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2025

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Articles 91 - 120 of 971

Full-Text Articles in Materials Science and Engineering

Imaging Of Dynamic Processes In Materials With A Laser-Wakefield Accelerator, J. Kang, R. J. Shalloo, M. J. Higgins, S. J.D. Dann, J. N. Gruse, C. I.D. Underwood, A. F. Antoine, C. Arran, C. D. Baird, M. D. Balcazar, N. Bourgeois, J. A. Cardarelli, K. Krushelnick, S. P.D. Mangles, C. D. Murphy, N. Lu, P. P. Rajeev, M. P. Selwood, D. R. Symes, C. P. Ridgers, A. G.R. Thomas, C. Thornton, Z. Najmudin, P. G. Sanders, P. D. Staublin, A. J. Shahani, M. J.V. Streeter Dec 2025

Imaging Of Dynamic Processes In Materials With A Laser-Wakefield Accelerator, J. Kang, R. J. Shalloo, M. J. Higgins, S. J.D. Dann, J. N. Gruse, C. I.D. Underwood, A. F. Antoine, C. Arran, C. D. Baird, M. D. Balcazar, N. Bourgeois, J. A. Cardarelli, K. Krushelnick, S. P.D. Mangles, C. D. Murphy, N. Lu, P. P. Rajeev, M. P. Selwood, D. R. Symes, C. P. Ridgers, A. G.R. Thomas, C. Thornton, Z. Najmudin, P. G. Sanders, P. D. Staublin, A. J. Shahani, M. J.V. Streeter

Michigan Tech Publications

Betatron x rays generated from laser-wakefield accelerators are a promising source for imaging dynamic processes in materials. Here, we present proof-of-concept imaging of microstructural evolution in a hypermonotectic Al-Bi alloy, which consists of liquid Bi particles in a solid Al matrix. The images capture the elongation and fragmentation of Bi particles upon isothermal annealing. Because of the femtosecond time scale of the betatron source, the images are not subject to motion blur, whereas the accessibility of the source allows for studies of long-term processes such as annealing. The high-resolution data reveal that the evolution of Bi particles is mediated by …


Production Of Recombinant Β-Galactosidase Protein In Bombyx Mori (Bmn1) Baculovirus Insect Cells, Shuhrat Sh. Khasanov, Jumanazar Ch Mengturayev, Jaloliddin M. Abdurakhmanov, Dilmurodjon B. Turdaliyev, Shakhnoz S. Azimova Dec 2025

Production Of Recombinant Β-Galactosidase Protein In Bombyx Mori (Bmn1) Baculovirus Insect Cells, Shuhrat Sh. Khasanov, Jumanazar Ch Mengturayev, Jaloliddin M. Abdurakhmanov, Dilmurodjon B. Turdaliyev, Shakhnoz S. Azimova

CHEMISTRY AND CHEMICAL ENGINEERING

In this study we aimed to obtain a novel recombinant β-galactosidase baculovirus using the Bombyx mori baculovirus – insect cell expression system. A new recombinant plasmid was constructed on the basis of the pBacPAK8 transfer vector and cloned in E. coli cells. Subsequently, a recombinant baculovirus was generated in Bombyx mori cells, and efficient expression of the β-galactosidase gene was observed. The enzymatic activity of the protein was confirmed by the ONPG assay. The results demonstrated that the baculovirus – insect cell system expands the possibilities for producing proteins of industrial significance.


Photocatalytic Activity Of The Mixed Of Ti/Fe/Mo Oxide Composites For Degradation Of Nitrofurazone, Dilshoda R. Tursunova, Zuhra Ch. Kadirova, Shahlo Sh. Daminova, Kadriya Kh. Gabidullina Dec 2025

Photocatalytic Activity Of The Mixed Of Ti/Fe/Mo Oxide Composites For Degradation Of Nitrofurazone, Dilshoda R. Tursunova, Zuhra Ch. Kadirova, Shahlo Sh. Daminova, Kadriya Kh. Gabidullina

CHEMISTRY AND CHEMICAL ENGINEERING

The aim of study is synthesize mixed oxide composites based on titanium dioxide, iron and molybdenum oxides from industrial waste materials and evaluated for their photocatalytic degradation performance of nitrofurazone—a persistent and toxic antibiotic frequently detected in aquatic environments. Various Ti/Mo ratios (T95M5, T87.5M12.5, T75M25, and T50M50) were prepared through thermal treatment at 600 °C and characterized using XRD, UV–Vis and Raman spectroscopy to assess structural and optical properties.XRD and Raman analyses confirmed the presence of anatase-phase TiO₂ and Mo/Fe oxides, with optimal crystallinity and heterojunction formation observed in the T87.5M12.5 composite. UV–Vis spectroscopic studies demonstrated that this composite exhibited …


Gas Chromatographic Analysis Of Fractions Separated By Atmospheric Distillation Of Pyrolysis Distillate, Gulnora K. Komolova, Lola A. Yusupova Dec 2025

Gas Chromatographic Analysis Of Fractions Separated By Atmospheric Distillation Of Pyrolysis Distillate, Gulnora K. Komolova, Lola A. Yusupova

CHEMISTRY AND CHEMICAL ENGINEERING

The primary objective of this study is to optimize the process of isolating the C9 hydrocarbon fraction from pyrolysis distillate and to evaluate the impact of various temperature regimes on the product composition. To achieve this goal, the dry distillation process was conducted at three different temperatures: 152 °C, 159 °C, and 170 °C. Condensate samples obtained from each test were analyzed using gas chromatography (GC). The analysis results revealed that the fraction obtained at 152 °C yielded the most favorable outcome: the C9 fraction yield was 11.11%, which is higher than the values obtained at 159 °C (4.59%) and …


Lightweight Thermal Insulation Brick Based On Jerdanak Clay Shale, Obtained With The Addition Of Sawdust, Mastura Kh. Aripova, Sarvar T. Bozorov Dec 2025

Lightweight Thermal Insulation Brick Based On Jerdanak Clay Shale, Obtained With The Addition Of Sawdust, Mastura Kh. Aripova, Sarvar T. Bozorov

CHEMISTRY AND CHEMICAL ENGINEERING

The aim of this study was to produce lightweight thermal insulation bricks based on Djerdanak clay shale with the addition of wood sawdust. The starting materials were clay shale from the Djerdanak deposit, fireclay made from it, and wood chips—a waste product from the wood processing industry. The optimal brick composition was determined to include 60% clay shale, 40% fireclay made from clay shale, and 14% wood chips (over 100%). The apparent density of the optimal brick composition corresponds to an apparent product density of 1 g/cm³ and a compressive strength of 3.6 N/mm². The microstructure of the material demonstrates …


Waste Utilization Considering Volatiles Circulation Behavior In Cement Kilns, Geun-Seong Lee, Farrukh B. Erkinov, Zebo A. Babakhanova, Mukhammadamin Sh. Jololdinov, Mastura Kh. Aripova Dec 2025

Waste Utilization Considering Volatiles Circulation Behavior In Cement Kilns, Geun-Seong Lee, Farrukh B. Erkinov, Zebo A. Babakhanova, Mukhammadamin Sh. Jololdinov, Mastura Kh. Aripova

CHEMISTRY AND CHEMICAL ENGINEERING

Since the cement kiln process has various advantages for waste incineration, the waste utilization as alternative fuel has been widely applied in the cement process. For waste utilization in kiln process, it is necessary to operate within the range of not-affecting the clinker quality and the operation stability, and not-causing pollution problems, with ensuring the smooth clinker production. In order to quantitatively analyze the volatiles circulation phenomena during waste utilization as alternative fuel in the kiln process, the simplified volatiles circulation model is derived based on material balances of volatiles, from which the permissible waste utilization % as alternative fuel …


Physico-Chemical Study Of Interaction In The “Urea – Glycine – Water” System, Suvonkul E. Nurmonov, Saydullo Kh. Azimov Dec 2025

Physico-Chemical Study Of Interaction In The “Urea – Glycine – Water” System, Suvonkul E. Nurmonov, Saydullo Kh. Azimov

CHEMISTRY AND CHEMICAL ENGINEERING

A comprehensive physicochemical study of the aqueous “urea – glycine” system was conducted to establish the mechanisms of intermolecular interaction and stability parameters for the development of modified liquid nitrogen fertilizers (LNF). Isomolar series, visual-polythermal analysis, X-ray phase analysis (XRD), single-crystal X-ray diffraction (SC-XRD), IR spectroscopy, and thermal analysis (DTA/TGA) methods were applied. It was found that the interaction of components in solution leads to the formation of molecular associates stabilized by hydrogen bonds. The XRD and SC-XRD methods confirmed that no new individual chemical compounds are formed in the solid phase. It was proven that the addition of glycine …


Unlocking The Industrial Potential Of Khojaykon Sylvinite Through Mineralogical And Chemical Investigations, Elyor D. Eminov, Kholtura Ch. Mirzakulov, Gavkhar E. Melikulova, Ruslan Ch. Yorbobaev, Kamola S. Arifdjanova Dec 2025

Unlocking The Industrial Potential Of Khojaykon Sylvinite Through Mineralogical And Chemical Investigations, Elyor D. Eminov, Kholtura Ch. Mirzakulov, Gavkhar E. Melikulova, Ruslan Ch. Yorbobaev, Kamola S. Arifdjanova

CHEMISTRY AND CHEMICAL ENGINEERING

The purpose of this study is to analyze the chemical, mineralogical, and fractional composition of sylvinite from the Khodjaikan deposit in Uzbekistan in order to assess its potential for potassium fertilizer production. Using chemical analysis, XRD, and IR spectroscopy, the ore was found to contain KCl (19.5–30.1%), NaCl (62.08–71.85%), CaCl₂ (1.12–1.32%), and MgCl₂ (0.18–0.32%). The water-insoluble residue, mainly sulfates, carbonates, and silicates, was also identified. These findings are important for improving beneficiation processes and reducing waste. Comparison with the Verkhnekamsk deposit highlights the quality and potential of Khodjaikan sylvinite. The research supports sustainable resource management.


Changes In The Structure And Properties Of Titanium In The Process Of Pressure Treatment, Sardor S. Abriev, Nasiba U. Abduraimova, Zokir R. Akramov, Yulbarskhon N. Mansurov Dec 2025

Changes In The Structure And Properties Of Titanium In The Process Of Pressure Treatment, Sardor S. Abriev, Nasiba U. Abduraimova, Zokir R. Akramov, Yulbarskhon N. Mansurov

CHEMISTRY AND CHEMICAL ENGINEERING

Titanium is classified as a critical metal. It serves as a raw material for a wide range of industries owing to its unique properties – high strength at low density, corrosion resistance, and biocompatibility makes it indispensable. Uzbekistan and China possess primary resources for titanium production. However, the complexity of extraction and particularly processing, combined with high production costs, limits its large-scale use and increases the risk of shortages in industrial manufacturing. In this study, the structural and property evolution of titanium during pressure-based processing was investigated. Technology for producing powder titanium by metal forming methods is proposed. The results …


The Structure And Properties Of Er2o3 And Yb2o3 Based Ceramic Materials, Sintered Under High Pressure, Vladimir S. Urbanovich, Vadim D. Zhivulko, Eygeniy N. Poddenezhny, Ekaterina E. Trusova, Vladimir S. Niss Dec 2025

The Structure And Properties Of Er2o3 And Yb2o3 Based Ceramic Materials, Sintered Under High Pressure, Vladimir S. Urbanovich, Vadim D. Zhivulko, Eygeniy N. Poddenezhny, Ekaterina E. Trusova, Vladimir S. Niss

CHEMISTRY AND CHEMICAL ENGINEERING

The aim of the work was to obtain high-density optically transparent ceramic samples by sintering cubic modification Er2O3 and Yb2O3 oxides micropowders at the pressure of 7 GPa and the heating current power of 0.6–1.0 kW, which was demonstrated. Non-monotonic dependence of the density on the heating current power has been established. The maximum density values of 9.2 g/cm3 (Er2O3) and 9.8 g/cm3 (Yb2O3) were achieved at the power of 0.8 and 0.9 kW, respectively. During sintering, the cubic phase partially transforms into the …


Bond Behavior Of Full-Scale Beams Using Sustainable Self-Compacting Concrete, Hayder H. Alghazali, Atheer H.M. Algburi, John J. Myers Dec 2025

Bond Behavior Of Full-Scale Beams Using Sustainable Self-Compacting Concrete, Hayder H. Alghazali, Atheer H.M. Algburi, John J. Myers

Civil, Architectural and Environmental Engineering Faculty Research & Creative Works

Sustainable concrete is a step towards greener and more eco-friendly concrete construction practices, helping to solve global environmental problems. The present study focuses on the bond behavior between steel reinforcement and greener self-compacting concrete, specifically sustainable self-compacting concrete (SUS-SCC). Three SUS-SCC mixtures with different fly ash (FA) to cement replacement levels of [50, 60, and 70% (by mass)] were developed. Twelve full-scale SUS-SCC beams with a cross-section of (305 x 57) mm and a total length of 3048 mm were cast and tested using a four-point load test setup. The effect of longitudinal and lateral steel reinforcement ratios in the …


Integrating Dft And Machine Learning To Predict Structural Properties In High Entropy Alloys, Nathan Linton Dec 2025

Integrating Dft And Machine Learning To Predict Structural Properties In High Entropy Alloys, Nathan Linton

All Dissertations

In the past decade, a paradigm shift in the design of metal alloys has been observed. These new alloys are commonly referred to as high entropy alloys (HEAs), multi-principal element alloys (MPEAs), or complex, concentrated alloys (CCAs). In contrast to conventional alloys, which consist of one main element (for example 80%) with other elements in small amounts, HEAs are made of four or more main elements ranging from 5 to 35% each element. Due to the large presence of multiple elements, HEAs have shown substantial material property improvements over conventional alloys such as steel. For example, they have high ductility …


Additive Manufacturing Of Carbons From Commodity Polyolefins, Paul Smith Dec 2025

Additive Manufacturing Of Carbons From Commodity Polyolefins, Paul Smith

Dissertations

Though tremendous progress has been made engineering carbon materials across length-scales from the molecular to the macroscopic, on-demand macro-structural control of carbons is still developing. Many carbon materials like graphene, carbon nanotubes, activated carbons, and carbon fibers have powder or fiber form factors. Recent research has pioneered on-demand carbon production through additive manufacturing (AM) via 1) extrusion and post-processing of highly filled carbon slurries, or 2) printing and pyrolysis of polymeric carbon precursors such as polyimides, acrylated polyethylene glycol, and phenolics. While groundbreaking, most methods face challenges with adoption due to costly/complex materials and manufacturing processes, and large dimensional changes …


Effect Of Polymer Contaminants Sourced From Coated Paper On The Performance Of The Resulting Recycled Paper, Ezekiel J. Guevarra Dec 2025

Effect Of Polymer Contaminants Sourced From Coated Paper On The Performance Of The Resulting Recycled Paper, Ezekiel J. Guevarra

All Theses

The growing demand for sustainable packaging has accelerated the use of paper-based materials as alternatives to plastics. To provide barrier and functional properties, these materials are often modified with polymer coatings. While beneficial during use, such coatings can persist as contaminants during recycling, potentially disrupting fiber bonding and reducing the quality of recycled paper. This study examined the impact of extrusion-coated low-density polyethylene (LDPE) films and two aqueous dispersions (Vapor/Water-Barrier, Acrylic Film (VWAF) and Oil & Grease Barrier (OGBF)) on contaminant distribution and mechanical performance of recycled handsheets. Kraft paper coated at varying levels was repulped and formed into handsheets, …


Elucidating Differences In Constitutionally Isomeric Diamine- And Bisphenol-Based Polybenzoxazine Networks, Benjamin L. G. Morasch Dec 2025

Elucidating Differences In Constitutionally Isomeric Diamine- And Bisphenol-Based Polybenzoxazine Networks, Benjamin L. G. Morasch

Dissertations

This dissertation aims to expand the fundamental understanding of diamine-based benzoxazine chemistry by examining how synthesis influences the network properties of 4,4’-ddm and phenol-based (P-ddm) benzoxazine, compared to the constitutionally isomeric bisphenol-F and aniline-based (BF-a) benzoxazine. While bisphenol-based benzoxazines such as BF-a have been studied more extensively, diamine-based benzoxazines are still relatively unexplored due to the competition with the formation of 1,3,5-hexahydrotriazine intermediates and the inconsistent thermal and mechanical properties reported in the literature. These inconsistencies stem from factors including synthetic methods, curing conditions, and degradation during polymerization that have been overlooked.

To address these issues, this dissertation is organized …


Upcycling Commodity Polymers To Advanced Materials For Energy And Environmental Sustainability, Anthony Griffin-Espinoza Dec 2025

Upcycling Commodity Polymers To Advanced Materials For Energy And Environmental Sustainability, Anthony Griffin-Espinoza

Dissertations

Synthetic polymers play an essential role in nearly every aspect of our lives. Extending beyond single-use packaging, polymeric material design has progressed to attain tailorable architectures granting exceptional performance across advanced applications, including carbon-fiber reinforced polymer composites for aerospace, conductive materials for soft electronics, and drug carriers for biomedicine. While highly promising, intricately designed polymers needed to achieve excellent performance often have limited processability, complex synthetic methods, and expensive precursors. Furthermore, due to a lack of recyclability, commodity polymer waste streams result in both environmental impacts and a substantial loss of economic value. This dissertation focuses on developing robust strategies …


Understanding Crystallization Behaviors Of Polyethylene-Derived Vitrimers, Sara Valdez Dec 2025

Understanding Crystallization Behaviors Of Polyethylene-Derived Vitrimers, Sara Valdez

Dissertations

Polyolefins (POs), particularly polyethylene (PE) and polypropylene (PP), are among the most widely utilized polymers globally, valued for their low production costs and favorable mechanical properties stemming from their semicrystalline microstructure. However, their extensive use and improper disposal have raised serious environmental and human health concerns. In response, PO-derived covalent adaptable networks (CANs) have emerged, integrating dynamic chemistries to enable recyclability and sustainable end-of-life strategies. While existing literature has largely focused on novel CAN systems, structure–property relationships, and network rearrangement in relation to thermal transitions (e.g., topological freezing temperature), the influence of network formation on crystallinity and crystallization kinetics remains …


Effects Of Wc Additions On The Phase Formation Of (Hf,Nb,Ta,Ti,Zr)C-(Hf,Nb,Ta,Ti,Zr)B2 High Entropy Dual Phase Ceramics, Rubia Hassan, William G. Fahrenholtz, Gregory E. Hilmas Dec 2025

Effects Of Wc Additions On The Phase Formation Of (Hf,Nb,Ta,Ti,Zr)C-(Hf,Nb,Ta,Ti,Zr)B2 High Entropy Dual Phase Ceramics, Rubia Hassan, William G. Fahrenholtz, Gregory E. Hilmas

Materials Science and Engineering Faculty Research & Creative Works

High entropy dual phase (Hf,Nb,Ta,Ti,Zr)C-(Hf,Nb,Ta,Ti,Zr)B2 ultra-high temperature ceramics were produced from powders synthesized by boro-carbothermal reduction. Systematic additions of 2.5 wt%, 5 wt%, and 10 wt% WC were incorporated after powder synthesis. Additions of 2.5 wt% and 5 wt% WC dissolved into the host ceramics, resulting in complete solid solution formation and nearly full densification. In contrast, a secondary monoboride phase evolved for the composition with 10 wt% WC, in addition to the main high entropy carbide and diboride phases. Thermodynamic analysis revealed that WB formation was favorable for WC additions in the presence of metal diborides at the sintering …


Thermal Properties Of High Entropy Dual Phase (Hf,Nb,Ta,Ti,Zr,)C-(Hf,Nb,Ta,Ti,Zr)B2 Ceramics: Comparison With The High Entropy Single-Phase Ceramics And The Effect Of Wc Additions, Rubia Hassan, William G. Fahrenholtz, Gregory E. Hilmas Dec 2025

Thermal Properties Of High Entropy Dual Phase (Hf,Nb,Ta,Ti,Zr,)C-(Hf,Nb,Ta,Ti,Zr)B2 Ceramics: Comparison With The High Entropy Single-Phase Ceramics And The Effect Of Wc Additions, Rubia Hassan, William G. Fahrenholtz, Gregory E. Hilmas

Materials Science and Engineering Faculty Research & Creative Works

The heat capacity, thermal diffusivity and thermal conductivity of (Hf,Nb,Ta,Ti,Zr)C-(Hf,Nb,Ta,Ti,Zr)B2 high entropy dual phase ceramics were evaluated from room temperature to 1800 °C and compared with the constituent high entropy single phase ceramics of the same nominal compositions. Thermal conductivity of the (Hf,Nb,Ta,Ti,Zr)C-(Hf,Nb,Ta,Ti,Zr)B2 dual phase ceramic increased from 17.7 W m−1 K−1 at room temperature to 54 W m−1 K−1 at 1800 °C. The addition of WC to the dual phase ceramic reduced its thermal conductivity. For the addition of 5 wt% WC, room temperature thermal conductivity was 16.8 W m−1 K−1 …


Micro/Nanomechanical Properties Of Top-Seeded Melt Grown Ybco Single Crystals Determined Using Depth Sensing Indentation, Ugur Kolemen, Cafer Mert Yesilkanat, Fikret Yilmaz, Fatih Dogan, Orhan Uzun Dec 2025

Micro/Nanomechanical Properties Of Top-Seeded Melt Grown Ybco Single Crystals Determined Using Depth Sensing Indentation, Ugur Kolemen, Cafer Mert Yesilkanat, Fikret Yilmaz, Fatih Dogan, Orhan Uzun

Materials Science and Engineering Faculty Research & Creative Works

Mechanical properties of the bulk YBa2Cu3O7-x (YBCO) single crystal superconductor, prepared by using the Top Seeded Melt Growth (TSMG) method, were determined. Property measurements were conducted by the nanoindentation method under various loads and the micro indentation method at different temperatures. Hardness (H) and reduced elastic modulus (Er) values were calculated by using the Oliver–Pharr method. According to hf/h max values found from load- displacement curves, there is a sink in behavior around outer rim of the indents that was confirmed by atomic force microscopy (AFM) analysis. Nanoindentation analyses conducted on upper section, middle section and subsection revealed that all …


A Precipitation-Hardened High-Entropy Alloy With Excellent Mechanical Properties Additively Manufactured By In-Situ Alloying, Matthew Luebbe, Shahryar Mooraj, Jonathan Poplawsky, Hans Pommerenke, Wen Chen, Haiming Wen Dec 2025

A Precipitation-Hardened High-Entropy Alloy With Excellent Mechanical Properties Additively Manufactured By In-Situ Alloying, Matthew Luebbe, Shahryar Mooraj, Jonathan Poplawsky, Hans Pommerenke, Wen Chen, Haiming Wen

Materials Science and Engineering Faculty Research & Creative Works

Studies on precipitation-hardened high-entropy alloys (PHEAs) have demonstrated high strength, good ductility, and thermal stability, making them excellent candidates for high-temperature structural applications such as nuclear reactors. However, many complex parts for those applications would need to be produced via additive manufacturing (AM), whose rapid cooling rates and multiple heating cycles could change the microstructure of the chosen alloys and accordingly their mechanical properties. A PHEA, (Fe0.3Ni0.3Mn0.3Cr0.1)88Ti4Al8, which was developed and produced via conventional manufacturing in our previous work with high strength but low ductility, was chosen to test the effects of AM on the microstructure and mechanical properties. Scanning …


Variable-Temperature Plasmonic High-Entropy Carbides, Simon Divilov, Sean D. Griesemer, Robert C. Koennecker, Michael J. Ammendola, Adam C. Zettel, Hagen Eckert, Jeffrey R. Shallenberger, Xiomara Campilongo, William G. Fahrenholtz, Arrigo Calzolari, Douglas E. Wolfe, Stefano Curtarolo Dec 2025

Variable-Temperature Plasmonic High-Entropy Carbides, Simon Divilov, Sean D. Griesemer, Robert C. Koennecker, Michael J. Ammendola, Adam C. Zettel, Hagen Eckert, Jeffrey R. Shallenberger, Xiomara Campilongo, William G. Fahrenholtz, Arrigo Calzolari, Douglas E. Wolfe, Stefano Curtarolo

Materials Science and Engineering Faculty Research & Creative Works

Effective thermal management at variable and extreme temperatures face limitations for the development of novel energy and aerospace applications. Plasmonic approaches, shown to be capable of tailoring black-body emission, could be effective if materials with high-temperature and tunable plasmonic resonance were available. Here, we report a synergy between experimental and theoretical results proving that many high-entropy transition metal carbides, consisting of four or more metals at equal molar ratio, have plasmonic resonance at room, high (>1000∘C) and variable temperatures. We also found that these high-entropy carbides can be tuned and show considerable plasmonic thermal cycling stability. This paradigm-shift approach …


The Comparison Of Dixon–Mood And 1/Nf Methods For Fatigue Limit Estimation Of 17–4 Ph Stainless Steel (H900), Arthur Pallar Pallar Dec 2025

The Comparison Of Dixon–Mood And 1/Nf Methods For Fatigue Limit Estimation Of 17–4 Ph Stainless Steel (H900), Arthur Pallar Pallar

Masters Theses

This study compares two methods for estimating the fatigue limit of 17-4 PH stainless steel (H900): the Dixon–Mood staircase and Kujawski 1/Nf linear method. Tests were conducted on an MTS Acumen 3 kN system under axial tension–tension loading at R = 0.1 and 50 Hz, following the standard practice defined in ASTM E466-15. Flat specimens were fabricated by water-jet cutting and polished. Tensile tests verified mechanical properties consistent with published data for the H900 condition. Fifteen specimens tested by the staircase method yielded a mean fatigue limit of 1138 MPa. The 1/Nf analysis using four specimens produced 1159 MPa, 2 …


Advancements In Visualization, Post-Processing And Ai-Enhanced Modeling Of Multi-Scale Micromechanics For Composite Materials, Joao Guilherme Brites Rei Dec 2025

Advancements In Visualization, Post-Processing And Ai-Enhanced Modeling Of Multi-Scale Micromechanics For Composite Materials, Joao Guilherme Brites Rei

Masters Theses

This study addresses some of the primary deficits of a localization/homogenization workflow for composite materials by focusing on the visualization and enhancement of models based on GMC and HFGMC, with emphasis on their implementation within the NASMAT ecosystem.

This thesis details the development of two dynamic, ParaView-based plugins that convert large hierarchical simulation outputs into interactive insights. While NASMATDiscreteElement systematizes RUC creation with transparent parametrization in a reproducible GUI, NASMATExplorerRUC enables the inspection of deeply nested datasets through accurate cell picking and synchronizes comparisons between parent and child views. Additionally, a shallow U-Net neural network is optimized on HFGMC data …


Effect Of Powder Recycling On Powder Characteristics And Mechanical Properties Of Materials Produced By Laser Powder Bed Fusion (Lpbf): A Review, Mihiretu Ganta, Marta Kurek, Arezoo Emdadi, Tadeusz Łagoda, Marek Pagáč Dec 2025

Effect Of Powder Recycling On Powder Characteristics And Mechanical Properties Of Materials Produced By Laser Powder Bed Fusion (Lpbf): A Review, Mihiretu Ganta, Marta Kurek, Arezoo Emdadi, Tadeusz Łagoda, Marek Pagáč

Materials Science and Engineering Faculty Research & Creative Works

As the Laser powder bed fusion (LPBF) process advances toward industrial-scale production, the sustainability of metal powder feedstocks has become a focal point of research. The powder recycling approach, while environmentally and economically favorable, results in a series of physicochemical variations that could compromise the part quality. The resulting variation in powder characteristics with powder recycling could affect the powder layer density and melt pool dynamics, resulting in defect formation and hindering the structural integrity of LPBFed parts. These alterations pose significant constraints to mechanical performance, particularly in fatigue-sensitive applications where even minor imperfections can substantially reduce service life. The …


Polypropylene/Polyethylene Blends With Asymmetric Viscosity: Fabrication, Characterization, And Recycling Potential, Bernadine Daichendt Dec 2025

Polypropylene/Polyethylene Blends With Asymmetric Viscosity: Fabrication, Characterization, And Recycling Potential, Bernadine Daichendt

All Dissertations

Polyolefin materials, polypropylene (PP) and polyethylene (PE), are widely used in day-to-day life both commercially and industrially, offering versatile applications due to their mechanical and chemical properties. The high consumption rate of these materials makes them important targets for recycling efforts. However, there are multiple contributing factors leading to low recycling of PP and PE, chiefly sorting factors: chemical similarity, changed properties after multiple rounds of processing, and the use of processing aids. It is necessary to point out that, because of multiple melt processing cycles, recycled PP has decreased molecular weight due to chain scission. Conversely, recycled PE molecular …


Optical Characterization Of Ge And Gesn Grown In Aspect Ratio Trapping Structures For Enhanced Emitter Performance, Abdulla Said Ali Dec 2025

Optical Characterization Of Ge And Gesn Grown In Aspect Ratio Trapping Structures For Enhanced Emitter Performance, Abdulla Said Ali

Graduate Theses and Dissertations

Silicon (Si) began dominating the electronics industry since 1960s, the dominance came due to its affordability and well developed fabrication processes. But when it comes to light emitting devices and photonics devices in general, the indirect bandgap of Si has caused many scientists to search for alternative semiconductor materials that can deliver better light emission, materials that can also improve wavelengths detection which is also very limited when it comes to Si, reduce losses and greater light amplification, all this while still being affordable. Despite these limitations, Si has been widely used in Complementary Metal Oxide Semiconductor (CMOS) manufacturing and …


Emerging Solid Electrolytes For Solid-State Sodium Batteries: Synthesis And Interface Study., Xiaolin Guo Dec 2025

Emerging Solid Electrolytes For Solid-State Sodium Batteries: Synthesis And Interface Study., Xiaolin Guo

Electronic Theses and Dissertations

Over the past decade, solid-state batteries have attracted significant attention as the next-generation energy storage technology due to their higher energy density and enhanced safety. Given the abundant sodium (Na) resources relative to lithium (Li), the development of sodium-based batteries has become increasingly compelling. Within a solid-state battery, the solid electrolytes (SEs) serve the dual function of (i) electronically insulating and physically separating the electrodes, and (ii) transporting ions between the anode and cathode. To meet these essential requirements, ideal SEs must process high ionic conductivity with negligible electronic conductivity, robust structural and chemical stability, a wide electrochemical window, and …


Data Driven Design Of Ultra High Performance Concrete Prospects And Application, Bryan K. Aylas-Paredes, Taihao Han, Advaith Neithalath, Jie Huang, Ashutosh Goel, Aditya Kumar, Narayanan Neithalath Dec 2025

Data Driven Design Of Ultra High Performance Concrete Prospects And Application, Bryan K. Aylas-Paredes, Taihao Han, Advaith Neithalath, Jie Huang, Ashutosh Goel, Aditya Kumar, Narayanan Neithalath

Electrical and Computer Engineering Faculty Research & Creative Works

Ultra-high-performance concrete (UHPC) is a specialized class of cementitious composites that is increasingly used in various applications, including bridge decks, connections between precast components, piers, columns, overlays, and the repair and strengthening of bridge elements. The mechanical and durability properties of UHPC are significantly influenced by factors such as low water-to-binder ratios, the inclusion of supplementary cementitious materials (SCMs), and fiber reinforcement. Machine learning (ML) has been employed to predict the performance of UHPC and optimize its mixture designs by using various raw materials. This study first provides a comprehensive review of ML applications in UHPC, focusing on predicting workability, …


Investigating The Performance Of Fibre Reinforced Plastic Repairs To Timber Marine Civil Structures At His Majesty’S Naval Base Devonport, Anna G. Walther Dec 2025

Investigating The Performance Of Fibre Reinforced Plastic Repairs To Timber Marine Civil Structures At His Majesty’S Naval Base Devonport, Anna G. Walther

The Plymouth Student Scientist

This paper explores Fibre Reinforced Plastics (FRPs) as a composite repair method to restore and enhance mechanical properties of timber marine civil structures within the context of His Majesty’s Naval Base (HMNB) Devonport. To support this, timber composite specimens were manufactured and subjected to flexural and compressive strength tests. Comparisons are made to literature sources for initial predictions, in addition to hand calculations and Finite Element Analysis (FEA) models on SolidWorks. Data demonstrates that FRPs can be used as a cost-effective and beneficial method of repairing timber marine structures. Experimental data demonstrates an ability to restore compressive strength parallel to …