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Full-Text Articles in Materials Science and Engineering

Determination Of The Constitutive Equations For 1080 Steel And Vascomax 300, Zachary A. Kennan Jun 2005

Determination Of The Constitutive Equations For 1080 Steel And Vascomax 300, Zachary A. Kennan

Theses and Dissertations

The objective of this research is to establish a better representation of the components utilized in a gouging event being considered in research leading to a better understanding of the Holloman High Speed Test Track. Gouging occurs when two metals are traveling at a slight incline to each other at velocities nearing 1.5 kilometers per second, and results in a structural failure of both the metals. The gouging process occurs at very high strain rates, which results in non-linear stress-strain relations. The coefficients that lead to the Johnson-Cook equations have been determined by the Split Hopkinson Bar test for 1080 …


Application Of Functionally Graded Materials In Aircraft Structures, William G. Cooley Mar 2005

Application Of Functionally Graded Materials In Aircraft Structures, William G. Cooley

Theses and Dissertations

A Functionally Graded Material (FGM) is a material which has a continuous variation of material properties through-the-thickness. This thesis will explore analysis of FGM flat plates and shell panels, and use FGM's unique characteristics to retrofit a cracked exhaust wash structure. FGMs are first characterized as flat plates under pressure and thermal loading. Next, FGM shell panels are characterized under thermal loading. Conclusions drawn from FGM characterization are used to develop a patch to retrofit a cracked aircraft exhaust wash structure. The exhaust wash structure is first analyzed to provide a baseline and then several FGM patches are evaluated on …


Creep Behavior Of An Oxide/Oxide Composite With Monazite Coating At Elevated Temperatures, Sean S. Musil Mar 2005

Creep Behavior Of An Oxide/Oxide Composite With Monazite Coating At Elevated Temperatures, Sean S. Musil

Theses and Dissertations

This study focuses on experimental investigation of stress-rupture behavior (creep response) of an oxide/oxide composite in a cross-ply (0/90) lay-up at elevated temperature. The test material, Nextel 610/monazite/alumina composite, employs monazite, an oxidation-resistant interfacial coating designed to improve performance at elevated temperatures. The experimental program included monotonic tensile tests to failure and creep-rupture tests at elevated temperatures. Tensile tests served to establish an ultimate tensile strength (UTS) for the material. The ensuing creep-rupture tests involved stress levels at varying percentages of the UTS. Stress-rupture curves at 900 and 1100 degrees C were established. A family of creep curves for various …


Dynamic Characterization Of Thin Deformable Pvdf Mirror, Eric M. Trad Mar 2005

Dynamic Characterization Of Thin Deformable Pvdf Mirror, Eric M. Trad

Theses and Dissertations

Methodology for the design and fabrication of 5 inch diameter membrane-like mirror structures is explored, resulting in test articles with areal densities as low as 1.57 kg/m2 and a thickness of 1.5 mm. Each optical structure has 7 control patches etched into the PVDF layer, which can be used as actuators. These test articles are utilized to demonstrate the capabilities of an acquisition system to make measurements of static and dynamic actuation of the mirror surface. Static deformations are analyzed statistically and determined to yield maximum deformations in the actuated regions of -2.1 micro with a standard deviation of 0.33 …


An Investigation Of A Simplified Gouging Model, Gregory S. Rickerd Mar 2005

An Investigation Of A Simplified Gouging Model, Gregory S. Rickerd

Theses and Dissertations

Gouging is a type of structural failure that becomes important when two metals slide against each other at velocities in the range of 1.5 kilometers per second. A computer model has previously been used to model the development of gouging at the Holloman High Speed Test Track. This model has not been experimentally verified to be correct, due to the complexity of the model. This research develops a simplified model that can be experimentally verified. The computer program utilized in this research was studied to determine the most appropriate options to use in simulations. This was accomplished by modeling a …


Effects Of Temperature And Shot-Peening Intensity On Fretting Fatigue Behavior Of Titanium Alloy Ti-6al-4a, Salman Albinali Mar 2005

Effects Of Temperature And Shot-Peening Intensity On Fretting Fatigue Behavior Of Titanium Alloy Ti-6al-4a, Salman Albinali

Theses and Dissertations

Effects of temperature and shot-peening intensity on fretting fatigue behavior of Ti-6Al-4A were investigated in this study. S-N curves were obtained for both room and elevated temperatures (260 C) for two different shot-peened intensities (4A and 10A). Stress relaxation behavior under both fretting fatigue at elevated temperature and temperature exposure only were also investigated after their measurements were calculated using X-ray diffraction method. The crack initiation location and the crack angle orientation along the surface were determined using optical and scanning electron microscopy (SEM). Cracks initiated near the trailing edge of the tested specimens. Cracks initiated on the contact surface …


Experimentation And Analysis Of Composite Scarf Joint, Benjamin M. Cook Mar 2005

Experimentation And Analysis Of Composite Scarf Joint, Benjamin M. Cook

Theses and Dissertations

Composite bonded scarf repairs were examined by experimentally measuring and analytically predicting the residual curing strains and strains due to mechanical loading. To accomplish this a three prong approach was used: a full strain field through a repaired laminate's thickness was measured for both a loaded specimen and a specimen with the residual strain released, models were developed for comparison to both states, and data was collected for large tensile test specimens at various stages of being scarf repaired. A ~14:1 straight scarfed one-inch wide specimen was used to collect Moire interferometry data to calculate a full strain field due …


Biaxial Fatigue Behavior Of Niti Shape Memory Alloy, Daniel M. Jensen Mar 2005

Biaxial Fatigue Behavior Of Niti Shape Memory Alloy, Daniel M. Jensen

Theses and Dissertations

Nitinol is a shape memory alloy (SMA) capable of martensite-to-austenite phase transformations enabling shape-memory behavior. Shape-memory properties make Nitinol a strong candidate material for use in aircraft applications such as actuators. Structural integrity and reliability of torque tube actuators must be assured before this material can be used in flight-critical components. Thorough understanding of the fatigue response of the material is essential for a structurally-sound SMA actuator design. The present effort investigates pure torsion and combined tension-torsion fatigue behavior of Nitinol at room temperature. Monotonic tests in tension and torsion were conducted to typify uni-directional stress-strain behavior. Fully-reversed torsion fatigue …


Effect Of Temperature And Steam Environment On Fatigue Behavior Of An Oxide-Oxide Continuous Fiber Ceramic Composite, Chalene A. Eber Mar 2005

Effect Of Temperature And Steam Environment On Fatigue Behavior Of An Oxide-Oxide Continuous Fiber Ceramic Composite, Chalene A. Eber

Theses and Dissertations

There is an ever-increasing need for materials that maintain high strength and fracture toughness at elevated temperatures and in complex environments. Advanced aerospace applications are motivating the development of composite materials that can meet demanding requirements. This research effort investigates mechanical behavior of an oxide-oxide continuous fiber ceramic composite (CFCC) consisting of a porous alumina matrix reinforced with mullite/alumina Nextel 720 fibers developed specifically for advanced aerospace applications. Tension-tension fatigue behavior of this CFCC was studied at 1200 and 1330 °C in laboratory air and 100% steam environments. Fatigue resistance and retained strength properties were determined. Effects of environmental degradation …


Thermal Characteristics Of Pitch Based Carbon Foam And Phase Change Materials, Kevin W. Wierschke Mar 2005

Thermal Characteristics Of Pitch Based Carbon Foam And Phase Change Materials, Kevin W. Wierschke

Theses and Dissertations

Phase-change thermal energy storage devices offer thermal control systems an option that allows a smaller heat sink to be used by absorbing the thermal energy quickly and storing it in the phase change to prevent failure of electronic components and then slowly releasing the heat to the heat sink. This paper experimentally determined the transient response of carbon foam with a phase-change material by measuring the response to a step temperature input to test samples. The transient response was recorded until steady state was reached. An analytic response was created and compared against the measured response. A simplified analytic prediction …


Tensile Stress Rupture Behavior Of A Woven Ceramic Matrix Composite In Humid Environments At Intermediate Temperature, Kevin J. Larochelle Mar 2005

Tensile Stress Rupture Behavior Of A Woven Ceramic Matrix Composite In Humid Environments At Intermediate Temperature, Kevin J. Larochelle

Theses and Dissertations

Stress rupture tests on the SylramicTM fiber with an in-situ layer of boron nitride, boron nitride interphase, and SiC matrix ceramic matrix composite were performed at 550°C and 750°C with 0.0, 0.2, or 0.6 atm partial pressure of water vapor, pH2O. The 550°C, 100-hr strengths were 75%, 65% and 51% of the monotonic room temperature tensile strength, respectively. At 750°C, the strengths were 67%, 51%, and 49%, respectively. Field Emission Scanning Electron Microscopy analysis estimated the total embrittlement times for 550°C with 0.0, 0.2, and 0.6 atm pH2O were >63 hrs, >38 hrs, and between …


Detection Of Residual Stress In Sic Mems Using Μ-Raman Spectroscopy, John C. Zingarelli Mar 2005

Detection Of Residual Stress In Sic Mems Using Μ-Raman Spectroscopy, John C. Zingarelli

Theses and Dissertations

Micro-Raman (µ-Raman) spectroscopy is used to measure residual stress in two silicon carbide (SiC) poly-types: single-crystal, hexagonally symmetric 6H-SiC, and polycrystalline, cubic 3C-SiC thin films deposited on Si substrates. Both are used in micro-electrical-mechanical systems (MEMS) devices. By employing an incorporated piezoelectric stage with submicron positioning capabilities along with the Raman spectral acquisition, spatial scans are performed to reveal areas in the 6H-SiC MEMS structures that contain residual stress. Shifts in the transverse optical (TO) Stokes peaks of up to 2 cm-1 are correlated to the material strain induced by the MEMS fabrication process through the development of phonon …


Effects Of Variable Contact Load On Fretting Fatigue Behavior Of Shot-Peened And Un-Peened Titanium Alloy, Chia-Hawa Lee Dec 2004

Effects Of Variable Contact Load On Fretting Fatigue Behavior Of Shot-Peened And Un-Peened Titanium Alloy, Chia-Hawa Lee

Theses and Dissertations

Fretting fatigue occurs between two components in contact under relative motion and reduces fatigue life when compared with plain fatigue. Shot-peening, on the other hand, is the most commonly used cold working process to improve material fatigue resistance in aeronautical industries. Nearly all work accomplished to date has assumed a constant contact load while investigating fretting fatigue. The primary goal of this study was to explore fretting fatigue behavior under constant and variable contact load configurations using both shot-peened and un-peened specimens made up of Ti-6Al-4V alloy. Contact loads were applied with four different frequencies. Applied axial loads were also …


Monotonic, Creep-Rupture, And Fatigue Behavior Of Carbon Fiber Reinforced Silicon Carbide (C/Sic) At An Elevated Temperature, John M. Engesser Mar 2004

Monotonic, Creep-Rupture, And Fatigue Behavior Of Carbon Fiber Reinforced Silicon Carbide (C/Sic) At An Elevated Temperature, John M. Engesser

Theses and Dissertations

The main objective of this research effort was to examine the impact that cyclic loading frequency has on the life of a C/SiC composite at an elevated temperature of 550°C. Cyclic loading of C/SiC was investigated at frequencies of 375 Hz, 10 Hz, 1 Hz, and 0.1 Hz. Creep-Rupture tests and tests that were combinations of creep-rupture and fatigue were also accomplished. A monotonic tensile test was performed at 550°C and compared to a room temperature monotonic test. This study showed that an elevated temperature of 550°C has very little effect on the Ultimate Tensile Strength (UTS) of C/SiC. The …


Optical Characterization And Modeling Of Compositionally Matched Indium Arsenide-Antimonide Bulk And Multiple Quantum Well Semiconductors, Scott C. Phillips Mar 2004

Optical Characterization And Modeling Of Compositionally Matched Indium Arsenide-Antimonide Bulk And Multiple Quantum Well Semiconductors, Scott C. Phillips

Theses and Dissertations

Indium arsenide-antimonide (InAsSb) semiconductors have been determined to emit in the 3-5 micrometer range, the window of interest for countermeasures against infrared electro-optical threats. This experiment set out to cross the bulk to quantum well characterization barrier by optically characterizing two sets of compositionally matched type I quantum well and bulk well material samples. Absorption measurements determined the band gap energy of the bulk samples and the first allowed subband transition for the quantum wells. By collecting absorption spectra at different temperatures, the trend of the energy transitions was described by fitting a Varshni equation to them. The expected result …


The Evaluation Of The Damping Characteristics Of A Hard Coating On Titanium, Christopher M. Blackwell Mar 2004

The Evaluation Of The Damping Characteristics Of A Hard Coating On Titanium, Christopher M. Blackwell

Theses and Dissertations

Engine failures due to fatigue have cost the Air Force an estimated $400 million dollars per year over the past two decades (Garrison, 2001). Damping treatments capable of reducing the internal stresses of fan and turbine blades to levels where fatigue is less likely to occur have the potential for reducing cost while enhancing reliability. This research evaluates the damping characteristics of magnesium aluminate spinel, MgO+Al2O3, (mag spinel) on titanium plates. The material and aspect ratio were chosen to approximate the low aspect ratio blades found in military gas turbine fans. The plates were tested with …


Experimental And Computational Analysis Of Modes In A Partially Constrained Plate, Robert M. Vandawaker Mar 2004

Experimental And Computational Analysis Of Modes In A Partially Constrained Plate, Robert M. Vandawaker

Theses and Dissertations

The field of structural health monitoring (SHM) attempts to reduce labor and cost by allowing technicians to monitor selected properties of an aircraft's structure to detect impending failure. This research examines methods to detect damage to a thermal protection system (TPS) tile using representative 2024-T3 aluminum plates. Plates are subjected to modal analysis in single and joined conditions in an attempt to provide the capability of sensing damage to a tile on the surface of a vehicle while the sensors remain on the superstructure of the airframe. Jointly, the development of a means to model the system using finite element …


Controlled-Stress Large-Area Pulsed Laser Deposition Of Yttria Stabilized Zirconia, Paul C. Rounsavall Sep 2003

Controlled-Stress Large-Area Pulsed Laser Deposition Of Yttria Stabilized Zirconia, Paul C. Rounsavall

Theses and Dissertations

The US Air Force has need of parabolic-shaped membrane mirrors for surveillance satellites. The current polymer membrane technology has been unable to overcome shape deformation problems caused by intrinsic stresses from the membrane casting and mounting processes. One proposed solution was to coat the membrane mirrors with a stressed coating to compensate for shape deformations. Thus, the research presented in this dissertation produced controlled-stress large-area pulsed laser deposition (PLD) grown thin films on polymer substrates and investigated optical time-of-flight (TOF) sensor systems and Raman spectroscopy for control for the PLD process with respect to thin film stress. Initially, the PLD-grown …


Electrical Activation Studies Of Silicon Implanted Alx Gal-X N And Coimplanted Gan, Elizabeth A. Chitwood Mar 2003

Electrical Activation Studies Of Silicon Implanted Alx Gal-X N And Coimplanted Gan, Elizabeth A. Chitwood

Theses and Dissertations

A comprehensive study of the electrical activation of silicon implanted AlxGa1-xN was performed as a function ion dose, anneal temperature, and aluminum mole fraction, Also, GaN coimplanted with silicon and nitrogen was investigated. Room temperature Hall effect measurements were used to determine carrier concentration and mobility. All the samples had a 500 Å encapsulant of AlN, and were implanted at room temperature with 200 keV silicon ions at doses ranging from 1x1013 to 1x1015 /cm2. The GaN was also implanted with nitrogen under the same conditions in doses of 9x1012 to …


Luminescence Studies Of Ion-Implanted Gallium Nitride And Aluminum Gallium Nitride, Erin N. Claunch Mar 2003

Luminescence Studies Of Ion-Implanted Gallium Nitride And Aluminum Gallium Nitride, Erin N. Claunch

Theses and Dissertations

Recently, research on the wide bandgap semiconductors such as GaN and Al(x)Ga(1-x)N became very popular for their applications on various devices. Therefore comprehensive and systematic luminescence studies of Si implanted AlxGa1-xN, Mg doped GaN, and Si+N implanted GaN grown on sapphire substrates by molecular beam epitaxial method have been made as a function of ion dose and anneal temperature.


Smart Structures For Control Of Optical Surfaces, D. Michael Sobers Jr. Mar 2002

Smart Structures For Control Of Optical Surfaces, D. Michael Sobers Jr.

Theses and Dissertations

The development of lightweight, large-aperture optics is of vital importance to the Department of Defense and the US Air Force for advancing remote sensing applications and improving current capabilities. Synthetic polymer optics offer weight and flexibility advantages over current generation glass mirrors, but require active control to maintain tight surface figure tolerances. This research explores the feasibility of using imbedded piezoelectric materials to control optical surfaces. Membrane-based and stiff piezo-controlled mirrors were constructed to develop and validate control techniques. Test results verified that surface control on the order of tens of wavelengths is possible using these systems.


Characterization Of The Optical And Electrical Properties Of Proton-Irradiated 4h-Silicon Carbide, Heather C. Crockett Mar 2002

Characterization Of The Optical And Electrical Properties Of Proton-Irradiated 4h-Silicon Carbide, Heather C. Crockett

Theses and Dissertations

Epitaxial n-type 4H-silicon carbide (SiC) is irradiated with 2 MeV protons to evaluate the dislocation damage effects on the optical and electrical characteristics of the material. Semiconductor materials with a high tolerance to radiation fields have applications in several aerospace power and satellite systems. SiC is under investigation due to its potential for such space material applications. The optical properties of the material are investigated using temperature-dependent photoluminescence (PL) and the effects of proton irradiation on the electrical properties are evaluated using current-voltage measurements and constant-voltage deep level transient spectroscopy (CV-DLTS). Subsequent high-temperature thermal annealing and recovery of the irradiated …


Measurements Of Neutron Induced Surface And Bulk Defects In 4h Silicon Carbide, Kent T. Jones Mar 2002

Measurements Of Neutron Induced Surface And Bulk Defects In 4h Silicon Carbide, Kent T. Jones

Theses and Dissertations

Epitaxial n-type 4H-silicon carbide (SiC) is irradiated with 2 MeV protons to evaluate the dislocation damage effects on the optical and electrical characteristics of the material. The optical properties of the material are investigated using temperature-dependant photoluminescence (PL) and the effects of proton irradiation on the electrical properties are evaluated using current-voltage measurements and constant-voltage deep level transient spectroscopy (CV-DLTS). Subsequent high-temperature thermal annealing and recovery of the irradiated material is investigated over the temperature range of 900-1500°C. Proton-induced irradiation damage is apparent in the 4H-SiC material, affecting both the optical and electrical characteristics of the devices. The radiative behavior …


Fretting Fatigue Behavior Of A Titanium Alloy Ti-6al-4v At Elevated Temperature, Onder Sahan Mar 2002

Fretting Fatigue Behavior Of A Titanium Alloy Ti-6al-4v At Elevated Temperature, Onder Sahan

Theses and Dissertations

The purpose of this research is to investigate the fretting fatigue behavior of the titanium alloy Ti-6Al-4V at elevated temperature is investigated. Fretting and plain fatigue experiments are conducted at 260 °C. Crack initiation location and crack initiation orientation is measured and fretting and plain fatigue life data of the specimens from these tests are obtained. Fatigue parameters capable of predicting the number of cycles to specimen failure, the crack location and the crack orientation along the contact surface are analyzed. The parameters are calculated by using the computed stresses and strains obtained from the finite element analysis. The mechanisms …


Electrical Activation Studies Of Ion Implanted Gallium Nitride, James A. Fellows Nov 2001

Electrical Activation Studies Of Ion Implanted Gallium Nitride, James A. Fellows

Theses and Dissertations

A comprehensive and systematic electrical activation study of Si-implanted GaN was performed as a function of ion implantation dose, anneal temperature, and implantation temperature. Additionally, Mg-implanted GaN was also investigated. Temperature-dependent Hall effect measurements and photoluminescence (PL) spectra were used to characterize the samples. GaN wafers capped with AlN were implanted with Si ions at doses ranging from 1x1013 to 5x1015 cm-2 and annealed from 1050 to 1350 °C. The optimum anneal temperature for samples implanted with the higher Si doses is around 1350 °C, exhibiting nearly 100% electrical activation efficiency. Exceptional mobilities and carrier concentrations were …


Single-Sided Noninvasive Inspection Of Multielement Sample Using Fan-Beam Multiplexed Compton Scatter Tomography, Matthew A. Lange Jun 2001

Single-Sided Noninvasive Inspection Of Multielement Sample Using Fan-Beam Multiplexed Compton Scatter Tomography, Matthew A. Lange

Theses and Dissertations

As aircraft age, corrosion forms upon unobservable surfaces, particularly at the junction of the sheet aluminum and the steel rivets used to attach the sheets to the airframe, degrading the aircraft s airworthiness. Previous research developed a noninvasive technique for the evaluation of the material composition of aluminum surfaces, utilizing the information encoded in the energy spectra of Compton-scattered gamma emissions. The spectra are gathered by a six-element, high purity germanium detector array. A, first principles, deterministic computer code is used to reconstruct a two-dimensional map of the electron density of aluminum samples. Previous efforts, to image pure aluminum samples, …


Time-Resolved Photoluminescence Of Inas/Gainsb Quantum Well Lasers, Michael R. Mckay Jun 2001

Time-Resolved Photoluminescence Of Inas/Gainsb Quantum Well Lasers, Michael R. Mckay

Theses and Dissertations

In the world of semiconductor photonic device fabrication, one important objective may be to extract as much light as possible from the device. In these devices, photons are created when electrons recombine with holes by transitioning from a high-energy state to a lower one. Unfortunately, electron-hole recombination does not always result in the formation of a photon. There are three basic types of recombination: the first results in the formation of a photon and is called radiative recombination; and the second and third, known as Shockley-Read-Hall and Auger recombination, result in the heating of the device and do not produce …


Fatigue Response Of Thin Stiffened Aluminum Cracked Panels Repaired With Bonded Composite Patches, Jason B. Avram Mar 2001

Fatigue Response Of Thin Stiffened Aluminum Cracked Panels Repaired With Bonded Composite Patches, Jason B. Avram

Theses and Dissertations

This research investigated the fatigue response of precracked and patched 2024-T3 Aluminum panels with stiffeners. Patches were single-sided, unidirectional three ply boron/epoxy. Stiffeners were 2024-T3 aluminum and were riveted and bonded on. Disbonds were introduced into the repair bondline by inserting teflon strips. Three disbond configurations were investigated rack tip disbond (CTD) located at the edge of the patch in the path of crack propagation, full-width disbond (FWD) covering the entire crack, and end disbond (ED) located at each end of the patch and covering the full width. Each repaired panel was subjected to tension/tension cyclic fatigue with a maximum …


Photoluminescence Of Single Quantum Well Structures In Gallium Arsenide, Christian A. Bartholomew Mar 2001

Photoluminescence Of Single Quantum Well Structures In Gallium Arsenide, Christian A. Bartholomew

Theses and Dissertations

The continued development of state-of the-art semiconductor technologies and devices by the United States Air Force and the Department of Defense requires accurate and efficient techniques to evaluate and model these new materials. Of particular interest to the Air Force are quantum well structures which can be used for small-scale laser sources in fly-by-light applications, as efficient infrared countermeasures to heat-seeking missiles, or as advanced seekers in optically guided missiles. This thesis provides the initial experimental procedures and data necessary to begin producing accurate yet robust models. Although carrier effective masses could not be evaluated using hot-electron photoluminescence, photoluminescence excitation …


Optical And Etching Studies Of Native Aluminum Oxide Layers For Use In Microcavity Photonic Devices, William L. Bernhard Mar 2001

Optical And Etching Studies Of Native Aluminum Oxide Layers For Use In Microcavity Photonic Devices, William L. Bernhard

Theses and Dissertations

Optical communication and computing systems are required to meet future information transfer and processing needs. Microcavity devices serve as an enabling technology to implement and integrate optoelectronic systems. It is important to understand the optical and mechanical properties of materials utilize within microcavity devices. Only then is it possible to accurately model and analyze structures. Microcavity structures incorporating a high aluminum content AlGaAs layers are designed, grown, processed, and measured. The processing of these devices includes the conversion of high aluminum-content AlGaAs layers to native aluminum oxide (AlO) layers through the process of thermal oxidation. This selective conversion of microcavity …