Materials Science and Engineering Commons^™

Powder Rolling Of Cnt-Reinforced Aluminum Strips, Mostafa Abdel-Fattah El-Borady

Archived Theses and Dissertations

Multi walled carbon nanotubes (MWCNT) were added to aluminum powder (99.97% pure) to produce a composite material. Three mixing techniques were examined

1 Low energy mixing: Using a Turbula mixer with two different speeds 48 and 67 rpm.

2 High energy mixing: Using a ball mill without adding any balls in the mixing jars with two speeds 300 and 400 rpm.

3 Ball milling: Using the ball mill (with steel balls) to mix higher CNT weight fraction samples for the electrical resistivity tests.

The mixtures were packed in copper cans and rolled in a rolling machine to compact the mixture; …

Prerapation And Supercapacitor Property Of Al Doped Co3O4, Xin Ge, Ye Chen, Chun-Xia Zhang, Chang Shu

Journal of Electrochemistry

With KOH as precipitator to prepare Aluminum doped Co₃O₄,X-ray diffraction indicated that the doping Al did not change the crystal structure of Co₃O₄.Electrochemical properties of the sample were tested by cyclic voltammetry and constant-current charge/discharge.The results showed that the chemical doping improved the specific capacitance.When the mol ratio of Co(Ⅱ) with Al(Ⅲ)was 1∶0.05,the specific capacitance was up to 518.07 F/g within 0～400 mV potenitial at current density 5 mA/cm².

Processing, Microstructural And Mechanical Characterization Of Mechanically Alloyed Al-Al2o3 Nanocomposites, Pushkar Katiyar

Electronic Theses and Dissertations

Aluminum-alumina nanocomposites were synthesized using mechanical alloying of blended component powders of pure constituents. This study was performed on various powder mixtures with aluminum as the matrix and alumina as the reinforcement with volume fractions of 20, 30, and 50 % and Al2O3 particle sizes of 50 nm, 150 nm, and 5 µm. X-ray diffraction (XRD) and scanning electron microscopy (SEM) techniques were used for the crystal structure and microstructural characterization of the powders at different stages of milling. Al2O3 powders with 50 nm and 150 nm particle size were predominantly of γ-type, while Al2O3 of 5 µm size was …

Alum And Pacl Coagulation, Winarni Winarni

Makara Journal of Technology

Alum and PACl Coagulation. Coagulation occurs by interaction of aluminum hydrolysis products with the contaminant such as colloidal particles. It is necessary to consider the different aluminum species that may present during specific conditions, since the mechanism of turbidity removal is dependent upon them. PACl consists of preformed aluminum hydrolysis products, which are stable below pH 6 and less sensitive than in situ hydrolysis product, alum. The benefits of PACl relative to alum have been investigated as a function of pH and Al dosages. Specific conditions and aluminum species that exist during the certain mechanisms of coagulation are discussed. Results …

The Effects Of Patch Properties On The Debonding Behavior Of Patched Beam-Plates, Anette M. Karlsson

Mechanical Engineering Faculty Publications

The debonding characteristics of patched structures are investigated in this study by means of an analytical model. In particular, the effects the lay-up sequence and edge tapering of a carbon-reinforced epoxy patch, as well as the beveling of an aluminum patch, have on the initiation, stability, and extent of the debonding are considered. The results presented show that both the degree of edge-tapering and the patch properties must be carefully selected in order to optimize the patched structure. It is also shown that when designing a patched system, it is important to model the correct boundary and load conditions to …

Cracking In Cycloaliphatic Epoxy/Aluminum Composite Electrical Bushings, Keith Alan Parker

Doctoral Dissertations

The problem of cracking in electrical apparatus bushings as a result of thermal stresses was investigated. The bushings were composed of cycloaliphatic epoxy insulators with embedded aluminum conductors. The problem is due to the difference in coefficients of thermal expansion of the two materials. A solution to the problem had been to coat the conductors before they were formed together with the epoxy insulators. The coating was assumed to prevent cracking by allowing movement between the two materials as their dimensions changed during thermal expansion and contraction. The contribution of the coating was to be established.

The hypothesis was that …

Long-Term Effects Of Neutron Absorber And Fuel Matrix Corrosion On Criticality, William Culbreth, P. Zielinski

Mechanical Engineering Faculty Research

Proposed waste package designs will require the addition of neutron absorbing material to prevent the possibility of a sustained chain reaction occurring in the fuel in the event of water intrusion. Due to the low corrosion rates of the fuel matrix and the Zircaloy cladding, there is a possibility that the neutron absorbing material will corrode and leak from the waste container long before the subsequent release of fuel matrix material. An analysis of the release of fuel matrix and neutron absorber material based on a probabilistic model was conducted and the results were used to prepare input to KENO-V, …

Growth Of A Preferentially Oriented Aluminum Single Crystal, John George Bjeletich

Bachelors Theses and Reports, 1928 - 1970

When studying some anisotropic property of a specific metal, such as the critical shear stress of aluminum, it is desirable that the test specimen be a single crystal with the crystal axes preferentially oriented. Therefore, it is necessary to obtain a single crystal by one of the methods mentioned and by use of x-rays to determine the orientation. Once the single crystal is obtained and the orientation known, it is possible to grow a preferentially oriented aluminum single crystal by a method generally known as "seeding". The purpose of this thesis problem was to grow a crystal by utilizing the …

Stress-Induced Martensite Transformation In An Alloy Of The Copper-Aluminum-Nickel System, Gary D. Alexander

Bachelors Theses and Reports, 1928 - 1970

It was intended that the alloy be thoroughly investigated for martensite transformation that would make the alloy "super-elastic," but due to the many difficulties that arose this was not possible. Attempts to grow a single crystal from the cast alloy were not successful because of the difficulties that were encountered with the Kanthal resistance furnace (referred to later). Consequently, the growing of the single crystal was abandoned and the alloy was tested in the poly-crystalline form.

The Zone-Refining Of Aluminum And Magnesium With Copper As The Major Impurity, Russell E. Hoar

Bachelors Theses and Reports, 1928 - 1970

The purpose of this paper is to report on the investigation of the possibility of removing impurities from the two important light metals, aluminum and magnesium, by applying the principles of zone-refining. The impurities in these metals are namely iron, silicon, and copper, which is the main impurity. Copper and iron come from the reduction cells, while silicon is introduced during the preparation of the material for the reduction bath.

The Zone-Refining Of Aluminum With Copper As The Major Impurity, Arlan Edward Rathke, Russell E. Hoar

Bachelors Theses and Reports, 1928 - 1970

The purpose of this paper is to report on the investigation of the possibility of removing impurities from the two important light metals, aluminum and magnesium, by applying the principles of zone-refining. The impurities in these metals are namely iron, silicon, and copper, which is the main impurity. Copper and iron come from the reduction cells, while silicon is introduced during the preparation of the material for the reduction bath.

The Construction And Operation Of A Universal Specimen Mount With Protective Lead Shield For The Purpose Of Determining Pole Figures Using The Schulz-Decker Transmission Technique, Richard L. Fausner

Bachelors Theses and Reports, 1928 - 1970

It was the purpose of this study to construct a universal mount, to construct a protective lead shield, to operate the instrument, and to provide a pole figure using the transmission method of Schulz and Decker. There are at present several lengthy x-ray methods of determining the grain orientation of metals. These methods are mainly photographic. In order to provide a rapid means of obtaining the necessary information concerning the grain orientation of a metal, a universal mount was constructed.

The Effect Of Germanium On The Current Efficiency In The Electrolysis Of Pure Zinc Sulfate Solution, Keith R. Bock

Bachelors Theses and Reports, 1928 - 1970

It has long been recognized that electrolytic zinc cells are extremely sensitive to impurities. In fact, cer­tain impurities present in amounts as low as 0.1 mg/1 cause a serious loss of current efficiency. Also, the presence of several impurities in the electrolyte may accelerate the detrimental effect of each impurity.

Recrystallization Of High Purity Aluminum, Virgil H. Griswold Jr.

Bachelors Theses and Reports, 1928 - 1970

If a metal is first cold-worked and then heated to a sufficient temperature for an adequate length of time, the hardening properties due to cold-working disappear, and the metal will return more or less to its original state. Upon examination of the microstructure, we find that new grains have replaced the old grains through what is called recrystallization. The final size of the recrystallized grains depends upon three important variables--the degree of cold-work or deforma­tion, annealing temperature, and annealing time.

The Effect Of Manganese On The Age Hardening Of Aluminum-Copper Alloys, Keith P. Burgess

Bachelors Theses and Reports, 1928 - 1970

It is known that age-hardening occurs in alloys of the solid solution type containing a hardening constituent, of a metal or metallic compound which is more soluble in the solvent phase at higher tempertures than at lower temperatures.

The Metallography Of Aluminum Casting Alloys, Donald D. Goehler

Bachelors Theses and Reports, 1928 - 1970

The purpose of this thesis is to supply the Montana School of Mines with an up to date source of information concerning the metallography of aluminum casting alloys. This thesis is designed as a continuing project. Ultimately, it is hoped that a catalog containing all the typical structures of aluminum casting alloys will develop.

The Age-Hardening Of Aluminum With Mgzn2, Sidney E. Worthen

Bachelors Theses and Reports, 1928 - 1970

The purpose of this thesis is to investigate the age-hardening of aluminum with magnesium and zinc in such proportions as to conform to the compound MgZn₂.

Because of a lack of time and proper equipment, the only property investigated was the hardness as indicated by the Rockwell Superficial Hardness Tester.

The Age Hardening Of Silver With Copper-Silicide, Joseph Edward Shaw

Bachelors Theses and Reports, 1928 - 1970

The successful application of the phenomenon of pre­cipitation hardening to aluminum and copper has indicated the possibility of hardening all metals in the same way. The phenomenon of age hardening was discoveredin 1911, and since that time much research has been car­ried on in all parts of the world on various alloy sys­tems.

Structure Of Eutectics, Dilip K. Das

Bachelors Theses and Reports, 1928 - 1970

The present paper is a result of work done on the study of structures of eutectics of a certain eutectic-forming binary systems. In this research work no systems with intermetallic compounds have been studied.

The Electroplating Of Cadmium From Sulfate Solutions, Lewis S. Prater

Bachelors Theses and Reports, 1928 - 1970

It has been proven that cadmium forms a very satisfactory plate on steel, which has to withstand severe corrosion, especially the corrosion of sea water and spray. The metal is now successfully plated electrolytically from cyanide solutions, but wherever work is carried on with cyanide, there is great danger of poisoning to the workers.

The Electrolytic Deposition Of Chromium Upon Aluminum, E. Fults, L. D. Voerge

Bachelors Theses and Reports, 1928 - 1970

The purpose or this investigation is primarily to determine the best conditions for plating chromium on aluminum. The work was carried out with the hope of obtaining coherent deposits, and of determin­ing the conditions under which such deposits may be duplicated.