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Masters Theses

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Full-Text Articles in Materials Science and Engineering

Reduction Of Zinc Sulphide In A Vacuum, Tien-Shih Liu Jan 1949

Reduction Of Zinc Sulphide In A Vacuum, Tien-Shih Liu

Masters Theses

"The successful large scale commercial application of high vacuum for high temperature metallurgical operations is a comparatively new development. The use of Pidgeon and the carbothermic processes for the production of magnesium during the war forced a perfection of both equipments and techniques for high vacuum operations. This opens broadly the way for a great expansion of vacuum metallurgy. Vacuum operation is thus no more a laboratory method - it is a kind of industrial practice. Many metallurgical operations, which cannot be carried out by ordinary processes, are made feasible when conducted in a reduced pressure. typical examples are the …


The Effects Of Moisture In Grog Upon Dry Pressed Mixes Containing Grog, Charles L. Mckinnis Jan 1948

The Effects Of Moisture In Grog Upon Dry Pressed Mixes Containing Grog, Charles L. Mckinnis

Masters Theses

"It has been found that the aging of clay-grog-water mixes before pressing proves to be quite beneficial. The purpose of the aging period is to allow the added water to disseminate throughout the mixture of clay (plastic) and grog (non-plastic) in an effort to bring about the best bonding action possible. The clay-grog-water mixture, if not aged, is of a sticky consistency; while, if the same mixture is aged for twenty-four (24) hours, it is readily workable. This process of aging has long been recognized as a "must" in the Ceramic Industry in obtaining mixtures of ideal workability"--Introduction, page 2.


A Study Of The Separation Of Wolframite From Tin-Oxide, Chih-Wen Ying Jan 1948

A Study Of The Separation Of Wolframite From Tin-Oxide, Chih-Wen Ying

Masters Theses

"A number of mines in china, Bolivia, England, and other countries contain both tin-oxide and wolframite. Owing to the fact that the specific gravity of tin-oxide and wolframite is so nearly the same, considerable difficulty is experienced in making a gravity separation, and all attempts to do so by wet or dry concentration have given very poor results. The perfection of magnetic separators has done much to mitigate this difficulty, so that now complex ores of this nature can be treated in a satisfactory manner. The mixed concentrate from the tables or other concentrators, after being roasted to expel sulfur …


A Test Method For Measuring The Flow In Refractory Materials At High Temperatures, Christen Knudsen Jan 1948

A Test Method For Measuring The Flow In Refractory Materials At High Temperatures, Christen Knudsen

Masters Theses

"One of the most important properties of refractory materials is the ability to resist stress which may either be directly applied or originate in the material. The factors which govern the resistance to stress include the modulus of elasticity, the ultimate strength under different types of stress, and the "flow" characteristics which become of importance when the material is stressed at the temperature at which plasticity is developed. Systematic determinations of the mechanical properties such as modulus of elasticity and ultimate or breaking stress is rather difficult or more or less impossible to carry out at the temperature at which …


A Preliminary Investigation Of The Titanium-Tin Equilibrium System, James Eugene Reynolds Jan 1948

A Preliminary Investigation Of The Titanium-Tin Equilibrium System, James Eugene Reynolds

Masters Theses

"Titanium is estimated to comprise about .63% of the lithosphere and atmosphere. This would render it the ninth in abundance of all the elements, and fourth in abundance of the metals suitable for mechanical and structural uses, being exceeded only by iron, aluminum, and magnesium. It is approximately 400 times more abundant than lead, which is generally considered to be quite plentiful. The chief restriction of the commercial availability of titanium in its pure form has been the difficulty of reducing it from its ores. Several methods have been proposed in the past and recent years, and R. S. Dean …


A Study Of The Retort Zinc Distillation Process, Albert Hoffman Jan 1948

A Study Of The Retort Zinc Distillation Process, Albert Hoffman

Masters Theses

"The problem of this thesis is to determine the optimum density of packing of the charge to a zinc retort under exact industrial conditions of temperatures and materials as it affects the production of zinc metal. It is well known that the quantity of zinc produced per cycle is benefited by increasing the density of charging, but increased density of packing or charging is limited by the diffusion, through the charge of the gases necessary to carry on the reduction reactions. In commercial practice there is also a secondary limitation dependent primarily upon the rate at which the heat can …


An Investigation Of The Reduction Of Rutile Copper Oxide Mixtures With Magnesium, Tryggve Smedsland Jan 1948

An Investigation Of The Reduction Of Rutile Copper Oxide Mixtures With Magnesium, Tryggve Smedsland

Masters Theses

"It is known that the addition of titanium to certain types of brasses and bronzes gives them additional valuable properties. The copper-titanium master alloy which is the natural addition agent for making these brasses can not, however, be used if it has been made aluminothermically. It appears that aluminum in the master alloy makes it useless for the above purpose. It should, therefore, be worth while to determine if it is possible to produce a copper-titanium alloy by some method which eliminates the contamination by aluminum, and which would give a copper-titanium which could be used with advantage as an …


Properties Of Wire Suitable For The Fabrication Of Wire Cloth, Campbell William Floyd Funk Jan 1948

Properties Of Wire Suitable For The Fabrication Of Wire Cloth, Campbell William Floyd Funk

Masters Theses

"In the highly competative [sic] wire cloth industry, improvement of product quality is of paramount importance. With an eye to the future, the Ludlow Saylor Wire Company of St. Louis decided to embark upon a research program with the hope of improving the quality of their products above already high standards. An industrial research fellowship was instituted at the Missouri School of Mines and Metallurgy at Rolla for graduate research studies of the metallurgical, mechanical and chemical properties of wire as the [sic] pertain to the weaving of industrial wire cloth. Although relatively small quantities of wire are defective, their …


Studies Of Contact Angles On Oxidized Copper Minerals, John Stewart Carr Jan 1948

Studies Of Contact Angles On Oxidized Copper Minerals, John Stewart Carr

Masters Theses

"Effective flotation of an ore is the result of several factors: selection of suitable reagents; the proper combination of reagents, processing conditions of the operation proper such as time intervals involved and the machinery used. To focus the investigation on a specific field it was decided to investigate in some detail the behaviour of the more popular collectors toward oxidized copper minerals. This investigation was carried out chiefly by applying contact-angle measurements as obtained with the various collectors on the basic carbonate and oxide copper minerals. This basic information was desirable before carrying out actual flotation tests. There was little …


Effect Of Chromium, Molybdenum, Tungsten, And Vanadium Additions On The Physical Properties Of 1.4 Percent Titanium-Copper, Edward Palmer Patterson Jan 1947

Effect Of Chromium, Molybdenum, Tungsten, And Vanadium Additions On The Physical Properties Of 1.4 Percent Titanium-Copper, Edward Palmer Patterson

Masters Theses

"Titanium, an element reported to be ninth most abundant of the elements in the earth's crust, has received very little experimental attention as an alloying element in non-ferrous metallurgy. In copper, titanium produces an age-hardening effect, which makes it of great value to copper manufacturers of fabricated products. Yet, but a handfull of men have investigated the copper-titanium equilibrium diagram, and the titanium rich portion of the diagram still remains a mystery. No work has been done on ternary alloys of copper-titanium to this date, as far as recorded information is concerned, and it is hoped that the present work …


The Use Of Carbides In Refractories, James Adamson Crookston Jan 1947

The Use Of Carbides In Refractories, James Adamson Crookston

Masters Theses

"With the new demands being made on the ceramic industry in mind, it was thought that an investigation of the ceramic possibilities of certain high melting refractory materials might prove of interest and value. The high melting materials are the oxides, carbides, nitrides, borides, and hydrides. Since a great deal of work has been done on the oxides, and relatively little on the others, the oxides were dismissed. Of the other groups, the carbides seemed interesting. Of the carbides, the following materials were chosen for investigation: Boron Carbide (B₄C), Zirconium carbide (ZrC), and Titanium carbide (TiC). These materials were chosen …


The Use Of Wetting Agents In Clay Bodies, Nathan Russell Sewell Jan 1947

The Use Of Wetting Agents In Clay Bodies, Nathan Russell Sewell

Masters Theses

"It has been observed that one of the weak points in the present method of commercially preparing stiff mud bodies is the de-airing process, which involves passing them thru a vacuum chamber. Difficulties in maintaining a good vacuum, power costs, and work stoppages due to clogged vacuum chambers, are some of the problems. It was thought that perhaps a very definite contribution could be made in the field of ceramic engineering if some method could be devised for preparing a workable ceramic body of good dry and fired properties without the use of a vacuum chamber. In attacking the problem, …


Ceramic Possibilities Of Some Missouri Clays And Shales, Leonard Nathanael Larson Jan 1947

Ceramic Possibilities Of Some Missouri Clays And Shales, Leonard Nathanael Larson

Masters Theses

"Although many of the shales and clays of Missouri have in the past been, or are presently being used for the manufacture of heavy clay products such as face brick, common brick, sewer pipe, and tile, there is in these post-war years a significant shortage of these products within the state and country. Especially in the northwestern part of Missouri is there a distinct shortage, as only one structural clay plant is known to be operating in that area. The St. Louis and Southeastern Missouri districts are better prepared to meet construction demands, with several structural clay plants operating at …


Rapid Determination Of Alumina In Diaspore Clays, Matthew Julius Kerper Jan 1947

Rapid Determination Of Alumina In Diaspore Clays, Matthew Julius Kerper

Masters Theses

"The alumina content of the diaspore clay is the index to its refractoriness, so it is important to know the alumina content of the diaspore clay. Diaspore is mined in comparatively small pits and naturally the alumina content will vary from pit to pit and will vary to a considerable extent in the same pit. Since a uniform finished product is desired, the alumina content of each pit must be known and frequent checks run on the output of the pits. Chemical analysis is the standard method of determining the amount of alumina in clays. The main objections to chemical …


An Investigation Of Various Properties Of The 60co-40cr Alloy, Roger David Moeller Jan 1947

An Investigation Of Various Properties Of The 60co-40cr Alloy, Roger David Moeller

Masters Theses

"The binary alloys of Co-Cr have had a few practical applications in our modern economy due to their high cost. The only extensive field of application has been developed in recent years in the manufacture of high temperature alloys for such equipment as gas turbines, jet engines, and turbo-superchargers. The use of these materials has been limited, due to their high cost, to small parts such as rotor blades in gas turbines. To reduce cost and to add desirable or eliminate undesirable properties, the binary alloys have, from the beginning, been modified with varying amounts of other metals. The modified …


The Solubility Of Copper In High-Iron And Low-Iron Slags, Charles Burroughs Gill Jan 1947

The Solubility Of Copper In High-Iron And Low-Iron Slags, Charles Burroughs Gill

Masters Theses

"A thesis giving the details of construction of a rotating induction furnace and its use to experimentally determine the amounts of copper absorbed in high-iron and low-iron slags at various temperatures. A rotating induction furnace is advantageous for slag study in that the slag is contained in a molten pure metal cup and does not come in contact with any refractory, which would be attacked by the slag and contaminate it. The molten pure metal cup is formed by melting the pure metal in a refractory crucible and spinning this inside an induction coil. The induction coil supplies heat for …


A Study Of Certain Properties Of A Cobalt-Chromium-Manganese Alloy For High Temperature Service, Robert Lewis Ray Jan 1947

A Study Of Certain Properties Of A Cobalt-Chromium-Manganese Alloy For High Temperature Service, Robert Lewis Ray

Masters Theses

"The vast amount of attention that has been given to the development of high-temperature service alloys since about 1940 has resulted in the production of numerous compositions for many elevated temperature applications. Particularly in the aircraft industry, with the jet engine, and the power industry, with the gas turbine, have these applications been most demanding. War research has developed a large number of high-temperature service alloys, many of which are in use today, and the alloy ingredients vary widely...it may be readily be seen that there is no one alloy, or one system of alloys which has been developed that …


Beneficiation Of A Zinc Rich Oxidized Ore From Nuevo LéOn, MéXico, Jorge Casas Nieto Jan 1947

Beneficiation Of A Zinc Rich Oxidized Ore From Nuevo LéOn, MéXico, Jorge Casas Nieto

Masters Theses

"Rich zinc ores are relatively rare now in this country but are still abundant in countries like México, that have not yet developed all their mineral potentialities. In almost all Mexican zinc districts there has been reported sporadic production of oxidized ores, although until now no specially designed plants have been built for the beneficiation of such ores. Generally the zinc carbonate and zinc silicate ores are hand picked and shipped to this country for beneficiation. The Mexican production of zinc ores has never been steady, because of economic factors such as bad transportation systems and lack of market for …


Some Preliminary Work On Metaphosphates In Ceramics, John Frederick Burst Jan 1947

Some Preliminary Work On Metaphosphates In Ceramics, John Frederick Burst

Masters Theses

"For a good many years the accepted method of cementing ceramic joints was with a mixture of fire clay grog and a plastic clay binder. This did not prove too satisfactory for several reasons. Usually when enough plastic clay was added to give good workability the vitrification was lowered to such an extent that either excessive shrinkage or excessive bloating occurred, depending upon the extent to which the vitrification point was exceeded...In order to obtain a cement with high strength throughout a long firing range the manufacturers have turned to the addition of various organic binders and inorganic fluxes. Most …


Action Of Diatoms On Clay, Joseph Harvey Renfrew Jan 1946

Action Of Diatoms On Clay, Joseph Harvey Renfrew

Masters Theses

"With the recent trend toward the use of higher temperatures and more severe service conditions in the metallurgical and refractories industries there has developed a constantly greater demand for high-alumina clays, that is, clays in which the alumina content is considerably above that of pure kaolinite, Alâ‚‚O₃2SiO₂·Hâ‚‚O. However, the known reserves of good diaspors are so small that ceramic engineers are already turning to basic refractories in order to have sufficient materials for work at high temperatures. Even the slightest reflection on the needs of the refractories industry will show that such substitutions are strictly limited, and possible only where …


The Age Hardening Of Copper-Manganese-Nickel Alloys, William James Barnett Jan 1946

The Age Hardening Of Copper-Manganese-Nickel Alloys, William James Barnett

Masters Theses

"The Bureau of Mines in conjunction with their Electrolytic Manganese Alloys program has developed a series of age hardening copper-manganese-nickel alloys having properties which compare favorably with those of copper-beryllium alloys...An unusual and highly desirable characteristic of these alloys is their insensitiveness to rate of cooling from the solution temperature. Air cooled and water quenched samples will have identical time hardness curves on being aged. Instead of requiring closely controlled conditions characteristic of many age hardening alloys, these alloys cannot be subjected to a thermal mechanical handling which will prevent hardening on their being subsequently heated to the aging temperature. …


Ceramic Properties Of The Clays Of The Polo Gas Field, Clarence Arthur Lambelet Jan 1946

Ceramic Properties Of The Clays Of The Polo Gas Field, Clarence Arthur Lambelet

Masters Theses

"In Western and Northwestern Missouri there exist many natural gas fields of such limited size and of such great dispersion that it is not economical to utilize their products by the construction of pipe lines to consuming centers. Thus a large source of natural wealth is lying idle. This wealth could be utilized, however, if some manufacturing process requiring large amounts of fuel were located in the vicinity...The availability of fuel is the reason for interest in the area, though an investigation should be made to assure the quality and quantity of the fuel in any selected area. the adequacy …


Flotation Of The Oxidized Ores Of Zinc, Fred Henry Bunge Jan 1946

Flotation Of The Oxidized Ores Of Zinc, Fred Henry Bunge

Masters Theses

"There is no satisfactory method of concentrating the finely disseminated oxide ores of zinc. Gravity methods of concentrating such ores may be used for coarsely crystalline materials in which the zinc material is free at approximately 10- to 35-mesh or coarser. In addition, gravity methods of concentration do not give a satisfactory separation on those ores in which the gangue mineral is small. As a result there is need for a method of beneficiating various deposits of oxidized zinc ores. The two commercially important oxidized zinc minerals under consideration are smithsonite, the zinc carbonate and hemimorphite, frequently referred to as …


A Study Of The Separation Of Feldspar From Missouri Granite, Vernon Louis Kasten Jan 1945

A Study Of The Separation Of Feldspar From Missouri Granite, Vernon Louis Kasten

Masters Theses

"The greatest use of feldspar is as a flux in the Ceramic Industry where it is used in the manufacture of abrasives, floor tile, terra cotta, china, and earthenware of all types. It is also used in the manufacture of glass and enamels, and much is used as grinding medium in powdered form because it is softer than the common abrasive, quartz...Missouri Granites are composed of feldspar, quartz, mica, and other materials, which may or may not occur in all the samples. It is the purpose of this investigation to attempt a separation of the feldspar from these other components …


A High Alumina Concentrate From Low-Grade Burley Clay, Leonard Stearns Jan 1942

A High Alumina Concentrate From Low-Grade Burley Clay, Leonard Stearns

Masters Theses

"The principal source of raw material for the production of high-alumina refractories are the diaspore clays of Missouri. These highly refractory clays contain a large percentage of the mineral, diaspore, a monohydrate of alumina whose theoretical chemical formula is Al₂O₃ʺH₂O. The clays as mined contain from 85 to 65 per cent alumina...Diaspore clays as now found fill sandstone-lined "sink holes" or depressions in the parts of the district underlain by rocks of the Pennsylvanian Age. They are rough open-textured clays, grey or buff in color usually, containing the mineral diaspore in the form of shot-like particles or "oolites." There are …


Determination Of Alkalies In Portland Cement By The Dropping Mercury Electrode Method, William Joseph Smothers Jan 1942

Determination Of Alkalies In Portland Cement By The Dropping Mercury Electrode Method, William Joseph Smothers

Masters Theses

"In many industries whose product or products contain alkalies, the determination of the amount present is very essential from a control standpoint. This present investigation is concerned with a method for quantitative determination of sodium and potassium as accurately as by customary chemical methods and which will require less time in its operation. Portland cement is a product in which the amount of sodium and potassium present is of prime importance. This importance of the alkalies upon the behavior of concrete was first noticed in California where, after numerous tests, it was definitely shown that with certain aggregates there was …


Constitution And Properties Of Manganese-Copper Alloys, James Harrison Jacobs Jan 1940

Constitution And Properties Of Manganese-Copper Alloys, James Harrison Jacobs

Masters Theses

"This work was undertaken because of the recently revived interest in the use of manganese as an alloying element. This revival of interest has been mainly due to the development of the process for electro-deposition of manganese by the U. S. Bureau of Mines. Prior to the work of the bureau of Mines there was no commercial source of high purity manganese. Manganese made by the electrolytic process contains less than .03% impurities, while manganese made by other methods contains as high as 3% impurities. The use of high purity manganese as a base for alloys should open up an …


Laboratory Concentration Of A Lead-Zinc-Fluorspar Ore From Southern Illinois, Shiou-Chuan Sun Jan 1938

Laboratory Concentration Of A Lead-Zinc-Fluorspar Ore From Southern Illinois, Shiou-Chuan Sun

Masters Theses

"The purpose of this investigation was to ascertain the feasibility of preparing marketable products from a rather complex sulphide-fluorspar ore"--Object, page 2. "The ore was examined exhaustively by chemical, microscopic, and mineralogical methods of analysis. After a thorough knowledge of the physical characteristics of the ore had been obtained, flotation concentration tests were made to separate the sulfide minerals from the fluorspar and to attempt to prepare lead-zinc and fluorspar concentrates of marketable grade"--Scope of Work Done, page 2.


Austenite Grain-Size In Low-Carbon Steels And The Coercive Force Of Case Carburized Steels, Thomas Robert Graham Jan 1936

Austenite Grain-Size In Low-Carbon Steels And The Coercive Force Of Case Carburized Steels, Thomas Robert Graham

Masters Theses

"The objective of this investigation was to investigate the various methods for determining austenite grain-size and make a comparison of the results obtained by these methods"--Introduction, page 2.


The Control Of Anode Corrosion, Edward Arthur Godat Jan 1932

The Control Of Anode Corrosion, Edward Arthur Godat

Masters Theses

"This particular study of the control of anode corrosion in connection with the production of zinc by electrolytic deposition from commercial solutions is a continuation of work started at the Missouri School of Mines and Metallurgy in 1929. It is not a new problem or even a new phase of the problem, but rather an attempt to confirm some of the ideas brought out in previous work and to perhaps more definitely establish some of the conclusions drawn from insufficient data, by more extensive tests and by attacking the problem from a slightly different angle"--Introduction, page 1.