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Microstructural Changes To Proso Millet Protein Bodies Upon Cooking And Digestion, Paridhi Gulati, You Zhou, Christian Elowsky, Devin J. Rose

Department of Food Science and Technology: Faculty Publications

Cooking results in a drastic decline in digestibility of proso millet proteins, panicins. Scanning electron and confocal microscopy were used to observe morphological changes in proso millet protein bodies upon cooking and digestion that could be associated with the loss in digestibility. Spherical protein bodies (1–2.5 mm) were observed in proso millet flour and extracted protein. Cooking did not result in any noticeable change in the size or shape of the protein bodies. However, upon digestion with pepsin the poor digestibility of cooked proso millet protein was clearly evident from the differences in microstructure of the protein bodies: large cavities …

Structural And Permeability Characterization Of Zn-Li Ferrites, M H Mesbah Ahmed, A. K. M. Akther Hossain, Shamima Choudhury

Turkish Journal of Physics

Structural characterization and magnetic properties of Zn-substituted Li ferrites with composition \linebreak Zn$_{x}$Li$_{0.45-x/2}$Fe$_{2.55-x/2}$O$_{4}$ (where x = 0.0, 0.1, 0.2, 0.3, 0.4, and 0.5) were studied by varying sintering temperature T$_{S}$ (where T$_{S}$ = 1000, 1050, 1100, 1150, 1200, and 1250 $^{\circ}$C) of the six samples. The single-phase cubic spinel structure was found by XRD patterns and scanning electron microscopy revealed the microstructure of all the samples. Permeability (real, $\mu_{i}'$ and imaginary, $\mu _{i}'')$ was found to increase with Zn substitution and also with sintering temperature. The real part of initial permeability ($\mu_{i}')$ was found to depend on the density and …

Seed Structure And Its Taxonomic Implications For Genus Thlaspi Sensu Lato Sectionsnomisma, Thlaspi, And Pterotropis (Brassicaceae), Mehmet Cengi̇z Karai̇smai̇loğlu, Osman Erol

Turkish Journal of Botany

We studied morphological and anatomical characteristics of seeds of 22 taxa in the sections Nomisma, Thlaspi, and Pterotropis of Thlaspi sensu lato from Turkey and the significance of these characters in a taxonomical context. The results show that the taxa differ from each other in terms of seed shape and color. The seed size ranges from 1.25 mm to 2.99 mm in length and from 0.66 mm to 2.16 mm in width, Thlaspi rosulare and T. tatianae having the largest and T. annuum having the smallest seeds. The seed surface ornamentation is classified into nine types: reticulate-areolate, scalariform, reticulate, reticulate-foveate, …

Seed Structure Of Some Taxa Of The Genus Crocus L. (Iridaceae) Series Crocus, Mehmet Cengi̇z Karai̇smai̇loğlu, Levent Şik, Almila Gemi̇ci̇oğlu, Osman Erol

Turkish Journal of Botany

In this study, the macro- and micromorphological seed characteristics of the genus Crocus L. series Crocus taxa, including C. pallasii , C. turcicus , C. dispathaceus , C. asumaniae , C. mathewii , C. thomasii , C. oreocreticus , and C. cartwrightianus , were observed. Morphological characteristics, such as the size, shape, color, and seed surface structures, were analyzed using stereo and scanning electron microscopes. Testa layer structures including the outer and inner testae, phytomelan layer structure and thickness, and seed endosperm cell features were studied. Differences in the seed, raphe size, seed surface patterns, inner testa features, and phytomelan …

Enhanced Corrosion Resistance And Cytocompatibility Of Biomimetic Hyaluronic Acid Functionalised Silane Coating On Az31 Mg Alloy For Orthopaedic Applications, Sankalp Vinod Agarwal, Marie Noëlle Labour, David A. Hoey, Brendan Duffy, James Curtin, Swarna Jaiswal

Articles

This paper reports the corrosion resistant and cytocompatible properties of the hyaluronic acid-silane coating on AZ31 Mg alloy. In this study, the osteoinductive properties of high molecular weight hyaluronic acid (HA, 1–4 MDa) and the corrosion protection of silane coatings were incorporated as a composite coating on biodegradable AZ31 Mg alloy for orthopaedic applications. The multi-step fabrication of coatings first involved dip coating of a passivated AZ31 Mg alloy with a methyltriethoxysilane-tetraethoxysilane sol-gel to deposit a dense, cross-linked and corrosion resistant silane coating (AZ31-MT). The second step was to create an amine-functionalised surface by treating coated alloy with 3-aminopropyl-triethoxy silane …

Comparative Study Of Cv3 Carbonaceous Chondrites Allende And Bali Using Micro-Raman Spectroscopy And Sem/Eds, Raka Paul

All Graduate Theses, Dissertations, and Other Capstone Projects

The birth of the solar system (over 4 billion years) is speculated to have happened from a nebula, swirling and compacting in localized regions to eventually form the Sun and planets. This complex process consists of numerous changes and intermediary steps, yet to be fully understood. Carbonaceous chondritic meteorites are relics of that process and therefore have potential to reveal information about the formation history. Several theories have been formulated linking their composition to planet formation. This study focusses on two carbonaceous chondritic specimens, Allende and Bali, both of the group CV and petrologic type 3. CV meteorites are abundant …

Compositional And Topographical Characterization Of Carbonaceous Chondritic Meteorites Moss And Murray Using Micro-Raman Spectroscopy And Sem/Eds, Aaron Stokke

All Graduate Theses, Dissertations, and Other Capstone Projects

Carbonaceous chondritic meteorites are considered some of the most primitive surviving materials from the formation of our solar system. Thus, these objects can provide information about planet formation through their physical properties (such as structure, composition, and morphology) which can be characterized using microscopy and spectroscopy techniques. In this work, the analytical methods of Raman spectroscopy, scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), and optical microscopy are applied to determine the mineralogical, topographical, and elemental compositions of two carbonaceous chondritic fragments: Moss and Murray. Both samples were comprised of chondrules and matrix while Moss contained chondrule rims and Murray …

The Relationship Between Structural Parameters And Mechanical Properties Of Cactus Spines, Jorge Armando Martinez, Pamela Liz Szeto, Theresa Mae Stewart

Materials Engineering

Considering an increasing interest in renewable, biodegradable resources that exhibit excellent mechanical properties, 24 species of cactus spines were investigated using three-point bend testing, X-ray diffraction (XRD) for structural parameters, and scanning electron microscopy (SEM) to analyze fracture surfaces. Additionally, a density of about 1.3 g/cm3 was measured for each spine utilizing the displacement method, closely matching existing data from literature. The flexural modulus varied greatly between species, ranging from 1.22 GPa (Echinocactus polycephalus) to 43.58 GPa (Stenocereus thurberi). In addition, flexural strength and strain to failure was also measured for each spine. XRD analysis of …

Design, Evaluation, And Particle Size Characterization Of An In-Duct Flat Media Particle Loading Test System For Nuclear-Grade Asme Ag-1 Hepa Filters, Matthew Christopher Wong

Theses and Dissertations

The design and performance evaluation of in-duct, isokinetic samplers capable of testing flat sheet, nuclear-grade High Efficiency Particulate Air (HEPA) filters simultaneously with a radial filter testing system is discussed in this study. Evaluations within this study utilize challenge aerosols of varying particle diameters and masses such as hydrated alumina, Arizona test dust, and flame-generated acetylene soot. Accumulated mass and pressure drop for each in-duct sampler is correlated to the full-scale radial filter accumulated mass from initial to 10 in w. c. of loading. SEM imaging of samples at 25%, 50%, 75% and 100% loading verifies particle sizes with instrumentation …

Using Principal Component Analysis To Improve Fallout Characterization, Derek W. Haws

Theses and Dissertations

Previous research conducted at Lawrence Livermore National Laboratory (LLNL) and the Air Force Institute of Technology (AFIT) has shown a correlation between actinide location and elemental composition in fallout from historic weapons testing. Fifty spherical fallout samples were collected from near ground zero of a surface burst weapons test. The samples were mounted in an aluminum puck then ground and polished to a hemisphere exposing the central plane. Physical morphologies of the samples ranged from clear to opaque with inclusions, voids, and/or uniform characteristics. Spectroscopy data were collected using optical microscopes and scanning electron microscopy (SEM), with radioactivity recorded through …

Thermal Conductivity Performance Of Polypropylene Composites Filled With Polydopamine-Functionalized Hexagonal Boron Nitride, Lin Chen, Hong-Fei Xu, Shao-Jian He, Yi-Hang Du, Nan-Jie Yu, Jun Lin, Sergei I. Nazarenko

Faculty Publications

Mussel-inspired approach was attempted to non-covalently functionalize the surfaces of boron nitride (BN) with self-polymerized dopamine coatings in order to reduce the interfacial thermal barrier and enhance the thermal conductivity of BN-containing composites. Compared to the polypropylene (PP) composites filled with pristine BN at the same filler content, thermal conductivity was much higher for those filled with both functionalized BN (f-BN) and maleic anhydride grafted PP (PP-g-ma) due to the improved filler dispersion and better interfacial filler-matrix compatibility, which facilitated the development of more thermal paths. Theoretical models were also applied to predict the composite thermal conductivity in which the …

Micromorphological Studies On The Genus Lotus L. (Fabaceae: Loteae) From Egypt, Momen Zareh, Ahmed Faried, Nashwa Farghaly

Turkish Journal of Botany

Trichomes, epidermal cell features, and seed coat sculpturing of 12 Lotus taxa from Egypt were studied using scanning electron microscopy. In addition, statistical analysis for the taxa under investigation was carried out. The results revealed that trichomes have high taxonomic significances between studied taxa. Anticlinal and periclinal cell walls and epidermal cell shape for the stem, leaf, and calyx for each taxon were examined. Seed coat sculpturing exhibited 4 main different surface patterns categories: rugose, reticulate, sulcate, and verrucate. These features can serve as good diagnostic characters at the species level of the genus Lotus.

Regulation Of Functional Activities And Essential Oil Production In Vetiveria Zizanioides L. Nash After γ-Irradiated Sodium Alginate Elicitation, Asfia Shabbir, Mohammad Masroor Akhtar Khan, Yawar Sadiq, Hassan Jaleel, Bilal Ahmad, Moin Uddin

Turkish Journal of Biology

Upon irradiation, marine polysaccharides undergo depolymerization, leading to formation of oligosaccharides that elicit various biological activities in plants. Taking a step further on the previously established growth-promoting activity of irradiated sodium alginate (ISA), structural rearrangements in ISA were analyzed using complementary techniques to develop an understanding of the structure-property relationship. The essential oil (EO) of vetiver (Vetiveria zizanioides L. Nash) immensely benefits the perfumery industry, proving itself as an economically important crop. A pot experiment was designed to test the effect of water-soluble ISA fractions on the growth, physiology, and EO production of vetiver. The structural characterization of radiation-induced sodium …

A Comparative Study Of Intraradicular Enterococcus Faecalis Biofilm Removal With Three Root Canal Treatment Systems: A Scanning Electron Microscopy Evaluation, Cyrous Ardalan

Theses and Dissertations

The objective of this study was to evaluate the biofilm removal efficacy of three root canal treatment systems: ProUltra® PiezoFlow™, traditional needle irrigation, and the GentleWave® system in an ex-vivo benchtop study. Twenty-four extracted maxillary and mandibular molars were selected. Teeth were all instrumented to a master apical file size #25 with 4% taper. Teeth were then randomly divided into four experimental groups and two control groups. The root canals were inoculated with a culture of Enterococcus faecalis and incubated for five weeks to form a biofilm. Each group was then treated with one of the different root canal treatment …

Biochemical And Histological Differences Between Costal And Articular Cartilages, Michael W. Stacey

Bioelectrics Publications

Biologically, costal cartilage is an understudied tissue type and much is yet to be learned regarding underlying mechanisms related to form and function, and how these relate to disease states, specifically chest wall deformity. Chest wall deformities have a component of inheritance, implying underlying genetic causes; however the complexity of inheritance suggests multiple genetic components. At our Centre investigations were performed on gene expression of key select genes from costal cartilage removed at surgery of patients with chest wall deformity to show high expression of decorin, a key player in collagen fiber formation and growth. Also, the degree of tissue …

New Marked Point Process Models For Microscopy Images, Dae Woo Kim

Open Access Dissertations

In developing new materials, the characterization of microstructures is one of the key steps. To characterize the microstructure, many microscope modalities have been devised and improved over decades. With the increase in image resolution in the spatial and time domains, the amount of image data keeps increasing in the fields such as materials science and biomedical engineering. As a result, image processing plays a critical role in this era of science and technology. In materials image analysis, image segmentation and feature detection are considered very important.

The first part of this research aims to resolve the segmentation problem caused by …

The Higher-Level Phylogeny Of Cerambycidae Sensu Lato And New Insights Into The Structure Of Tufted Antennae, Stephanie Haddad

Electronic Theses and Dissertations

Cerambycidae (longhorned beetles) is a species-rich family of mostly wood-feeding beetles containing nearly 35,000 species. It belongs to the superfamily Chrysomeloidea and includes many ecologically and economically significant species. The higher-level phylogeny of Cerambycidae has never been robustly reconstructed using molecular phylogenetic data or a representative sample of higher taxa, and its internal relationships and evolutionary history remain the subjects of ongoing debate. As such, the systematics and evolution of Chrysomeloidea were reviewed herein to provide context for reconstructing the phylogeny of longhorned beetles using molecular phylogenetic data/analyses. The first higher-level molecular phylogeny of Cerambycidae was reconstructed via analysis of …

Modification And Utilization Of Nanoporous Gold For Loading And Release Of Drugs, Ibtisam Mohammed Al-Badri

Theses

Nanoporous gold (np-Au) is a sponge-like structure of gold, which can be created by removing the less noble element from the precursor alloy, most typically silver or copper, using different chemical or electrochemical methods. It consists of interconnected ligaments and gaps between the ligaments, whose width can range from a few nanometers to a few hundreds of nanometers, creating a high surface area-to-volume ratio. Due to its many important properties (e.g., conductivity, high surface area-to-volume ratio, plasmonic response, biocompatibility, chemically inertness, and physically robustness), np-Au is suitable for different types of applications, including as a transducer for biosensors, in catalysis, …

Evaluation Of Strain Distortion Correction Protocol Using Scanning Electron Microscopy And Digital Image Correlation, Alexandra Mallory, Alberto Mello, Michael Sangid

The Summer Undergraduate Research Fellowship (SURF) Symposium

Scanning electron microscopy in combination with digital image correlation (SEM-DIC) is a useful technique for measuring strain in materials at the micro-scale. In particular, it can be used to identify micro-scale strain localizations that are the precursor to material failure. While SEM produces high resolution images of the microstructure, the images also contain a large amount of distortion that, during DIC, will result in distorted strain values that require correction. In this project, a nickel-based alloy underwent cyclic mechanical fatigue at three different high temperatures to a targeted maximum strain. Scanning electron microscopy imaging was done on a 200x150μm area …

Investigation Of Bond, Microstructure And Post-Fire Behavior Of Gfrp Reinforcement For Concrete, Omid Gooranorimi

Open Access Dissertations

Glass fiber reinforced polymer (GFRP) bars are emerging as concrete reinforcements especially in applications where corrosion resistance properties are required. This dissertation focuses on bond properties, microstructure and post-fire behavior of GFRP bars. First, the bond of three GFRP bars with different surface characteristics was investigated by performing pull-out tests. A parametric bond-slip relationship was proposed for the GFRP bar with sand coated surface. The parameters were found by performing sensitivity analysis. The proposed bond-slip law was employed in an FEM model to predict the failure mode. Additionally, the model was employed in a GFRP-RC slab to replace the unrealistic …

Electrospinning Of Polymeric Solutions Using Opuntia Ficus-Indica Mucilage And Iron Oxide For Nanofiber Membranes For Treating Arsenic Contaminated Water, Venkatesh Eppili

USF Tampa Graduate Theses and Dissertations

Water is the essential part of every organism and it is also a vital constituent of healthy living and diet. Unfortunately water contamination over the past decade has increased dramatically leading to various diseases. As technology advances, we are detecting many pollutants at smaller levels of concentrations. Arsenic (As) is one of those major pollutants, and Arsenic poisoning is a condition caused due to excess levels of arsenic in the body. The main basis for Arsenic poisoning is from ground water which naturally contains high concentrations of arsenic. A case study from 2007 states that over 137 million people in …

Synthesis And Properties Of Acrylated Epoxidized Soybean Oil Copolymers And Their Composites With Natural Fillers, Andrew Jacob Fox

Honors Theses

As the global supply of petrochemicals diminishes, the polymer industry will need to incorporate renewable resources into the production process. Acrylated expoxidized soybean oil, a modified plant oil, is one possible candidate for use as a monomer in plastics. When polymerized alone, AESO creates a fairly unusable polymer, with poor physical and material properties. To improve the properties, the monomer can be copolymerized with styrene and other additives and can be incorporated into a composite to further increase the usability. By using biorenewable fillers, the overall use of nonrenewable materials in the composite can be further decreased. In this research, …

The Micrograph Image Of Early Experimental Dental Caries In Permanent Teeth, Vo Truong Nhu Ngoc, Truong Manh Dung, Le Quynh Anh, Pham Thi Hong Thuy, Tran Tuan Anh

Journal of Dentistry Indonesia

Study on the structure and the mechanism of the formation of early caries is an important premise for evaluating the caries-preventive methods. Objective: To describe micrograph images of experimental carious lesions at early stage in permanent teeth in Vietnamese. Methods: There were 60 permanent extracted premolars from patients aged 18-25 used in this study. After cleaning and removing the remaining soft tissue, each tooth was painted with acid-resistant coating leaving an enamel window of approximately 1 × 1mm2 on the buccal surface. The artificial carious lesion was performed by soaking the teeth for 96 hours in the demineralization solution and …

Direct Imaging Of Coexisting Ordered And Frustrated Sublattices In Artificial Ferromagnetic Quasicrystals, Barry Farmer, Vinayak Shantaram Bhat, Eric Teipel, J. Unguris, D. J. Keavney, Jeffrey Todd Hastings, Lance E. De Long

Physics and Astronomy Faculty Publications

We have used scanning electron microscopy with polarization analysis and photoemission electron microscopy to image the two-dimensional magnetization of permalloy films patterned into Penrose P2 tilings (P2T). The interplay of exchange interactions in asymmetrically coordinated vertices and short-range dipole interactions among connected film segments stabilize magnetically ordered, spatially distinct sublattices that coexist with frustrated sublattices at room temperature. Numerical simulations that include long-range dipole interactions between sublattices agree with images of as-grown P2T samples and predict a magnetically ordered ground state for a two-dimensional quasicrystal lattice of classical Ising spins.

Synthesis And Characterization Of Kesterite Cu2znsns4 (Czts) Thin Films For Solar Cell Application, Mohamed M.A. Abusnina

Electronic Theses and Dissertations

The quaternary compound Cu₂ZnSnS₄ (CZTS) gained considerable attention in the last decade due to its potential as an active-layer semiconductor for low-cost thin-film solar cells. The material is composed of nontoxic and Earth-abundant constituents, has optical properties suitable for photovoltaic application, and can be synthesized using a wide variety of methods.

Polycrystalline CZTS was grown in this work using vacuum-based deposition to first deposit metal films (precursors) of Cu, Zn, and Sn. In a subsequent step, the precursors underwent an annealing treatment in sulfur vapor environment (sulfurization) to form CZTS. Using sputtering, a physical vapor deposition (PVD) …

Vietnamese Ganoderma: Growth, Peculiarities, And Low-Molecular Composition Compared To European And Siberian Strains, Olga Tsivileva, Thao Nguyen, Long Vu, Nikolai Yurasov, Marina Chernyshova, Alexander Petrov, Viktor Galushka, Alexei Markin, Oleg Koftin

Turkish Journal of Botany

The species from the genus Ganoderma are known to be extremely important macrofungi in fundamental biological, medicinal, and socioeconomic aspects. The present communication describes the brief morphological description, macro- and microscopic details, and chemical constituents of the representatives of five species of Ganoderma mushroom collected from different sites in Vietnamese National Parks. These species were Ganoderma colossus, G. Neojaponicum, G. Cattienensis, G. Lucidum, and G. Applanatum. Three additional herbarium strains of Ganoderma from European and Siberian regions have been implemented in the present framework for the purposes of comparison. Cultural characterization on solid and liquid fermentation, and scanning electron microscopy …

Needle Characteristics Of Lebanon Cedar (Cedrus Libani A.Rich.): Degradation Of Epicuticular Waxes And Decrease Of Photosynthetic Rates With Increasing Needle Age, Ayli̇n Güney, Reiner Zimmermann, Anna Krupp, Klaus Haas

Turkish Journal of Agriculture and Forestry

The evergreen conifer Cedrus libani A.Rich. İs frost- and drought-tolerant and of economic and ecological importance. It has valuable timber and thus has promising potential for cultivation within and outside its natural distribution. Our aim was to determine the morphological and physiological characteristics of C. Libani needle leaves with respect to epicuticular waxes, photosynthetic assimilation rates, and needle age. The study was conducted in the Cedar Research Forest near Elmalı, Antalya (SW Turkey) at 1650 m a.s.l. An equation to calculate needle surface area from needle length was created (R2 = 0.96) for adult cedar needles. The form factor for …

Characterization Of The Ability Of Yeast Probiotics And Paraprobiotics To Directly Interact With Gram-Positive And Gram-Negative Bacteria, Gabriel Alviola Posadas

Theses and Dissertations

Yeast probiotics and paraprobiotics, live and inactivated yeast cells, respectively, improve health and performance of livestock by stabilizing the intestinal microbial community. They have also been used for infection prevention and treatment. Despite much research already conducted, the mechanism of direct antagonism, or adhesion of bacteria to the probiotic/paraprobiotic, is under characterized. Additionally, it is unknown which probiotic/paraprobiotic is optimal to use for specific infections. The interactions between the yeast and certain pathogens were analyzed qualitatively with scanning electron microscopy (SEM) and quantitatively with membrane filtration assays. Gram-positive bacteria were found to exhibit specificity under SEM. Through membrane filtration, Listeria …

Application Of 3d Printing Technology In Porous Anode Fabrication For Enhanced Power Output Of Microbial Fuel Cells, Bin Bian

Electronic Thesis and Dissertation Repository

Microbial fuel cells (MFCs) are widely researched for application in wastewater treatment. However, the current anodes used in MFCs often suffer from high fabrication cost and uncontrollable pore sizes. In this thesis, three-dimensional printing technique was utilized to fabricate anodes with different micro pore sizes for MFCs. Copper coating and carbonization were applied to the printed polymer anodes to increase the conductivity and specific surface area. Voltages of MFCs with various anodes were measured as well as other electrochemical tests such as linear sweep voltammetry and electrochemical impedance spectroscopy. 3D copper porous anode produced higher maximum voltages and power densities …

An Evaluation Of Biofield Treatment On Thermal, Physical And Structural Properties Of Cadmium Powder, Mahendra Kumar Trivedi, Gopal Nayak, Shrikant Patil, Rama Mohan Tallapragada, Omprakash Latiyal, Snehasis Jana

Mahendra Kumar Trivedi