Chemical Engineering Commons^™

Intelligent Method Of Dynamic Control For A Class Of Stochastic Nonlinear Systems, Isamidin Khakimovich Siddikov, Davronbek Abdalimovich Khalmatov, Gulchekhra Rakhimjanovna Alimova, Dilnoza Rakhmanovna Khushnazarova

Chemical Technology, Control and Management

The paper considered the problems of researching the stabilisation system and backstepping control of stochastic nonlinear systems. The characteristics of stochastic nonlinear dynamic control systems are random signals with normal lawful distribution, which significantly complicates task control. In stochastic control, it is necessary to determine the trajectories of the control variables in order to achieve the desired control objective at minimum cost. Since the mathematical equations of stochastic nonlinear systems are not always constant, not every model-based controller can be accurate. Therefore, in this work, a neuro-fuzzy network is used to evaluate the parameters of the control system with backstepping, …

Reinforcement Learning In A Virtual World: A Study Of Ppo And Sac Within Unity Ml Agents, Rufat Mammadzada

Chemical Technology, Control and Management

This study explores the use of Unity3D as a versatile platform for developing, training, and evaluating intelligent agents through reinforcement learning. Leveraging the Unity ML-Agents Toolkit, a dynamic 3D environment was created to examine agent learning behavior using two advanced algorithms: Proximal Policy Optimization (PPO) and Soft Actor-Critic (SAC). The simulation environment consisted of navigable terrain bounded by red borders, with collectible blue balls serving as rewards and a purple cube representing the agent. A carefully designed reward system was implemented to encourage goal-directed behavior and penalize inefficiency, while time constraints introduced an additional challenge requiring both precision and speed. …

Development Trends And Priority Research Fields Of Electrochemical Discipline In The 15th Five Year Plan Period, Lin Zhuang, Wen-Bin Cai, Heng-Xing Ji, Qing Li, Gong-Wei Wang, Sen Xin, Qing Zhao, Fang-Yi Cheng, Yu-Guo Guo, Lan-Qun Mao, Yang Tian, Fei Wu, Li-Min Zhang, Yan Xiang, Jin-Song Hu, Rui Cao, Li Xiao, Hua-Bing Tao, Wei Xing, Dong-Ping Zhan, Hong-Gang Liao, Mei-Ling Xiao, Bin Ren, Zhang-Quan Peng, Rui Wen, Xiang Wang, Yue-Feng Song, Hou-Fu Lv, Bao-Yu Xia, Guo-Xiong Wang, Jun Cheng, Zhi-Pan Liu, Min Zhou, Bing Huang, Cun-Pu Li, Yu-Qin Zou, Shuang-Yin Wang, Hai-Bo Lin, Zi-Dong Wei

Journal of Electrochemistry

In fulfillment of the national science-and-technology development agenda, the Department of Chemical Sciences of the National Natural Science Foundation of China (NSFC) convened the Strategic Symposium on the Fifteenth Five-Year (2026–2030) Development Plan for Electrochemistry held in Xiamen on 29 August, 2025—the culminating year of the Fourteenth Five-Year (2021–2025) Development Plan. More than forty leading experts in the field of electrochemistry participated with spanning nine thematic fronts: Interfacial Electrocatalysis, Interfacial Electrochemistry for Energy Storage, Bioelectrochemistry, Electrochemistry of Hydrogen Energy, Electrochemical Micro-/Nano-Manufacturing, Operando Electrochemical Characterization, Electro-Thermal Coupling Catalysis, Theoretical and Computational Electrochemistry, and Electrochemical Synthesis. The forum assembled China’s foremost electrochemical …

Bridging Materials And Energy Storage Mechanisms In Zn-I2 Batteries, Rong-Qi Liu, Wen-Shuo Shang, Jin-Tao Zhang

Journal of Electrochemistry

Zinc-iodine (Zn-I₂) batteries have emerged as a compelling candidate for large-scale energy storage, driven by the growing demand for safe, cost-effective, and sustainable alternatives to conventional systems. Benefiting from the inherent advantages of aqueous electrolytes and zinc metal anodes, including high ionic conductivity, low flammability, natural abundance, and high volumetric capacity, Zn-I₂ batteries offer significant potential for grid-level deployment. This review provides a comprehensive overview of recent progress in three critical domains: positive-electrode engineering, zinc anode stabilization, and in situ characterization methods. On the cathode side, anchoring iodine to conductive matrices effectively mitigates polyiodide shuttling and enhances …

Significantly Enhanced Oxygen Reduction Reaction Activity In Co-N-C Catalysts Through Synergistic Boron Doping, Chang Lan, Jing-Sen Bai, Xin Guan, Shuo Wang, Nan-Shu Zhang, Yu-Qing Cheng, Jin-Jing Tao, Yu-Yi Chu, Mei-Ling Xiao, Chang-Peng Liu, Wei Xing

Journal of Electrochemistry

The weak adsorption energy of oxygen-containing intermediates on Co center leads to a considerable performance disparity between Co-N-C and costly Pt benchmark in catalyzing oxygen reduction reaction (ORR). In this work, we strategically engineer the active site structure of Co-N-C via B substitution, which is accomplished by the pyrolysis of ammonium borate. During this process, the in-situ generated NH₃ gas plays a critical role in creating surface defects and boron atoms substituting nitrogen atoms in the carbon structure. The well-designed CoB₁N₃ active site endows Co with higher charge density and stronger adsorption energy toward oxygen species, …

Series Reports From Professor Wei’S Group Of Chongqing University: Advancements In Electrochemical Energy Conversions (2/4): Report 2: High-Performance Water Splitting Electrocatalysts, Ling Zhang, Wang-Yang Wu, Qiu-Yue Hu, Shi-Dan Yang, Li Li, Rui-Jin Liao, Zi-Dong Wei

Journal of Electrochemistry

The unavailability of high-performance and cost-effective electrocatalysts has impeded the large-scale deployment of alkaline water electrolyzers. Professor Zidong Wei’s group has focused on resolving critical challenges in industrial alkaline electrolysis, particularly elucidating hydrogen and oxygen evolution reaction (HER/OER) mechanisms while addressing the persistent activity-stability trade-off. This review summarizes their decade-long progress in developing advanced electrodes, analyzing the origins of sluggish alkaline HER kinetics and OER stability limitations. Professor Wei proposes a unifying “12345 Principle” as an optimization framework. For HER electrocatalysts, they have identified that metal/metal oxide interfaces create synergistic “chimney effect” and “local electric field enhancement effect”, enhancing selective …

Local Electric Fields Coupled With Cl− Fixation Strategy For Improving Seawater Oxygen Reduction Reaction Performance, Yu-Rong Liu, Miao Zhang, Yan-Hui Yu, Ya-Lin Liu, Jing Li, Xiao-Dong Shi, Zhen-Ye Kang, Dao-Xiong Wu, Peng Rao, Ying Liang, Xin-Long Tian

Journal of Electrochemistry

Development of robust electrocatalyst for oxygen reduction reaction (ORR) in a seawater electrolyte is the key to realize seawater electrolyte-based zinc-air batteries (SZABs). Herein, constructing a local electric field coupled with chloride ions (Cl⁻) fixation strategy in dual single-atom catalysts (DSACs) was proposed, and the resultant catalyst delivered considerable ORR performance in a seawater electrolyte, with a high half-wave potential (E_1/2) of 0.868 V and a good maximum power density (Pmax) of 182 mW·cm⁻² in the assembled SZABs, much higher than those of the Pt/C catalyst (E_1/2: 0.846 V; Pmax: 150 mW·cm^{−2 …}

Detecting Electrical Submersible Pump (Esp) Failures And Estimating Run Life Using Artificial Neural Networks, Mostafa Ahmed Sobhy

Theses and Dissertations

Electric Submersible Pumps (ESPs) are one of the important artificial lift methods for sustaining production in mature and high-water-cut wells; but may suffer frequent failures due to mechanical, electrical, hydraulic, chemical, and operational failures. These failures can yield substantial deferred production and intervention costs. Plenty of ESP installations are fitted with downhole sensors. Yet, it is observed that the current industry practice underutilizes the wealth of available sensor and operational data and lacks standardized, explainable failure-type identification and classification.

In this thesis, a comprehensive Machine Learning (ML) and Deep Learning (DL) framework was introduced for ESPs that simultaneously estimates remaining …

Optimizing Beer Fermentation Through Intelligent Control, Azizbek Nodirbekovich Yusupbekov, Mirjalol Yusupov

Chemical Technology, Control and Management

This paper presents an intelligent control approach for optimizing the beer fermentation process using fuzzy logic and adaptive neuro-fuzzy inference systems. By incorporating multivariable inputs—temperature error and pH deviation—the proposed system effectively handles the nonlinear dynamics and biological variability inherent in fermentation. Simulation results demonstrate improved control accuracy, responsiveness, and robustness compared to conventional methods, making the approach suitable for integration in modern brewery automation systems.

Application Of Neural Networks For Intelligent Processing Of Sensor Signals In The Control Of Technological Process Parameters, N.R. Yusupbekov, Yu.Sh. Avazov, G.Kh. Rashidov

Chemical Technology, Control and Management

This scientific article investigates the problem of analyzing technological process parameters in the fields of chemistry, energy, and metallurgy based on sensor data and applying intelligent signal processing methods. The main objective is to evaluate the effectiveness of artificial intelligence and deep learning models for intelligent analysis, forecasting, and anomaly detection of data obtained from sensors. Time-series data collected from industrial sensors were analyzed using LSTM (Long Short-Term Memory) and Autoencoder neural networks, as well as the Kalman filter. At the first stage of the study, sensor signals were denoised and their true state was estimated using the Kalman filter. …

Algorithms For The Synthesis Of Adaptive Control Systems Based On The Speed-Gradient Method, Oxunjon Boborayimov

Chemical Technology, Control and Management

This paper discusses the synthesis algorithms for adaptive control systems based on the speed-gradient method. Adaptive control systems with implicit reference and adjustable models are synthesized using speed-gradient techniques, which reduce the requirements for the main control loop structure and the completeness of measurement data. Stable adaptive decentralized control algorithms are developed for a class of interconnected systems with nonlinear local dynamics and uncertainties, ensuring the stability of individual subsystems and the overall system while accounting for their interactions. To incorporate inter-subsystem interactions into the overall control law, an adaptation algorithm based on the speed-gradient method is introduced. A synthesis …

Finding The Shortest And Optimal Path With Metaheuristic And Madm Methods, Narmin Ibrahim Hasanli

Chemical Technology, Control and Management

The article had described a method for finding the shortest and most optimal path among cities. The data had been taken from the TSPLIB library, which had provided standard examples for the Traveling Salesman Problem. This approach had integrated the advantages of the meta-heuristic technique and the Multi Attribute Decision Making method to solve the problem effectively. In the first stage, the population based meta-heuristic method ACO (Ant Colony Optimization) had found optimal solutions in large search spaces. The use of pheromone trails, heuristic information and an iterative search process had given the opportunity to find the best or near-best …

Modeling Of Urea Drying And Granulation Process In Fluidized Bed, Jalolitdin Pakhritdinovich Mukhitdinov, Aleksey Viktorovich Schulz

Chemical Technology, Control and Management

This article is devoted to the mathematical modeling of urea drying and granulation processes in a fluidized bed. A brief description is provided for the functional blocks included in the mathematical model, along with the required parameters that form an integrated representation of the technological process. The SR-POLAR model is used to describe a phase equilibrium between the components involved. The interconnections between functional blocks are shown in the process flow diagram. Block diagrams for modeling a multi-chamber granulation unit and the cooling system for the resulting granules are presented. Granule growth in the fluidized bed is described using a …

Algorithms For Assessing Soil Salinity Levels Based On Remote Sensing Imagery, Bobomurod Mamitjonovich Tojiboev

Chemical Technology, Control and Management

This article investigates methods for assessing soil salinity levels based on satellite (remote sensing) imagery and their calculation algorithms. Determining the degree of salinity plays a crucial role in the rational use of land resources and increasing agricultural efficiency. The study analyzes indices for determining soil salt content using remote sensing technologies, particularly multispectral images obtained from satellite systems such as Landsat and Sentinel (for example, SI - Salinity Index, NDVI - Normalized Difference Vegetation Index, and others). Furthermore, algorithms are developed based on these indices that enable automatic determination of salinity assessments. Artificial intelligence, machine learning, and geographic information …

Research And Development Of Intelligent Measurement Systems, Odil Abdujalilovich Jumaev, Mahmudov Giyosjon Baqoyevich

Chemical Technology, Control and Management

The article discusses modern methods for developing intelligent measuring systems. Intelligent measuring systems are systems based on intelligent technologies that not only accurately measure physical or chemical quantities, but also have the ability to self-analyze, diagnose and make management decisions. The article comprehensively examines the architecture, components of such systems, the organization of their software and hardware, the relationship of sensors and artificial intelligence algorithms. It also analyzes the practical application and prospects of intelligent measuring systems in such areas as industry, medicine, energy, ecology, transport.

Modern Methods Of Self-Monitoring, Diagnostics, And Fault Tolerance In Flow Measurement Systems, Elbek Ortiqov

Chemical Technology, Control and Management

This article investigates various methods and tools for self-monitoring and fault tolerance in flow measurement transducers used in industrial processes. The study focuses on key techniques such as the use of redundancy, generation of reference values, analysis of measurement signals, and control of disturbance variables. These methods allow transducers to detect potential faults, ensure reliable operation, and maintain measurement accuracy even under adverse conditions. The article highlights how self-monitoring contributes to improving system safety, increasing reliability, and reducing downtime. It also discusses the integration of intelligent monitoring systems that support predictive maintenance and real-time diagnostics. Fault-tolerant sensors with self-monitoring capabilities …

Synthesis Of A Control System For Thermal Energy Facilities Using The Quantum Photon Spin Method, Isomiddin Siddikov, N.S Yakubova

Chemical Technology, Control and Management

Increasing energy efficiency and reducing fuel consumption in the process of generating electricity and heat at thermal power plants is one of the urgent tasks. Such systems operate under conditions of random changes in external and internal influences, as well as measurement uncertainties, which reduce the quality of control. In order to overcome this problem, it was proposed to develop an intelligent control system using the quantum photon-spin method to control technological units of thermal power plants. In the proposed approach, a multi-dimensional heating boiler device was taken as a control object, and the simulation modeling of the control system …

Increasing The Robustness Of A Control System For A Complex Dynamic Plant By Correcting Nonlinearity In The Warping Process, Tukhtamurod Khayitmurodovich Avezov, Zokhid Ergashboyevich Iskandarov

Chemical Technology, Control and Management

The paper discusses the challenges of enhancing the robustness of a control system for a complex dynamic plant by addressing nonlinearity in the warping process. Devices that ensure the stability of the control system against parameter non-stationarity on the warping machine are referred to as state controllers. The operating principle of these devices relies on providing artificial nonlinearity to the rear connection circuit of the control system's actuator. However, this nonlinearity is implemented using components that consider the parameters of low control quality. Therefore, it is necessary to continuously adjust the nonlinearity parameters to, on one hand, reduce the load …

Evaluation Of Deep Learning Techniques In Road Sign Recognition, Latafat Abbas Gardashova, Haji Fakhraddin Hajiyev

Chemical Technology, Control and Management

Deep learning has transformed the computer vision field and greatly improved the performance and efficiency of road sign recognition systems. This research compares different deep learning methods, such as Convolutional Neural Networks (CNNs), Recurrent Neural Networks (RNNs), and hybrid models, in terms of their ability to effectively detect and classify road signs under various conditions. The study compares performance measures such as accuracy, processing speed, and robustness to environmental conditions like low lighting, occlusion, and adverse weather. The results show that CNN-based methods, especially those with transfer learning and ensemble techniques, have better performance in real-time scenarios. Problems like computational …

Superhydrophilic Porous Coooh Nano-Architecture With Abundant Oxygen Vacancies For Enhanced Urea Electrooxidation At Ampere-Level Current Densities, Wen-Jing Lv, Xiao-Man Tang, Xue-Tong Wang, Wen-Cai Liu, Jian-Wen Zhu, Guo-Jing Wang, Yuan-Zhi Zhu

Journal of Electrochemistry

The conversion of urea-containing wastewater into clean hydrogen energy has gained increasing attention. However, challenges remain, particularly with sluggish catalytic kinetics and limited long-term stability of urea oxidation reaction (UOR). Herein, we report the loosely porous CoOOH nano-architecture (CoOOH LPNAs) with hydrophilic surface and abundant oxygen vacancies (O_v) on carbon fiber paper (CFP) by electrochemical reconstruction of the CoP nanoneedles precursor. The resulting three-dimensional electrode exhibited an impressively low potential of 1.38 V at 1000 mA·cm⁻² and excellent durability for UOR. Furthermore, when tested in an anion exchange membrane (AEM) electrolyzer, it required only 1.53 V at …

Design And Optimization Of Anode Catalysts For Direct Ethanol Fuel Cells: Advances And Challenges In C-C Bond Activation And Selective Modulation Of The C1 Pathway, Kai-Chi Qin, Meng-Tian Huo, Yu Liang, Si-Yuan Zhu, Zi-Hao Xing, Jin-Fa Chang

Journal of Electrochemistry

Direct ethanol fuel cells (DEFCs) are a promising alternative to conventional energy sources, offering high energy density, environmental sustainability, and operational safety. Compared to methanol fuel cells, DEFCs exhibit lower toxicity and a more mature preparation process. Unlike hydrogen fuel cells, DEFCs provide superior storage and transport feasibility, as well as cost-effectiveness, significantly enhancing their commercial viability. However, the stable C–C bond in ethanol creates a high activation energy barrier, often resulting in incomplete electrooxidation. Current commercial platinum (Pt)- and palladium (Pd)-based catalysts demonstrate low C–C bond cleavage efficiency (

Investigating Resilience Of Cyberattack Detection Using Lyapunov-Based Economic Model Predictive Control To Data Poisoning, Helen Durand, Akkarakaran Francis Leonard

Chemical Engineering and Materials Science Faculty Research Publications

Cyberattacks may be performed on process control systems due to their integration of networking and computing with physical systems. Prior work in our group has developed detection strategies for nonlinear systems under sensor, actuator, and combined sensor and actuator attacks which can ensure, under characterizable conditions, that attacks can be detected before they cause safety issues. However, this work did not take into account the potential that an attacker could attempt to provide data to a process that causes an attack to remain undetected but that also is consistent with different process dynamics than those which the process has. This …

Response Of Dynamic Processes With Control Implemented On A Noisy Quantum Computer, Shilpa Narashimhan, Dominic Messina, Henrique Oyama, Helen Durand

Chemical Engineering and Materials Science Faculty Research Publications

A major challenge to determining the applicability (and potential outperformance over classical computers) of a quantum computer (QC) within chemical manufacturing processes is quantum noise. Computations by a QC are error-prone due to the influence of quantum noise inherent to the hardware. Errors in control inputs may destabilize a chemical process and lead to unsafe conditions for manufacturing personnel and the environment. The response of a process with control implemented on a QC to errors due to noise must be investigated thoroughly. In this work, the impacts of control input errors due to quantum noise on a process are modeled …

Heuristic Strategies For Process Stabilization Using Proportional Control Implemented By A Noisy Quantum Simulator, Keshav Kasturi Rangan, Helen Durand

Chemical Engineering and Materials Science Faculty Research Publications

Processing and storage demands of industrial processes are causing fields such as optimization, scheduling, and control to assess the effectiveness of quantum devices in their applications. A key objective of control systems is to ensure process safety. This paper focuses on the potential of quantum devices to compute control inputs that maintain system safety despite sources of nondeterminism inherent to currently available quantum devices (quantum noise). In our previous work, we employed a quantum simulator to assess whether a quantum implementation of a proportional (P) control law could stabilize a single-input/single-output system under quantum noise approximated from a real quantum …

Tools To Design Algorithms For Implementing Control Over Quantum Computers, Shilpa Narashimhan, Jihan Abou Halloun, Kip Nieman, Helen Durand

Chemical Engineering and Materials Science Faculty Research Publications

Quantum computers (QCs) may find future applications within control systems that operate manufacturing processes. For application within control engineering, quantum algorithm development must be led by control engineers. However, control engineers may face challenges in designing quantum algorithms for control engineering problems. In this work, we provide several path-finding studies that leverage engineering tools such as optimization, encryption, and computational "short-cuts" toward making algorithm design for QC easier for control engineers.

Techno-Enviro-Economic Approach For Electrification Of Rural And Shrimp Farming Regional Development Of An Isolated Island In Indonesia By Utilizing Hybrid Renewable Energy Systems, Fiqih Akbar Wijaya, Mohammad Akita Indianto

Journal of Materials Exploration and Findings

One of the challenges in developing and archipelagic countries such as Indonesia is maintaining energy demand in rural and isolated areas due to difficulties in electrical distribution. For instance, in areas like Bawean Island, no additional electricity capacity has been introduced in the past year, leading to an unmet potential customer demand. One of the possible options is by utilizing Hybrid Renewable Energy Systems (HRES) that are integrated with existing fossil fuel-based energy systems to support the growing energy demand in the remote island. A case study in Bawean Island is conducted with the projected energy demand covers the energy …

Regulating The Amount Of Graphene Oxide For Enhanced Capacitive Energy Storage Of Mof Derived Materials, Yong-Ji Qin, Jing-Quan Yang, Hao Wang, Mei-Ling Lian, Pei-Pei Jia, Jun Luo, Xi-Jun Liu, Jun-Feng Liu

Journal of Electrochemistry

In pursuit of more efficient and stable electrochemical energy storage materials, composite materials consisting of metal oxides and graphene oxide have garnered significant attention due to their unique structures and exceptional properties. Graphene oxide (GO), a two-dimensional material with an extremely high specific surface area and excellent conductivity, offers new possibilities for enhancing the electrochemical performance of metal oxides. In this work, we synthesized metal- organic framework (MOF) and GO composites by regulating the amount of GO, and successfully prepared composites of metal oxides supported by nitrogen-doped carbon frameworks and GO through a simple one-step calcination process. Based on the …

A Smart System For Detecting Anatomic And Histological Symptoms Of Diseased Agricultural Plants, Rustam Baratov, Himola Sunnatillayeva, Alimardon Mamatovich Mustafoqulov

Chemical Technology, Control and Management

This study describes a novel agricultural plant disease detecting smart system, capable of handling measured plant body parameters and images received by high resolution camera at the same time. The proposed plant disease detection method is based on evaluation of the signals received by measured and controlled plant body physical parameters like resistance, temperature and capacitance of the plant stem and image processing. An analogue plant model based on an electrical circuit with distributed parameters was developed. In addition, in the article the block diagram of the smart system for the early detection of plant diseases, the circuit diagram, its …

Development And Experimental Validation Of A Non-Invasive Blood Group Detection System, Nurath K. Nurudini

Tanzania Journal of Engineering and Technology (TJET)

An individual's blood group consists of red blood cell antigens whose composition is determined by protein presence, antigen structure, and gene series. Persons aged above six months have significant anti-A and/or anti-B in their serum. During transplantation and transfusion, ABO blood group identification is the most essential factor. The conventional method involves drawing blood samples from patients, and the blood group is determined based on the antigen-antibody reaction. This method consists of adding chemical reagents. However, this requires time of operation, and throughput analysis is high, and the process is also challenging to interpret. Accurate and rapid identification of blood …

Energy Optimal Coverage Motion Trajectory Generation Using A Fourth-Order Motion Profile, Mathias Halinga

Tanzania Journal of Engineering and Technology (TJET)

Industrial machines are widely used in manufacturing sector to manufacture several products to meet customer demands. Most of these industries runs all the time throughout a day leading to high operating cost. To cut costs and satisfy customer demand for precise products, industrial machines’ motion generation is important in improving machine motion precision while using less energy. This study presents a coverage motion energy optimization which is generated by linear interpolation of each segment described by the fourth-order motion profile. The phase changes in the profile are attained with continuity of machine kinematic limits jerk, acceleration, and velocity, which are …