Engineering Commons^™

Imperfections In A Silicon Crystal Studied By The X-Ray And Density Method, Pierre Borgeaud

Masters Theses

"The study of imperfections in several crystals of silicon was conducted by the x-ray and density method"--Abstract, page 2.

A Thermodynamic Study Of The System Pbo-Pbs, John P. Hager

Masters Theses

"An experimental investigation was conducted in order to determine the thermodynamic and kinetic behavior of the system PbO-PbS.

The thermodynamic behavior of the system PbO-PbS was studied by measuring the P_SO₂ in argon-SO₂ mixtures equilibrated with various PbO-PbS mixtures in a recirculating-type equilibrium apparatus, and analyzing the condensed phases by means of X-ray diffraction.

The effect of temperature and PbO/PbS ratio on the rate of SO₂ evolution was investigated in order to determine the reaction mechanisms involved in the approach to equilibrium.

A sodium hydroxide, hydrogen peroxide titration technique was employed in the analysis of SO_{2 …}

Preparation Of Casting Slips Containing Ferrous Powders And Alginates, Robert Eugene Newcomer

Masters Theses

"The preparation of casting slips containing ferrous powders dispersed by alginates was studied and an attempt was made to determine the mechanism by which suspension was attained. The colloidal aspects of preparing ceramic casting slips are discussed and an analogy is drawn to preparation of metallic slips suspended by alginates.

Sodium and ammonium alginates were used to suspend stainless steel and iron powders. The effect of NaOH, HC1, and various phosphate additions on the properties of slips and algin solutions was considered.

It was found that colloidal concepts can not be applied to explain observed behavior in the system studied. …

A Thermodynamic Study Of The Germanium Sulphides, Satya Prakash Jain

Masters Theses

"The experimental determination of some of the thermodynamic properties of germanium sulphide phases was conducted by a hydrogen reduction technique. The equilibrium H₂S/H₂ ratios were determined as a function of temperature for the two phase equilibria GeS₂-GeS and GeS-Ge. A Tutwiler analysis technique was used to analyze the equilibrated gas mixture for hydrogen sulphide content.

A detailed description is given for the process and the apparatus used in performing the experiments for equilibration of H₂S/H₂ gas mixture. The methods used for the preparation of germanium sulphide phases are also discussed.

The investigation …

A Thermodynamic Study Of Germanium Sulfides, Sham Lal Malhotra

Masters Theses

"The vapour pressure of germanium monosulfide (liquid) was determined by a boiling point method. An expression for the vapour pressure as a function of temperature was obtained and the heat of vapourization calculated. Using the heat of sublimation data obtained by other investigators, the heat of fusion was calculated.

The thermodynamic properties, change of standard free energy (Δ F°) heat content (Δ H°) and entropy (Δ S°); of germanium disulfide were determined by using an indirect method. The equilibrium H₂S/H₂O ratios are determined for the reaction:

GeS₂ (s) + 2H₂O(g) = GeO_{2 …}

A Dissolution Rate Study In Hydrofluoric Acid Of Titanium And The Alpha Solid Solutions Of Oxygen In Titanium, John L. Ratliff

Masters Theses

"The dissolution mechanism of titanium in hydrofluoric acid was studied by collecting the hydrogen evolved during the dissolution reaction. A concentration range of 0.05 N to 0.50 N and a temperature range of 15°C to 45°C were employed for the determination. Values of the reaction order and energy of activation were determined for both pure titanium and the alpha solid solutions of oxygen in titanium and found to be the same within experimental limits. This indicated that the reaction giving rise to hydrogen evolution on the surfaces of both pure titanium and the TiO_x alloys was the same. The …

Colorado "Rush To The Rockies Centennial" Spectroscopy Conference

Rocky Mountain Conference on Magnetic Resonance

Program from the Colorado "Rush to the Rockies Centennial" Spectroscopy Conference, sponsored by the Rocky Mountain Spectroscopy Society. Held in Denver, Colorado, August 10-11, 1959.

Identification Of Inclusions In Armco Ingot Iron By The Use Of Polarized Light, Carl A. Plate

Bachelors Theses and Reports, 1928 - 1970

It is the author's hope that by systematically investigating the inclusions in ingot iron and comparing their specific properties with the properties of substances known to exist as inclusions, a rapid and accurate method may be found to identify them using a polarizing microscope. Where possible photomicrographs will be used to illustrate the results obtained so that the reader may obtain a better picture of the effects produced by polarized light.

An Investigation Of The Fundamental Factors Affecting The Green Ball Characteristics In Pellet Formation, Thomas J. Wright

Bachelors Theses and Reports, 1928 - 1970

The purpose of this investigation is to determine the relative effects on the quality and characteristics of the pellets. Once the major factors effecting agglomerating materials are understood, formerly poor and nonagglomerating materials may be affected so that they will produce good quality agglomerates. Should the factors prove difficult to vary or impossible at least they may be identified and understood, thus serving as a guide for further attack or judgment in overall process design.

An Investigation Of The Effectiveness Of Certain Organic Compounds In The Flotation Of Manganese Oxide Minerals, Johannes P. Dreyer

Bachelors Theses and Reports, 1928 - 1970

This thesis has to do with the selective flotation of the manganese oxide minerals in an ore from Charco Redondo Mine, Oriente Province, Cuba. Since a sound knowledge of the nature of the emulsion-induced flotation process of these minerals does not exist, experimental research constitutes the most valuable resource for determining the extent to which different reagents influence the process. Moreover, a correlation of experimental results with the chemical and physical properties of the minerals and reagents can lead to the improvement of existing theories regarding the mechanism of a process.

Separation And Concentration Of Stibiconite, William Howard Painter

Bachelors Theses and Reports, 1928 - 1970

Primarily, the purpose of this study is to separate stibiconite from associated gangue minerals. The ore containing antimony, as an oxide stibiconite, occurs in Mexico and its benefication would be an advantage to the mineral resources of that country. While the deposit from which this ore is derived is American owned, the resource is presently non-economic. A concentrate must be derived of suitable grade for its use in a smelting operation and from which metallic antimony would be produced.

Streaming Potential Studies On Rutile, Albert R. Rule

Bachelors Theses and Reports, 1928 - 1970

This investigation was undertaken to determine some of the electrokinetic properties exhibited by rutile in solutions of various electrolytes. Results presented in this thesis are for rutile in solutions of conductivity water and in potassium chloride solutions. The data obtained in this investigation are presented graphically in the body of the thesis and are tabulated in the appendix for convenience.

Electrical Methods Of Mineral Concentration, Gordon F. Ziesing

Bachelors Theses and Reports, 1928 - 1970

The evaluation of a mineral-dressing method cannot be carried out successfully without an initial understanding of the basic fundamentals and concepts governing the operation of the method. Experimentation, governed by the understanding of the basic concepts, together with intelligent conclusions based on the experimental data, complete the evaluation of the dressing method.

Electrical concentration, being the given dressing method, will be evaluated as discussed above. As they are thoroughly covered by Mora (13), the fundamental concepts will not be given a lengthy discussion.

Electric Arc Furnace Production Of Standard-Grade Ferromanganese, Curtis Bates

Bachelors Theses and Reports, 1928 - 1970

The purpose of this investigation is to determine an operating procedure for electric arc furnace production of standard ferromanganese. An attempt was made to determine a charge which would give steady power consumption in the furnace and at the same time keep the manganese content in the slag to a minimum.

Stress-Induced Martensite Transformation In An Alloy Of The Copper-Aluminum-Nickel System, Gary D. Alexander

Bachelors Theses and Reports, 1928 - 1970

It was intended that the alloy be thoroughly investigated for martensite transformation that would make the alloy "super-elastic," but due to the many difficulties that arose this was not possible. Attempts to grow a single crystal from the cast alloy were not successful because of the difficulties that were encountered with the Kanthal resistance furnace (referred to later). Consequently, the growing of the single crystal was abandoned and the alloy was tested in the poly-crystalline form.

Growth And Examination Of Calcium Single Crystals, Richard W. Roberts

Bachelors Theses and Reports, 1928 - 1970

This report is in two sections. The first section relates to a vacuum technique for growing single crystals of calcium. The second section discusses the results of an X-ray examination of crystals of zinc by the back reflection Laue method.

The Identification Of Montana Clays By X-Ray Analysis, George Mason Maxwell

Bachelors Theses and Reports, 1928 - 1970

This thesis is to be written with the assumption that the reader is familiar with the more elementary facts of X-ray crystal analysis, such as the production and properties of X-rays, and the Bragg reflection law.

The purpose of this paper is to report on the investigations carried on to find some relatively simple means of identifying Montana Clays.

The Identification Of Montana Clays By X-Ray Analysis, David Stephen Malyevac

Bachelors Theses and Reports, 1928 - 1970

The purpose of this study is to identify the various Montana clay minerals by means of X-ray diffraction. The ultimate aim of this investigation is to identify the different clay mixtures through an analysis of their respective diffraction patterns, and diffraction patterns obtained after various chemical and thermal treatments.

Electrolytic Refining Of Copper By The Series System, Jerome Yopps

Bachelors Theses and Reports, 1928 - 1970

The purpose of this thesis investigation was to determine the characteristics of the series system of electrolytic refining of copper.

Magma 1959, Associated Students Of The Montana State School Of Mines.

Magma 1948-1997

Any year book has as its prime purpose the depiction of a school year in a manner that will recall the maximum of memories in future years. The Magma this year utilizes memories as a theme, but places a slight accent on those of the graduating seniors.

The Effect Of Rare Earth Additions On Low Alloy Steel, Sukh Dev Sehgal

Masters Theses

"Rare earth metals have for some years been used as an inoculant in nonferrous foundry practice and lately in the production of nodular iron. It has been reported that addition of rare earth metal to certain grades of stainless steel so improve the hot malleability that reduction of large size ingots in the blooming mill is now possible. It has been reported that considerable improvement in soundness and mechanical properties of steel castings and wrought products have been attained as a result of small additions of rare earth metals and oxides. In practically all investigations, it has been reported that …

Mechanization Of First Stage Graphitization In Fe- C-Si- Alloys, Dildar S. Gill

Masters Theses

"The purpose of this investigation was to study the mechanism of first stage graphitization in iron-carbon-silicon alloys in the light of results obtained by Taub, and to propose a new mechanism of graphitization. The results of preliminary experiments confirmed the findings of Taub as regards the precipitation of secondary carbides. Therefore, it was decided to extend the investigation so as to include the study of growth of secondary carbides. In order to know the chief factor responsible for the growth of secondary carbides, the activation energy was calculated. Another factor which was investigated was the site of graphite nuclei formation”--Purpose …

X-Ray Diffraction Study Of The Metal Powder Compacts, Rajendra Sharan

Masters Theses

"Various theories have been put forward about the mechanism of compacting and sintering processes. None of these theories are confirmed. The reason is that most of these theories are based on observations on metallographic specimens, which is not a particularly good tool for such a study. Little data using xray diffraction analysis is available and there seems to be a great need of making a thorough investigation in this direction.

The main object of this investigation is to study xray diffraction patterns of green compacts of aluminum, nickel and copper powders pressed under different compacting pressures to see if any …

The Vapor Pressures Of Pbo-Sb₂O₃-Sio₂ Mixtures., John Henry Smith

Masters Theses

"The removal of antimony is one of the important steps in the production of pure lead. The process of removing antimony from impure lead bullion is called "lead softening". The most common method used is to blow air into a bath of impure molten lead. The impurities, primarily antimony, arsenic and tin, if present, are oxidized and form a slag or "dross" which floats on the surface of the lead bath. A considerable amount of lead is oxidized in this step and joins the other oxidized compounds in the dross. This dross is skimmed from the bath of molten lead …

The Effect Of Heating Chill Cast Eutectics, Robert Lewis Dreshfield

Masters Theses

"This investigation is the result of the author's specific interest in two phase systems. In the past, considerable work has been done investigating the alteration of eutectoid structures; however, eutectic structures have been neglected to a great extent. Tammann did some work on the subject in 1937 as did Brown and Guy in more recent times. In both of the above cases the eutectic structure was altered by cold working and subsequent heating of the alloy.

Tammann also noted that eutectics chill cast in liquid air display a vastly different structure than those cast under equilibrium conditions and that there …

Some Properties Of Chrome-Magnesite Mixtures And Calcium Aluminate Cement-Magnesite Mixtures, Edward Charles Duderstadt

Masters Theses

"The knowledge of the physical and chemical properties of refractories is of great importance in determining their usefulness and application. The thermal expansion of refractories is of particular importance in that it affects the thermal stability of the product. A high coefficient of thermal expansion leads to greater spalling and destruction of the bricks in use. It is, therefore, desirable to develop compositions having low coefficients of thermal expansion. This investigation was undertaken (1) to determine some of the properties of chromite-magnesite refractory mixtures in an attempt to determine the optimum composition of these mixtures, the specific properties including thermal …

Lattice Constants, Thermal Expansion Coefficients And Perfection Of The Phase Tio, Hsiung Wei Li

Masters Theses

"TiO is one of the intermediate phases in the titanium - oxygen system with a crystal structure of the sodium chloride type. The phase extends from about 22 to 29 weight or about 46 to 55 atomic percent oxygen. A comprehensive survey of the physical properties of the phase has been made in previous investigations (see review of literature), but only impure titanium was available at that time. Therefore, some revision of the measurements had to be made. Also, neither the thermal expansion coefficients nor the temperature at which the lattice constants were measured were reported.

For precision determination of …

Imperfections Within Ti₂O₃ And Tio₂ Phases In The Titanium-Oxygen System, Tatsuhiko Ejima

Doctoral Dissertations

“The hexagonal-rhombohedral Ti₂O₃ phase in the Ti-O system extends from 32.5 to 34.5% oxygen b.w., with the exact composition of Ti₂O₃ nearly in the middle of the phase. Seven samples of different composition within that phase were made, and the lattice constants (a and c) and the density of each sample were determined.

The plots of the constants against the composition of the samples revealed a deviation from Vegard’s rule when approaching the exact composition of Ti₂O₃. The lattice constants of this compound, obtained by graphical interpolation were; a_{25 …}

A Study Of The Recrystallization And The Mechanical Properties Of Indium, Louis John Reitsma Jr.

Doctoral Dissertations

"The recrystallization temperature and the mechanical properties of tensile strength, elongation, reduction in area and hardness were determined for 99.97% indium. Metallographic techniques were developed and stress rupture data were obtained.

Single crystals of indium were grown in a horizontal furnace with a traveling temperature zone, and sectioned in a strain-free manner, with an etch-cutter. Because of the low recrystallization temperature of indium, no further work was done on the single crystals.

The effect of recrystallization on electrical resistance, thermoelectric force, hardness, bending strength, crystallographic orientation and microstructure was studied. The range of recrystallization temperature for small amounts of cold …

A Thermodynamic Study Of The Zirconium Sulfides, Andrew Hessler Larson

Doctoral Dissertations

"A hydrogen reduction technique was used to determine some thermodynamic properties of various zirconium sulfide phases. The equilibrium H₂S/H₂ ratios were determined as a function of temperature and composition of the condensed sulfide phases. The hydrogen sulfide content of the equilibrated gas mixtures was analyzed by an iodimetric titration procedure.

A detailed description is given for the method and apparatus used both in the preparation of the various sulfide phases and in their equilibration with a hydrogen-hydrogen sulfide gas mixture.

The composition ranger 59 to 67 atomic per cent sulfur was studied over a temperature range of …