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Articles 23941 - 23970 of 27383
Full-Text Articles in Engineering
Preparation And Photoelectrochemical Properties Of Fe-Doped Tio2 Nanotube Arrays, Jing Li, Lan Sun, Hui-Fang Zhuang, Cheng-Lin Wang, Rong-Gui Du, Chang-Jian Lin
Preparation And Photoelectrochemical Properties Of Fe-Doped Tio2 Nanotube Arrays, Jing Li, Lan Sun, Hui-Fang Zhuang, Cheng-Lin Wang, Rong-Gui Du, Chang-Jian Lin
Journal of Electrochemistry
The Fe-doped TiO2 nanotube arrays were fabricated in Fe(NO3)3-HF mixing solutions by electrochemical anodic oxidation method,and characterized by FESEM,Raman,XPS and DRS.The effect of Fe concentratiions on photoelectrochemical property of the arrays was also investigated.The diameters and lengths of Fe-doped TiO2 nanotube arrays were 50~90 nm and about 200 nm,respectively.Compared with the undoped TiO2 nanotube arrays,the absorption edge of Fe-doped TiO2 nanotube arrays appeared red shifting.The more Fe content,the larger red shifting,in addition,the photocurrent of Fe-doped TiO2 nanotube arrays increased obviously.
Cyclic Voltammetry And In Situ Ftir Studies Of Cyanide Adsorption On Nanostructured Au Film Electrode In Alkaline Solutions, Chun-Hua Zhen, Chun-Jie Fan, Shi-Gang Sun
Cyclic Voltammetry And In Situ Ftir Studies Of Cyanide Adsorption On Nanostructured Au Film Electrode In Alkaline Solutions, Chun-Hua Zhen, Chun-Jie Fan, Shi-Gang Sun
Journal of Electrochemistry
The adsorption of cyanide(CN-) on electrodes of nanometer scale thin film of gold supported on glassy carbon(nm-Au/GC) in alkaline solutions were investigated using cyclic voltammetry and in situ FTIR spectroscopy.It has revealed that the electrodeposited nanostructured Au thin film exhibited AIREs(abnormal infrared effects) for CN-adsorption,which manifested 3 nonlinear IR spectral features: inversion of the direction of CN-band,enhancement of IR absorption of adsorbed CN-species(about 39.2 folds) and increase in the FWHM(full width at half maximum) of CN-band.
Quick Tester With Usb Interface For The Corrosion Protection Properties Of Organic Coating, Xiang-Dong Zhuo, Chang-Jian Lin
Quick Tester With Usb Interface For The Corrosion Protection Properties Of Organic Coating, Xiang-Dong Zhuo, Chang-Jian Lin
Journal of Electrochemistry
According to the principle of multiple dynamic potential scaning polarization,a quick tester with USB interface for the fast study of corrosion resistance properties of organic coating/ metal system has been developed.This tester is portable,facile,practical,and has a strong function for data collection and data treatment.It is not only suitable for the accelerated test in laboratory,but also for the quick test and evaluation to the corrosion resistance of the organic coating/metal system in industrial spots.
Electrochemical Performances Of Copper/Activated Carbon Composites, Lan-Ting Li, Qiang Xie, Wen Yan, Yan-Yan Wang, Wen-Wen Xing
Electrochemical Performances Of Copper/Activated Carbon Composites, Lan-Ting Li, Qiang Xie, Wen Yan, Yan-Yan Wang, Wen-Wen Xing
Journal of Electrochemistry
The development and improvement of electrode materials can result in the enhancement of the performances of electrochemical capacitor.In this paper various copper/activated carbon composites were prepared in the presence of different amounts(from 0% to 40%) of copper nitrate from bituminous coal.Then different electrodes were prepared from copper oxide,activated carbon and copper/activated carbon composites,respectively,and were characterized by cyclic voltammetry,alternative current(AC) impedance,charge-discharge at constant current and maintenance of the self-potential.The results showed that the proper amount of copper in copper/activated carbon composites positively influenced the electrochemical performances of electrodes,and the capacitance of copper/activated carbon composites was larger than that of the total …
Preparation Of Zn-Ni Alloy Whisker By Electrochemical Method, Zhen-Hai Liang, Xi-Hua Xia
Preparation Of Zn-Ni Alloy Whisker By Electrochemical Method, Zhen-Hai Liang, Xi-Hua Xia
Journal of Electrochemistry
The Zn-Ni alloy whiskers were prepared by electrochemical method and were characterized by XRD, SEM and EDS methods. The results showed that Ni5Zn21 and Ni3Zn22 whiskers were obtained with the length of 2~4 μm and the diameter of 250 nm, thereby the rations of length/diameter fell between 8 and 16. The electrochemical behavior was investigated by cyclic voltammetry method simultaneously. A new method was provided on whisker preparation based on this work.
Synthesis And Electrochemical Characteristics Of Li[Li(0.167)Mn(0.583)Ni(0.25)]O2 Cathode Material, Ling-Yan Yu, Wei-Hua Qiu, Fang Lian, Jia-Yuan Huang, Xao-Li Kang, Wei Liu
Synthesis And Electrochemical Characteristics Of Li[Li(0.167)Mn(0.583)Ni(0.25)]O2 Cathode Material, Ling-Yan Yu, Wei-Hua Qiu, Fang Lian, Jia-Yuan Huang, Xao-Li Kang, Wei Liu
Journal of Electrochemistry
The cathode material of Li[Li0.167Mn0.583Ni0.25]O2 was synthesized by low-heat solid state reaction.The results of XRD and FESEM indicated that the powders of the material were well crystallized with the uniform diameters ranging from 60 nm to 100 nm and could be indexed as α-NaFeO2 structure(R3-m space). Galvanostatic charge-discharge tests showed that the electrode delivered the capacity of about 120 mAh/g with good cyclability when cycled in 2.5~4.4V at 0.5C. When the cut-off potential was set up to 4.6V, the cathode delivered much larger capacities with the maximum of 234 mAh/g. It was …
A Study Of Co2 Absorption Using Jet Bubble Column, Setiadi Setiadi, Nita Tania Hadiyani, Hantizen Hantizen, Dijan Supramono
A Study Of Co2 Absorption Using Jet Bubble Column, Setiadi Setiadi, Nita Tania Hadiyani, Hantizen Hantizen, Dijan Supramono
Makara Journal of Technology
A Study of CO2 Absorption Using Jet Bubble Column. The phenomenon of plunging jet gas-liquid contact occurs quite often in nature, it's momentum carries small air bubbles with it into the reactor medium. The momentum of the liquid stream can be sufficient to carry small bubbles completely to the bottom of the vessel. A stream of liquid falling toward a level surface of that liquid will pull the surrounding air along with it. It will indent the surface of the liquid to form a trumpet-like shape. If the velocity of the stream is high enough, air bubbles will be pulled …
The Development Of Inverter Fuzzy Logic Control For Induction Motor Control By Vector Control Method In Electric Vehicle, Era Purwanto, Mohammad Ashary, Subagio Subagio, Mauridhi Heri Purnomo
The Development Of Inverter Fuzzy Logic Control For Induction Motor Control By Vector Control Method In Electric Vehicle, Era Purwanto, Mohammad Ashary, Subagio Subagio, Mauridhi Heri Purnomo
Makara Journal of Technology
The development of Inverter Fuzzy Logic Control for Induction Motor Control by Vector Control Method in Electric Vehicle. In response to concerns about energy cost, energy dependence, and environmental damage, a rekindling of interest in electric vehicles (EV’s) has been obvious. Thus, the development of power electronics technology for EV’s will take an accelerated pace to fulfill the market needs, regarding with the problem in this paper is presented development of fuzzy logic inverter in induction motor control for electric vehicle propulsion. The Fuzzy logic inverter is developed in this system to directed toward developing an improved propulsion system for …
Internet Congestion Control System, Pranoto Hidaya Rusmin, Carmadi Machbub, Agung Harsoyo, Hendrawan Hendrawan
Internet Congestion Control System, Pranoto Hidaya Rusmin, Carmadi Machbub, Agung Harsoyo, Hendrawan Hendrawan
Makara Journal of Technology
Internet Congestion Control System. Internet congestion occurs when resource demands exceeds the network capacity. But, it is not the only reason. Congestion can happen on some users because some others user has higher sending rate. Then some users with lower sending rate will experience congestion. This partial congestion is caused by inexactly feedback. At this moment congestion are solved by the involvement of two controlling mechanisms. These mechanisms are flow/congestion control in the TCP source and Active Queue Management (AQM) in the router. AQM will provide feedback to the source a kind of indication for the occurrence of the congestion …
Substrates Preparation From Woody Tropical Waste Biomass For Biohydrogen Production, Dwi Susilaningsih, Theresia Umi Harwati, Khairul Anam, Yopi Yopi
Substrates Preparation From Woody Tropical Waste Biomass For Biohydrogen Production, Dwi Susilaningsih, Theresia Umi Harwati, Khairul Anam, Yopi Yopi
Makara Journal of Technology
Substrates Preparation from Woody Tropical Waste Biomass for Biohydrogen Production. Addressing to the global warming problem, energy crisis and pollution, hydrogen production by micro-organisms using biotechnological approach should be considered, since it fulfils the recent society requirement to safely produce, renewable and environmental friendly energy. Hydrogen is one of the most promising green energy sources, because it is easily converted to electricity and cleanly combustible. There are three types of micro-organisms for hydrogen production, the first is cyanobacteria through the photosynthesis process, the second is anaerobic bacteria, which use organic substances as electron donor and energy and convert them to …
Building Fire Safety Audit At Faculty X, University Of Indonesia, Year 2006, Fatma Lestari, Rm. Yodan Amaral Panindrus
Building Fire Safety Audit At Faculty X, University Of Indonesia, Year 2006, Fatma Lestari, Rm. Yodan Amaral Panindrus
Makara Journal of Technology
Building Fire Safety Audit at Faculty X, University of Indonesia, Year 2006. Fire may cause loss of life, material and valuable assets. The objective of this study is to conduct audit for fire safety and emergency response in the building at Faculty X, University of Indonesia, Depok. The audit results on the building fire safety facilities including emergency response and preparedness are then compared to the Building Code Australia (BCA) and Indonesian regulation on the building fire safety (Kep.MenPU.No 10 and 11/KPTS/2000). The building selected are Building A, B, C, D, F and G. Building classification for A, B, D, …
Ad Hoc On-Demand Distance Vector (Aodv) Routing Protocol Performance Evaluation On Hybrid Ad Hoc Network: Comparison Of Result Of Ns-2 Simulation And Implementation On Testbed Using Pda, Riri Fitri Sari, Abdusy Syarif, Bagio Budiardjo
Ad Hoc On-Demand Distance Vector (Aodv) Routing Protocol Performance Evaluation On Hybrid Ad Hoc Network: Comparison Of Result Of Ns-2 Simulation And Implementation On Testbed Using Pda, Riri Fitri Sari, Abdusy Syarif, Bagio Budiardjo
Makara Journal of Technology
Ad Hoc on-Demand Distance Vector (AODV) Routing Protocol Performance Evaluation on Hybrid Ad Hoc Network: Comparison of Result of Ns-2 Simulation and Implementation on Testbed using PDA. In Mobile Ad hoc NETwork (MANET), node supplemented with wireless equipment has the capacity to manage and organise autonomously, without the presence of network infrastructures. Hybrid ad hoc network, enable several nodes to move freely (mobile) to create instant communication. Independent from infrastructure. They could access the Local Area Network (LAN) or the Internet. Functionalities of ad hoc network very much dependent on the routing protocol that determines the routing around node. Ad …
Biomass Production Chlorella Vulgaris Buitenzorg Using Series Of Bubble Column Photo Bioreactor With A Periodic Illumination, Anondho Wijanarko, Dianursanti Dianursanti, Muryanto Muryanto, Josia Simanjuntak, Praswasti Pembangun Dyah Kencana Wulan, Heri Hermansyah, Misri Gozan, Roekmijati Widaningroem Soemantojo
Biomass Production Chlorella Vulgaris Buitenzorg Using Series Of Bubble Column Photo Bioreactor With A Periodic Illumination, Anondho Wijanarko, Dianursanti Dianursanti, Muryanto Muryanto, Josia Simanjuntak, Praswasti Pembangun Dyah Kencana Wulan, Heri Hermansyah, Misri Gozan, Roekmijati Widaningroem Soemantojo
Makara Journal of Technology
Chlorella vulgaris Buitenzorg cultivation using three bubble column photo bioreactors arranged in series with a volume of 200 mL for 130 hours shows an increase of biomass production of Chlorella vulgaris Buitenzorg up to 1.20 times and a decrease of the ability of CO2 fixation compared to single reactor at a periodic sun illumination cycle. The operation conditions on cultivation are as following: T, 29.0oC; P,1 atm.; UG, 2.40 m/h; CO2, 10%; Benneck medium; and illumination source by Phillip Halogen Lamp 20W /12V/ 50Hz. Other research parameters such as microbial carbon dioxide transferred rate (qco2), CO2 transferred rate (CTR), energy …
The Effect Of Ozone And Zeolite Concentration To The Performance Of The Treatment Of Wastewater Containing Heavy Metal Using Flotation Process, Eva Fathul Karamah, Setijo Bismo, Hotdi M. Simbolon
The Effect Of Ozone And Zeolite Concentration To The Performance Of The Treatment Of Wastewater Containing Heavy Metal Using Flotation Process, Eva Fathul Karamah, Setijo Bismo, Hotdi M. Simbolon
Makara Journal of Technology
The Effect of Ozone and Zeolite Concentration to the Performance of the Treatment of Wastewater Containing Heavy Metal Using Flotation Process. Industrial wastewater which contains heavy metal cannot be disposed to the environment directly, due to its toxicity. In this research, separation of metal from wastewater was conducted by sorptive flotation method, using Lampung natural zeolite as bonding agent. The most common diffuser used in the flotation process is air or oxygen. In this research, ozone is used as diffuser because it is a stronger oxidant and more dissolvable in water than oxygen. Besides, ozone is a coagulant aid and …
The Role Of 1 And 9 Wt.% Zn In Precipitation Hardening Of Aa319 Aluminium, Bondan Tiara Sofyan, Sari Susanti, Ridwan R. Yusfranto
The Role Of 1 And 9 Wt.% Zn In Precipitation Hardening Of Aa319 Aluminium, Bondan Tiara Sofyan, Sari Susanti, Ridwan R. Yusfranto
Makara Journal of Technology
The Role of 1 and 9 wt.% Zn in Precipitation Hardening of AA319 Aluminium. Aluminium alloys are widely used for automotive application due to its low density and high corrosion resistance. For economic reason, casting of automotive products always uses aluminium scrap as charging materials that may result in fluctuation of content of alloying element, such as Zn. This research studies the role of Zn in precipitation hardening of AA319 aluminium alloys. Hardness and tensile testing were conducted to study the mechanical properties of the alloys, while ageing response was followed by hardness measurements. Evolution of microstructures was observed by …
Factor Analysis Of Interface Problems Among Construction Parties - A Case Study Of Mrt, Rong-Yau Huang, Chin-Tien Huang, Hung Lin, Wen-Hsiang Ku
Factor Analysis Of Interface Problems Among Construction Parties - A Case Study Of Mrt, Rong-Yau Huang, Chin-Tien Huang, Hung Lin, Wen-Hsiang Ku
Journal of Marine Science and Technology–Taiwan
With the rapid development of technology and the increasingly bigger size of constructions, the involved parties are required to pay more attention to all types of difficult interface problems than ever before. By considering the mass rapid transit system (MRTS) as an example, several problems resulting from complicated mechanical, electrical, civil, and track interfaces led to enormously extra losses in the construction process. Accordingly, this paper intends to use quantitative methods to categorize a variety of interface problems in the MRTS construction projects as well as identify their individual impacts in order to clarify these interface problems. The analysis results …
Robust Control Of Uncertain Time-Delay Systems Via Sliding Mode Control And Lmi- H∞ Technique, Ming-Chang Pai
Robust Control Of Uncertain Time-Delay Systems Via Sliding Mode Control And Lmi- H∞ Technique, Ming-Chang Pai
Journal of Marine Science and Technology–Taiwan
This paper presents a proportional-integral sliding mode control (PISMC) methodology for a class of linear uncertain systems with state delays. The systems are assumed to have structured, mismatched, and time-varying parameter uncertainties as well as mismatched and bounded external disturbances. Based on Lyapunov stability theorem and linear matrix inequality (LMI) H∞ technique, a sufficient condition is derived to guarantee the global stability of the dynamics and a prescribed H∞ norm bound of disturbance attenuation for all admissible uncertainties. Furthermore, this scheme assures robustness against state delays, parameter uncertainties and disturbances. Finally, an example is given to illustrate the feasibility of …
Application Of Maximum-Efficiency Tracking Control To Backlight Module Based On Phase-Locked Loop Technique, Chang-Hua Lin, Ying Lu
Application Of Maximum-Efficiency Tracking Control To Backlight Module Based On Phase-Locked Loop Technique, Chang-Hua Lin, Ying Lu
Journal of Marine Science and Technology–Taiwan
Maximum-efficiency tracking control applied in the backlight module is proposed in this paper. The backlight system incorporates a phase-locked loop (PLL) as a feedback mechanism to promote both the system efficiency and stability. To overcome the drawbacks of the conventional electromagnetic transformer and to miniaturize the backlight module, the piezoelectric transformer (PT) is adopted for driving the cold cathode fluorescent lamp (CCFL). To avoid the system efficiency decreases due to the temperature effect of PT, the PLL is utilized to track immediately the optimal operating frequency of PT for achieving maximum output efficiency under various ambient temperatures. The feedback parameter …
Design And Implementation Of An All-Digital Real-Time Underwater Acoustic Transceiver Using Digital Signal Processors, Fu-Sheng Lu, Ching-Hsiang Tseng, Bin-Chong Wu
Design And Implementation Of An All-Digital Real-Time Underwater Acoustic Transceiver Using Digital Signal Processors, Fu-Sheng Lu, Ching-Hsiang Tseng, Bin-Chong Wu
Journal of Marine Science and Technology–Taiwan
In this paper, an all-digital transceiver for real-time underwater acoustic (UWA) communications is developed using digital signal processors (DSPs). The design of the transceiver is based on the direct-sequence spread-spectrum (DS/SS) modulation scheme, in which the timing synchronization is efficiently achieved by employing a sliding correlator and a modified noncoherent delay-locked loop for code acquisition and tracking, respectively. In addition, an equal-gain combiner (EGC) and an adaptive decision-feedback equalizer (DFE) are included in the receiver to enhance its interference rejection capability under multipath fading environments. Several real-time UWA transmission tests are conducted in an experimental water tank to evaluate the …
Profile Design Of Piston Ring Using Inverse Method, Li-Ming Chu, Yuh-Ping Chang, Jung-Hua Yang
Profile Design Of Piston Ring Using Inverse Method, Li-Ming Chu, Yuh-Ping Chang, Jung-Hua Yang
Journal of Marine Science and Technology–Taiwan
This study aims to develop an algorithm for designing the piston ring profile and pressure distribution using an inverse method. The proposed algorithm needs to obtain load and boundary conditions for estimating not only a smooth curve in the piston ring profile, but also in the pressure distribution. The algorithm is developed from Reynolds integral and force balance equations. The least-squares error method, variational method, Gauss-Seidel method and Newton-Raphson method are employed to calculate the piston ring profile. Simulation results reveal that the greater the degree of the polynomial function used, the greater the maximum pressure ( Pmax ), load …
Guaranteed Cost Control Of Uncertain Linear Systems Via Discrete-Time Variable Structure Control, Ming-Chang Pai
Guaranteed Cost Control Of Uncertain Linear Systems Via Discrete-Time Variable Structure Control, Ming-Chang Pai
Journal of Marine Science and Technology–Taiwan
This paper presents a design of realizing the guaranteed cost control problem for uncertain linear systems via discrete-time variable structure control (VSC) scheme. The uncertainties in the system are assumed to be norm-bounded and time-varying. Based on the discrete-time VSC technique, the proposed controller can drive the system into a pre-specified switching surface to obtain the desired dynamic performance and the chattering phenomenon is eliminated. Sufficient conditions for the existence of guaranteed cost control are presented, and the problem of designing guaranteed cost control is converted to a convex optimization problem with linear matrix inequality (LMI) constraints. Finally, simulation results …
Cu Doping Lifepo4 And Its Electrochemical Performance, Ming-Sen Zheng, Shan-Ke Liu, Shi-Gang Sun, Quan-Feng Dong
Cu Doping Lifepo4 And Its Electrochemical Performance, Ming-Sen Zheng, Shan-Ke Liu, Shi-Gang Sun, Quan-Feng Dong
Journal of Electrochemistry
LiFePO4 and LiFePO4 doped with Cu2+ ions were synthesized by solid-state reactions.The structure of LiFePO4 and the Fe valence were analyzed by the XRD(X-ray diffraction) and XPS(X-ray photoelectron spectroscopy) respectively.The Cu doping position in LiFePO4 is discussed.It has found that the volume of LiFePO4 by doping Cu2+ ions is reduced.The minim Cu2+ ions doping does not almost change the binding energy of Fe2p1/2 in LiFePO4.According to the experiment results,we conclude that most of the Cu2+ ions substitute the Fe2+ ions in LiFePO4 when a …
A Study On Supercapacitor Based On Aligned Carbon Nanotubes, Xiao-Yan Ye, Yan-Zhi Wang, Hai-Yan Song, Zhuo Sun, Pin-Gang He, Yu-Zhi Fang
A Study On Supercapacitor Based On Aligned Carbon Nanotubes, Xiao-Yan Ye, Yan-Zhi Wang, Hai-Yan Song, Zhuo Sun, Pin-Gang He, Yu-Zhi Fang
Journal of Electrochemistry
Large scale vertically aligned carbon nanotubes(ACNTs) with uniform length and diameter were prepared by the pyrolysis of iron(Ⅱ) phthalocyanine at low pressure.The ACNTs were activated by electrolyte-activation,acid-activation or electrochemical activation.The performance of the capacitor based on activated ACNTs was characterized by cyclic voltammograms which was of rectangular shape,impedence spectroscopy in which the phase is above 80° and the result specific capacitance was 16～32 F/g,which suggest that the ACNTs are the promising material for the supercapacitor.
Preparation And Electrochemical Performance Of Ordered Mesoporous Titanium Phosphate As Cathode Material For Li-Ion Battery, Qiong Wang, Attia Adel, Zhi-Cong Shi, Yong Yang
Preparation And Electrochemical Performance Of Ordered Mesoporous Titanium Phosphate As Cathode Material For Li-Ion Battery, Qiong Wang, Attia Adel, Zhi-Cong Shi, Yong Yang
Journal of Electrochemistry
Ordered porous titanium phosphate materials were prepared by using the surfactant template combined with the sol-gel method. The samples were characterized by small angle X-ray diffraction(SA-XRD) method, N2 adsorption/desorption techniques,high resolution transmission electron microscopy(HRTEM) and element analysis. It is found that the calcination temperature is a big influence on the porous structure, and electrochemical performance of the titanium phosphate materials, and the mesoporous titanium phosphate showed good performance in the electrochemical test, the first discharge capacity is 94 mAh/g at the current density of 150 mA/g. On the other hand, the no porous material with a low capacity of …
Synthesis Of Adipic Acid From Cyclohexanol By Electrochemical Oxidation Using Cr2O72-/Cr3+ As Indirect Oxidant, Zhen-Hai Liang, Yu-Qing Cui, Hong-Yan Sun
Synthesis Of Adipic Acid From Cyclohexanol By Electrochemical Oxidation Using Cr2O72-/Cr3+ As Indirect Oxidant, Zhen-Hai Liang, Yu-Qing Cui, Hong-Yan Sun
Journal of Electrochemistry
Adipic acid was synthesized by electro-oxidation of cyclohexanol taking Cr2O72-/Cr3+ as indirect oxidant.The best technological conditions were optimized by orthogonal experiment.The optimum condition are as follows: the temperature is 35 ℃,ratio of crude material is n(cyclohexanol)∶n(Cr2O72-)=0.4∶1 and concentration of H2SO4 is 4 mol·L-1.Under these conditions,the yield of adipic acid can reach 70.29%.Moreover,The effects of concentration of Ag2SO4,(NH4)2SO4,H2SO4and current density on the formation of Cr2O72-were also …
Mechanism Of The Cathode Reduction Of Ti(Ⅳ) In Molten Na3Alf6-Alf3, Hai-Bin Sun, Xiu-Rong Zuo, Zhi-Guo Zhong, Xue-Hui Hu
Mechanism Of The Cathode Reduction Of Ti(Ⅳ) In Molten Na3Alf6-Alf3, Hai-Bin Sun, Xiu-Rong Zuo, Zhi-Guo Zhong, Xue-Hui Hu
Journal of Electrochemistry
The mechanism of TiO2 electrode process has been investigated by cyclic voltammetry and chronopotentiometry on the tungsten filament in molten Na3AlF6-AlF3 salts at 990 ℃.The experimental results showed that electrochemical reduction of Ti(Ⅳ) precede were two steps,firstly Ti(Ⅳ) was reduced to Ti(Ⅱ),then Ti(Ⅱ) was reduced to Ti,namely: Ti(Ⅳ)→Ti(Ⅱ)→Ti.