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Articles 22441 - 22470 of 27413

Full-Text Articles in Engineering

Mechanical And Thermal Properties Of Polypropylene Reinforced By Calcined And Uncalcined Zeolite, Nurdin Bukit Nov 2012

Mechanical And Thermal Properties Of Polypropylene Reinforced By Calcined And Uncalcined Zeolite, Nurdin Bukit

Makara Journal of Technology

This study was carried out to compare mechanical and thermal properties of polypropylene (PP) reinforced with uncalcined and calcined zeolites. The PP samples were reinforced with zeolites at various quantities of 2, 4, and 6 (wt %). The comparison of the two types of zeolite was based on mechanical properties, including tensile strength, elongation at break, and Young’s modulus, and thermal characteristics analyzed using DSC, and DTA/TGA technique. The results obtained clearly revealed that both zeolites were able to significantly increase tensile strength and Young’s modulus of the samples, with calcined zeolite was found to work better. Addition of calcined …

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Benchmark For Country-Level Earthquake Strong-Motion Instrumentation Program, Widjojo Adi Prakoso, I Nyoman Sukanta Nov 2012

Benchmark For Country-Level Earthquake Strong-Motion Instrumentation Program, Widjojo Adi Prakoso, I Nyoman Sukanta

Makara Journal of Technology

An empirical study to develop benchmark models at country-level to assess the suggested number of earthquake strongmotion stations based on a framework encompassing geographic, demographic, and socio-economic parameters is reported. The models are to provide a working estimate of the required number of stations for improving the strongmotion instrumentation program of Indonesia. National earthquake strong-motion networks of New Zealand, Japan, Taiwan, Iran, Turkey, and Italy were used as the references. The parameter proposed is the number of stations in land area of 1,000 km2, and three models based on the exponential regression analysis are presented as functions of population density, …

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Worst Case Of Relative Disturbance Gain Array For Uncertain Distillation System, Rudy Agustriyanto, Jie Zhang Nov 2012

Worst Case Of Relative Disturbance Gain Array For Uncertain Distillation System, Rudy Agustriyanto, Jie Zhang

Makara Journal of Technology

This article discusses the constrained nonlinear optimization formulation for calculating the worst case of lower and upper bounds of relative disturbance gain array (RDGA) for uncertain process models. The proposed approach seeks the minimum and maximum values of the relative disturbance gains subject to the constraints in which the process and disturbance gains are within their uncertainty ranges. RDGA ranges are useful for control structure determination and the related robustness, as they provide information regarding the sensitivity to gain uncertainties. The proposed method is demonstrated by ternary distillation column case study. Closed loop simulation results support the analysis based on …

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Biodiesel Production From Waste Cooking Oil Using Hydrodinamic Cavitation, Muhammad Dani Supardan, Satriana Satriana, Mahlinda Mahlinda Nov 2012

Biodiesel Production From Waste Cooking Oil Using Hydrodinamic Cavitation, Muhammad Dani Supardan, Satriana Satriana, Mahlinda Mahlinda

Makara Journal of Technology

The aim of this research was to study biodiesel production from low cost feedstock of waste cooking oil (WCO) using hydrodynamic cavitation apparatus. A two-step processes esterification process and transesterification process using hydrodynamic cavitation for the production of biodiesel from WCO is presented. The first step is acid-catalyzed esterification process for reducing free fatty acid (FFA) content of WCO and followed by base-catalyzed transesterification process for converting WCO to biodiesel as the second step. The result of esterification process with methanol to oil molar ratio of 5 and temperature of 60 oC showed that the initial acid value of WCO …

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Knowledge Dictionary For Information Extraction On The Arabic Text Data, Wahyu Syaifullah Jauharis Saputra, Agus Zainal Arifin, Anny Yuniarti Nov 2012

Knowledge Dictionary For Information Extraction On The Arabic Text Data, Wahyu Syaifullah Jauharis Saputra, Agus Zainal Arifin, Anny Yuniarti

Makara Journal of Technology

Information extraction is an early stage of a process of textual data analysis. Information extraction is required to get information from textual data that can be used for process analysis, such as classification and categorization. A textual data is strongly influenced by the language. Arabic is gaining a significant attention in many studies because Arabic language is very different from others, and in contrast to other languages, tools and research on the Arabic language is still lacking. The information extracted using the knowledge dictionary is a concept of expression. A knowledge dictionary is usually constructed manually by an expert and …

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Full Issue Nov 2012

Full Issue

International Journal of Interpreter Education

No abstract provided.

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Bs News November/December Nov 2012

Bs News November/December

Building Services Engineering

No abstract provided.

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In Situ Pm-Irras Studies Of A Floating Bilayer Lipid Membrane At Au(111) Electrode Surface, Su Zhangfei, Kycia Annia, Jay Leitch J., Lipkowski Jacek Oct 2012

In Situ Pm-Irras Studies Of A Floating Bilayer Lipid Membrane At Au(111) Electrode Surface, Su Zhangfei, Kycia Annia, Jay Leitch J., Lipkowski Jacek

Journal of Electrochemistry

In situ Polarization modulation infrared reflection absorption spectroscopy (PM-IRRAS) was used to study the structure of a DMPC + cholesterol + GM1 floating bilayer lipid membrane (fBLM) at a Au(111) surface. 1-thio-beta-D-glucose (beta-Tg) was self-assembled onto the Au electrode to increase the overall hydrophilicity of the surface. The fBLM was deposited on the beta-Tg self-assembled monolayer (SAM) using a combination of Langmuir-Blodgett/Langmuir-Schaefer (LB/LS) techniques. The carbohydrate headgroups of the GM1 molecules were physically adsorbed to the beta-Tg SAM forming a water rich cushion between the fBLM and the modified gold substrate. The PM-IRRAS spectra indicate that the DMPC molecules within …

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Underpotential Deposition Of Copper On Pt(S)[N(100)X(110)] Stepped Surfaces, Gisbert Rubn, Climent Vctor, Herrero Enrique, M. Feliu Juan Oct 2012

Underpotential Deposition Of Copper On Pt(S)[N(100)X(110)] Stepped Surfaces, Gisbert Rubn, Climent Vctor, Herrero Enrique, M. Feliu Juan

Journal of Electrochemistry

The underpotential deposition of Cu on platinum stepped surfaces composed of (100) terraces and (110) monoatomic steps has been studied in different acidic solutions. It has been found that the initial stage of copper deposition on the surface takes place simultaneously on terrace and step sites, irrespective of the nature of the adsorbing anion. During the voltammetric deposition of a full monolayer, several peaks can be observed. The analysis of the dependence of the peak charge with the step density allows assigning the different peaks to different deposition sites. The peak appearing at most positive potentials corresponds to the deposition …

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The Oxidation Of Hydrogen Peroxide On Nanostructured Rhodium Microelectrodes, N. Bartlett Philip, F. Esterle Thomas Oct 2012

The Oxidation Of Hydrogen Peroxide On Nanostructured Rhodium Microelectrodes, N. Bartlett Philip, F. Esterle Thomas

Journal of Electrochemistry

Mesoporous Rh films were deposited onto platinum microelectrodes from the H1 lyotropic liquid crystalline phase of C12EO8 (octaethyleneglycol monododecyl ether). The electrodes show well defined voltammetry for the oxidation and the reduction of hydrogen peroxide at low concentrations (<10 mmol•L-1) with excellent stability for operation at neutral pH. Based on the hysteresis in the current and the potential dependence the oxidation of hydrogen peroxide occurs through a CEE mechanism involving Rh(OH)3 on the mesoporous Rh electrode surface. At higher hydrogen peroxide concentrations the current reaches a plateau that is due to either saturation of the binding sites for hydrogen peroxide or limitation of the reaction due to acidification of the solution within the pores. For the thin films (below 200 nm) the hydrogen peroxide calibration curves we …

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Electrochemical Synthesis Of Silver-Tetracyanoquinodimethane Nanorods At Agar Supported Water/1,2-Dichloroethane Interface, Li Huang, Yixian Wang, Michael V. Mirkin, Bin Ren, Dongping Zhan Oct 2012

Electrochemical Synthesis Of Silver-Tetracyanoquinodimethane Nanorods At Agar Supported Water/1,2-Dichloroethane Interface, Li Huang, Yixian Wang, Michael V. Mirkin, Bin Ren, Dongping Zhan

Journal of Electrochemistry

Silver-tetracyanoquinodimethane (AgTCNQ) is an important charge transfer salt due to its high conductivity and other electronic properties. In this communication, we report the synthesis of AgTCNQ at the liquid/liquid interface. Agar was used as a gelling agent to support water/1,2-dichloroethane (DCE) interface. Silver ions were transferred from the hydrogel into DCE phase, where they combined with TCNQ- to form AgTCNQ nanorods. The developed method can provide a new route for synthesis of functional materials based on the electrochemistry at the liquid/liquid interface.

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Integration Of Accounting-Based And Option-Based Models To Predict Construction Contractor Default, Lung-Ken Tsai, Hui-Ping Tserng, Hsien-Hsing Liao, Po-Cheng Chen, Wen-Pei Wang Oct 2012

Integration Of Accounting-Based And Option-Based Models To Predict Construction Contractor Default, Lung-Ken Tsai, Hui-Ping Tserng, Hsien-Hsing Liao, Po-Cheng Chen, Wen-Pei Wang

Journal of Marine Science and Technology–Taiwan

This paper aims to predict construction contractor default, which is excluded by most extant studies, due to the distinct characteristics of construction industry. Default predicting models developed in past literatures are mostly built by accounting information, yet accounting sheets have innate flaws. To calculate default probability, several recent studies applied the option pricing theory, which presumes that the stock market is efficient. This presumption isn't always true in real life. In this paper, a hybrid model is proposed. It combines information from both models by inputting the default probability from the option-based model into the accounting-based model. As the measure …

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An Excited System Design For The Maximum Output Of Induction Generator Based On Vector Control, Ding-Tsair Su, Ying-Shing Shiao, Koan-Yuh Chang, Wen-Jer Chang Oct 2012

An Excited System Design For The Maximum Output Of Induction Generator Based On Vector Control, Ding-Tsair Su, Ying-Shing Shiao, Koan-Yuh Chang, Wen-Jer Chang

Journal of Marine Science and Technology–Taiwan

In this paper, without using the mechanical speed regulator, we propose a scheme that can control the output power of an induction generator by controlling the excited current. To attain this goal, an inverter is designed as a current controlled source, to supply an excited current for the induction generator. Furthermore, using the dq axes theory, a vector controller is designed by a digital signal processor (DSP) for controlling the inverter which supplies excited current appropriately in accordance with the wind speed to regulate the induction generator output power. Finally, the experimental results have shown good performances of the proposed …

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A Partition Dummy Sequence Insertion Papr Reduction Method Of The Ofdm System, Chi-Min Li, Jia-Chyi Wu, Chao-Chin Tseng Oct 2012

A Partition Dummy Sequence Insertion Papr Reduction Method Of The Ofdm System, Chi-Min Li, Jia-Chyi Wu, Chao-Chin Tseng

Journal of Marine Science and Technology–Taiwan

OFDM (Orthogonal Frequency Division Multiplexing) technique has been widely adopted in many wireless communication systems due to its high data-rate transmission ability and robustness to the multipath fading channel. One major drawback of the OFDM signal is the high peak-toaverage power ratio (PAPR) problem. The high PAPR results in the in-band distortion and out-of-band radiation when the OFDM signal is fed into a nonlinear power amplifier (PA). In this paper, we propose a partition dummy sequence insertion (PDSI) method to reduce the PAPR problem. Simulation results of the PAPR reduction and bit error rate (BER) performance for the proposed method …

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Port Management Improvement Strategies Based On Simulation Model, Wen-Chih Huang, Tu-Cheng Kuo, Ching-Tsyr Wu, Cheng-Chen Kuo Oct 2012

Port Management Improvement Strategies Based On Simulation Model, Wen-Chih Huang, Tu-Cheng Kuo, Ching-Tsyr Wu, Cheng-Chen Kuo

Journal of Marine Science and Technology–Taiwan

Management performance of container terminal is an important factor of port competitiveness. In the past, ports had often increased performance by expanding the number of berths and equipment. However, recent global recession has significantly dampened the growth of the international trade. Thus, port authority must seek effective utilization of the capacities of its container terminals. Most ocean carriers in the Port of Kaohsiung in Taiwan rent multiple berths that are often dispersed to different container terminals, resulting in inefficient handling. Establishing terminal operators to optimize berth assignment may resolve this problem. The objective of this research is to construct a …

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Performance Comparison Of The Stbc-Ofdm Decoders In A Fast Fading Channel, Chi-Min Li, Guo-Wei Li, Han-Yi Liu Oct 2012

Performance Comparison Of The Stbc-Ofdm Decoders In A Fast Fading Channel, Chi-Min Li, Guo-Wei Li, Han-Yi Liu

Journal of Marine Science and Technology–Taiwan

In a fast fading channel, the orthogonality of the two consecutive STBC-OFDM symbols will be destroyed and the received signals can not be perfectly separated. As a result, the bit error rate (BER) performance will be degraded seriously. In this paper, we analyze several co-channel interference (CCI) cancellation decoders for the STBC-OFDM in a fast fading channel including the Alamouti method, SIC method, ML method, DMLD method, and a proposed DZFD method. The proposed DZFD method has the advantage of reducing the computational complexity for the DMLD method. We also conduct the outdoor channel measurements to verify the CCI cancellation …

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Effects Of Non-Newtonian Couple Stresses On The Dynamic Characteristics Of Wide Rayleigh Step Slider Bearings, Jaw-Ren Lin, Li-Ming Chu, Wei-Liang Liaw Oct 2012

Effects Of Non-Newtonian Couple Stresses On The Dynamic Characteristics Of Wide Rayleigh Step Slider Bearings, Jaw-Ren Lin, Li-Ming Chu, Wei-Liang Liaw

Journal of Marine Science and Technology–Taiwan

To provide more information in fluid-film lubricated bearings, the effects of non-Newtonian couple stresses on the dynamic characteristics of Rayleigh step slider bearings have been presented in this paper. According to the results, the effects of non-Newtonian couple stresses signify an improvement in the bearing characteristics. Comparing with the Newtonian-lubricant Rayleigh step bearing, the nonNewtonian couple stress effects provide an increase in the steady load-carrying capacity, the dynamic stiffness coefficient and the dynamic damping coefficient, as well as a reduction in the steady volume flow rate required. In order to guide the use of the present study, a numerical example …

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Behavior Of Regular Triangular Joints Under Cyclic Shearing, Shuh-Gi Chern, Tsu-Chiang Cheng, Wen-Ya Chen Oct 2012

Behavior Of Regular Triangular Joints Under Cyclic Shearing, Shuh-Gi Chern, Tsu-Chiang Cheng, Wen-Ya Chen

Journal of Marine Science and Technology–Taiwan

Synthetic regular triangular joints made of gypsum plaster were cyclicly sheared to measure asperity degradation and mathematical behavior of regular triangular joints. Laboratory cyclic shear tests were conducted for three joint types under three different normal stresses. Asperity degradation and shear strength of joints were found to be a function of joint roughness, normal stress, shearing displacement and number of loading cycles. Based on the experimental results, mathematical models were developed for evaluation of shear strength in cyclic loading conditions. Comparison of the test results with that of the proposed model, it was found a good agreement was observed.

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Free Vibration Analysis Of A Hybrid Beam Composed Of Multiple Elastic Beam Segments And Elastic-Supported Rigid Bodies, Hsien-Yuan Lin, Chin-Yu Wang Oct 2012

Free Vibration Analysis Of A Hybrid Beam Composed Of Multiple Elastic Beam Segments And Elastic-Supported Rigid Bodies, Hsien-Yuan Lin, Chin-Yu Wang

Journal of Marine Science and Technology–Taiwan

This paper aims at presenting a method to determine the “exact” natural frequencies and mode shapes of a hybrid beam composed of multiple elastic beam segments and multiple rigid bodies with each rigid body connected with two adjacent elastic beam segments. Furthermore, each rigid body has its own mass and rotary inertia, and is supported by a translational spring and/or a rotational spring. First, based on the equations of the continuity of deformations and the equilibrium of moments and forces for each of the intermediate rigid bodies and boundary conditions, the coefficient matrices of the entire hybrid beam are derived. …

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Optimal Dynamic Temporal-Spatial Paramter Inversion Methods For The Marine Integrated Element Water Quality Model Using A Data-Driven Neural Network, Ming-Chang Li, Shu-Xiu Liang, Zhao-Chen Sun, Guang-Yu Zhang Oct 2012

Optimal Dynamic Temporal-Spatial Paramter Inversion Methods For The Marine Integrated Element Water Quality Model Using A Data-Driven Neural Network, Ming-Chang Li, Shu-Xiu Liang, Zhao-Chen Sun, Guang-Yu Zhang

Journal of Marine Science and Technology–Taiwan

Certain marine water quality or ecosystem model parameters vary in space and time because of different plankton taxonomic compositions over a large domain. The same parameter vectors can result in suboptimal calibration. In the present paper, a data-driven model based on an artificial neural network is developed to inverse the values of model parameters dynamically. All training data used are calculated using numerical water quality models from the results of multiparameter matching design cases such that physical properties are not disturbed. The aim is to determine the relationship between the model parameters and the pollution concentration values of interior stations. …

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A Model For Designing M-Agriculture Applications For Dairy Farming, Amos Gichamba, Ismail A. Lukandu Oct 2012

A Model For Designing M-Agriculture Applications For Dairy Farming, Amos Gichamba, Ismail A. Lukandu

The African Journal of Information Systems

In the recent past, developing countries have experienced major technological advancements including high mobile phone penetration. With the implementation of innovative technological solutions (e.g. mobile-based systems in key economic activities such as agriculture), there is need to develop models that software developers and researchers can use to design solutions. This paper aims to study the implementation of mobile systems in agriculture and presents a model for designing such applications. This study shows that models exist for general mobile applications design and development, although none specifically suits mobile agriculture applications. A model for designing and implementing M-Agriculture applications is presented. The …

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Bs News September/October Sep 2012

Bs News September/October

Building Services Engineering

No abstract provided.

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Influences Of Particle Size And Sulfuric Acid Treatment On The Electrochemical Performance Of Bamboo Charcoal, Yu Yao, Ai-Shui Yu Aug 2012

Influences Of Particle Size And Sulfuric Acid Treatment On The Electrochemical Performance Of Bamboo Charcoal, Yu Yao, Ai-Shui Yu

Journal of Electrochemistry

The bamboo charcoal had been milled and treated by sulfuric acid. The influences of as-prepared material particle size and sulfuric acid treatment on the electrochemical performance had been studied. The result displays that the bamboo charcoal with mean particle size about 5 μm has the best first coulombic efficiency. Sulfuric acid treatment could raise the discharge capacity of bamboo charcoal, and the first discharge capacity of 328.2 mAh·g-1 was obtained with the bamboo charcoal treated by sulfuric acid for 18 h. Furthermore, the capacity of 302.3 mAh·g-1 could be maintained for 50 cycles, showing good cycle performance.

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Preparation And Performance Of Sn-Co-M-C（M = Zn, Fe）Composites As An Anode Material, Guo-Qing Fang, Wei-Wei Liu, Shi-Ci He, Qian Zhang, Jun-Wei Zheng, De-Cheng Li Aug 2012

Preparation And Performance Of Sn-Co-M-C（M = Zn, Fe）Composites As An Anode Material, Guo-Qing Fang, Wei-Wei Liu, Shi-Ci He, Qian Zhang, Jun-Wei Zheng, De-Cheng Li

Journal of Electrochemistry

The anode materials of Sn-Co-M-C (M = Zn, Fe) composites were prepared by carbothermal reduction method from metal oxides and sucrose in N2 atmosphere. Their structural and electrochemical properties were studied by XRD, SEM and charge-discharge test. Among them, the Sn-Co-Zn-C composite showed higher specific capacity and good cycle performance. The initial specific discharge capacity of 571 mAh·g-1 could be obtained, while 369 mAh·g-1 was still kept after 45 cycles.

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Preparation And Electrochemical Performance Of Nanostructured Mno2 Materials, Wen Wu, Dan-Dan Zhou, Meng-Yan Hou, Yong-Yao Xia Aug 2012

Preparation And Electrochemical Performance Of Nanostructured Mno2 Materials, Wen Wu, Dan-Dan Zhou, Meng-Yan Hou, Yong-Yao Xia

Journal of Electrochemistry

Nanostructured MnO2 materials were prepared in a micro-emulsion medium using sodium dodecyl sulfate (SDS）as a surfactant by a redox reaction between potassium permanganate and aniline. The morphologies of the obtained MnO2 were critically dependent on the concentrations of SDS. The particle sizes varied with the change in the micro-emulsion medium. The optimized properties of MnO2 material obtained with the surfactant concentration of 0.2 mol.L-1 had a specific surface area of 228.2 m2.g-1, and delivered a specific capacitance of 237 F.g -1 in 1 mol.L-1 Li2SO4. Additionally, a …

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Carbon Nanotubes With Ni2P Nanoparticles As A Counter Electrode In Dye-Sensitized Solar Cells, Yan-Ye Dou, Nan-Fu Yan, Guo-Ran Li, Xue-Ping Gao Aug 2012

Carbon Nanotubes With Ni2P Nanoparticles As A Counter Electrode In Dye-Sensitized Solar Cells, Yan-Ye Dou, Nan-Fu Yan, Guo-Ran Li, Xue-Ping Gao

Journal of Electrochemistry

Carbon nanotubes (CNTs) supported by Ni2P nanoparticles are prepared and used as a counter electrode in dye-sensitized solar cells (DSSCs) for the first time. The CNTs-Ni2P composite was prepared by the heat treatment of a mixed precursor including nickel chloride, sodium hypophosphite and CNTs in argon atmosphere. The X-Ray diffraction (XRD) results indicate that the as-prepared sample consists of hexagonal Ni2P and carbon nanotubes. No peaks of other nickel phosphides are observed in the XRD pattern. Microstructure of the Ni2P-CNTs composite was investigated using transmission electron microscopy (TEM). It is shown that the Ni …

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A Facile Approach To Prepare Lifepo4/C Composite With High-Rate Performance, Peng Zhang, Ling-Bin Kong, Yong-Chun Luo, Long Kang Aug 2012

A Facile Approach To Prepare Lifepo4/C Composite With High-Rate Performance, Peng Zhang, Ling-Bin Kong, Yong-Chun Luo, Long Kang

Journal of Electrochemistry

The LiFePO4/C composite electrode material was synthesized by a moderate in situ carbothermal reduction method at 600 °C using FeCl3·6H2O, LiOH·H2O, and NH4H2PO4 as starting materials, soluble starch sol as a carbon source and a reducing agent. This method is readily reproducible and possibly feasible to carry out large-scale synthesis. The structure and morphology of the LiFePO4/C samples were investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The synthesized LiFePO4/C composite was in pure phase of olivine-type, …

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Electrochemical Performances Of Layered Polypyrrole/Chemically Reduced Graphene Oxide Nanocomposites As Supercapacitor Electrodes, Si-Zhe Xu, Xue-Jiao Zhou, Kun Wu, Yong-Qiang Yang, Hai-Xia Wu Aug 2012

Electrochemical Performances Of Layered Polypyrrole/Chemically Reduced Graphene Oxide Nanocomposites As Supercapacitor Electrodes, Si-Zhe Xu, Xue-Jiao Zhou, Kun Wu, Yong-Qiang Yang, Hai-Xia Wu

Journal of Electrochemistry

Nanocomposites of polypyrrole (Ppy) and chemically reduced graphene oxide (CRGO), Ppy/CRGO, have been fabricated through in-situ polymerization of pyrrole on graphene oxide (GO) sheets. The as-synthesized Ppy/CRGO composites were characterized complementarily using scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and Fourier transformed infrared spectroscopy (FT-IR). By controlling the initial ratio of the GO to pyrrole, the layered composites could be obtained and their thickness could be tuned properly. The Ppy/CRGO electrodes were prepared using a mechanical compressing technique and their electrical conductivity and electrochemical properties were characterized systematically. We demonstrated that as electrodes for supercapacitor, the Ppy/CRGO composites with Ppy …

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Electrochemical Corrosion And Protection Of Copper Foil Treated By Surface Siloxane Filming, Wei-Jun Miao, Yu-Bao Zhang, Ning-Yu Gu, Feng Liu Aug 2012

Electrochemical Corrosion And Protection Of Copper Foil Treated By Surface Siloxane Filming, Wei-Jun Miao, Yu-Bao Zhang, Ning-Yu Gu, Feng Liu

Journal of Electrochemistry

Copper foil specimens were immersed in hydro-alcoholic solution of 3-amino-propyl-trimethoxy-silane (γ-APS) to prepare a protective self-assembled siloxane membrane on the surface. Potentiodynamic polarization and electrochemical impedance spectroscopic tests were performed in 0.1 mol.L-1 NaCl to evaluate the effects of the self-assembled siloxane membranes prepared at different pH of γ-APS on corrosion of copper foil. The surface morphology of siloxane membrane was studied by SEM. Experimental results revealed that the γ-APS self-assembled siloxane membranes effectively inhibited the corrosion of copper foil and the optimum anti-corrosion effect was found when the pH value of the silane solution was 7.

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Electrochemical Immunosensor Based On Polycalconcarboxylic Acid Modified Electrode For The Determination Of Alpha-Fetoprotein, Xiao Lin, Shao-Huang Weng, Jian-Zhang Zhou, Ai-Lin Liu, Xin-Hua Lin, Yong-Ji You Aug 2012

Electrochemical Immunosensor Based On Polycalconcarboxylic Acid Modified Electrode For The Determination Of Alpha-Fetoprotein, Xiao Lin, Shao-Huang Weng, Jian-Zhang Zhou, Ai-Lin Liu, Xin-Hua Lin, Yong-Ji You

Journal of Electrochemistry

A highly sensitive electrochemical immunosensor based on novel electropolymerized polycalconcarboxylic acid modified electrode (poly-CCA/GC) has been fabricated for the detection of alpha-fetoprotein (AFP). The differences of the poly-CCA/GC electrodes before and after the immobilization of AFP antibody were characterized via scanning electron microscopy (SEM) and electrochemical impedance spectroscopy (EIS). The immobilization of antibody/antigen/antibody-HRP sandwich was formed on the poly-CCA modified electrode for the determination of special AFP concentrations. The electrochemical signals generated from the HRP which catalyzed the TMB substrate were measured. Experiment results indicated that the developed immunosensor showed a good sensitivity and precision.

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