Materials Science and Engineering Commons^™

The Role Of Si3n4 Amorphous Phase In Nc-Tin/A-Si3n4 Nanocomposites In Increases The Hardness And Thermal Stability, Keba Moto

Makara Journal of Technology

The role of Si3N4 amorphous phase in nc-TiN/a-Si3N4 nanocomposites will be shown and compared with polycrystalline ZrN/Ni which has no such amorphous phase (non-composites). The presence of amorphous phase Si3N4 increases the hardness of film as well as the toughness of the bulk nanocomposites under indentation load. It has been observed that nc-TiN/a-Si3N4 nanocomposites films has higher thermal stability than ZrN/Ni polycrystalline films.

The Effects Of Corrosive Chemicals On Corrosion Rate Of Steel Reinforcement Bars: I. Swamp Water, Sulistyoweni Widanarko, Henki W. Ashadi, Andri Krisnadi Wicaksono

Makara Journal of Technology

Most of infrastructures using steel concrete to reinforce the strength of concrete. Steel concrete is so vulnerable to chemical compounds that can cause corrosion. It can happen due to the presence of chemical compounds in acid environment in low pH level. These chemical compounds are SO4 2-, Cl-, NO3 -. There are many swamp area in Indonesia. The acid contents and the concentration of ion sulphate, chlorides, and nitrate are higher in the swamp water than in the ground water .The objective of this research was to find out the influence of corrosive chemicals in the swamp water to the …

Biodiesel's Characteristics Preparation From Palm Oil, Tilani Hamid. S, Rachman Yusuf

Makara Journal of Technology

Biodiesel’s characteristics preparation from palm oil. Using vegetable oils directly as an alternative diesel fuel has presented engine problems. The problems have been attributed to high viscosity of vegetable oil that causes the poor atomization of fuel in the injector system and pruduces uncomplete combustion. Therefore, it is necessary to convert the vegetable oil into ester (metil ester) by tranesterification process to decrease its viscosity. In this research has made biodiesel by reaction of palm oil and methanol using lye (NaOH) as catalyst with operation conditions: constant temperature at 60 oC in atmosferic pressure, palm oil : methanol volume ratio …

Development Of Hardness Measurement Procedure For Nanocomposite Nc-Tin/A-Si3n4, Keba Moto

Makara Journal of Technology

Hardness of nc-TiN/a-Si3N4 nanocomposites which was determined by using two methods of measurements i. e. depth sensing method and remaining plastic indentation area that were magnified by using SEM (Scanning Electron Microscope) lie in the good agreement. The hardness value is not influenced by the biaxial and residual compressive stress. The measurement of the biaxial stress on the substrate shows a very small value of biaxial stress as well as the constant hardness and crystallite size against annealing temperature. Therefore, the reported hardness value here is the intrinsic value that depend on its microstructure properties.

Analogy Method Development For Cost Estimation Of Software Design, Riyanarto Sarno, Joko Lianto Buliali, Siti Maimunah

Makara Journal of Technology

The important aspect of planning and managing software development project is to estimate the cost of a project. There are several methods for estimating the cost of a software development project, and the Analogy method is a method which gives relatively better estimates. This paper shows that the modified Analogy method selects a closer project reference, estimates more accurate project effort and cost. This study enhances the cost estimate technique by including valid and complete cost parameters, therefore the estimate of a project cost is better than the result of the standard Analogy method.

The Effects Of Corrosive Chemicals On Corrosion Rate Of Steel Reinforcement Bars: Ii. Swamp Sludges, Henki W. Ashadi, Sulistyoweni Widanarko, Irma Gusniani

Makara Journal of Technology

A polluted environment will influence the building age. The objective of this research was to find out the influence of corrosive chemicals within the sludge swamp area with the corrosion rate of steel concrete. Corrosion in steel concrete usually occur in acid area which contain of SO4 2-, Cl- and NO3 -. The research treatment used by emerging ST 37 and ST 60 within 60 days in ‘polluted’ sludge swamp area. Three variation of ‘polluted’ swamp sludge were made by increasing the concentration a corrosive unsure up to 1X, 5X and 10X. The corrosion rate measured by using an Immersion …

Correlation Between The Xps Peak Shapes Of Y1bu2cu3o7-X And Film Quality, Paul N. Barnes, Sharmila M. Mukhopadhyay, Timothy J. Haugan, Swaminathan Krishnaswami, Justin C. Tolliver, Iman Maartense

Mechanical and Materials Engineering Faculty Publications

X-ray photoelectron spectroscopy (XPS) depth profiling was used to investigate the compositional and chemical profile of a typical YBCO coated conductor architecture. Results of the process revealed that the Y(3d) photoelectronic peak shape in these films is very different from bulk YBCO. To investigate this, several samples of Y i Ba2Cu307_„ thin films were intentionally created of varying quality. The films were deposited on LaA10 3 by pulsed laser deposition with ./c. values ranging from poorly conducting up to several MA/cm2. Initial results indicated a potential correlation between the Y(3d) XPS peak shape (full-width-half-maximum) of the YBCO and the film …

Design And Analysis For Melt Casting Metallic Fuel Pins Incorporating Volatile Actinides, Xiaolong Wu

UNLV Theses, Dissertations, Professional Papers, and Capstones

Fundamental issues related to the selection of a metallic fuel casting furnace design are presented and discussed including heating mechanisms, casting issues, crucible design, and issues related to the mass transport of americium. The process of evaluating all of these different criteria is undertaken to select a concept that would have the greatest chance of success for casting americium in a metallic fuel rod. Based on this evaluation process, a concept for the casting of metallic fuel pins containing high vapor pressure materials is selected and discussed. The important physics of this concept include mass transport of americium from the …

Modeling And Simulation Of The Chemical Etching Process In Niobium Cavities, Qin Xue

UNLV Theses, Dissertations, Professional Papers, and Capstones

Niobium Cavities are important parts of the integrated NC/SC high-power linear accelerator (linac) that can accelerate over 100 mA of protons to several GeV. Surface finish of the niobium cavity plays an important role of achieving the best performance of niobium cavity. The chemical etching techniques have been widely used.

Chemical etching of the inner surface of the cavity is achieved by circulating acid through it. The acid interacts with the surface and eliminates imperfections. During the etching process, a pipe with baffles is inserted within the cavity to direct the flow along the surfaces.

A 2-D, axisymmetric, steady state, …

Investigation Of Forces Acting On Plain Discs, S. M. Mpanduji

Tanzania Journal of Engineering and Technology (TJET)

An investigation was carried out to study the mutually perpendicular forces generated by rotating and non-rotating plain discs similar to those used in disc ploughs. Experiments were conducted in a soil bin containing sand loam soil (Ryton sand) where forces were measured while changing disc rake and sweep angles. The results showed that draught forces were higher for non-rotating discs, while vertical and lateral forces were lower compared to rotating discs. Rotating discs were found to be suitable for counteracting high side forces because of less draught and higher lateral forces. The recommended optimum angles are between 8°–12° for disc …

Simulations Of Nematic Liquid Crystals: Confined Geometries, Phase Transitions And Topological Defects, Nikolai V. Priezjev

Mechanical and Materials Engineering Faculty Publications

The physics of liquid crystals is an exciting field of research with important practical applications. In this dissertation we present the results of simulation studies of nematic liquid crystals using Monte Carlo and molecular dynamic techniques. In our first project we performed Monte Carlo Simulations of the Lebwohl-Lasher (LL) model of nematic liquid crystals confined to cylindrical cavities with perpendicular anchoring. In this particular geometry one has an interesting interplay between bulk and surface energies, which results in different director configurations inside the cylinder. Our work reconciled the apparent contradictions between the results of earlier simulations and approximate analytics theories. …

Design And Analysis Of A Process For Melt Casting Metallic Fuel Pins Incorporating Volatile Actinides, Yitung Chen, Darrell Pepper, Randy Clarksean

Fuels Campaign (TRP)

UNLV has developed and will continue to develop process models for the analysis of melt casting processes. This work will continue to be performed under the guidance of Argonne National Laboratory (ANL) engineers to ensure that their knowledge and experience benefits the project. The research to be conducted during the second year will center on performing detailed analyses on a conceptual design of an inductively heated skull-crucible casting furnace. Processing conditions will be analyzed, basic models utilized, and detailed heat and mass transfer models will be developed to analyze the most promising processes. The goal of this second year is …

Modeling, Fabrication, And Optimization Of Niobium Cavities: Phase Ii, Robert A. Schill Jr., Mohamed Trabia

Transmutation Sciences Materials (TRP)

Niobium cavities are important parts of the integrated NC/SC high-power linacs. Over the years, researchers in several countries have tested various cavity shapes. They concluded that elliptically shaped cells are the most appropriate shape for superconducting cavities. The need for very clean surfaces led to the use of a buffered chemical polishing procedure for surface cleaning to get good performance of the cavities. This proposal discusses the second phase of research in the second year of the project.

The first phase (starting Summer 2001) has resulted in improving the basic understanding of multipacting and the process of chemical etching. Based …

Use Of Positron Annihilation Spectroscopy For Stress-Strain Measurements, Ajit K. Roy

Transmutation Sciences Materials (TRP)

The purpose of this collaborative research project involving the University of Nevada, Las Vegas (UNLV) and Idaho State University (ISU) is to evaluate the feasibility of determining residual stresses of welded (after pre-straining) engineering materials using a new nondestructive technique based on positron annihilation spectroscopy. The proposed technique is to use γ-rays 2 from a small MeV electron Linac to generate positrons inside the sample via pair production. This method can be used for materials characterization and investigation of defects in thick samples that could not be accomplished by conventional positron techniques or other nondestructive methods. The data generated will …

Study Effect Of Salt Washing Process On Content And Iodium Stability Of Salt, Nelson Saksono

Makara Journal of Technology

Effect of Salt Washing Process on Content and Iodium Stability of Salt. Salt washing process should increase the salt quality. It should clean the salt from sludge or clay and also reduce the impurity compound such as Mg, Ca and the reductor content. The objective of these reseach is to assess the effect of washing process on the content og hygroscopic impurities compound (Ca and Mg), and reductor content of salt. The research also investigate the water absorbing, pH, KIO3 content as function of time to obtain effect of washing process on KIO3 stability in salt. The experiment result shows …

Making Alloys (Ti1 - Xalx) N Using Plasma Cvd Technique From Alcl3 Powder, H2 And N2 Gas ,With Solvent Ticl4, Keba Moto

Makara Journal of Technology

The substitution of Ti atoms by Al atoms in TiN lattice sites to form (Ti1-xAlx)N is clearly demonstrated by the coatings which were deposited on steel substrate and using plasma CVD technique. The presence of Al atoms in TiN lattice site is shown by means of XRD and EDX techniques: lattice parameters decreasing of TiN as the fraction of Al increases (XRD) and precipitation of hexagonal AlN phase (XRD) as the fraction of Al exceeding 0.8 (EDX). The hardness of these coating are just around 30 GPa, which is beyond the values reported in literatures.

Integrating Passenger And Modulo As Learning Tools For Collaborative Engineering Education, Kalamullah Ramli, Frank Schwarz, Stefan Werner, A Halim Shamsuddin, Axel Hunger

Makara Journal of Technology

The University of Indonesia (UI), Gerhard Mercator University (GMU), the Universiti Kebangsaan Malaysia (UKM) have agreed to cooperate as partners to develop a joint bachelor (3+1) and masters (1+1) degree, and collaborate in the research fi elds of multimedia- and internet-based learning and application level active networks. This paper describes the introduction of the Offshore Project and the extending of information technology applications to the partner institutions in this international cooperation which would very much enhance the operations of the new initiative in engineering education, which could provide students in far distance with more fl exible learning environment.

Effects Of 0.25 % Mo (Molybdenum) Which Is Contained In The Ductile Cast Iron On Mechanical Properties Of Austempered Ductile Iron (Adi)., Nukman Nukman, Bustanul Arifin, Bambang Sugiarto

Makara Journal of Technology

The aim of this research is to investigate the effects of 0.25 % Mo (Molybdenum) which is contained in the ductile cast iron on mechanical properties of Austempered Ductile Iron (ADI). The various temperatures and the holding times are used in the heat treatment processes. Using a given 0.25 % Mo in the ductile iron, ADI's alloyed developes a higher ultimate tensile stress value and decreases the elongation if we compare with the as cast (non alloy ductile iron). The higher impact energy value obtained at 9000 C austenization and 375o C austempering temperatures during 60 minutes holding times. The …

The Manufacturing Properties Of Galvanised Steel Sheet With Hexagonal And Tetragonal Network Of Circle Holes, Rahmat Saptono

Makara Journal of Technology

Galvanized steel sheet of 0.8 mm in thickness was drilled with circle holes of 2.5 mm diameter and spacing arranged in tetragonal and hexagonal pattern. The manufacturing properties of specimen were studied through drawing and stretching simulative test. It was concluded from the results that, at high ratio of punch to hole diameter (40/2.5), the drawing properties (LDR) of both square and hexagonal perforated sheet were slightly lower than that of solid sheet, while hexagonal perforated showing LDR somewhat higher than the square one. The stretching properties (LDH) of sheet, however, were much lower than that of solid sheet while …

The Effect Of Temperature On The Optical Absorptive And Reflective Behavior Of Metals, Thomas A. Hunyady

Mechanical & Aerospace Engineering Theses & Dissertations

In the five decades since its invention, the laser has been used to commercially process materials in an increasingly diverse number of ways. The precise control over the delivery of the incident energy that is afforded by a laser allows for a wide variety of applications. All of these processes depend in some way on two important physical properties of the material being treated. These properties are known as the optical reflectivity and absorptivity of a material. The values of each of these properties are different for each material and are influenced by a number of factors, including surface roughness, …

Develops The Software Of Dsp Processor For The Cdma Circuitry, Arman Djohan D.

Makara Journal of Technology

This research develops the software of DSP Processor type TMS320C54X for the CDMA circuitry. This research apply two algorithms namely Mathematic Algorithm and table lookup Algorithm. From both algorithms, the research examine what algorithm have the fasted processing time and the smallest memory occupation. From the examination results the Mathematic Algorithm have 20.62 milliseconds processing time and the Table lookup algorithm have 14.08 milliseconds processing time. The Table lookup algorithm have the fastest processing time because the Matematic algorithm need the rounding process of the fi gure. Eventhough such processing time is not exceed from the 125 millisecond of delay …

Object Classfification In Computer Vision With Discriminant Analysis, Amir Hamzahan

Makara Journal of Technology

A robotic sensor system is always supported by a computer system called ‘computer vision’. The important concept of computer vision is object classfifi cation. In this study two algorithms for object classifi cation in this system will be compared. Firstly, A simple method that do not need complex computation and that considered as an informal method is called binary tree decision structure. This method is based on modest caracteristic decriptors of an object such as vertical line, horizontal line or ellipse line. Unfortunately this method has weakness in recognize an image that contaminated by a noise. Secondly, a more formal …

Fretting Fatigue Behavior Of A Titanium Alloy Ti-6al-4v At Elevated Temperature, Onder Sahan

Theses and Dissertations

The purpose of this research is to investigate the fretting fatigue behavior of the titanium alloy Ti-6Al-4V at elevated temperature is investigated. Fretting and plain fatigue experiments are conducted at 260 °C. Crack initiation location and crack initiation orientation is measured and fretting and plain fatigue life data of the specimens from these tests are obtained. Fatigue parameters capable of predicting the number of cycles to specimen failure, the crack location and the crack orientation along the contact surface are analyzed. The parameters are calculated by using the computed stresses and strains obtained from the finite element analysis. The mechanisms …

Modeling, Fabrication, And Optimization Of Niobium Cavities – Phase I: Quarterly Progress Report November 20, 2001 - February 20, 2002, Robert A. Schill Jr., Mohamed Trabia

Transmutation Sciences Materials (TRP)

Multipacting is one of the major loss mechanisms in RF superconductivity cavities for accelerators. This loss mechanism limits the maximum amount of energy/power supported by the cavities. Optimal designs have been identified in others’ studies. In practice, these designs are not easily manufactured. Chemical etching processes used to polish the cavity walls result in a nonuniform surface etch. A nonuniform surface etch will leave some unclean areas with contaminants and micron size particles. These significantly affect multipacting. Further, a nonuniform etch will leave areas with damaged grain structure, which is not good for superconducting properties. Typically, the depth of chemical …

Strongly Screened Vortex Lattice Model With Disorder, C. Giardina', Nikolai V. Priezjev, J. M. Kosterlitz

Mechanical and Materials Engineering Faculty Publications

The three dimensional XY model with quenched random disorder and finite screening is studied. We argue that the system scales to model with λ≃0≃T and the resulting effective model is studied numerically by defect energy scaling. In zero external field we find that there exists a true superconducting phase with a stiffness exponent θ≃+1.0 for weak disorder. For low magnetic field and weak disorder, there is also a superconducting phase with θ≃+1.0 which we conjecture is a Bragg glass. For larger disorder or applied field, there is a non superconducting phase with θ≃−1.0. We estimate the critical external field whose …

Nitriding Of Titanium By Inductively Coupled Plasma, Abdul Hakim Hashim

Student Works (2000-2009)

A RF planar coil inductively coupled plasma syslem (ICP) is used in this project to nitride a commercially pure titanium substrate. The system is powered by a 600 W, 13.56 MHz, 50 Ω RF generator. The impedance matching is achieved by using an air­-core step-down transformer and a tunable vacuum capacitor. The electrical discharge characteristics of argon and argon-nitrogen admixture plasmas are investigated. Coil current, ion density and RF power transferred in the plasma at different pressure are studied. Nitriding of titanium using the system is found to be able to produce θ-TiN, ε-Ti2N and α-Ti(N) layers, as confirmed by …

Modeling, Fabrication, And Optimization Of Niobium Cavities, Robert A. Schill Jr., Mohamed Trabia, Yitung Chen

Transmutation Sciences Materials (TRP)

All technologies for the transmutation of nuclear waste require a large source of neutrons. One of the principal methods of generating these neutrons is by using a particle accelerator to bombard a heavy metal target. One of the more promising designs for particle accelerators for transmutation systems is the Superconducting Radio Frequency (RF) high-current linear accelerator (linac). The power supplies for these systems have three major components: niobium cavities, power couplers, and cryomodules. This research project will develop models to predict the behavior and performance of the niobium cavities, which will then be used to design and optimize the superconducting …

Heat Transfer In A Thin Liquid Film In The Presence Of Electric Field For Non-Isothermal Interfacial Condition, Rama S.R. Gorla, Jorge E. Gatica, Bahman Ghorashi, Pijarn In-Eure, Larry W. Byrd

Chemical & Biomedical Engineering Faculty Publications

Heat transfer enhancement in an evaporating thin liquid film using the electric field under non-isothermal interfacial condition is presented. A new mathematical model subjected to van der Waals attractive forces, the capillary pressure and the electric field is developed to describe the heat transfer enhancement in the evaporating thin liquid film. The effect of an electrostatic field on the curvature of the thin film, evaporative flux, pressure gradient distribution, heat flux, and heat transfer coefficient in the thin film is presented. The results show that the electric field can enhance heat transfer in the thin liquid film significantly. In addition, …

Modeling, Fabrication, And Optimization Of Niobium Cavities: Phase Ii Second Quarterly Report, Robert A. Schill Jr., Mohamed Trabia

Transmutation Sciences Materials (TRP)

Niobium cavities are important parts of the integrated NC/SC high-power linacs. Over the years, researchers in several countries have tested various cavity shapes. They concluded that elliptically shaped cells are the most appropriate shape for superconducting cavities. The need for very clean surfaces lead to the use of a buffered chemical polishing produce for surface cleaning to get good performance of the cavities. Up to this point, the second phase has resulted in the design of an experimental setup for the fluid flow experiment. Other experimental activities include the evaluation of a vacuum system are underway. Little reportable progress has …

Effect Of Polymer-Surface Mobility On Adhesion In Poly(Methyl Methacrylate)-Tape System, Bhavesh C. Gandhi, Frank D. Blum, Lokeswarappa R. Dharani

Chemistry Faculty Research & Creative Works

The interaction between two polymer layers, especially adhesion between them, plays an important role in polymer processing and other applications. Detailed knowledge of the molecular structure and dynamics of polymer interfaces, and how they relate to macroscopic mechanical properties, should help designers construct more functional systems. Unfortunately, there have been few studies where both molecular and macroscopic studies have been performed on similar systems. In previous studies from our group, we have probed the dynamics of poly(methyl acrylate) (PMA) and thermal behavior of poly(methyl methacrylate) (PMMA) on silica. These studies helped us paint a picture for strongly bound molecules on …