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Full-Text Articles in Mechanical Engineering

Hemodynamic Investigations In Intracranial Aneurysms: A Commentary, Hang Yi, Mark Johnson, Luke Bramlage, Zifeng Yang, Bryan Ludwig Feb 2023

Hemodynamic Investigations In Intracranial Aneurysms: A Commentary, Hang Yi, Mark Johnson, Luke Bramlage, Zifeng Yang, Bryan Ludwig

Mechanical and Materials Engineering Faculty Publications

Intracranial aneurysms (IAs) are abnormal bulges in a blood vessel in the brain that have a potential to rupture and even causing a stroke, which can lead to lasting brain damage, long-term disability, or even loss of life. It has been widely acknowledged that hemodynamic factors, e.g., instantaneous wall shear stress, time-averaged wall shear stress, wall shear stress gradient, gradient oscillatory number, oscillatory shear index, pulsatile blood flow waveform (flow rate magnitude and shape, physical flow period), relative residence time/turnover time, blood pressure, and vortex (i.e., size, location, and numbers), have a close relationship with the pathobiology (i.e., initiation, growth, …


Accurate Evaluation Of The Direction-Dependent Mechanical Properties Of Ideal Single Crystals: A Comparative Ab Initio Study, Jaylan Ali Elhalawani Feb 2023

Accurate Evaluation Of The Direction-Dependent Mechanical Properties Of Ideal Single Crystals: A Comparative Ab Initio Study, Jaylan Ali Elhalawani

Theses and Dissertations

The mechanical properties of a single crystal or a grain in a polycrystalline material are highly dependent on the direction of the applied load. Key properties of interest are the Young’s modulus and the Poisson ratio in the small strain limit, and the ideal tensile strength in the large strain regime. Prior atomistic computations of these properties interchangeably used two approaches. In one approach the stress-strain response is explicitly calculated via a numerical tensile test experiment. In the second approach the second order single crystal elastic constants are computed via small deformations and then used in analytical equations to derive …


Launching A 3d Printing Program For Students: Recommendations And Best Practices For Libraries, Wilhelmina Randtke, Lee Bareford Feb 2023

Launching A 3d Printing Program For Students: Recommendations And Best Practices For Libraries, Wilhelmina Randtke, Lee Bareford

Georgia Library Quarterly

The Georgia Southern University Libraries launched a 3D printing program for students in July 2022. Prior to launch, library employees at two of Georgia Southern University’s campuses investigated options for implementing safe, affordable, and sustainable 3D printing in existing academic libraries without retrofitting costly ventilation systems into existing facilities. This article describes the reasons why the Georgia Southern University Libraries thought that a 3D printing program could fulfill a service need for students across university colleges and departments and outlines some of the challenges, best practices, and unique innovations that the library’s employees experienced throughout the program launch process. The …


Synthesizing Ti–Ni Alloy Composite Coating On Ti–6al–4v Surface From Laser Surface Modification, Yitao Chen, Joseph William Newkirk, Frank W. Liou Feb 2023

Synthesizing Ti–Ni Alloy Composite Coating On Ti–6al–4v Surface From Laser Surface Modification, Yitao Chen, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

In This Work, a Ni-Alloy Deloro-22 Was Laser-Deposited on a Ti–6Al–4V Bar Substrate with Multiple Sets of Laser Processing Parameters. the Purpose Was to Apply Laser Surface Modification to Synthesize Different Combinations of Ductile TiNi and Hard Ti2Ni Intermetallic Phases on the Surface of Ti–6Al–4V in Order to Obtain Adjustable Surface Properties. Scanning Electron Microscopy, Energy Dispersion Spectroscopy, and X-Ray Diffraction Were Applied to Reveal the Deposited Surface Microstructure and Phase. the Effect of Processing Parameters on the Resultant Compositions of TiNi and Ti2Ni Was Discussed. the Hardness of the Deposition Was Evaluated, and Comparisons with …


Freespan Analysis For Subsea Pipeline Integrity Management Strategy, Nurul Hadi, Muhammad Helmi, Edo Cathaputra, Dedi Priadi, Donanta Dhaneswara Jan 2023

Freespan Analysis For Subsea Pipeline Integrity Management Strategy, Nurul Hadi, Muhammad Helmi, Edo Cathaputra, Dedi Priadi, Donanta Dhaneswara

Journal of Materials Exploration and Findings

Abstract. Over a rough seabed or on seabed subject to scour, freespans can occur when contact between a subsea pipeline and the seabed is lost over an acceptable distance. When this exceeds the allowable freespan length, design stresses can be exceeded, and a vortex induced vibration (VIV) response can be initiated, resulting in the risk of fatigue failure. If this is not predicted and controlled properly, it will affect pipeline integrity, leading to expensive rectification and intervention work. Freespan analysis consisted primarily of a screening check in which the as-found freespans from Remotely Operated Vehicle (ROV) or multibeam Side …


Effect Of Austenization And Repeated Quenching On The Microstructures And Mechanical Properties Of Wear-Resistant Steel, Yanuar Nugraha, Myrna Ariati Mochtar Jan 2023

Effect Of Austenization And Repeated Quenching On The Microstructures And Mechanical Properties Of Wear-Resistant Steel, Yanuar Nugraha, Myrna Ariati Mochtar

Journal of Materials Exploration and Findings

This study was focused on determining the effect of repeated austenitization and quenching on mechanical properties and microstructure. The experiment was carried out in a rolled quencher facility with a heat treatment process of one to two times, with parameters of an austenizing temperature of 9500C and quenching at a temperature of 8500C with pressurized water media. Testing of specimens, including microstructure observations and hardness testing. The repeated heat treatment process showed an increase in hardness of 0.79% on one-time repeated heat treatment and 1.65% on two repeated heat treatments. This occurs due to the presence accompanied by refinement of …


Advanced Microstructural Characterization Of Functionally Graded Dental Ceramic Material For Materials-Informed Finishing, Angani Vigneswaran Jan 2023

Advanced Microstructural Characterization Of Functionally Graded Dental Ceramic Material For Materials-Informed Finishing, Angani Vigneswaran

Theses and Dissertations--Manufacturing Systems Engineering

Yttria-stabilized tetragonal zirconia polycrystal (Y-TZP) has gained popularity as the choice of material for dental prosthetics. Ivoclar Vivadent’s IPS e.max ZirCAD Prime dental ceramic incorporates a unique gradient technology that varies the yttria content over the thickness of the material. The top layer is composed of 5Y-TZP which is desired for its optical properties while the bottom layer is composed of a much stronger 3Y-TZP. In between the two layers, 5Y-TZP and 3Y-TZP are mixed to form a transition layer. Varying the amount of yttria allows for more esthetically pleasing translucency in the visible areas of the restoration without compromising …


Investigation Of Fiber Orientation And Mechanical Properties Of Pyrolysis Recycled Carbon-Fiber Reinforced Thermoset Composite, Reva N. Simmons, Harry Lee, Garam Kim Jan 2023

Investigation Of Fiber Orientation And Mechanical Properties Of Pyrolysis Recycled Carbon-Fiber Reinforced Thermoset Composite, Reva N. Simmons, Harry Lee, Garam Kim

Discovery Undergraduate Interdisciplinary Research Internship

With increasing demand of carbon fiber reinforced fiber thermoset composites, establishing a sustainable cycle for these materials becomes crucial. Pyrolysis is a process of reclaiming carbon fiber from thermoset composites by thermally degrading the polymer at high temperatures allowing the fibers to be extracted. Carbon fiber reclaimed through current pyrolysis processes for thermoset composites typically loses its original shape and orientation, making it difficult to reorganize the fibers. This study investigated the feasibility of maintaining the fiber orientations for continuous fiber reinforced thermoset composite during pyrolysis by stitching the carbon fiber layup to a conformable copper mesh during the manufacturing …


An Experimental Study On The Mechanical Properties And Chemical Composition Of Lcd 3d Printed Specimens, Sebastian Gomez Jan 2023

An Experimental Study On The Mechanical Properties And Chemical Composition Of Lcd 3d Printed Specimens, Sebastian Gomez

College of Graduate Studies: Theses & Dissertations

Additive manufacturing technologies have been enhanced throughout the years yet have surprised the manufacturing industry due to their high-end surface finish and dimensional accuracy. Different experiments have been done to identify a specific phenomenon known in the vat-polymerization field. Distortion and dimensional inaccuracy tend to affect the overall properties of the process, either physical or chemical. This approach allows the understanding of how the physical properties have been affected and how to study the chemical properties to avoid this type of phenomenon. The chemical reaction between polymer and UV light has been studied and experimented with to the point that …


Performance Evaluation Of Composite Sandwich Structures With Additively Manufactured Aluminum Honeycomb Cores With Increased Bonding Surface Area, M. Rangapuram, S. K. Dasari, Joseph William Newkirk, K. Chandrashekhara, H. Misak, P. R. Toivonen, D. Klenosky, T. Unruh, J. Sam Jan 2023

Performance Evaluation Of Composite Sandwich Structures With Additively Manufactured Aluminum Honeycomb Cores With Increased Bonding Surface Area, M. Rangapuram, S. K. Dasari, Joseph William Newkirk, K. Chandrashekhara, H. Misak, P. R. Toivonen, D. Klenosky, T. Unruh, J. Sam

Materials Science and Engineering Faculty Research & Creative Works

Modern aerostructures, including wings and fuselages, increasingly feature sandwich structures due to their high-energy absorption, low weight, and high flexural stiffness. The face sheet of these sandwich structures are typically thin composite laminates with interior honeycombs made of Nomex or aluminum. Standard cores are structurally efficient, but their design cannot be varied throughout the structure. With additive manufacturing (AM) technology, these core geometries can be altered to meet the design requirements that are not met in standard honeycomb cores. This study used a modified aluminum honeycomb core, with increased surface area on the top and bottom, as the core material …


Investigation Of Manufacturing Techniques For Magnetorheological Elastomers To Expand Feasibility In A Diverse Array Of Applications, Austin S. Robbins Jan 2023

Investigation Of Manufacturing Techniques For Magnetorheological Elastomers To Expand Feasibility In A Diverse Array Of Applications, Austin S. Robbins

College of Graduate Studies: Theses & Dissertations

Magnetorheological elastomers, or MREs, are smart composite materials with controllable physical and mechanical properties when introduced to an external stimulus of a magnetic field. The controllability of these properties is highly tunable by the selection of the elastomeric matrix, concentration of magnetically permeable particles, introduction of additives, and the alignment of the constituents during the curing process. The fabrication of MREs typically calls for a mold that is filled with an MRE mixture to create the final desired geometry after curing. These molds are frequently placed under a magnetic field which orients the micron sized magnetic particles along the magnetic …


Effect Of Platelet Length And Stochastic Morphology On Flexural Behavior Of Prepreg Platelet Molded Composites, Siavash Sattar, Benjamin Beltran Laredo, Sergii G. Kravchenko, Oleksandr G. Kravchenko Jan 2023

Effect Of Platelet Length And Stochastic Morphology On Flexural Behavior Of Prepreg Platelet Molded Composites, Siavash Sattar, Benjamin Beltran Laredo, Sergii G. Kravchenko, Oleksandr G. Kravchenko

Mechanical & Aerospace Engineering Faculty Publications

Prepreg platelet molding compound (PPMC) can be used to create structural grade material with a heterogeneous mesoscale morphology. The present work considered various platelet lengths of the prepreg system IM7/8552 to study the effect of platelet length on the flexural behavior of PPMC composite. A progressive failure finite-element analysis was used to understand competing failure modes in PPMC with the different platelet length. The interlaminar and in-plane damage mechanisms were employed to describe complex failure modes within the mesostructure of PPMCs. Experimental results of the flexural tests of the PPMC with different platelet length sizes were used to validate the …


Aerosol Synthesis Of Tungsten Bronze Particles For Nir Shielding, Hao Tu Jan 2023

Aerosol Synthesis Of Tungsten Bronze Particles For Nir Shielding, Hao Tu

Theses and Dissertations

This dissertation emphasizes the need for efficient energy use in buildings and transportation due to global warming and the energy crisis. It suggests that improving energy efficiency can help reduce energy consumption and emissions and support sustainability. The dissertation introduces various transparent materials that can block near-infrared (NIR) radiation from solar radiation to save energy and money, and it highlights the growing market value of such products. The dissertation compares tungsten bronze with other NIR shielding materials and shows its advantages. The dissertation introduces a cheap and environmentally friendly method for continuously producing tungsten bronze particles via aerosol synthesis. Particle …


Comparison Of The Thermal Stability In Equal-Channel-Angular-Pressed And High-Pressure-Torsion-Processed Fe–21cr–5al Alloy, Maalavan Arivu, Andrew Hoffman, Jiaqi Duan, Jonathan Poplawsky, Xinchang Zhang, Frank W. Liou, Rinat Islamgaliev, Ruslan Valiev, Haiming Wen Jan 2023

Comparison Of The Thermal Stability In Equal-Channel-Angular-Pressed And High-Pressure-Torsion-Processed Fe–21cr–5al Alloy, Maalavan Arivu, Andrew Hoffman, Jiaqi Duan, Jonathan Poplawsky, Xinchang Zhang, Frank W. Liou, Rinat Islamgaliev, Ruslan Valiev, Haiming Wen

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Nanostructured Steels Are Expected to Have Enhanced Irradiation Tolerance and Improved Strength. However, They Suffer from Poor Microstructural Stability at Elevated Temperatures. in This Study, Fe–21Cr–5Al–0.026C (Wt%) Kanthal D (KD) Alloy Belonging to a Class of (FeCrAl) Alloys Considered for Accident-Tolerant Fuel Cladding in Light-Water Reactors is Nanostructured using Two Severe Plastic Deformation Techniques of Equal-Channel Angular Pressing (ECAP) and High-Pressure Torsion (HPT), and their Thermal Stability between 500–700 °C is Studied and Compared. ECAP KD is Found to Be Thermally Stable Up to 500 °C, Whereas HPT KD is Unstable at 500 °C. Microstructural Characterization Reveals that ECAP KD …


Development Of Corn Kernel-Based Biocomposite Films For Food Packaging Applications, Swastika Bera Jan 2023

Development Of Corn Kernel-Based Biocomposite Films For Food Packaging Applications, Swastika Bera

Electronic Theses and Dissertations

Most of the current and active food packaging resources and methods are nonbiodegradable and nonrenewable therefore harmful to the environment. Due to this, alternate sources of food packaging materials are in high demand. In this study, a bio-composite film has been developed, with Corn kernel powder as fiber reinforcement which is mixed with gelatin, and lignin two biopolymers as the matrix. The effect of Corn Kernel (CK) reinforcement on the Gelatin/Lignin (G/L) matrix on mechanical and barrier properties has been studied. CK has shown great potential as reinforcement to natural polymer, gelatin, and lignin (G/L) for food packaging applications as …


Microstructure, Mechanical Properties And Oxidation Behavior Of Refractory Multi-Principal Element Alloys By Laser Remelting And Conventional Manufacturing, Visharad Jalan, Seth Crawford, Sung Heng Wu, Frank W. Liou, Haiming Wen Jan 2023

Microstructure, Mechanical Properties And Oxidation Behavior Of Refractory Multi-Principal Element Alloys By Laser Remelting And Conventional Manufacturing, Visharad Jalan, Seth Crawford, Sung Heng Wu, Frank W. Liou, Haiming Wen

Mechanical and Aerospace Engineering Faculty Research & Creative Works

Refractory Multi-Principal Element Alloys (RMPEAs), HfNbTaTiZr, (HfNbTaTiZr)9Cr, and (HfNbTaTiZr)9Al, Were Manufactured using Vacuum Arc Melting Followed by Laser Remelting to Mimic Additive Manufacturing. the Microhardness of the As-Cast HfNbTaTiZr, (HfNbTaTiZr)9Cr, and (HfNbTaTiZr)9Al Samples after Arc Melting Was Measured as 6.20, 7.63, and 6.89 Gpa, respectively. after Laser Remelting and Re-Solidification, the Hardness Increased by ~ 30% for Each Composition; the Hardest Was (HfNbTaTiZr)9Cr Measured at 9.60 GPa, While the Softest Was HfNbTaTiZr with a Hardness of 8.42 GPa, Which Was Still Harder Compared to All the Other Samples. the Addition …


Recycling Metal Chips Into Usable Materials, Alex Mortensen, Ben Mortensen Jan 2023

Recycling Metal Chips Into Usable Materials, Alex Mortensen, Ben Mortensen

Williams Honors College, Honors Research Projects

This report entails the scope, design considerations, and plans for creating a metal chip converter into metal briquettes. The construction is a set of machines with multiple processes to make the conversion happen. The process includes washing fine metal chips, drying them off, compressing them, and melting them down into usable briquettes. This project is intended to make a simple process to recycle metal chips into usable material for reuse. The project's objective is to reduce the costs of storage and recycling waste by offering a solution to recycle it into materials the shop can reuse.


Study Of Bounds For Effective Moduli Of Polycrystals And Composites Using Variational Principle For Probabilistic Measures, Md. Tofiqul Islam Jan 2023

Study Of Bounds For Effective Moduli Of Polycrystals And Composites Using Variational Principle For Probabilistic Measures, Md. Tofiqul Islam

Wayne State University Dissertations

Tensors that are invariant with respect to subgroups of 3D group of rotations were constructed first by Lokhin and Sedov (J. Appl. Math. Mech. (PMM), 1963, 27, 597-629). In this paper we do one more step and derive formulas for the elastic modulus tensors for all symmetry groups from the Lokhin-Sedov results. The tensor basis obtained in this way has an advantage of being built upon the same tensors that are used in construction of nonlinear tensor functions. One consequence of the formulas derived is that the number of types of anisotropic elastic behaviors is ten. There is a long- …


Dome Tester, Clark Bates, Nikolas M. Kulin Jan 2023

Dome Tester, Clark Bates, Nikolas M. Kulin

Williams Honors College, Honors Research Projects

We are reconfiguring and modifying the previously built dome tester to be more user friendly and mechanically applicable. This has a long-term goal of being a usable teaching tool for manufacturing education within the college of engineering and polymer sciences. The dome tester pushes a metal dome into a clamped sheet of metal to test its forming limits and where necking occurs. We have implemented a better method of viewing the sheet sample as it is being deformed, and improved measuring methods for the distance a sample is deformed. By introducing these changes in conjunction with improved documentation of the …


Stability Of Ruddlesden-Popper Phase Lanthanum Nickelate As Air Electrode For Reversible Solid Oxide Cells, Daniel De Lorenzo Moreira Jan 2023

Stability Of Ruddlesden-Popper Phase Lanthanum Nickelate As Air Electrode For Reversible Solid Oxide Cells, Daniel De Lorenzo Moreira

Graduate Theses, Dissertations, and Problem Reports (ETD)

This thesis studied the long-term stability of Ruddlesden-Popper phase Lanthanum Nickelate under operating conditions as the air electrode for Reversible Solid Oxide Cells (R-SOC). Renewable energies have gone through increase in popularity throughout the last decades, mainly due to the consequences of the rapid population growth in the world. These new energies have been pointed as the rightful successor of fossil fuel energies in order to decrease the environmental impact of our day-to-day life. Solid Oxide Fuel Cells as well as Solid Oxide Electrolysis Cells are believed to be the key to stabilizing the energy supply when environmental conditions are …


Mechanical Design Of A Microwave Imaging Device For Breast Cancer Detection In Mri Scanners, Grace M. Player Jan 2023

Mechanical Design Of A Microwave Imaging Device For Breast Cancer Detection In Mri Scanners, Grace M. Player

Dartmouth College Master’s Theses

This project seeks to develop an updated version of a microwave imaging device for use in conjunction with breast MRI, improving upon existing technology and developing novel concepts for the device. It posits three primary redesign targets for updating the previous system: resizing the system height, making the device more iteration- friendly, and improving the overall manufacturability of the device by replacing custom components with commercially available alternatives. All three of these redesign targets are met in the new design, V2.0. The height is reduced by reducing antenna travel and height, embedding some components, and shortening the tank wall, resulting …


Solid-State Electrolytes For Long Duration Molten Sodium Batteries, Ryan C. Hill Jan 2023

Solid-State Electrolytes For Long Duration Molten Sodium Batteries, Ryan C. Hill

Theses and Dissertations--Chemical and Materials Engineering

Rechargeable batteries have become a staple of modern society, driving the development and expansion of portable electronics and electric vehicles. The long lifetime and high energy density provided by batteries have made them excellent candidates for use in the emerging field of long duration, grid-scale energy storage. However, traditional battery chemistries, such as Li-ion, are not an ideal solution for grid-scale storage, due to high-cost raw materials that are often sourced from volatile markets. Sodium-based batteries are a promising alternative for long duration storage, owing to the domestic abundance of raw materials and energy densities that nearly rival that of …


Conductive 3d Nano-Biohybrid Systems Based On Densified Carbon Nanotube Forests And Living Cells, Roya Bagheri, Alicia K. Ball, Masoud Kasraie, Aparna Chandra, Xinqian Chen, Ibrahim Miskioglu, Zhiying Shan, Parisa Pour Shahid Saeed Abadi Jan 2023

Conductive 3d Nano-Biohybrid Systems Based On Densified Carbon Nanotube Forests And Living Cells, Roya Bagheri, Alicia K. Ball, Masoud Kasraie, Aparna Chandra, Xinqian Chen, Ibrahim Miskioglu, Zhiying Shan, Parisa Pour Shahid Saeed Abadi

Michigan Tech Publications

Conductive biohybrid cell-material systems have applications in bioelectronics and biorobotics. To date, conductive scaffolds are limited to those with low electrical conductivity or 2D sheets. Here, 3D biohybrid conductive systems are developed using fibroblasts or cardiomyocytes integrated with carbon nanotube (CNT) forests that are densified due to interactions with a gelatin coating. CNT forest scaffolds with a height range of 120–240 µm and an average electrical conductivity of 0.6 S/cm are developed and shown to be cytocompatible as evidenced from greater than 89% viability measured by live-dead assay on both cells on day 1. The cells spread on top and …


Mechanical Behavior Of Metallic Core-Shell Nanoparticles Under Compressive Loading, Phillip Tomich Jan 2023

Mechanical Behavior Of Metallic Core-Shell Nanoparticles Under Compressive Loading, Phillip Tomich

Graduate Research Theses & Dissertations

Core/shell metallic nanoparticles have been shown to be a promising material type for additive manufacturing in the aerospace and automotive fields. Within additive manufacturing they will be used to accurately make an array of nanoparticles within the grains of metal matrix composites. This in turn will help to strengthen the material while remaining ductility and light weight. In this study, copper/aluminum core/shell nanoparticles are compressed under [100], [110], [111], and [112] directions to showcase their anisotropic material properties. Models of their individual counterparts were also investigated. There are no previous works showing the deformation mechanisms of copper/aluminum core/shell nanoparticles. Molecular …


Multimaterial, Core-Shell Direct Ink Writing Of Flexible Strain Sensors For Pneumatically-Actuated Soft Robotic Hinge Joints, John Michael Burke Jan 2023

Multimaterial, Core-Shell Direct Ink Writing Of Flexible Strain Sensors For Pneumatically-Actuated Soft Robotic Hinge Joints, John Michael Burke

Graduate Theses, Dissertations, and Problem Reports (ETD)

Direct ink writing (DIW) provides for an expansive material library and the ability to print multiple materials with tailored functionalities in a controllable and single-step process. Particularly beneficial is the net shape printing under ambient conditions of a wide range of materials normally incompatible with one another. Coaxial DIW is a 3D printing technique that allows for two dissimilar inks to be extruded simultaneously in a co-flow manner. In this work, custom-designed coaxial nozzles were 3D-printed using a stereolithography printer. Composite inks comprised of thermoplastic polyurethane and silver were developed and studied. The coaxial nozzles were then used to co-extrude …


Mechanical And Morphological Characterization Of Energy Materials By Nanoindentation And Scanning Probe Microscopy, Jacob Hempel Jan 2023

Mechanical And Morphological Characterization Of Energy Materials By Nanoindentation And Scanning Probe Microscopy, Jacob Hempel

Theses and Dissertations--Physics and Astronomy

The demand for robust materials in energy-based applications such as solid electrolytes for batteries, piezoelectric composites for mechanical energy harvesting, or new polymer materials for polymer binders in composite electrodes is on the rise. Mechanical degradation is the most common way for devices to fail in operation, thus a thorough understanding of a material’s mechanical properties is essential for application purposes.

In this dissertation, the mechanical characterization of novel boron cluster solid electrolytes is presented. Therein, we determine the elastic modulus and hardness of these compounds using instrumented indentation. A comparison is made against other solid electrolytes. It is found …


Investigation Of Microstructurally Dependent Mechanical Properties Of Cold Sprayed Copper Using Correlative Microscopy, Quintin Otto Jan 2023

Investigation Of Microstructurally Dependent Mechanical Properties Of Cold Sprayed Copper Using Correlative Microscopy, Quintin Otto

UNF Graduate Theses and Dissertations

This project employs multi-instrument materials characterization to analyze material made with the “Cold Spray” additive manufacturing process. Cold spray is an emerging additive manufacturing technique with unique benefits resulting from its low temperature adhesion process induced by plastic deformation. Metallic powder collides at high speeds creating three dimensional materials and coatings without the need for melting. Copper cold sprayed specimens were analyzed using a series of imaging techniques to characterize the microstructure at varying levels of detail and magnification. Scanning electron microscopy and electron back scattered diffraction were paired with microhardness testing to generate a correlative comparison between microstructure and …


Modified Reactive Sputter Deposition Of Titanium Nitride Thin Films Via Hipims With Kick-Pulse And Improvement Of The Structure-Zone Model, Andrew Miceli Jan 2023

Modified Reactive Sputter Deposition Of Titanium Nitride Thin Films Via Hipims With Kick-Pulse And Improvement Of The Structure-Zone Model, Andrew Miceli

UNF Graduate Theses and Dissertations

Direct current (DC) and radio frequency (RF) sputtering methods have been commonplace in industry for several decades and widely studied in literature. Hard films of nitrides, such as titanium nitride (TiN), have been deposited using reactive DC sputtering onto cutting tools and medical devices extensively as well. For these applications, the films require excellent adhesion, high density, and high hardness. High-Power Impulse Magnetron Sputtering (HIPIMS) has emerged over the last several years as a method to produce films with increased density and mechanical properties. Process-structure-property relationships for reactive HIPIMS are not yet well developed. Additionally, conventional HIPIMS suffers from relatively …


System Analysis Of An Internal Combustion Engine (Ice) – Solid Oxide Fuel Cell (Sofc) Hybrid Cycle, Jose Javier Colon Rodriguez Jan 2023

System Analysis Of An Internal Combustion Engine (Ice) – Solid Oxide Fuel Cell (Sofc) Hybrid Cycle, Jose Javier Colon Rodriguez

Graduate Theses, Dissertations, and Problem Reports (ETD)

Due to the intermittent nature of renewable energy and the rigid operation of existing coal plants, the need for flexible power generation technology is eminent. Hybrid energy systems have shown potential for flexible, grid following dynamics while maintaining higher efficiencies. The work below focuses on the performance analysis of a proposed 100 kW pressurized Internal Combustion Engine (ICE) and Solid Oxide Fuel Cell (SOFC) hybrid system. The un-utilized fuel from the SOFC stack provided the chemical energy to operate the engine. A turbocharger was used to deliver the necessary air flow for both the stack and engine. An external reformer …


Material Characterization Of Thermoplastic Polyurethane (Tpu) And Thermoplastic Elastomers (Tpe) For Development Of 3d-Printed Surrogate Organs For Medical Training, Anastasia Elizabeth Lucci Jan 2023

Material Characterization Of Thermoplastic Polyurethane (Tpu) And Thermoplastic Elastomers (Tpe) For Development Of 3d-Printed Surrogate Organs For Medical Training, Anastasia Elizabeth Lucci

Graduate Theses, Dissertations, and Problem Reports (ETD)

Cadaveric specimens are a necessary, albeit limited, resource for training medical students on basic surgical skills. The availability of surrogate 3D-printed organs would readily allow access to resources that could reduce or potentially eliminate the need for cadaveric specimens or, at a minimum, provide students the opportunity to practice with 3D-printed surrogates before transitioning to those specimens. This research focuses on determining which thermoplastic material most closely mimics mechanical properties such as hardness and stiffness of human organs and allows 3D printing surrogate organs to be used as safe, educational tools. Relatively “soft” materials such as thermoplastic polyurethanes (TPU) and …