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Articles 301 - 330 of 436

Full-Text Articles in Materials Science and Engineering

High Temperature Degradation Of 5250-4 Polymer Resin, Patrick E. Link Jun 2007

High Temperature Degradation Of 5250-4 Polymer Resin, Patrick E. Link

Theses and Dissertations

5250-4 bismaleimide resin is used in high performance polymer matrix composites with high temperature aeronautical applications. This thesis investigated the thermal and oxidative degradation of 5250-4 neat resin powder in argon, air, and oxygen environments. The powder was aged at 163 deg. C, 177 deg. C, and 190 deg. C in all environments for at least 250 hours. Isothermal thermo-gravimetric analysis demonstrated that weight loss was negligible for aging in the argon environment, indicating weight loss is the result of an oxidative process at these temperatures. The 5250-4 powder exhibited an initial period of weight gain before eventually losing weight …

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Optical Parametric Oscillation In Orientation-Patterned Gallium Arsenide, Scott A. Shell Mar 2007

Optical Parametric Oscillation In Orientation-Patterned Gallium Arsenide, Scott A. Shell

Theses and Dissertations

Tunable laser sources in the mid-infrared (MIR) spectral range are required for several Air Force applications. Existing lasers with output in the near-infrared can be converted to more desirable MIR by using nonlinear effects. Orientation patterned gallium arsenide (OPGaAs) is a promising nonlinear conversion material because it has broad transparency and can be engineered for specific pump laser and output wavelengths using quasi-phase matching techniques. This research examines optical parametric oscillation (OPO) of several OPGaAs samples using a 2.052 micrometers wavelength Tm, Ho:YLF pump laser. Of the seven samples available the five that were capable of getting OPO output with …

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Cobalt Doping Of Semiconducting Boron Carbide Using Cobaltocene, Lonnie Carlson Mar 2007

Cobalt Doping Of Semiconducting Boron Carbide Using Cobaltocene, Lonnie Carlson

Theses and Dissertations

The decomposition of cobaltocene and metacarborane (closo-1,7-dicarba-decaborane) under low energy electron irradiation at about 200 K results in a material with the Fermi level closer to the valence band than the material resulting from the decomposition of metacarborane alone. This indicates that cobaltocene provides a relatively p-type dopant as seen in ultraviolet photoemission spectroscopy/inverse photoemission spectroscopy. Upon warming to room temperature, however, the Fermi level shifts towards the conduction band, suggesting an n-type dopant. This temperature dependent surface photovoltage effect is not compelling evidence for the majority carrier type but does suggest an increase in the carrier concentration …

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Characterization Of Intercalated Graphite Fibers For Microelectromechanical Systems (Mems) Applications, Bryan W. Winningham Mar 2007

Characterization Of Intercalated Graphite Fibers For Microelectromechanical Systems (Mems) Applications, Bryan W. Winningham

Theses and Dissertations

Research was accomplished to characterize the electrical and physical characteristic changes of the Thornel® P-100 carbon fiber and five variants when intercalated with 96% sulfuric acid and incorporated the use of Microelectromechanical Systems (MEMS) structures for testing purposes. The five fiber variants were oxidized in 1 M nitric acid at 0.5 A for 30 seconds, 1 and 2 minutes, the last two samples were detreated at 1150 °C for one hour prior to the nitric acid treatment. The fibers were mounted onto a MEMS die, placed into a chip carrier, sulfuric acid added, the chip carrier sealed and testing accomplished. …

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An Exploration Of Several Structural Measurement Techniques For Usage With Functionally Graded Materials, Robert A. Reuter Dec 2006

An Exploration Of Several Structural Measurement Techniques For Usage With Functionally Graded Materials, Robert A. Reuter

Theses and Dissertations

Titanium / titanium boride functionally graded 6"x 1"x1" beams were subjected to a four-point beam test in order to critique the value of several measurement techniques. Also, finite element analysis results were compared with experimental values and general observations about the experiment were recorded. Uniform 85% TiB /15% Ti and uniform commercially pure titanium specimens were also subjected to the same loading conditions as a control. Techniques used include digital image correlation, fiber optic strain gauging, strain gauging, and differential infrared thermography techniques. The strain data results were compared with one another and to linear finite element models. It was …

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Modeling Fracture In Z-Pinned Composite Co-Cured Laminates Using Smeared Properties And Cohesive Elements In Dyna3d, Jason K. Freels Sep 2006

Modeling Fracture In Z-Pinned Composite Co-Cured Laminates Using Smeared Properties And Cohesive Elements In Dyna3d, Jason K. Freels

Theses and Dissertations

The purpose of the present research was three-fold: 1) gain a more sophisticated understanding of the response of co-cured composite joints with and without through-thickness reinforcement (TTR), 2) compare the behavior of specimens reinforced with various sizes and densities of reinforcement, and 3) use experimental data to verify the existing DYNA3D smeared property model. Double cantilever beam, end-notch flexure and T-section specimens reinforced with 0.011" diameter z-pins at 2% and 4% volume densities were tested to determine the mode I, mode II and mixed mode (I and II) behavior. Results were added to preliminary research in which tests were conducted …

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Effects Of Environment On Creep Behavior Of Two Oxide-Oxide Ceramic Matrix Composites At 1200°C, Pavlos Koutsoukos Sep 2006

Effects Of Environment On Creep Behavior Of Two Oxide-Oxide Ceramic Matrix Composites At 1200°C, Pavlos Koutsoukos

Theses and Dissertations

Previous studies by the advisor and graduate students examined creep behavior of the Nextel720/Alumina CMC in air and in 100% steam environments at 1200 and 1330°C. Results showed that while this oxide/oxide system exhibits an exceptionally high fatigue limit at 1200°C it also experiences substantial strain accumulation under sustained loading conditions. Furthermore, these earlier investigations revealed a significant degrading effect of 100% steam environment on material performance under both static and cyclic loadings. The present effort will investigate creep rupture behavior of Nextel720/Alumina composite in the inert gas environment. In addition, creep rupture behavior of Nextel720/Aluminosilicate CMC will be investigated …

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Effects Of Polishing Shot-Peened Surfaces On Fretting Fatigue Behavior Of Ti-6al-4v, Kasey S. Scheel Sep 2006

Effects Of Polishing Shot-Peened Surfaces On Fretting Fatigue Behavior Of Ti-6al-4v, Kasey S. Scheel

Theses and Dissertations

The research of this thesis was done to investigate the effects of polishing a shot-peened specimen of Ti-6Al-4V on the fretting fatigue life of that specimen. The shot-peening process, though one of the most beneficial techniques in prolonging fretting fatigue life, creates a textured surface that may lead to problems on the micro level. This research was done in an attempt to further improve the peening process by examining the effects of another surface treatment to be used in conjunction, surface polishing. The rough peened surface may contain abrupt changes in surface geometry that act as stress risers, which are …

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Characterization Of Passivated Indium Antimonide, Catherine Ann Taylor Jun 2006

Characterization Of Passivated Indium Antimonide, Catherine Ann Taylor

Theses and Dissertations

Infrared absorption and photoluminescence measurements have been used to optically characterize bulk-grown, 680-μm thick, indium antimonide (InSb), both as-grown and after passivation by either anodization or a 700-Å layer of silicon oxide (SiOx). Spectra were obtained using Fourier transform infrared (FT-IR) spectroscopy. Results include the effects of sample temperature in the range of 10 to 300 K and 4.636 μm laser pump power in the range of 28 mW to 1.43 W for the photoluminescence spectrum.

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Effects Of Frequency And Environment On Fatigue Behavior Of An Oxide-Oxide Ceramic Matrix Composite At 1200°C, Griffin Hetrick Jun 2006

Effects Of Frequency And Environment On Fatigue Behavior Of An Oxide-Oxide Ceramic Matrix Composite At 1200°C, Griffin Hetrick

Theses and Dissertations

Advances in aeronautical engineering in the 21st century depend upon materials that can perform well in extreme environments such as high temperatures and oxidizing conditions. Nextel™720/Alumina (N720/A) is an oxide/oxide ceramic matrix composite with a porous alumina matrix that has been identified as a candidate material for such applications. This research investigated the effects of frequency on fatigue response of N720/A at 1200°C in both air and steam environment. Prior investigation of this material by Eber [8] in 2005 studied fatigue behavior at 1200°C in air and in steam environments at the frequency of 1.0 Hz. The current research focused …

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Wear Analysis Of Cu-Al Coating On Ti-6al-4v Under Fretting, Karl N. Murray Jun 2006

Wear Analysis Of Cu-Al Coating On Ti-6al-4v Under Fretting, Karl N. Murray

Theses and Dissertations

The effects of changes in the coefficient of friction (CoF) between the contacting surfaces on the fretting wear characteristics of Cu-Al coating on Ti-6Al-4V were investigated. This Cu-Al coating is part of a system that is applied to titanium turbine blades to reduce fretting at the interface. In the application, there is a solid lubricant that is added on top of the coating as an assembly aid and to help reduce the friction while the lubricant remains within the contact. Previous studies have researched the characteristics of the coating without the additional lubricant. In this study, liquid motor oil was …

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Effect Of Environment On Creep Behavior Of An Oxide/Oxide Cfcc With ±45° Fiber Orientation, Gregory T. Siegert Jun 2006

Effect Of Environment On Creep Behavior Of An Oxide/Oxide Cfcc With ±45° Fiber Orientation, Gregory T. Siegert

Theses and Dissertations

Aerospace applications require materials capable of maintaining superior mechanical properties while operating at high temperatures and oxidizing environments. Nextel™ 720/A (N720/A), an oxide/oxide ceramic matrix composite (CMC) with a porous alumina matrix was developed specifically to provide improved long-term properties and performance at 1200°C. This research evaluated the creep behavior of N720/A with a ±45° fiber orientation at 1200°C in: laboratory air, steam, and argon environments. Creep-rupture tests at the creep stress levels of: 45, 40, 35, and 15 MPa were conducted in each environment.
The ultimate tensile strength of N720/A with ±45° fiber orientation was 55 MPa, the elastic …

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Optical Characterization Of Thick Growth Orientation-Patterned Gallium Arsenide, Joshua W. Meyer Mar 2006

Optical Characterization Of Thick Growth Orientation-Patterned Gallium Arsenide, Joshua W. Meyer

Theses and Dissertations

Tunable laser sources in the mid-infrared (MIR) spectral range are required for several Air Force applications. Existing lasers with output in the near-infrared can be converted to more desirable MIR by using nonlinear effects. Orientation patterned gallium arsenide (OPGaAs) is a promising nonlinear conversion material because it has broad transparency and can be engineered for specific pump laser and output wavelengths using quasi-phase matching techniques. This research examines the optical quality of seven OPGaAs crystal samples and explores the design of an optical parametric oscillator (OPO) device. The Air Force Research Laboratory Electro-Optical Countermeasures Technology Branch obtained the samples from …

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Characterization Of Stress In Gan-On-Sapphire Microelectromechanical Systems (Mems) Structures Using Micro-Raman Spectroscopy, Francisco E. Parada Mar 2006

Characterization Of Stress In Gan-On-Sapphire Microelectromechanical Systems (Mems) Structures Using Micro-Raman Spectroscopy, Francisco E. Parada

Theses and Dissertations

Micro-Raman (µRaman) spectroscopy is an efficient, non-destructive technique widely used to determine the quality of semiconductor materials and microelectromechanical systems. This work characterizes the stress distribution in wurtzite gallium nitride grown on c-plane sapphire substrates by molecular beam epitaxy. This wide bandgap semiconductor material is being considered by the Air Force Research Laboratory for the fabrication of shock-hardened MEMS accelerometers. µRaman spectroscopy is particularly useful for stress characterization because of its ability to measure the spectral shifts in Raman peaks in a material, and correlate those shifts to stress and strain. The spectral peak shift as a function of stress, …

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Passive Multiple Beam Combination In Optical Fibers Via Stimulated Brillouin Scattering, Kirk C. Brown Mar 2006

Passive Multiple Beam Combination In Optical Fibers Via Stimulated Brillouin Scattering, Kirk C. Brown

Theses and Dissertations

Many active methods of scaling laser brightness have been demonstrated in recent years. The goal of this research was to demonstrate the feasibility of passively combining multiple laser beams using Stimulated Brillouin Scattering (SBS) in a long multimode optical fiber. This method of combination employed a “Gatling gun” fiber array that allowed several collimated beams to be focused by a lens into an optical fiber. The retroreflected Stokes beam is passed through the center of the beam combiner for analysis. In addition to experimental methodology and equipment used, the theoretical and historical background of SBS in optical fibers is provided. …

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Analysis Of Photoconductive Properties In Ge2Sb2Te5 (Gst) Chalcogenide Films For Applications In Novel Electronics, John R. V. Chezem Mar 2006

Analysis Of Photoconductive Properties In Ge2Sb2Te5 (Gst) Chalcogenide Films For Applications In Novel Electronics, John R. V. Chezem

Theses and Dissertations

This thesis investigated the thermal phase-change properties in Ge2Sb2Te5 (GST) chalcogenide-based films and determined the feasibility of coupling the GST with photosensitive DNA material for novel optical device applications. Modeling and testing of GST were researched with the approach that GST would react as a resistive mechanism through thermal manipulation. A test structure was fabricated with a 2-micronmeter MEMS fabrication process. GST material was deposited (by RF sputtering) on the surface of the test structures. The GST was analyzed primarily in the amorphous to crystalline transition states due to more distinct changes in the resistance …

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Some Aspects Of The Mechanical Response Of Bmi 5250-4 Neat Resin At 191°C: Experiment And Modeling, John G. Balaconis Mar 2006

Some Aspects Of The Mechanical Response Of Bmi 5250-4 Neat Resin At 191°C: Experiment And Modeling, John G. Balaconis

Theses and Dissertations

The mechanical response of BMI 5250-4 neat resin at 191 degrees C was studied using both creep and recovery tests where several variables were allowed to change. In these tests, the effect of stress rate, prior history, and panel variability were all taken into account. During the creep test, the material showed both primary and secondary creep over 20 h. The recovery tests showed full recovery after it was subjected to 80% UTS. The higher stress rate caused a much greater response in both creep and recovery tests. The prior history was studied by allowing the specimens to go through …

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Characterization Of Functionally Graded Materials, Benjamin D. Chapman Mar 2006

Characterization Of Functionally Graded Materials, Benjamin D. Chapman

Theses and Dissertations

The purpose of this study was to characterize the behavior of a functionally graded material through experimentation and analytical modeling. Functionally graded materials are a ceramic metal composite which transitions from metal on one face to ceramic on the opposite face. Creating reliable models required verifying the material properties. This was accomplished through the use of a static modulus of elasticity test as well as a dynamic ping test. The natural frequencies from the dynamic test were compared with finite element models to determine which material properties most accurately represented the functionally graded material. It was found that the material …

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Characteristics Of Two-Dimensional Triangular And Three-Dimensional Face-Centered-Cubic Photonic Crystals, Jeffery D. Clark Mar 2006

Characteristics Of Two-Dimensional Triangular And Three-Dimensional Face-Centered-Cubic Photonic Crystals, Jeffery D. Clark

Theses and Dissertations

The fabrication of photonic crystals (PhC) with photonic band gaps (PBG) in the visible range is a difficult task due to the small structural feature sizes of the PhC. The particular type of PhC examined is a two-dimensional (2-D) triangular structure with a PBG designed for visible wavelengths with applications in visible integrated photonic systems. This work examines the processes involved and viability of fabricating 2-D triangular PhC's by a variety of techniques: focused ion beam, electron lithography and holographic photo-polymerization/lithography. The design of the PhC was based on a program created to display gap maps for triangular structures. The …

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Graphitized Carbon Foam With Phase Change Material, Angelinda D. Fedden Mar 2006

Graphitized Carbon Foam With Phase Change Material, Angelinda D. Fedden

Theses and Dissertations

This thesis examines the transient heating and cooling responses of graphitized carbon foam infiltrated with phase change material (PCM). The carbon foam provides rapid heat transfer throughout the PCM volume, while the PCM stores the heat for later removal. The foam/PCM system was heated with a copper heating block, and then cooled with a liquid-cooled heat removal block. Infiltrating the foam with PCM significantly increased the length of time before the system reached maximum temperature. The temperature response of the foam/PCM system was consistent over multiple cycles of heating and cooling. A high density foam had a faster heating and …

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Fretting Fatigue Behavior Of Shot-Peened In 100, Jonathan L. Ng Mar 2006

Fretting Fatigue Behavior Of Shot-Peened In 100, Jonathan L. Ng

Theses and Dissertations

The fretting fatigue behavior of shot-peened of IN 100 was investigated in this study. S-N curves were obtained for two different shot-peened intensities (7A and 12A) and were compared to those of unpeened specimens. Stress relaxation behavior under fretting fatigue was also investigated after their measurements were obtained using the X-ray diffraction method. The crack initiation location and the crack angle orientation along the surface were determined using optical and scanning electron microscopy (SEM). Cracks initiated near the trailing edge and on the contact surface for both 7A and 12A shot-peened specimens. Finite element analysis was performed using commercially available …

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Creep-Rupture Behavior Of A Woven Ceramic Matrix Composite At Elevated Temperatures In A Humid Environment, Jennifer L. Ryba Mar 2006

Creep-Rupture Behavior Of A Woven Ceramic Matrix Composite At Elevated Temperatures In A Humid Environment, Jennifer L. Ryba

Theses and Dissertations

This study focused on moisture and temperature effects on the embrittlement and stress-rupture life of the SiC/SiC CMC Syl-iBN/BN/SiC. The Syl-iBN/BN/SiC is composed of Sylramic fibers with an in-situ layer of boron nitride (Syl-iBN), boron nitride interphase (BN), and SiC matrix. Stress rupture tests and monotonic tests were performed on the specimens. Tests were conducted under 100% humidity and laboratory air environments at three temperatures, 450°C, 750°C, and 950°C. These temperatures were chosen because they fall below the intermediate range, within the range, and above the range, respectively. This study found that while this CMC does experience embrittlement at intermediate …

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Characterization Of Compressive Creep Behavior Of Oxide/Oxide Composite With Monazite Coating At Elevated Temperature, Patrick R. Jackson Mar 2006

Characterization Of Compressive Creep Behavior Of Oxide/Oxide Composite With Monazite Coating At Elevated Temperature, Patrick R. Jackson

Theses and Dissertations

The compressive creep behavior of a N610/monazite/alumina composite was investigated in this work. The composite consists of a porous alumina matrix reinforced with NextelTM610 fibers coated with monazite in a symmetric cross-ply (0°/90°/0°/90°)s orientation. Compressive stress-strain behavior was investigated as well. The addition of monazite coating resulted in ~ 35% loss in compressive strength at 900°C and in ~45% loss in compressive strength at 1100°C. Compressive creep behavior was examined at 900 and 1100°C for creep stresses ranging from 50 to 95 MPa. Primary and secondary creep regimes were observed at both temperatures. Minimum creep rate was reached in all …

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Effect Of Hold Times On Fatigue Behavior Of Nextel 720™/Alumina Ceramic Matrix Composite At 1200°C In Air And In Steam Environment, John M. Mehrman Mar 2006

Effect Of Hold Times On Fatigue Behavior Of Nextel 720™/Alumina Ceramic Matrix Composite At 1200°C In Air And In Steam Environment, John M. Mehrman

Theses and Dissertations

The aerospace field requires structural materials that can maintain superior mechanical properties while subjected to high temperatures and oxidizing environments. This research investigated the effect of hold times at maximum load on fatigue performance of a Nextel 720/Alumina ceramic matrix composite at 1200 C, explored the influence of environment on material response to cyclic loading with hold times at maximum load, and assessed the effects of loading history on material behavior and environmental durability. The N720/A composite relies on an oxide/oxide composition for inherent oxidation resistance and a porous matrix with no interphase between the fiber and matrix for damage …

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Validation Of A Scaled Plane Strain Hypervelocity Gouging Model, Ronald J. Pendleton Mar 2006

Validation Of A Scaled Plane Strain Hypervelocity Gouging Model, Ronald J. Pendleton

Theses and Dissertations

The phenomenon of high speed impact is of great interest to the Air Force of Scientific Research and the Air Force Research Laboratory's Holloman High Speed test track. Rocket sled tests at the facility frequently are limited to velocities lower than actually attainable due to damage to the rail in the form of gouges. Direct observation of the gouging phenomenon is not currently possible. This leaves computational modeling as the only means to study the phenomenon. A computer model has previously been used to model the development of gouging at the Holloman High Speed Test Track. However, this model has …

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Creep-Rupture And Fatigue Behaviors Of Notched Oxide/Oxide Ceramic Matrix Composite At Elevated Temperature, Mark A. Sullivan Mar 2006

Creep-Rupture And Fatigue Behaviors Of Notched Oxide/Oxide Ceramic Matrix Composite At Elevated Temperature, Mark A. Sullivan

Theses and Dissertations

Oxide/oxide composites are being considered for use in high temperature aerospace applications where their inherent resistance to oxidation provides for better long life properties at high temperature than most other ceramic matrix composites (CMCs). One promising oxide/oxide CMC is Nextel 720/A (N720/A) which uses an 8-harness satin weave (8HSW) of Nextel 720 fibers embedded in a porous alumina matrix. Possible aerospace applications for N720/A will likely require inserting holes into the material for mounting and cooling purposes. The notch characteristics must be understood to ensure designs using the material are sufficient for the desired application. This research effort examined the …

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Carrier Lifetime Dynamics Of Epitaxial Layer Hvpe Gallium Arsenide Using Time-Resolved Experiments, Wayne E. Eikenberry Mar 2006

Carrier Lifetime Dynamics Of Epitaxial Layer Hvpe Gallium Arsenide Using Time-Resolved Experiments, Wayne E. Eikenberry

Theses and Dissertations

GaAs is a potential semiconductor material for producing both mid-infrared and terahertz radiation using the new technique of quasi-phase matching in an orientationally patterned GaAs (OP-GaAs) crystal. OP-GaAs is grown using a fast growth process called hydride vapor phase epitaxy (HVPE). Unfortunately, HVPE produces a high number of defects. These defects cause Shockley-Read-Hall recombination rates to dominate over Auger and radiative recombination rates. The carrier lifetime from four OP-GaAs samples are reported here using two different experimental techniques. The first experiment used a streak camera to measure the carrier lifetime via time-resolved photoluminescence. The temporal resolution of the streak camera …

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Multiple Channel Laser Beam Combination And Phasing Using Stimulated Brillouin Scattering In Optical Fibers, Brent W. Grime Dec 2005

Multiple Channel Laser Beam Combination And Phasing Using Stimulated Brillouin Scattering In Optical Fibers, Brent W. Grime

Theses and Dissertations

Brightness scaling lasers using stimulated Brillouin scattering (SBS) in optical fibers is explored. A multiple-channel amplifier approach is used to increase the total power of a laser system while avoiding a significant burden on a single channel. The work explores two approaches utilizing both SBS beam cleanup and SBS piston error conjugation. A unique beam combiner that takes advantage of the SBS beam cleanup properties of a long, gradient-index multimode fiber was designed and tested. The beam combiner was developed to combine multiple-channel laser beams simultaneously with high input and output coupling efficiency. The design for the SBS beam combiner …

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Rate Dependence And Short Term Creep Behavior Of Pmr-15 Neat Resin At 23 And 288°C, Candice M. Westberry Sep 2005

Rate Dependence And Short Term Creep Behavior Of Pmr-15 Neat Resin At 23 And 288°C, Candice M. Westberry

Theses and Dissertations

This research focuses on experimental investigation of rate-dependent behavior and short-term creep of PMR-15 neat resin at 23 and 288°C. Effect of loading rate on monotonic stress-strain behavior was explored in monotonic tests at constant stress rates of 0.75, 0.075, and 0.0075 MPa/s at 23 and 288°C. In addition, effect of prior stress rate on creep behavior was explored in creep tests preceded by uninterrupted loading to a target stress. At each temperature three creep tests were conducted for a given stress level, where loading rate was changed from test to test. Creep stress levels were 30 and 25 MPa …

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High Temperature Chemical Degradation Of Pmr-15 Polymer Resins, Grant W. Robinson Jun 2005

High Temperature Chemical Degradation Of Pmr-15 Polymer Resins, Grant W. Robinson

Theses and Dissertations

PMR-15 is a polymer resin for glass and carbon reinforced composites used for high temperature, civilian and military aerospace applications. The harsh environments of PMR-15 applications lead to long term structural degradation and, in turn, impact the readiness capabilities of the system. This study investigated the thermal and oxidative degradation of PMR-15 neat resin powder through the use of thermal gravimetric analysis (TGA) in oxygen, argon and air at isothermal hold temperatures of 260, 288, 316, and 343 °C for 250 hours. The TGA measured the degradation by recording the change in neat resin powder mass versus time. The qualitative …

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