martensitic Transformation And Residual Stress Development In Stress Superposed Incremental Forming Of Ss304, Elizabeth M. Mamros, Fabian Maaß, Thomas Gnaupel-Herold, A. Erman Tekkaya, Brad L. Kinsey, Jinjin Ha

Faculty Journal Articles

Stress superposition is one of the strategies used in metal deformation processes to increase the material formability, decrease the required forming forces, and create highly customized components. To investigate the effects of tensile and compressive stresses superposed to the single point incremental forming (SPIF) process, experiments and numerical simulations were conducted for a stainless steel 304 (SS304) truncated square pyramid geometry. Tensile stresses were superposed in-plane on the specimen blank by a custom hydraulic frame, and compressive stresses were incorporated via a polyurethane die. Identified parameters for a martensitic transformation kinetics model for SS304 were used in a two-step finite …


Assessment Of H2s-Induced Cracking Susceptibility In Steam Line Pipes And Weld Zones During Geothermal Well Construction, Riene Kaelamanda Pragitta, Yudha Pratesa May 2025

Assessment Of H2s-Induced Cracking Susceptibility In Steam Line Pipes And Weld Zones During Geothermal Well Construction, Riene Kaelamanda Pragitta, Yudha Pratesa

Journal of Materials Exploration and Findings

The susceptibility of steam line pipes, especially in the HAZ (heat-affected zone) and weldment areas, to hydrogen sulfide in the geothermal industry is crucial to understand from the early stages, particularly during construction. The combination of tensile stress from residual stresses after welding and metallurgical phase transformation makes the joint areas vulnerable to sulfide stress cracking. This condition becomes even more extreme when the equipment operates during the well stimulation phase. This research assesses the severity of H₂S-induced cracking using NACE MR0175 and ISO 15156-1 standards, focusing on the effects of pH and partial pressure of H₂S (pH₂S …


Physical Characterization Of Copper Anode Slimes, Carter Glynn, Michael S. Moats Apr 2025

Physical Characterization Of Copper Anode Slimes, Carter Glynn, Michael S. Moats

Miners Solving for Tomorrow Research Conference

No abstract provided.


L.G. Twidwell Fifty-Six Years Of Research A Summary, Larry G. Twidwell Apr 2025

L.G. Twidwell Fifty-Six Years Of Research A Summary, Larry G. Twidwell

Metallurgical & Materials Engineering

Larry G. Twidwell, D.Sc. is Emeritus Professor in the Department of Metallurgical and Materials Engineering at Montana Technological University. He has fifty-six years of experience in teaching and directing research in Metallurgical and Materials Engineering at Montana Tech. Twidwell and his graduate students and coworkers have conducted research emphasizing extractive metallurgy and the application of extractive metallurgical engineering to the treatment of metallurgical wastes, process waters and byproducts. Four books, seventy-seven M.Sc. theses, one-hundred-thirty refereed publications and one hundred-eight national and international presentations have resulted from their research efforts. Twidwell has received several outstanding teacher/researcher awards during his tenure at …


Data-Driven Decision Making For Quality Control In Foundry Applications, Ronit Shetty Apr 2025

Data-Driven Decision Making For Quality Control In Foundry Applications, Ronit Shetty

Dissertations

In the transformative landscape of Industry 4.0, advanced quality control in manufacturing demands innovative methods for processing and analyzing datasets. This dissertation presents a comprehensive study on leveraging high volume data and machine learning to enhance decision making in the foundry industry. The research explores three crucial challenges in the foundry industry: predicting surface roughness, monitoring refractory coating thicknesses, and comparing feature extraction techniques for surface quality classification. The findings underscore the transformative potential of integrating advanced feature engineering techniques and machine learning into manufacturing quality control.

The first of the three challenges introduces a framework that integrates digital images …


Intelligent Turning Cyber-Physical Systems Modeling Using Sysml, Prithbey Raj Dey, David Lee Enke, Mario F. Buchely Mar 2025

Intelligent Turning Cyber-Physical Systems Modeling Using Sysml, Prithbey Raj Dey, David Lee Enke, Mario F. Buchely

Engineering Management and Systems Engineering Faculty Research & Creative Works

Cyber-Physical Systems (CPS) support industrial automation that incorporates people, hardware, signal, computation, and control using networking to achieve desired results. The complex automated CPS design demands a standard and comprehensive approach to appropriately identify the system requirements, define the architecture, and model the relationships among the software and hardware components. Systems Modeling Language (SysML) provides the capability for a comprehensive modeling to capture the desired design requirements in the systems architecture. SysML enables performance estimation of the model by analyzing constraints while identifying interactions among the components through various behavioral diagrams. In this paper, SysML is applied to the design …


Improvement Of Microcracking And Mechanical Properties Of Tungsten Fabricated Via Laser Powder Bed Fusion Through Alloying With Reactive Secondary Constituents, William S. Mockel Mar 2025

Improvement Of Microcracking And Mechanical Properties Of Tungsten Fabricated Via Laser Powder Bed Fusion Through Alloying With Reactive Secondary Constituents, William S. Mockel

Theses and Dissertations

Tungsten (W), a Group VI transition metal, possesses a number of advantageous properties, most notably its impressive mechanical performance at extreme temperatures. While tungsten's nature render traditional manufacturing methods difficult, additive manufacturing through laser powder bed fusion (LPBF) presents a promising avenue for fabricating tungsten components. However, the material’s high ductile-to-brittle transition temperature combined with the embrittling effect of impurities mean that the residual stresses imparted by LPBF result in microcracking in tungsten, degrading its usefulness. This study sought to improve the characteristics of LPBF-W through the removal of embrittling oxygen content via alloying with low concentrations of reactive elements, …


Fatigue Behaviour Of Al 6063 Alloy In Heat Treated, Deep Cryogenic Treated And Equal Channel Angular Pressing (Ecap) Processed Conditions, Sreearravind M Feb 2025

Fatigue Behaviour Of Al 6063 Alloy In Heat Treated, Deep Cryogenic Treated And Equal Channel Angular Pressing (Ecap) Processed Conditions, Sreearravind M

Theses and Dissertations

This research focuses on improving the Low Cycle Fatigue (LCF) life of Al6063 using three different processing techniques – Heat Treatment (HT), Deep Cryogenic Treatment (DCT), and Equal Channel Angular Pressing (ECAP). Al 6063, widely used in structural applications, has limited fatigue performance, necessitating the exploration of advanced processing techniques to enhance its LCF life.

In HT phase, Al 6063 T5 samples were subjected to solid solution HT followed by air and water quenching. The air-quenched (T6A) and water-quenched (T6W) samples were subjected to precipitation hardening. The Ultimate Tensile Strength (UTS) of the T6A sample increased to 188 MPa from …


Selective Leaching Of Rare Earth Elements From Complex Rare Earth Ore Using Deep Eutectic Solvents, Frank Agyemang, Mehran Saddat, Zainab Nasrullah, Richard Ladouceur Feb 2025

Selective Leaching Of Rare Earth Elements From Complex Rare Earth Ore Using Deep Eutectic Solvents, Frank Agyemang, Mehran Saddat, Zainab Nasrullah, Richard Ladouceur

Metallurgical & Materials Engineering

Rare earth elements (REEs) are valuable for various modern technological applications, including metallurgy, machine building, radio electronics, instrument engineering, nuclear engineering, and manufacturing. The extraction and separation of rare earth elements (REEs) from their complex ores is challenging due to their distinct physical and chemical properties, contributing to their market scarcity. At present, REE recovery utilizes traditional pyro- or hydrometallurgical processes. The overall process in the recovery and separation of individual elements from complex REE systems suffers from high energy demands and the use of many hazardous chemicals that negatively impact the environment. With the growing trend toward a circular …


Impurity Behavior In Cast Copper Anodes: Implications For Electrorefining In A Circular Economy, Agustin Morales-Aragon, Daniel Sánchez-Rodas, Guillermo Ríos, Michael S. Moats Feb 2025

Impurity Behavior In Cast Copper Anodes: Implications For Electrorefining In A Circular Economy, Agustin Morales-Aragon, Daniel Sánchez-Rodas, Guillermo Ríos, Michael S. Moats

Materials Science and Engineering Faculty Research & Creative Works

The behavior of impurities in cast copper was investigated to simulate production with increased utilization of secondary sources within the framework of a circular economy. The incorporation of impurities, particularly Ni, Sn, and Sb, from recycled Cu may significantly impact the electrorefining process. In this study, commercial anodes were doped with Ni, Sn, and Sb concentrations of 2500–6500 g/t, 300–900 g/t, and 450–950 g/t, respectively. Anode concentrations of Pb and Bi were maintained at 1000 g/t and 350 g/t, respectively. As concentrations were examined at two levels, 860 or 1700 g/t, depending on the commercial anode used to create the …