Chemical Engineering Commons^™

Thermal Conductivity Characterization Of High Oleic Vegetable Oils Based Hybrid Nanofluids Formulated Using Gnp, Tio2, Mos2, Al2o3 Nanoparticles For Mql Machining, Anthony Chukwujekwu Okafor, Tobechukwu Kingsley Abor, Saidanvar Esanjonovich Valiev, Ignatius Echezona Ekengwu, Abiodun Saka, Monday Uchenna Okoronkwo

Mechanical and Aerospace Engineering Faculty Research & Creative Works

This paper presents the results of thermal conductivity characterization of six high oleic soybean oil (HOSO) and four high oleic canola oil (HOCO)-based hybrid nanofluids formulated with four types of nanoparticles (Graphene nanoplatelet (xGnP), TiO2, MoS2, and Al2O3) at nanoparticles wt.% concentration from 1 % to 7 % in 1 % increment using the two-step method for use in MQL machining of difficult-to-cut metals. Thermal conductivity of the formulated hybrid nanofluids were measured using Thermtest Transient Hot Wire Liquid Thermal Conductivity Meter at temperatures from 25 °C to 75 °C in increment of 10 °C. Obtained results showed that thermal …

Fabrication And Performance Of Scalable Bio-Engineered Porous Layers For Efficient Co2 Capture, Mary Sharon Rose Bondugula

Theses and Dissertations

This dissertation addresses the critical challenge of mitigating climate change by advancing CO2 capture technologies. As global CO2 emissions continue to rise, effective methods for capturing and separating CO2 from industrial processes are essential to combat climate change. Existing CO2 capture systems, such as Pressure Swing Adsorption (PSA) and Temperature Swing Adsorption (TSA), often rely on packed bed designs that face limitations, including poor heat and mass transfer, slow gas diffusion, and low thermal conductivity, reducing their efficiency. To overcome these challenges, this dissertation explores innovative solutions by developing advanced adsorbent coatings and scalable bed configurations.

This research begins by …

High Energy Density Lithium-Ion Battery Materials., Rachel Dewees

Electronic Theses and Dissertations

Growth of the EV industry has created an increased demand for Li-ion battery electrode materials, and support of a robust lithium-ion battery supply chain is a national imperative. For mainstream acceptance in the American market, the range of EVs must be improved, i.e., the energy density of the battery must be increased. Increasing the specific capacity of the electrode materials is the most direct strategy for increasing the energy density of the battery. Silicon anode materials have a theoretical capacity of over 3700 mAh·g^-1 - an order of magnitude beyond that of the graphitic materials which are currently implemented. …

Monitoring Of Laser Soldering Process In Hybrid Additive Manufacturing, Alexander P. Pustinger

Open Access Theses & Dissertations

Additive manufacturing (AM) has been a maturing technology that has expanded over the course of the last decade in major advancements especially in accessibility, process monitoring, modeling, and stock material design. As its industry use is growing, the demand for added improvements such as multi-functionality increases, such as with a hybrid system that allows for modification of printed parts with different electrical components like the Foundry Multi-3D system. The system's purpose is to create AM parts with multifunctional electrical components with the vision to expand to other areas of interest in manufacturing such as ISAM. This work explores the use …

Collapse Of Pre-Covid-19 Differences In Performance In Online Vs. In-Person College Science Classes, And Continued Decline In Student Learning, Gregg R. Davidson, Hong Xiao, Kristin Davidson

Faculty and Student Publications

Abstract: Studies comparing student outcomes for online vs. in-person classes have reported mixed results, though with a majority finding that lower-performing students, on average, fare worse in online classes, attributed to the lack of built-in structure provided by in-person instruction. The online/in-person outcome disparity was normative for non-major geology classes at the University of Mississippi prior to COVID-19, but the difference disappeared in the years after 2020. Previously distinct trendlines of GPA-based predictions of earned-grade for online and in-person classes merged. Of particular concern, outcomes for in-person classes declined to match pre-COVID-19 online expectations, with lower-GPA students disproportionally impacted. Objective …

Kinetic Modeling Of Dust Grain Dynamics In Electrostatic Sieving, Aaron Berkhoff, Easton Ingram, Fateme Rezaei, Jeffrey Smith, David Bayless, William Schonberg, Daoru Han

Chemical and Biochemical Engineering Faculty Research & Creative Works

A new kinetic particle modeling framework was developed to investigate electrostatic transport of lunar regolith dust particles with applications to the concept of electrostatic sieving. the new approach is based on kinetic particle dynamics and includes major modules of sampling the particle size distribution, solving electric fields, and tracking motion of charged dust grains. a case study for a concept of electrostatic sieving was chosen to validate the new model. the simulation achieved similar performance of particle size classification as reported in the literature. the new model is computationally efficient (takes a few minutes on a PC-type laptop computer) so …

Hydrogen-Peroxide Intercalated Expanded Graphite Facilitates Large Enhancement In Thermal Conductivity Of Polyetherimide/Graphite Nanocomposites, Fatema Tarranum, Swapneel Danayat, Avinash Nayal, Zarin Tasmin Mona, Roshan Sameer Annam, Keisha Walters, Jivtesh Garg

Chemical Engineering Faculty Publications and Presentations

In this work, we prepared expanded graphite (EG) filler using hydrogen peroxide (H₂O₂) as an oxidizing agent to study its impact on the thermal conductivity (k) of polyetherimide (PEI) composite, compared to EG prepared using sodium chlorate (NaClO₃). Sulfuric acid was used as the primary intercalating agent for both synthesis routes. The use of H₂O₂ prepared EG (EG-H₂O₂) led to a remarkable ∼4030% enhancement (9.5 Wm⁻¹K⁻¹) in k of the PEI/EG composite, while the use of NaClO₃ prepared EG (EG-NaClO …

Electrified Membrane For Water Treatment And Resource Recovery: Advancing Multiscale Strategies In Gas-Involving Reactions, Jianan Gao

Dissertations

Multifunctional, modular, and scalable water treatment technologies that operate without chemical additives are crucial for addressing global water pollution challenges. While traditional membrane-based separation processes are crucial for ensuring clean water supplies, they primarily focus on pollutant removal rather than on the upcycling of pollutants into valuable resources. Electrified membrane filtration presents a robust alternative, utilizing minimal or no chemical additives and harnessing electrical power to directly reduce contaminants or produce reactive oxidants or reductants on-site.

This dissertation is dedicated to the development of innovative electrochemically reactive membranes designed to address three major challenges: (1) the engineering of electrocatalysts with …

Collision Dynamics Of Compound Droplets In Microchannels: A Combined Numerical And Data-Driven Study, S M Abdullah Al Mamun

Dissertations

Understanding and predicting the hydrodynamic interactions of micron-scale droplets is crucial in a wide range of industrial and real-life applications, including microfluidics, pharmaceutics, drug delivery, food science, and enhanced oil recovery. These multi-phase and multi-scale phenomena are further complicated by the presence of core droplets of an immiscible fluid within shell droplets, known as compound droplets. The collisions and interactions of droplets in emulsions are influenced by various physical and geometric parameters, leading to distinct rheological and dynamic responses. This research employs numerical methods for a systematic parametric study of both simple and compound droplet pair collisions under confined shear …

Capacitive Sensors With Ultra-Small Capacitance For Smart Measurement And Control Systems, Rustam Baratov, Farrux Jabbor O'G'Li Ko'charov

Chemical Technology, Control and Management

This article discusses methods of low capacitance measurement of capacitive sensors. The results of the study of the amplitude-frequency (AF) and phase-frequency (PF) response of measurement circuits of capacitive sensors for low capacitances measurement, consisting of RC - differentiating elements are presented. The input and output parameters of the differentiating circuit and the complex transfer function are analyzed. The research results show that low capacitances measurement by measuring the rectangular pulses duration is the most effective measurement method.

Production And Characterization Of Bio-Oil From Camelthorn Plant Using Slow Pyrolysis, Attia Attia Prof., Dina Aboelela Dr., Habibatallah Saleh Eng., Yasser Elhenawy Prof., Thokozani Majozi Prof., Mohamed Bassyouni Prof.

Biochemical Engineering

In this study, slow pyrolysis of the camelthorn plant process was conducted to produce bio-oil, biochar, and gas. The pyrolysis process was conducted between 400 and 550 °C under pressure 10 bar using a fixed bed reactor. The pyrolysis products were bio-oil, biogas, and biochar. These products were characterized using Fourier-transform infrared (FT-IR) model, gas analyzer, chromatographic analysis using GC–MS, and thermogravimetric analysis (TGA). The GC–MS results demonstrated composition of bio-oil, detecting several organic substances including levoglucosan, furan, acetic acid, phenol, and long-chain hydrocarbon. To further understand the chemical composition of bio-oil, FT-IR spectroscopy was conducted to determine functional groups. …

Inspection Planning Of Subsea Pipeline Using Risk-Based Inspection, Ni Luh Triska Adelia, Badrul Munir, Johny Wahyuadi Soedarsono

Journal of Materials Exploration and Findings

Pipelines are an important tool in oil and gas exploration. Pipeline is a transmission and liquid collection lines, including their accessories, which transport fluids from one plant to another. In transmission and collection process, there is a possibility of failure which can have minor to major impact on personnel injury, the environment and interrupt the business process. To maintain safety and to prevent accidents, the source and cause of failure needs to be calculated. Risk-based inspection (RBI) is a method that can be used to calculate the risk and determine the inspection planning both schedule and method, by combining the …

Natural Fiber Reinforced Composites For Sustainable Additive Manufacturing., Athira Nair Surendran

Electronic Theses and Dissertations

Carbon fiber is widely known for its exceptional strength, making it a sought-after material in composite manufacturing, especially with thermosets and thermoplastics. Its major applications span aerospace, wind turbines, sports equipment, automotive interior and exterior parts, robotics and medical equipment. Recently, carbon fiber filament manufacturing has gained attention due to the availability of desktop 3D printers and the versatility and customizability that comes with the realm of 3D printing. Commercial carbon fiber production, primarily from polyacrylonitrile (PAN), is energy-intensive and derived from crude oil, contributing to significant environmental impacts and poor recyclability. Alternatively, lignocellulosic natural fibers present a possible sustainable …

Fundamental Study Of Nonlinear Electrophoresis, Joseph Armakan Bentor

All Dissertations

Classical electrophoretic theory describes the linear response of particles suspended in Newtonian fluids under weak electric fields. When the electric field exceeds this weak limit, a nonlinear response arises due to non-uniform surface conduction over the curved particles. This nonlinear behavior introduces dependencies on fluid and particle properties not considered in the classical theory, offering potential advantages for microfluidic particle manipulation. While this phenomenon has been extensively studied theoretically and numerically in Newtonian fluids, experimental investigations have been relatively limited.

Fluid rheology can significantly alter particle dynamics under applied electric fields. Rheological properties like shear-thinning and elasticity which are not …

Experimental Study On The Effect Of Micro Concentrations Of Hybrid Nanofluids Through Microchannel Heat Sinks, Mohamed Salaheldin Elsherbiny, Moustafa Ali, Moatsem Shahin, Mahmoud El-Kady

Renewable Mechanical Energy

The current study examines the convective heat transfer coefficient experimentally. It assesses the performance of Al2O3, CuO, ZnO, and Ag/ distilled water nanofluids up to a tetra level of hybridization utilized in microprocessor cooling systems equipped with MCHS. An equal ratio of 50%, 33.3%, and 25% for di-, tri-, and tetra-nanofluids, respectively, with a focus on micro-volume fraction 0.025% and comparing it with 0.05%. Operating conditions were as follows: heat loading from 136.4 up to 196.4 watts; and flow rate from 0.35 up to 0.5 LPM. The findings showed that all types of mono nanofluids showed an increase in Nu …

Activity: Students Find Conceptual Errors In Ai Output, Janie Brennan

Generative AI Teaching Activities

Instructor asks ChatGPT questions related to a key concept to find one where ChatGPT has conceptual errors. Ask students to find the errors and explain them.

Investigating The Feasibility And Mechanisms Of Cold Spray Deposition Of Polymer-Based Powders On Fiber-Reinforced Composite Substrates, Nicholas Beau Mennie

Theses and Dissertations

Fiber-reinforced composites have become important structural components in industries such as aerospace and energy due to their high mechanical strength and relatively light structural weight. However, during operation, these materials can be prone to impact damage and disintegration. Effective protection via metalization and repair of composites would, therefore, reduce the cost and time for replacement parts. Polymer-based cold spray, while a relatively new technique, can be utilized to metalize and possibly repair composite materials subjected to impact-induced damage. In this work, studies involving polymers and composite cold spray were performed to enable the process of safeguarding, enhancing, or repairing various …

Interaction Of Particles With Plasma And Shock Produced By Pulsed Spark Discharge, Shomik Mukhopadhyay

Dissertations

Interactions of powders with high-temperature plasma and shockwaves occur in diverse scenarios, such as nuclear blasts, accidental industrial dust explosions, solid propellant combustion in explosive charges and when removing contaminants from surfaces. Electrostatic Discharge (ESD), known for generating shock and plasma, is a promising lab-scale technique for simulating these interactions. Studies with ESD involved placing powders near a spark-producing gap between electrodes and observing mechanical and chemical processes like particle motion and ignition. A limited range of spark conditions and material properties have been tested, which facilitated the development and validation of preliminary computational models describing this system. Significant gaps …

Analysis Of The Effect Of Different Surface Preparation Methods On Corrosion Resistance And Adhesion Strength Of Astm A36 Steel Substrate With Surface Tolerant Epoxy Paint As Coating Material, Irwan Wijaya Santoso, Daffa Aqila, Rini Riastuti, Rizal Tresna Ramadhani

Journal of Materials Exploration and Findings

In the industrial world, to extend the service life of materials, protection methods are carried out to slow down the material's corrosion rate. The protection method that is often used is the coating method. The coating method is a protection method by coating the substrate material using a coating material to prevent contact between the substrate material and the environment. In this research, the substrate material used is ASTM A36 steel and the coating material used is Surface Tolerant Epoxy paint. The independent variable used in this study lies in the surface preparation method which consists of: solvent cleaning, hand …

Synthesis Of Durable Zeolite 13x Insertion Coatings And Scaled-Up Experimental Demonstration For Co2 Capture, Daniel Jamil Hocheimy

Theses and Dissertations

Minimizing the energy requirement for capturing carbon dioxide (CO₂) from post-combustion sources is critical to efficient industrial decarbonization and subsequent mitigation of the effects of climate change. The current portfolio of CO₂ capture technologies includes absorption, membrane separation and packed bed adsorption, which suffer from high energy and temperature requirements, scalability, and location dependency issues. Adsorption-based systems could cater to these concerns; however, their current embodiments primarily use packed adsorbent bed design and electricity-driven vacuum pumps to regenerate them. While simple and easy to fabricate, these designs are not scalable and cannot use heat to regenerate them …

Assessment Of Risk Factors Related To Body Pain Complaints In Tanzania Construction Industry, Fatma K. Mohamed

Tanzania Journal of Engineering and Technology (TJET)

The construction industry is associated with risks that can result in musculoskeletal diseases. Although young male workers who are presumed to be healthy dominate the industry in Tanzania, body pain complaints have been widely reported. The aim of this study is to assess the prevalence and causes of body pains in workers. A cross-sectional study involving 396 workers was conducted. A chi square test was used for testing association of independent categorical variables and binary logistic regression analysis was used to determine predictors for body pain complaints. The results show that all study participants complained of at least one form …

Research On 3d Printing Resin Exposure Properties And Its Application On Centrifugal Microfluidic Platform Based On Fluorescence Detection, Zheng Qiao

LSU Doctoral Dissertations

This dissertation encapsulates significant advancements in the field of SLA 3D printing and centrifugal microfluidics. Central to the research is the development of a novel mathematical model for predicting trapped resin thickness in SLA 3D printing, a groundbreaking contribution that addresses a critical aspect of printing intricate structures. This model, the first to establish a mathematical relationship for resin thickness, is rooted in a comprehensive study of the resin curing process. The research leverages the concept of 'critical dosage' for resin curing, leading to a more refined and theoretically grounded approach for calculating curing thickness. Experimentation further validates the model, …

Globular Protein For Surface Modification Of Cellulosecontaining Materials, Nodira Saydaliyeva

Technical science and innovation

The purpose of this work is the chemical modification of cotton fabrics with natural globular protein. Modification was carried out in the process of finishing cotton fabrics, after decoction and bleaching in a continuous mode. The effect of modification on the strength, protein content and functional groups of cotton fabric has been studied. According to the results obtained using the AUTOGRAPH AGS-N machine, it was found that the modification of cotton fabrics with a solution of globular protein increases the strength of the treated fabrics, depending on the concentration of the modifier and the temperature regime. Treatment with a highly …

Dying Of Natural Silk Deglued By Various Methods, Venera Djavdatovna Khamidova

Technical science and innovation

Products made of natural silk are indispensable for their hygienic properties and will always be in great demand. To obtain an even and intense coloration on a textile material, it is necessary to ensure its effective preparation with the most complete removal of hydrophobic contaminants (both natural and silicone oils applied during the weaving process, lubricants, etc.), which hinder the dyeing of the substrate and reduce the color characteristics of the obtained colors. Therefore, the issue of preparing natural silk for dyeing is relevant. In view of the sensitivity of the main fiber-forming component of natural silk - fibroin to …

Thermo-Elasto-Plastic Stability Of Biaxially Loaded Hollow Rectangular Section Steel Beam-Columns With Applied Torsion, George Adomako Kumi

Civil & Environmental Engineering Theses & Dissertations

Presented herein is an experimental and theoretical study of biaxially loaded hollow rectangular section steel beam-columns with applied torsion at elevated temperatures. The theoretical analysis is based on a system of simultaneous materially nonlinear differential equations of equilibrium for which an iterative semi-analytic solution approach is formulated. Although the primary goal of this research is to study the influence of elevated temperatures on the steel member with the complex loading, rigorous analysis is also conducted of the member at ambient temperature for comparison. The experimental part of the study involves conducting tests on the members at both ambient and high …

Benchmarking Of A Sco2 Heat Exchanger Flow Loop, David Velasco

Doctoral Dissertations and Master's Theses

Heat transfer of supercritical carbon dioxide (sCO2) was studied experimentally by commissioning a sCO2 flow loop featuring a horizontal tube-in-tube counterflow heat exchanger with a circular cross section. The main objective was to establish experimental heat transfer research capabilities for sCO2 at Embry-Riddle Aeronautical University’s (ERAU) Thermal Science Lab. sCO2 experiences a drastic change in thermophysical properties near its critical point that results in unique heat transfer characteristics. The high pressures at which sCO2 exists make the large gradients in thermophysical and transport properties difficult to study, experimentally and numerically. However, understanding the heat transfer characteristics and thermophysical behavior of …

Cfd Study On Two-Phase Flow Patterns In A Pipe With 90º Elbow In Different Operating Conditions, Hagar Alm-Eldin Bastawissi, Mohammed Ahmed Khafagy, E. A. El Shenawy Prof. Dr., Ahmed M. Salem Dr

Journal of Engineering Research

Recently, CFD has offered a technological solution for modelling multi-phase flow in which we can make endless simulations with reduced expenses and effort in high accuracy results; we shall also mention that experimental studies have limitations for safety considerations when experimenting with flow in high temperature or pressure values or medium nature as in nuclear or chemical flows.In this paper, we used the ANSYS FLUENT CFD program to simulate the two-phase flow in a pipe to study the effect of attaching a 90-degree elbow fitting to the piping system, seeking to find out the change in the pattern and resulting …

Cost Estimation Proxy Models For Economic Evaluations In Petroleum Projects: A Case Study From The Onshore Gas Field In The Southern Coastal Tanzania Basin, Fulmence Kaborogo

Tanzania Journal of Engineering and Technology (TJET)

Petroleum economic evaluation involves estimating revenues from forecasted production profiles and field costs including capital expenditures (CAPEX), drilling expenses (DRILLEX), and operating expenses (OPEX). The existing cost-estimating tool requires several inputs making it time-intensive and difficult to use with few data during the early stages of projects. Majority of the previously developed time saving cost estimations proxy models rely on unrealistic assumptions that include uniform operational costs for different fields with a different number of wells, casings, and drilled depths. This work focused at developing proxy models that consider the variability of the development costs with different parameters. The developed …

Steminism: Analyzing Factors That Improve Retention Of Women In Stem, Kira Carter, Jane Kelley, Jason Vasser-Elong, Rc Patterson

Dissertations

Our co-authored research ‘Steminism: Analyzing Factors That Improve Retention for Women as STEM Majors’ analyzed factors that contributed to the retention of women in science, technology, engineering, and mathematics (STEM) programs at Missouri University of Science & Technology (Missouri S&T). Women make up half of the US population, and while careers in (STEM) are an integral part of the US economy, women are underrepresented in these career fields. The purpose of our dissertation is to address the underrepresentation of women in STEM majors. Our methodology included homogeneous sampling to collect qualitative data. More specifically, we consulted with academic advisors and …

Strategies To Mitigate Efflorescence In Walls Constructed Using Clays Bricks; A Review Article, Marwa Abdulkareem. Anber, Soran Abdulrahman Ahmad, Naros Rahman Mahmoud, Kawan Fuoad. Kayani, Mohammed Ali Abdulrehman

Al-Esraa University College Journal for Engineering Sciences

_{The construction of buildings, especially residential housing for communities, is a significant industry on a global scale. Masonry units such as bricks, blocks, and stones are often utilized materials. Bricks are highly regarded because to their widespread availability, cost-effectiveness, and excellent insulating capabilities. Nevertheless, the presence of efflorescence presents a difficulty in the construction of brick walls. Efflorescence refers to the process in which salts move to the outer layer of the brick, resulting in the formation of white deposits and negatively impacting its visual appeal. Efflorescence is caused by various circumstances, such as the existence of salts in bricks, …}