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Materials Science and Engineering Faculty Research & Creative Works

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Full-Text Articles in Metallurgy

The Influence Of Ti, Nb And V On The Hot Ductility Of As-Cast Microalloyed Steels, Madhuri Varadarajan, Laura Bartlett, Ronald J. O'Malley, Semen Naumovich Lekakh Sep 2020

The Influence Of Ti, Nb And V On The Hot Ductility Of As-Cast Microalloyed Steels, Madhuri Varadarajan, Laura Bartlett, Ronald J. O'Malley, Semen Naumovich Lekakh

Materials Science and Engineering Faculty Research & Creative Works

Microalloying with Ti, Nb and V, both individually and in combination, is a common method for producing steels with high strength and toughness. However, interaction with other elements and impurities can lead to cracking during continuous casting and rolling. The hot ductility of commercially cast V, Nb and Nb-V-Ti steels has been investigated using two experimental methods: tensile testing utilizing a servo-hydraulic load frame with a resistance furnace and thermomechanical testing using rapid joule heating. The temperature-dependent ductility of these steels is compared for both test methods. Factors that influence the ductility of these steels are discussed.


Processing And Properties Of Medium-Mn Trip Steel To Obtain A Two-Stage Trip Behavior, D. M. Field, L. G. Garza-Martinez, D. C. Van Aken Sep 2020

Processing And Properties Of Medium-Mn Trip Steel To Obtain A Two-Stage Trip Behavior, D. M. Field, L. G. Garza-Martinez, D. C. Van Aken

Materials Science and Engineering Faculty Research & Creative Works

Two medium-Mn steels of nominal composition 0.15C-2.0Si-10.5Mn-(0.75, 1.5) Al-0.04Nb-balFe (wt pct) were processed to produce sub-micron grain sizes of 0.65 and 0.80 μm. Mechanical testing was performed in three successive conditions: hot rolled, intercritically annealed, and cold rolled with subsequent intercritical annealing. Intercritical annealing was performed at 923 K for 20 hours. Electron-backscattered diffraction and X-ray diffraction were utilized to characterize the microstructure, consisting of α-ferrite, α-martensite, ε-martensite, and γ-austenite. Microstructural constituents were tracked during tensile deformation, and it was found that both steels exhibited two-stage TRIP with γ-austenite martensitically transforming first to ε-martensite and as strain increased ε-martensite transformed …


A Spatially Distributed Fiber-Optic Temperature Sensor For Applications In The Steel Industry, Muhammad Roman, Damilola Balogun, Yiyang Zuang, Rex E. Gerald Ii, Laura Bartlett, Ronald J. O'Malley, Jie Huang Jul 2020

A Spatially Distributed Fiber-Optic Temperature Sensor For Applications In The Steel Industry, Muhammad Roman, Damilola Balogun, Yiyang Zuang, Rex E. Gerald Ii, Laura Bartlett, Ronald J. O'Malley, Jie Huang

Materials Science and Engineering Faculty Research & Creative Works

This paper presents a spatially distributed fiber-optic sensor system designed for demanding applications, like temperature measurements in the steel industry. The sensor system employed optical frequency domain reflectometry (OFDR) to interrogate Rayleigh backscattering signals in single-mode optical fibers. Temperature measurements employing the OFDR system were compared with conventional thermocouple measurements, accentuating the spatially distributed sensing capability of the fiber-optic system. Experiments were designed and conducted to test the spatial thermal mapping capability of the fiber-optic temperature measurement system. Experimental simulations provided evidence that the optical fiber system could resolve closely spaced temperature features, due to the high spatial resolution and …


Spherical Cavity Expansion Approach For The Study Of Rigid-Penetrator’S Impact Problems, Mario Buchely, Alejandro Marañon May 2020

Spherical Cavity Expansion Approach For The Study Of Rigid-Penetrator’S Impact Problems, Mario Buchely, Alejandro Marañon

Materials Science and Engineering Faculty Research & Creative Works

In recent years, Spherical Cavity Expansion (SCE) theory has been extensively utilized to model dynamic deformation processes related to indentation and penetration problems in many fields. In this review, the SCE theory is introduced by explaining the different mathematical features of this theory, its solution, and a potential application to model the penetration of a rigid penetrator into a deformable target. First, a chronologically literature review of the most common models used to study this kind of penetration problems is introduced, focusing on the SCE theory. Then, the engineering model of penetration is presented using the SCE approach. The model …


Modeling Of Scrap Dissolution In Molten Iron For The Case Of Heat Transfer-Controlled Process By Different Approaches And Comparison Of Their Accuracies, Ajay Kumar Shukla, Brahma Deo, D. G.C. Robertson Jan 2020

Modeling Of Scrap Dissolution In Molten Iron For The Case Of Heat Transfer-Controlled Process By Different Approaches And Comparison Of Their Accuracies, Ajay Kumar Shukla, Brahma Deo, D. G.C. Robertson

Materials Science and Engineering Faculty Research & Creative Works

Dissolution of steel scrap in molten iron is studied by using analytical as well as numerical approaches for the case of a heat transfer-controlled process. The approaches used are Green's function approach, quasi-static approach, integral profile method (IPM) (with parabolic profile), and finite difference methods (FDM). Application of FDM explicit and FDM implicit with fixed grid and variable grid is described. Accuracy of all the approaches is compared in terms of total dissolution time evaluated from overall heat balance criterion. The selection rule of time step and deciding the suitable approach for achieving minimum error for different operating conditions, represented …


Aging Response On The Stress Corrosion Cracking Behavior Of Wrought Precipitation-Hardened Magnesium Alloy, G. R. Argade, S. K. Panigrahi, R. S. Mishra Jan 2020

Aging Response On The Stress Corrosion Cracking Behavior Of Wrought Precipitation-Hardened Magnesium Alloy, G. R. Argade, S. K. Panigrahi, R. S. Mishra

Materials Science and Engineering Faculty Research & Creative Works

Constant immersion testing and slow strain rate testing (SSRT) are conducted on wrought magnesium alloy in a 3.5 wt.% NaCl solution. After solution annealing (SA) at 525 °C for 8 h, the alloy was isothermally aged at 210 °C for 15 h, 48 h, and 144 h to obtain underaged (UA), peak-aged (PA), and overaged (OA) microstructures, respectively. After 32 days of constant exposure in chloride solution, the SA and UA samples showed the lowest (~ 0.10 mg cm−2 day−1) and the highest (~ 0.20 mg cm−2 day−1) weight loss, respectively. SSRT was carried out at an initial strain rate …


Grain Size Effects In Selective Laser Melted Fe-Co-2v, Wesley Everhart, Joseph William Newkirk Sep 2019

Grain Size Effects In Selective Laser Melted Fe-Co-2v, Wesley Everhart, Joseph William Newkirk

Materials Science and Engineering Faculty Research & Creative Works

The material science of additive manufacturing (AM) has become a significant topic due to the unique way in which the material and geometry are created simultaneously. Major areas of research within inorganic materials include traditional structural materials, shape memory alloys, amorphous materials, and some new work in intermetallics. The unique thermal profiles created during selective laser melting (SLM) may provide new opportunities for processing intermetallics to improve mechanical and magnetic performance. A parameter set for the production of Fe-Co-2V material with additive manufacturing is developed and efforts are made to compare the traditional wrought alloy to the AM version of …


Elevated Temperature Mechanical And Microstructural Characterization Of Slm Ss304l, G. R. Hecht, Sriram Praneeth Isanaka, Joseph William Newkirk Aug 2019

Elevated Temperature Mechanical And Microstructural Characterization Of Slm Ss304l, G. R. Hecht, Sriram Praneeth Isanaka, Joseph William Newkirk

Materials Science and Engineering Faculty Research & Creative Works

SLM built SS304L was annealed and water quenched to minimize residual stress and avoid carbide precipitation. Mini-tensile characterization of strength and elongation at temperature conditions up to 800°C, along with observations of the associated microstructural transformations were utilized to understand the changes produced in SLM SS304L. As-built and annealed specimens were found to exhibit decreasing strength and elongation with increasing temperature as expected. Carbide precipitates appeared after short times at high temperatures within both as-built and annealed specimens for all cases, but no brittle intermetallic phase development was observed for any of the temperatures investigated. While the lack of Sigma, …


Compressive And Bending Performance Of Selectively Laser Melted Alsi10mg Structures, D. Murphy, O. Fashanu, Myranda Spratt, Joseph William Newkirk, K. Chandrashekhara, H. Misak, D. Klenosky Aug 2019

Compressive And Bending Performance Of Selectively Laser Melted Alsi10mg Structures, D. Murphy, O. Fashanu, Myranda Spratt, Joseph William Newkirk, K. Chandrashekhara, H. Misak, D. Klenosky

Materials Science and Engineering Faculty Research & Creative Works

Selective laser melting (SLM) is a widely used additive manufacturing technique that effectively manufactures complex geometries such as cellular structures. However, challenges such as anisotropy and mechanical property variation are commonly found due to process parameters. In a bid to utilize this method for the commercial production of cellular structures, it is important to understand the behavior of a material under different loading conditions. In this work, the behavior of additively manufactured AlSi10Mg under compression, bending, and tension loads was investigated. Vertical and horizontal build directions are compared for each type of loading. Specimens were manufactured using the reduced build …


Comparison Of Fatigue Performance Between Additively Manufactured And Wrought 304l Stainless Steel Using A Novel Fatigue Test Setup, M. M. Parvez, Y. Chen, Joseph William Newkirk, Frank W. Liou Aug 2019

Comparison Of Fatigue Performance Between Additively Manufactured And Wrought 304l Stainless Steel Using A Novel Fatigue Test Setup, M. M. Parvez, Y. Chen, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

In this research, a novel adaptive controlled fatigue testing machine was designed for bending type high cycle fatigue test. A unique dual gauge section Krouse type mini specimen was designed for simply supported transverse bending. Displacement controlled fatigue tests were implemented using an electromechanical actuator. The variation in the control signal and load observed during the test provides unique insights into realizing the deterioration of the specimen due to fatigue. These analyses were utilized to compare the fatigue performance of wrought and additively manufactured 304L stainless steel. The influence of the build direction on fatigue performance was also investigated by …


Effective Elastic Properties Of Additively Manufactured Metallic Lattice Structures: Unit-Cell Modeling, Okanmisope Fashanu, David Murphy, Myranda Spratt, Joseph William Newkirk, K. Chandrashekhara, Ben Brown, John Porter Aug 2019

Effective Elastic Properties Of Additively Manufactured Metallic Lattice Structures: Unit-Cell Modeling, Okanmisope Fashanu, David Murphy, Myranda Spratt, Joseph William Newkirk, K. Chandrashekhara, Ben Brown, John Porter

Materials Science and Engineering Faculty Research & Creative Works

Lattice structures are lightweight materials, which exhibit a unique combination of properties such as air and water permeability, energy and acoustic absorption, low thermal conductivity, and electrical insulation. In this work, unit-cell homogenization was used to predict the effective elastic moduli of octet-truss (OT) lattice structures manufactured using selective laser melting (SLM). OT structures were manufactured using a Renishaw AM 250 SLM machine with various relative densities. Compression test was carried out at strain rate 5 x 10-3 m-1 using an MTS frame. Finite element analysis was used in the determination of the OT’s effective elastic properties. Results …


Mechanical Properties Of Heusler Alloys, Wesley Everhart, Joseph William Newkirk May 2019

Mechanical Properties Of Heusler Alloys, Wesley Everhart, Joseph William Newkirk

Materials Science and Engineering Faculty Research & Creative Works

Heusler alloys have been a significant topic of research due to their unique electronic structure, which exhibits half-metallicity, and a wide variety of properties such as magneto-calorics, thermoelectrics, and magnetic shape memory effects. As the maturity of these materials grows and commercial applications become more near-term, the mechanical properties of these materials become an important factor to both their processing as well as their final use. Very few studies have experimentally investigated mechanical properties, but those that exist are reviewed within the context of their magnetic performance and application space with specific focus on elastic properties, hardness and strength, and …


Effect Of Wall Thickness And Build Quality On The Compressive Properties Of 304l Thin-Walled Structures Fabricated By Slm, Myranda Spratt, Sudharshan Anandan, Rafid M. Hussein, Joseph William Newkirk, K. Chandrashekhara, Heath Misak, Michael Walker Aug 2018

Effect Of Wall Thickness And Build Quality On The Compressive Properties Of 304l Thin-Walled Structures Fabricated By Slm, Myranda Spratt, Sudharshan Anandan, Rafid M. Hussein, Joseph William Newkirk, K. Chandrashekhara, Heath Misak, Michael Walker

Materials Science and Engineering Faculty Research & Creative Works

The specific strength of lightweight lattice structures built with SLM is of interest to the aerospace industry. Honeycombs were manufactured with increasing wall thicknesses (which increases density) and tested under compression. The optimal strength to density ratio was determined from the resulting data. The build quality was also evaluated to determine how/if the results were influenced by the specimen quality. Differences between the nominal and as-built geometry were identified, but considered to be minimal. Microstructural evaluation of the specimens revealed a possible dependence on the ‘border scan’ properties, as the thickness of the specimens was such that the board scan …


Fast Prediction Of Thermal History In Large-Scale Parts Fabricated Via A Laser Metal Deposition Process, Lei Yan, Tan Pan, Joseph William Newkirk, Frank W. Liou, Eric E. Thomas, Andrew H. Baker, James B. Castle Aug 2018

Fast Prediction Of Thermal History In Large-Scale Parts Fabricated Via A Laser Metal Deposition Process, Lei Yan, Tan Pan, Joseph William Newkirk, Frank W. Liou, Eric E. Thomas, Andrew H. Baker, James B. Castle

Materials Science and Engineering Faculty Research & Creative Works

Laser metal deposition (LMD) has become a popular choice for the fabrication of near-net shape complex parts. Plastic deformation and residual stresses are common phenomena that are generated from the intrinsic large thermal gradients and high cooling rates in the process. Finite element analysis (FEA) is often used to predict the transient thermal cycle and optimize processing parameters; however, the process of predicting the thermal history in the LMD process with the FEA method is usually time-consuming, especially for large-scale parts. Herein, multiple 3D FEA models with simple assumptions on the heat source and its loading methods are compared and …


Development Of An Engineering Diagram For Additively Manufactured Austenitic Stainless Steel Alloys, Zachary T. Hilton, Joseph William Newkirk, Ronald J. O'Malley Aug 2018

Development Of An Engineering Diagram For Additively Manufactured Austenitic Stainless Steel Alloys, Zachary T. Hilton, Joseph William Newkirk, Ronald J. O'Malley

Materials Science and Engineering Faculty Research & Creative Works

Austenitic stainless steels are the most widely applied types of stainless steels, due to their good weldability and high corrosion resistance. A number of engineering diagrams exist for the purpose of providing insight into the behavior of these steels. Examples of these diagrams are constitution diagrams (aka Schaeffler Diagrams) which are used to approximate the solidification path of the alloy and the amount of retained ferrite in the solidified matrix. Other diagrams are the Suutala diagram, which approximates cracking susceptibility, and microstructural maps, which predict the solidification path by varying a processing parameter, such as cooling rate. By combining these …


Effect Of Thickness On The Structure And Corrosion Performance Of Sputtered Ce-Al-O Coatings On Al 2024-T3 Alloy Substrates, Yuanyuan Liu, Jiamu Huang, Lilu Qin, James B. Claypool, Matthew J. O'Keefe, Yiming Jiang Jan 2018

Effect Of Thickness On The Structure And Corrosion Performance Of Sputtered Ce-Al-O Coatings On Al 2024-T3 Alloy Substrates, Yuanyuan Liu, Jiamu Huang, Lilu Qin, James B. Claypool, Matthew J. O'Keefe, Yiming Jiang

Materials Science and Engineering Faculty Research & Creative Works

Ce-Al-O coatings with thicknesses between ca. 136 nm and 1094 nm were deposited on Al 2024-T3 alloy substrates using magnetron co-sputtering of independent Al and CeO2 targets. The Ce-Al-O coatings with thicknesses from ca. 136 nm to 490 nm were compact, dense, and did not have distinct X-ray diffraction peaks. The ca. 1094 nm thick Ce-Al-O coating exhibited a columnar-textured outer layer ∼700 nm thick and a dense, ∼390 nm thick inner layer. X-ray photoelectron spectroscopy analysis revealed that the Ce-Al-O coatings contained Ce (III) species, and that the Al/Ce atomic ratio decreased with increasing coating thickness. Electrochemical corrosion data …


Design And Fabrication Of Functionally Graded Material From Ti To Γ-Tial By Laser Metal Deposition, Xueyang Chen, Lei Yan, Joseph William Newkirk, Frank W. Liou Aug 2017

Design And Fabrication Of Functionally Graded Material From Ti To Γ-Tial By Laser Metal Deposition, Xueyang Chen, Lei Yan, Joseph William Newkirk, Frank W. Liou

Materials Science and Engineering Faculty Research & Creative Works

Functionally graded material (FGM) is one kind of advanced material characterized by a gradual change in properties as the position varies. The spatial variation of compositional and microstructure over volume is aimed to control corresponding functional properties. In this research, when 100% γ-TiAl was directly deposited on pure Ti substrate, cracks were formed within the γ-TiAl layer. Then a six-layer crack-free functionally graded material of Ti/TiAl was designed and fabricated by laser metal deposition (LMD) method, with composition changing from pure Ti on one side to 100% γ-TiAl on the other side. The fabricated FGM was characterized for material properties …


Studying Chromium And Nickel Equivalency To Identify Viable Additive Manufacturing Stainless Steel Chemistries, Zachary T. Hilton, Joseph William Newkirk, Ronald J. O'Malley Aug 2017

Studying Chromium And Nickel Equivalency To Identify Viable Additive Manufacturing Stainless Steel Chemistries, Zachary T. Hilton, Joseph William Newkirk, Ronald J. O'Malley

Materials Science and Engineering Faculty Research & Creative Works

Chromium and nickel equivalency modeling has long been used in welding to determine the weldability of steel chemistries. A study was conducted to determine the applicability of Cr-Ni modeling to the additive manufacturing process. Many AM methods involve rapid solidification of small melt pools, similar to welding. Chemistries with varying Cr/Ni ratios were selected for use in a selective laser melting process and modeled using known models. Initial results indicate that the standard "safe welding zone" may not directly apply to additive manufacturing. The capability to build with chemistries outside the weldability “safe zone” could result in improved and varied …


Control Of Columnar To Equiaxed Transition In Solidification Macrostructure Of Austenitic Stainless Steel Castings, Semen Naumovich Lekakh, Ronald J. O'Malley, Mark C. Emmendorfer, Brenton Hrebec Jan 2017

Control Of Columnar To Equiaxed Transition In Solidification Macrostructure Of Austenitic Stainless Steel Castings, Semen Naumovich Lekakh, Ronald J. O'Malley, Mark C. Emmendorfer, Brenton Hrebec

Materials Science and Engineering Faculty Research & Creative Works

Solidification macrostructure is of great importance for the properties and the quality of castings made from austenitic grade stainless steels (ASS) because there are limited options to change as-cast macrostructure in the solid condition. A typical cast macrostructure of ASS has a fine surface chilled zone followed by an elongated dendrite zone, columnar to equiaxed transition (CET) zone, and centrally located equiaxed crystals. Several castings from ASS were produced to determine the effects of casting geometry, chilling, and grain refinement on CET. The transient thermal field in solidified heavy castings was simulated and used to determine an isotherm velocity (V) …


Strain Phase Separation: Formation Of Ferroelastic Domain Structures, Fei Xue, Yongjun Li, Yijia Gu, Jinxing Zhang, Long-Qing Chen Dec 2016

Strain Phase Separation: Formation Of Ferroelastic Domain Structures, Fei Xue, Yongjun Li, Yijia Gu, Jinxing Zhang, Long-Qing Chen

Materials Science and Engineering Faculty Research & Creative Works

Phase decomposition is a well-known process leading to the formation of two-phase mixtures. Here we show that a strain imposed on a ferroelastic crystal promotes the formation of mixed phases and domains, i.e., strain phase separation with local strains determined by a common tangent construction on the free energy versus strain curves. It is demonstrated that a domain structure can be understood using the concepts of domain/phase rule, lever rule, and coherent and incoherent strain phase separation, in a complete analogy to phase decomposition. The proposed strain phase separation model is validated using phase-field simulations and experimental observations of PbTiO …


Protective Conversion Coating On Mixed-Metal Substrates And Methods Thereof, Matthew O'Keefe, Surender Maddela Sep 2016

Protective Conversion Coating On Mixed-Metal Substrates And Methods Thereof, Matthew O'Keefe, Surender Maddela

Materials Science and Engineering Faculty Research & Creative Works

Mixed-metal automotive vehicle bodies-in-white comprising ferrous metal surfaces, zinc surfaces, aluminum alloy surfaces, and magnesium alloy surfaces are cleaned and immersed in an aqueous bath comprising an adhesion promoter and an aqueous electrocoat bath (the adhesion promoter may be in the electrocoat bath. The adhesion promoter, which may be a cerium salt, is selected to react with each metal in the body surfaces to form an oxide layer that provides corrosion resistance for the surface and adherence for the deposited polymeric paint coating. The body is cathodic in the electrocoat deposition.


Structure And Corrosion Behavior Of Sputter Deposited Ce-Al-O Coating On Al 2024-T3 Alloy Substrates, Yuanyuan Liu, Jiamu Huang, James B. Claypool, Matthew J. O'Keefe Jan 2016

Structure And Corrosion Behavior Of Sputter Deposited Ce-Al-O Coating On Al 2024-T3 Alloy Substrates, Yuanyuan Liu, Jiamu Huang, James B. Claypool, Matthew J. O'Keefe

Materials Science and Engineering Faculty Research & Creative Works

Deposition of Ce-Al-O coatings on Al 2024-T3 alloy substrates was conducted by magnetron co-sputtering of CeO2 and Al targets. The incorporation of Al into the CeO2 film resulted in an amorphous or nanocrystalline structure with binding energy states different from Al, Al2O3, and CeO2. Electrochemical measurements indicated that the amorphous or nanocrystalline Ce-Al-O coating increased the corrosion resistance of bare Al 2024-T3 substrates by more than three orders of magnitude and exhibited a very different cathodic and anodic protective mechanism compared to Al and CeO2 coated and as-polished Al 2024-T3 samples. …


Evolution Of Non-Metallic Inclusions In Foundry Steel Casting Processes, Marc Harris, Von Richards, Ronald J. O'Malley, Semen Naumovich Lekakh Dec 2015

Evolution Of Non-Metallic Inclusions In Foundry Steel Casting Processes, Marc Harris, Von Richards, Ronald J. O'Malley, Semen Naumovich Lekakh

Materials Science and Engineering Faculty Research & Creative Works

The evolution of nonmetallic inclusions was examined for 4320 steel at an industrial steel foundry. The steel was followed from electric arc furnace melting through ladle refining to final casting. Timed sampling was performed at all stages of the process. Samples were analyzed using an automated SEM/EDS system. The overall evolution of oxide inclusions in terms of nucleation, growth, and flotation during liquid processing was studied using area fraction and average diameter. Chemical composition evolution was observed using a joint ternary plotting tool developed under this program. It was found that the use of zirconium as an addition for nitrogen/oxygen …


Structure And Corrosion Behavior Of Sputter Deposited Cerium Oxide Based Coatings With Various Thickness On Al 2024-T3 Alloy Substrates, Yuanyuan Liu, Jiamu Huang, James B. Claypool, Carlos E. Castano, Matthew J. O'Keefe Nov 2015

Structure And Corrosion Behavior Of Sputter Deposited Cerium Oxide Based Coatings With Various Thickness On Al 2024-T3 Alloy Substrates, Yuanyuan Liu, Jiamu Huang, James B. Claypool, Carlos E. Castano, Matthew J. O'Keefe

Materials Science and Engineering Faculty Research & Creative Works

Cerium oxide-based coatings from ∼100 to ∼1400 nm in thickness were deposited onto Al 2024-T3 alloy substrates by magnetron sputtering of a 99.99% pure CeO2 target. The crystallite size of CeO2 coatings increased from 15 nm to 46 nm as the coating thickness increased from ∼100 nm to ∼1400 nm. The inhomogeneous lattice strain increased from 0.36% to 0.91% for the ∼100 nm to ∼900 nm thick coatings and slightly decreased to 0.89% for the ∼1400 nm thick coating. The highest adhesion strength to Al alloy substrates was for the ∼210 nm thick coating, due to a continuous …


Enhancing Grain Refinement Of Austenitic Steel With Ti Additions By Melt Treatment Sequence Optimization, Gun Ge, Semen Naumovich Lekakh, Ronald J. O'Malley May 2015

Enhancing Grain Refinement Of Austenitic Steel With Ti Additions By Melt Treatment Sequence Optimization, Gun Ge, Semen Naumovich Lekakh, Ronald J. O'Malley

Materials Science and Engineering Faculty Research & Creative Works

No abstract provided.


Crystallographic Orientation Of The Ε → Α' Martensitic (Athermal) Transformation In A Femnalsi Steel, S. T. Pisarik, D. C. Van Aken Jan 2014

Crystallographic Orientation Of The Ε → Α' Martensitic (Athermal) Transformation In A Femnalsi Steel, S. T. Pisarik, D. C. Van Aken

Materials Science and Engineering Faculty Research & Creative Works

The presence of a thermal ε- and α-martensite (α') in the as-cast structure of a Fe-0.08C-1.95Si-15.1Mn-1.4Al-0.017N alloy has been revealed by electron backscattered diffraction analysis. The alloy exhibited two a thermal martensitic transformation described by γ → α' and γ → ε → α'. The Shoji-Nishiyama orientation relationship was observed between γ-austenite and ε-martensite, while α-martensite nucleated from γ-austenite exhibited a Kurdjumov-Sachs orientation relationship. Six crystallographic variants of α-martensite consisting of three twin-related variant pairs were observed in ε-bands. A planar parallelism of {0001}ε || {110}α' and a directional relation …


A Preliminary Study Of Deformation Behavior Of Friction Stir Welded Ti-6al-4v, Jiye Wang, Jianqing Su, Rajiv S. Mishra, Ray Xu, John A. Baumann Jan 2014

A Preliminary Study Of Deformation Behavior Of Friction Stir Welded Ti-6al-4v, Jiye Wang, Jianqing Su, Rajiv S. Mishra, Ray Xu, John A. Baumann

Materials Science and Engineering Faculty Research & Creative Works

A preliminary study of deformation behavior of friction stir welded (FSW) Ti-6Al-4V was performed using two different tools with cylindrical and stepped spiral pin design for the welding process. The nugget regions experienced temperature above β transus and the matrix transformed to fine acicular α during cooling of the nugget. By using stepped spiral pin design, a local region with much refined grain structure and significant tool debris particles were observed. Room temperature tensile test showed increased strength and decreased ductility in the material from this region. Fractographic analysis revealed that tool debris particles served as void nucleation sites. Tensile …


An Evaluation Of Creep Behaviour In Friction Stir Welded Ma754 Alloy, Jiye Wang, Wei Yuan, Rajiv S. Mishra, Indrajit Charit Jan 2014

An Evaluation Of Creep Behaviour In Friction Stir Welded Ma754 Alloy, Jiye Wang, Wei Yuan, Rajiv S. Mishra, Indrajit Charit

Materials Science and Engineering Faculty Research & Creative Works

Effect of friction stir welding (FSW) on microstructure and creep properties of oxide dispersion strengthened (ODS) alloy MA754 were investigated. Fine-grained microstructure developed in the weld zone. TEM results showed some degree of particle agglomeration as a result of intense material flow. Creep tests of the FSW material were carried out at 973 and 1073 K. Power law creep behavior was observed with stress exponent values of 6.9 and 6.3 at 973 and 1073 K, respectively. The results were compared to those of the as-received material. Creep resistance of FSW material was lower than that of as-received material associated with …


Scrap Dissolution In Molten Iron Containing Carbon For The Case Of Coupled Heat And Mass Transfer Control, Ajay Kumar Shukla, Brahma Deo, D. G.C. Robertson Dec 2013

Scrap Dissolution In Molten Iron Containing Carbon For The Case Of Coupled Heat And Mass Transfer Control, Ajay Kumar Shukla, Brahma Deo, D. G.C. Robertson

Materials Science and Engineering Faculty Research & Creative Works

The scrap dissolution in an actual process like the BOF is affected both by mass transfer and heat transfer. In this paper, the mass transfer of carbon in liquid melt is considered along with heat transfer. The approaches used in this paper to model the scrap dissolution phenomenon include the application of Green's function, quasi-static, integral profile, and the finite difference approach for different Biot numbers. Mass transfer coefficients are calculated using the Chilton-Colburn's analogy for the case of forced convection. Since the quasi-static approach requires the least computational time, it is used for a detailed parametric study, including the …


Role Of Air Gap In Scrap Dissolution Process, Ajay Kumar Shukla, Brahma Deo, D. G.C. Robertson Dec 2013

Role Of Air Gap In Scrap Dissolution Process, Ajay Kumar Shukla, Brahma Deo, D. G.C. Robertson

Materials Science and Engineering Faculty Research & Creative Works

The role of the air gap formed between scrap and a solidified metal shell at the beginning of the scrap dissolution process has been investigated. The effect of air gap has been investigated for different Biot numbers (10 to 100) and ratios of air gap to liquid melt heat transfer coefficient (0.1 to 0.9). The predictions of the mathematical model are compared with the experimental results reported elsewhere. The role of air gap is found to be significant only for low Biot numbers (< 50) and for low ratios of air gap to liquid melt heat transfer coefficient (< 0.25). © 2013 The Minerals, Metals & Materials Society and ASM International.