Discovery, Preparation And Identification Of A New Type Of Oxyphenisatine Di（Acetate） Analogue In Dietary Supplement,
2024
Hubei Provincial Institute for Food Supervision and Test, Wuhan, Hubei 430075, China;Hubei Provincial Engineering and Technology Research Center for Food Quality and Safety Test, Wuhan, Hubei 430075, China;Key Laboratory of Detection Technology of Focus Chemical Hazards in Animal-derived Food for State Market Regulation, Wuhan, Hubei 430075, China
Discovery, Preparation And Identification Of A New Type Of Oxyphenisatine Di（Acetate） Analogue In Dietary Supplement, Xia Jintao, Wu Wanqin, Zhu Songsong, Jiang Feng
Food and Machinery
Objective: To find, prepare and identify a new oxyphenisatine di（acetate） analogue. Methods: A suspected derivative of oxyphenisatine di（acetate） was found by high-performance liquid chromatography-quadrupole-time-of-flight-mass spectrometry during the routine screening of weight loss healthcare product. The compound was isolated and purified by column chromatography, and the possible structures were inferred from the information of isotope mass spectra, secondary ion mass spectra, one-dimensional and two-dimensional NMR spectra. Finally, all possible structures were prepared by de novo synthesis strategy, and their fine structures were confirmed by spectral comparison. Results： The compound was identified as 5-Cl oxyphenisatine di（acetate）, a new type of oxyphenisatine di（acetate）, …
Optimization Of Culture Conditions For Maximum Viable Count Of Brevibacillus Laterosporus Based On Mtt Colorimetry And Response Surface Methodology,
2024
College of Agriculture, Henan University of Science and Technology, Luoyang, Henan 471000, China
Optimization Of Culture Conditions For Maximum Viable Count Of Brevibacillus Laterosporus Based On Mtt Colorimetry And Response Surface Methodology, Song Peng, Li Lixiang, Zhao Biao, Wang Zele, Sun Xingxin
Food and Machinery
Objective: This study aimed to explore the optimal medium composition and culture conditions for obtaining the maximum viable count of Brevibacillus laterosporus. Methods: Based on establishing the correlation regression equation between the MTT colorimetric method and plate counting method, the optimal medium composition (carbon source, nitrogen source, inorganic salt) and fermentation conditions (initial pH, temperature, inoculation amount, KH2PO4) for obtaining the maximum viable count of B. laterosporus were optimized. Results: A significant linear correlation for viable count determination between MTT colorimetry and plate counting (R2>0.999) was found; Maltose, CaCl2, initial …
Green Analysis Of Glyphosate And Its Metabolite Amino Methyl Phosphoric Acid In Tea,
2024
Hubei Provincial Institute for Food Supervision and Test, Wuhan, Hubei 430075, China;Key Laboratory of Detection Technology of Focus Chemical Hazards in Animal-derived Food for State Market Regulation, Wuhan, Hubei 430075, China;Hubei Provincial Engineering and Technology Research Center for Food Quality and Safety Test, Wuhan, Hubei 430075, China
Green Analysis Of Glyphosate And Its Metabolite Amino Methyl Phosphoric Acid In Tea, Li Beibei, Wang Wei, Jiang Feng, Wang Huixia, Chen Li
Food and Machinery
Objective： This study aimed to develop an ion chromatography-tandem mass spectrometry (IC-MS/MS) for the analysis of glyphosate and its metabolite amino methyl phosphoric acid (AMPA) residues in tea without derivatization. Methods： Tea samples were ultrasonically extracted with 20 mmol/L NaOH aqueous solution and cleaned up by dispersive solid-phase extraction (150 mg primary-secondary amine (PSA), 15 mg C18, 15 mg graphitized carbon black (GCB)). The samples were separated on an ion chromatographic column AS11-HC-4 μm (2 mm×250 mm) by using an isometric elution procedure of 35 mmol/L aqueous solution of sodium hydroxide as mobile phase. A multiple reactions monitoring …
Migration Quality Of Formaldehyde In The Polylactic Acid Straw Detected By Hplc,
2024
Yangzhou Centre for Food and Drug Control, Yangzhou, Jiangsu 225000, China
Migration Quality Of Formaldehyde In The Polylactic Acid Straw Detected By Hplc, Hu Yun, Zou Yongping, Zhou Yuanyuan, Wang Shuai, Liang Zhichun
Food and Machinery
Objective: A formaldehyde detection method was established for the accurate analysis of the migration of formaldehyde in water and acid simulants from the polylactic acid straws. Methods: The preferred chromatographic conditions were: mobile phase water-acetonitrile (Vwater∶Vacetonitrile of 55∶45), column temperature of 35 ℃, detection wavelength of 355 nm. The optimized 2,4-dinitrophenylhydrazine derivative conditions were: the acetic acid in acidic 2,4-dinitrophenylhydrazine solution of 1.5 mL/100 mL (pH 3.07), the molar ratio of 2,4- dinitrophenylhydrazine of quadruple formaldehyde, the reaction temperature of 45 ℃, and the reaction time of 40 min. Results: The linear equation of formaldehyde-2,4-dinitrobenzene …
Rice Fatty Acid Detection Method Combining Hyperspectral Technology With Improved Lssvm,
2024
Lu'an Vocational and Technical College, Changzhi, Shanxi 046000, China
Rice Fatty Acid Detection Method Combining Hyperspectral Technology With Improved Lssvm, Fu Juanjuan, Chen Chunru, Huang Zhenlin, Sun Feng
Food and Machinery
Objective: To solve the problems of low accuracy and poor efficiency in the existing rice quality testing methods of food enterprises. Methods: Based on a hyperspectral data acquisition system, a fast and non-destructive detection method for stored rice quality was proposed, which combined an improved bacterial foraging algorithm and least squares support vector machine. By applying the improved bacterial foraging algorithm, the hyperparameters (regularization parameter and kernel parameter) of the least squares support vector machine were optimized to achieve rapid and non-destructive detection of rice quality. its performance was analyzed through experiments. Results: The proposed method can achieve rapid and …
Application Of Gas Chromatography Combined With Stoichiometry In Discriminant Analysis Of Pseudo Mixtures Of Walnut Oil And Rapeseed Oil,
2024
Nanyang Product Quality Inspection and Testing Center, Nanyang, Henan 473000, China
Application Of Gas Chromatography Combined With Stoichiometry In Discriminant Analysis Of Pseudo Mixtures Of Walnut Oil And Rapeseed Oil, Wu Shibo, Liu Yanqi, Li Chao, Ma Ning, Yao Heng, Wang Mengmeng
Food and Machinery
Objective: This study aimed to investigate different discriminant analysis models for pseudo-mixtures of walnut oil and rapeseed oil. Methods: Gas chromatography technology was used to analyze the fatty acid content in the adulterated mixture of walnut oil and rapeseed oil. Chemical stoichiometric methods were used to model the gas chromatography data, and discriminant analysis was performed on different proportions of walnut oil and rapeseed oil mixtures. Results: Pure walnut oil and adulterated walnut oil were distinguihed by using Principal Component Analysis (PCA) identified, and percentage of adulteration in the sample was calculated. 83.33% of the samples were successfully categorized using …
Rapid Determination Of Moisture Content Of High Cellulose And Lignin Materials By Near-Infrared Diffuse Reflectance Spectroscopy,
2024
College of Food Science and Technology, Hunan Agricutural University, Changsha, Hunan 410128, China;Hunan Onyear Industry Co., Ltd., Xiangtan, Hunan 411228, China
Rapid Determination Of Moisture Content Of High Cellulose And Lignin Materials By Near-Infrared Diffuse Reflectance Spectroscopy, Yao Li, Li Zongjun, Zhu Menjun, Dai Hairong, Li Xiaoyan
Food and Machinery
Objective: To establish a rapid method for moisture detection of high cellulose and lignin materials. Methods: The areca nut, a Chinese herbal medicine containing high cellulose and lignin, was selected. Use a near-infrared spectrometer to collect near-infrared diffuse reflectance spectra. Apply NIR Cal modeling software to preprocess the spectral data, select the optimal feature wavelengths, and use partial least squares (PLS) analysis to establish a quantitative model for areca nut moisture content. Results: A quantitative model for areca nut moisture content was acquired, with the coefficient of determination of 0.994 2, the root mean square of the calibration error (RMSEC) …
Numerical Simulation Of The Effect Of Freezing Sword Structure On The Ice Performance Of Block Ice Machine,
2024
Tianjin University of Commerce, Key Laboratory of Tianjin Refrigeration Technology, Tianjin 300314, China
Numerical Simulation Of The Effect Of Freezing Sword Structure On The Ice Performance Of Block Ice Machine, Sun Huan, Yang Kai, Liu Xiaotong
Food and Machinery
Objective: To add a freezing sword inside the evaporator of the ice mould of a direct-cooled block ice machine to achieve rapid ice production. Methods: COMSOL was used to simulate the effects of the cross-sectional shape of the freezing sword and the freezing sword inclination angle on the ice production process. Results: As the ice making process continued, the average internal temperature of the ice mould with additional freezing swords of different cross-sectional shapes decreased and the volume fraction of solid phase in the ice mould increasedd with time, but the average internal temperature of the ice mould with additional …
Establishment And Experiment Verification Of Screw Thrust Model Of Spiral Robot For Granary,
2024
School of Mechanical Engineering, Wuhan Polytechnic University, Wuhan, Hubei 430023, China
Establishment And Experiment Verification Of Screw Thrust Model Of Spiral Robot For Granary, Zhao Xianfeng, Yin Qiang, Yu Junpeng, Yang Liu, Zhang Yonglin
Food and Machinery
Objective： To clarify the interaction mechanism model between screw and grain in grain pile depth, and to determine the mechanical characteristics of screw of spiral robot for granary at different speeds and depths, so as to provide the design basis for the motion control system. Methods： Using mathematical model, combining Janssen grain storage pressure theory and Janosi shear-displacement equation, the shear stress model was established, and then the thrust model of screw was derived from the shear stress model. Through the design and construction of the experimental device, the combination of different speed and pressure was used to carry out …
Simulation Research On The Transfer And Collection Part Of Warehouse Bottom Surplus Grain Cleaning Device,
2024
School of Mechanical and Electrical Engineering, Henan University of Technology, Zhengzhou, Henan 450001, China
Simulation Research On The Transfer And Collection Part Of Warehouse Bottom Surplus Grain Cleaning Device, He Yingzhen, Wang Mingxu, Wang Wei, Li Shubo
Food and Machinery
Objective: To verify whether the structure design of the conveying part and the collecting part of the cleaning device designed for the surplus grain at the bottom of the cottage warehouse is reasonable, and to determine the key parameters of the device operation, so as to avoid the waste of procurement and manufacturing. Methods: Based on discrete element method, EDEM simulation software was used to simulate the operation effect of the transfer part and the collection part, and the drop rate was used as the evaluation parameter. Results: Through the observation and analysis of the simulation results, it was concluded …
Design And Processing Test Of Eel Automatic Filleting Machine,
2024
Hubei University of Technology, Hubei Engineering Technology Research Center for Intelligent Agricultural Machinery, Wuhan, Hubei 430068, China
Design And Processing Test Of Eel Automatic Filleting Machine, Liu Mingyong, Ouyang Zhouhuan, Han Xinguang, Xiang Xue, Zhu Lin
Food and Machinery
Objective: A special cutting mechanism for slicing elongated fish with smooth surface was designed. Methods: Taking the slimy eel as the research object, the mechanism of clamping and cutting operation was analyzed. Taking cutting quality and cutting time as test indexes, the influence of main parameters such as clamping wheel speed, cutting tool speed and clamping wheel surface geometry on cutting quality and cutting time were investigated. Results: The main factors affecting cutting quality were blade speed and clamping wheel limit height, and the most important factors affecting cutting time were clamping wheel speed. When the clamping wheel limit height …
Effects Of Irradiation Methods On Quality And Shelf Life Of Choerospondias Axillaris Pastilles,
2024
Hunan Province Grain and Oil Product Quality Monitoring Center, Changsha, Hunan 410008, China
Effects Of Irradiation Methods On Quality And Shelf Life Of Choerospondias Axillaris Pastilles, Mao Qingxiu, Xu Yuanfang, Chen Quling, Zhang Qiling, Li Wenge, Yang Yi
Food and Machinery
Objective: This study aimed to explore the best irradiation method and irradiation dose to treat Choerospondias axillaris pastilles. Methods: C. axillaris pastilles were irradiated with 0～10 kGy gradient dose of 60Co-γ ray and electron beam respectively, the changes of the indexes including microbial load, protein, fat, total sugar, L(+)-ascorbic acid, organic acids, pH value, sensory quality, and the shelf life quality stored in 0～360 days at room temperature were studied. Results: 60Co-γ ray and electron beam irradiation both had bactericidal effects on C. axillaris pastilles, all microbial limit indexes including aerobic bacterial count, coliform bacteria, …
Simulation And Analysis Of Forced Air Precooling Performance Of Apples With Different Fruit Diameters,
2024
Key Laboratory of Refrigeration Technology, Tianjin University of Commerce, Tianjin 300314, China;School of Mechanical Engineering, Tianjin University of Commerce, Tianjin 300314, China
Simulation And Analysis Of Forced Air Precooling Performance Of Apples With Different Fruit Diameters, Tian Jinjin, Gu Xudong, Zhang Zhe, Zhu Zhiqiang, Ji Xian
Food and Machinery
Objective: To analyze the effect of apples of different fruit diameters on differential pressure precooling under the same box. Methods: Based on the spherical analogy model and heat transfer theory, the CFD unsteady SST k-ω turbulence model was used to numerically simulate the differential pressure precooling of apples with different air supply air speed, temperature, box opening size and fruit diameter, and three different working conditions were selected for accuracy. The simulation scheme of mixed orthogonal test was used to discuss the effects of different factors and different fruit diameters on the cooling rate and pre-cooling uniformity. Results: …
Study Of Quality Changes In High Moisture Wheat After Hot Air Drying,
2024
School of Food and Strategic Reserves, Henan University of Technology, Zhengzhou, Henan 450001, China
Study Of Quality Changes In High Moisture Wheat After Hot Air Drying, Fan Mengke, Chen Pengxiao, Liu Ye, Zhu Wenxue, Jiang Mengmeng, Zhang Yurong, Wang Xiaowan, Wu Jianzhang
Food and Machinery
Objective: To study the effects of different drying processes on the quality of high moisture wheat. Methods: Investigates the changes of wheat quality under different drying processes in three dimensions: appearance quality, nutritional quality and processing quality. Three indicators, namely colour, wet gluten content and drying rate, were selected as response values and combined with response surface analysis to predict the optimal drying process for high moisture wheat. Results: Drying temperature was the main influencing factor. As the temperature increased, the colour of the wheat deepened, the crude protein content decreased, the wet gluten content decreased, the water absorption of …
Phenolic Compositions And In Vitro Antioxidant Activities Of Tartary Buckwheat Wine Lees,
2024
Wuliangye Yibin Co., Ltd., Yibin, Sichuan 644000, China;Solid-state Fermentation Resource Utilization Key Laboratory of Sichuan Province, Yinbin, Sichuan 644000, China
Phenolic Compositions And In Vitro Antioxidant Activities Of Tartary Buckwheat Wine Lees, Zhao Jiawei, Zheng Jia, Li Mao, Zhang Weijian, Yan Junlin
Food and Machinery
Objective: Explored the composition and content of phenolic compounds in tartary buckwheat wine lees, and study their antioxidant activity. Methods: Phenolic compounds in tartary buckwheat wine lees were analyzed by HPLC and LC-MS. And evaluating its antioxidant activity. Results: 7 phenolic compounds were identified from tartary buckwheat wine lees, including 5 flavonoids, with the highest content of rutin of （9.350±0.050） mg/g, followed by quercetin, isoquercetin, kaempferol-3-o-rutoside and kaempferol of two phenolic compounds. At 0.5 mg/mL, the scavenging rates of hydroxyl free radical, ABTS+ and DPPH free radical reached （73.29±0.09）%, （96.21±0.25）% and （82.55±0.68）%, respectively, with FRAP value of …
Changes Of Volatile Aroma Components And Biochemical Components In Fenghuang Dancong Tea During Processing,
2024
Institute of Chemistry and Environment Engineering, Hanshan Normal University, Chaozhou, Guangdong 521041, China
Changes Of Volatile Aroma Components And Biochemical Components In Fenghuang Dancong Tea During Processing, Li Zhangwei
Food and Machinery
Objective： This study aimed to optimize the processing technology of Fenghuang dancong tea. Methods： Headspace solid phase microextraction (HS-SPME), Gas chromatography-mass spectrometry (GC-MS), and spectrophotometer were used to extract, determine and analyze the volatile aroma and non-volatile biochemical components of Fenghuang dancong tea in different stages of processing. Results: The alcohols, aldehydes, ketones and esters showed a decreasing trend while the alkanes and aromatic ring substances exhibited an increasing trend during the processing. The contents of tea polyphenols, amino acids, caffeine, and catechin in non-volatile biochemical components decreased gradually during processing. The contents of soluble sugar and water extract increased …
Optimization Of Extraction Process And Structural Characterization Of Polysaccharides From Cornus Officinalis,
2024
College of Landscape and Food Engineering, Xuchang Vocational Technical College, Xuchang, Henan 461000, China
Optimization Of Extraction Process And Structural Characterization Of Polysaccharides From Cornus Officinalis, Xiao Fucai, Li Yingkui, Huang Fei, Gu Junhua
Food and Machinery
Objective: This study aimed to optimize the microwave assisted aqueous two-phase extraction (MATPE) process of polysaccharides from Cornus officinalis and obtain a uniform polysaccharide fraction. Methods: The best extraction technology was determined through an orthogonal experiment. To obtain a uniform polysaccharides fraction (COP-2-S), the crude extract of C. officinalis polysaccharides was purified using DEAE-52 cellulose and Sephadex G-100 column chromatography. The molecular weight of COP-2-S was determined by high performance gel permeation chromatography. The monosaccharide composition of COP-2-S was determined by gas chromatography. The structure of COP-2-S was characterized by UV, and IR spectra, and a scanning electron microscope. Results: …
Effect Of Different Drying Methods On The Edible Quality Of Tibetan Pork Jerky,
2024
Fujian Vocational College of Agriculture, Fuzhou, Fujian 350119, China
Effect Of Different Drying Methods On The Edible Quality Of Tibetan Pork Jerky, Lin Hua, Xu Daohuang
Food and Machinery
Objective: This study aimed to investigate the effect of different drying methods on the edible quality of dried Tibetan pork. Methods: The effects of four drying methods, namely frying, pre-cooking-frying, baking, and pre-cooking-baking, on the edible quality of Tibetan pork jerky were investigated using Tibetan pork as raw material. Results: Different drying methods had significant effects on the quality indexes of dried Tibetan pork such as color rendering, textural characteristics, and nutrient component. Among them, the frying group had the highest sensory score, uniform color, rich meat flavor, moderate hardness, and good eating quality. The baking group had a higher …
Preparation And Quality Evaluation Of Polygonati Rhizoma Modified Powder By Extrusion Cooking,
2024
School of Pharmacy, Hunan University of Chinese Medicine, Changsha, Hunan 410000, China
Preparation And Quality Evaluation Of Polygonati Rhizoma Modified Powder By Extrusion Cooking, Cao Yuxin, Zheng Tao, Luo Kun, Zheng Hui, Yang Yong
Food and Machinery
Objective: This study aimed to improve the functional characteristics of Polygonati rhizoma （PR）. Methods: Using the freeze-dried fresh PR and nine-steam-nine-bask processing PR as control products, the study comprehensively compared and analyzed human sensory, electronic sensory, color, fluidity, dissolving ability, extract content, total polysaccharide content and total saponin content in PR powder modified by extrusion cooking. Results: Extrusion cooking effectively eliminated the bad taste and improved the color and fluidity of PR powder. Compared with the nine-steam-nine-bask processing, extrusion cooking significantly increased the total polysaccharide content and total saponin content, with increase rates of 49.27% and 69.10%, respectively. Conclusion: …
Optimization Of Pectin Extraction From Immature Fruits Of Guanxi Pomelo By Lactobacillus Plantarum Fermentation,
2024
College of Ocean Food and Biological Engineering, Jimei University, Xiamen, Fujian 361021, China
Optimization Of Pectin Extraction From Immature Fruits Of Guanxi Pomelo By Lactobacillus Plantarum Fermentation, Ding Hongxia, Yang Yuanfan, Huang Shuan, Ni Hui
Food and Machinery
Objective: This study aimed to optimize the pectin extraction yield from immature fruits of Guanxi pomelo by L. plantarum fermentation and analysis of the properties of pectin extracted by L.s plantarum fermentation. Methods: Taking the extraction yield of pectin as the index, orthogonal test was used to optimize the process conditions of fermentation of immature fruits of Guanxi pomelo by L. plantarum, and the content of galacturonic acid, degree of esterification, protein, water-holding capacity, oil-holding capacity, emulsifying activity and emulsion stability of pectin were determined. Results: The optimal conditions for fermentation of immature fruits of Guanxi pomelo by L. …
