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Full-Text Articles in Materials Science and Engineering

Comparative Studies Of Radio Transparency And Dielectric Characteristics Of Polymer Composites, Azira Yermakhanova, Aidar Kenzhegulov, Berdiyar Baiserikov, Мohammed Meiirbekov, Nurlan Boguspayev Jan 2024

Comparative Studies Of Radio Transparency And Dielectric Characteristics Of Polymer Composites, Azira Yermakhanova, Aidar Kenzhegulov, Berdiyar Baiserikov, Мohammed Meiirbekov, Nurlan Boguspayev

Journal of Metals, Materials and Minerals

Aramid-epoxy composites and glass fiber reinforced plastics are widely used in the manufacturing of the fairing design for modern aerospace vehicles due to their excellent mechanical properties combined with radio transparency in wave transfer. In this paper, aramid-epoxy composite and fiberglass were fabricated by the vacuum infusion method for a comparative study on radio transparency and dielectric characteristics. The radio transparency of the studied materials was evaluated by free-space measurements in the frequency range of 1 GHz to 8.5 GHz. According to the radio transparency results, the aramid-epoxy composite undergoes less electromagnetic wave loss than glass fiber reinforced plastic. Modifying …


Effect Of Hatch Spacing In Selective Laser Melting Process Of Ti-6al-4v Alloy On Finished Surface Roughness: A Computational Study, Reettiporn Thongpron, Patiparn Ninpetch, Prasert Chalermkarnnon, Pruet Kowitwarangkul Jan 2024

Effect Of Hatch Spacing In Selective Laser Melting Process Of Ti-6al-4v Alloy On Finished Surface Roughness: A Computational Study, Reettiporn Thongpron, Patiparn Ninpetch, Prasert Chalermkarnnon, Pruet Kowitwarangkul

Journal of Metals, Materials and Minerals

The Selective Laser Melting (SLM) process is a promising additive manufacturing technology for producing complex metal parts. However, this process has certain limitations, including lack of fusion and defects, which can hinder its industrial applications. These challenges can be addressed by determining the appropriate overlap percentage parameters. This study used numerical simulation to explore the effect of overlap percentage on multi-track melting in the SLM process for Ti-6Al-4V. The simulation results categorize the multi-track melting morphologies into two distinct groups. The first group, (0% to 40% overlap), displays consistent surface roughness with an average Ra value of 7 µm. In …


Use Of Commercial Synthetic Filament Waste To Reinforce Biobased Poly(Butylene Succinate) With The Aid Of Compatibilizers, Nattakarn Hongsriphan, Alongkorn Popanna Jan 2024

Use Of Commercial Synthetic Filament Waste To Reinforce Biobased Poly(Butylene Succinate) With The Aid Of Compatibilizers, Nattakarn Hongsriphan, Alongkorn Popanna

Journal of Metals, Materials and Minerals

Since poly(butylene succinate) (PBS) has low rigidity for engineering application, this research attempted to reinforce PBS with poly(ethylene terephthalate) (PET) and polyamide-6 (nylon6) filaments with the reservation of polymer toughness. Filaments were chopped to be short fibers (length of 2 mm to 4 mm) and melt compounded with PBS pellets in the weight ratio of 1 wt%, 5 wt%, and 7 wt% using a twin-screw extruder that the temperature profile was set high enough for melting only PBS matrix. Two types of compatibilizers; hexamethylene diisocyanate (HMDI) or hexamethylene diamine (HMDA) of 0.05 wt% were used to treat fiber surface. It …


Structural, Morphological, Magnetic, And Dielectric Properties Of Copper-Substituted Cuxzn(1-X)Fe2o4 Nanoparticles: Green Synthesis, Gavisiddaiah Harisha, Ramakrishnaiah Thejas, B. Venkatagiriyappa Padmini, Chinnappa Reddy Devaraja, Malalkere Veerappa Murugendrappa, Koppa Mahadevappa Rajashekara Jan 2024

Structural, Morphological, Magnetic, And Dielectric Properties Of Copper-Substituted Cuxzn(1-X)Fe2o4 Nanoparticles: Green Synthesis, Gavisiddaiah Harisha, Ramakrishnaiah Thejas, B. Venkatagiriyappa Padmini, Chinnappa Reddy Devaraja, Malalkere Veerappa Murugendrappa, Koppa Mahadevappa Rajashekara

Journal of Metals, Materials and Minerals

Structural, Magnetic, and Dielectric investigations on the “CuX Zn(1-X) Fe2O4” X with stoichiometry (X=0, 0.3, 0.5, 0.7, and 1) were synthesized by solution combustion method using Aloe Vera extraction.  The X-ray diffraction method was utilized to characterize the as-synthesized Cu-Zn ferrites. The results indicated the presence of cubic spinel structure with Fd‒3 m space group, and absence of other contaminates. The lattice parameter was found to increase with the increase in Zinc concentration. The patterns of TEM confirm that the particle is within the nanometer range (35 nm to 50 nm). Magnetic properties investigated by vibrating sample magnetometry, reveal that …


Vibration Absorption Of As-Built And Post-Heat-Treated Ti-6al-4v Alloy Fabricated By Laser Powder Bed Fusion Additive Manufacturing, Masaaki Nakai, Kohei Nagaya, Kosuke Ueki, Hideki Kyogoku Jan 2024

Vibration Absorption Of As-Built And Post-Heat-Treated Ti-6al-4v Alloy Fabricated By Laser Powder Bed Fusion Additive Manufacturing, Masaaki Nakai, Kohei Nagaya, Kosuke Ueki, Hideki Kyogoku

Journal of Metals, Materials and Minerals

Vibration absorption of the Ti-6Al-4V alloy fabricated by laser powder bed fusion additive manufacturing (LPBF-AM) was evaluated following as-built and post-heat treatment (i.e., solution treatment followed by water quenching). The base plate was heated at 50°C or 200°C during building. Results showed that the vibration absorption of the as-built Ti-6Al-4V alloy was higher when the base plate was heated at 50°C than at 200°C. Further, the vibration absorption indicated strong anisotropy, with the highest vibration absorption in the direction perpendicular to the building direction and transverse to the laser scanning direction. However, after solution treatment followed by water quenching, the …


Zno Nanostructures Synthesized By One-Step Sol-Gel Process Using Different Zinc Precursors, Maneerat Songpanit, Kanokthip Boonyarattanakalin, Wisanu Pecharapa, Wanichaya Mekprasart Jan 2024

Zno Nanostructures Synthesized By One-Step Sol-Gel Process Using Different Zinc Precursors, Maneerat Songpanit, Kanokthip Boonyarattanakalin, Wisanu Pecharapa, Wanichaya Mekprasart

Journal of Metals, Materials and Minerals

Zinc oxide (ZnO) nanopowders have been widely applied in electronics, optics and photocatalytic applications depending on their morphological structure. In the bottom-up process, it is conceived that the different zinc precursors may result in different formations of ZnO nanostructures with exceptional morphology. This work focuses on ZnO material synthesized via the facile sol-gel synthesis using different zinc slat precursors, including zinc acetate, zinc nitrate, zinc sulphate, and zinc chloride. All zinc salt precursors were incorporated with sodium hydroxide and hexamethylenetetramine (HMTA) under mild thermal energy with consistent conditions to investigate ZnO formation. The as-prepared samples appeared in white powders with …


Development Of Forming Limit Diagrams For Motorcycle Fuel Tank Made From Aa5754-O Under Deep Drawing, Phiraphong Larpprasoetkun, Jidapa Leelaseat, Aeksuwat Nakwattanaset, Surasak Suranuntchai Jan 2024

Development Of Forming Limit Diagrams For Motorcycle Fuel Tank Made From Aa5754-O Under Deep Drawing, Phiraphong Larpprasoetkun, Jidapa Leelaseat, Aeksuwat Nakwattanaset, Surasak Suranuntchai

Journal of Metals, Materials and Minerals

The research studied forming limit curves (FLC) for aluminum alloy 5754-O (AA5754-O) and modified them using two methods. These methods aimed to create FLCs for application in describing the forming behavior of sheet metal material through a deep drawing process simulation in the PAM-STAMP program. The methods are as follows: The Nakajima test combined with a new method, a novel process for grid creation on the specimen: laser marking combined with elastic paints. A mathematical material model using the fracture model along with the yield criteria: YLD2000-2D and hardening law: Swift-Voce. The Keeler-Brazier modified equation was chosen as the fracture …


Investigating The Oxidation Behavior Of Mg-Zn Alloy: Effects Of Heating Rates, Gas Flow, Protective Atmosphere, And Alloy Composition, Tuğçe Nur Saraçoğlu, Safa Polat, Erkan Koç, Muwafaq Mashrah, Amir Najah Saud, Marta Michalska-Domańska Jan 2024

Investigating The Oxidation Behavior Of Mg-Zn Alloy: Effects Of Heating Rates, Gas Flow, Protective Atmosphere, And Alloy Composition, Tuğçe Nur Saraçoğlu, Safa Polat, Erkan Koç, Muwafaq Mashrah, Amir Najah Saud, Marta Michalska-Domańska

Journal of Metals, Materials and Minerals

Magnesium-zinc alloys offer promising lightweight properties but are prone to oxidation during high-temperature processing and usage. In this study, the oxidation behavior of Mg-Zn alloy was examined according to the inert gas type flow rate, heating rate and alloy amount. Initially, alloys were produced by adding zinc at weight percentages of 0.5%, 1.5%, and 2% using the casting method. The alloys were characterized using X-ray fluorescence (XRF), X-ray Diffraction (XRD), and scanning electron microscope (SEM) analyses, revealing the formation of dendritic Mg-Zn intermetallic within the alloy. The oxidation behavior of these alloys was examined via differential thermal analysis (DTA) and …


High-Performance No2 Gas Sensor Based On Reduced Graphene Oxide/Zro2 Hybrids, Ali Jabbar Fraih, N. Naeema, Fatima Fadhil Abbas Jan 2024

High-Performance No2 Gas Sensor Based On Reduced Graphene Oxide/Zro2 Hybrids, Ali Jabbar Fraih, N. Naeema, Fatima Fadhil Abbas

Journal of Metals, Materials and Minerals

The increasing concern over environmental pollution, particularly from nitrogen dioxide (NO2) emissions, necessitates the development of efficient NO2 detection sensors. This study introduces reduced graphene oxide (rGO)/ZrO2 hybrids for enhanced NO2 gas sensing. Utilizing a modified Hummer’s method, graphene oxide (GO) flakes were synthesized and subsequently sputtered with 10 nm ZrO2 film, followed by thermal annealing to produce rGO/ZrO2 hybrids. The hybrids were characterized using various techniques including SEM, TEM, AFM, Raman spectroscopy, and XRD, confirming successful synthesis and reduction of GO, as well as the formation of ZrO2 nanoparticles. Gas sensing tests revealed superior sensitivity to NO2 in the …


Phase Separation Promotes Fcc-Phase Mechanical Twinning In Alcocrfemo0.05ni2 High Entropy Alloy, Zifeng Zhang, Liang Chu, Jiqing Zhao, Bing Xu, Qilu Ye Jan 2024

Phase Separation Promotes Fcc-Phase Mechanical Twinning In Alcocrfemo0.05ni2 High Entropy Alloy, Zifeng Zhang, Liang Chu, Jiqing Zhao, Bing Xu, Qilu Ye

Journal of Metals, Materials and Minerals

The AlCoCrFeMo0.05Ni2 high entropy alloy (HEA) can remarkably enhance its ductility through high-temperature annealing. Nevertheless, the underlying mechanism remains under explored. Herein, we utilized molecular dynamics simulations (MD) to calculate the generalized stacking fault energy (GSFE) curves and uniaxial tensile behavior. Notably, the twin inclination of the FCC phase increases significantly after annealing. During plastic deformation, the FCC phase in the annealed alloy exhibits a substantially higher formation of twinning and stacking faults compared to the as-cast alloy. This increased twin inclination after annealing is the fundamental mechanism contributing to the enhancement of high-temperature ductility.


Recent Advances In Synthesis And Bio-Applications Of Natural Stabilizers For Metal Nanoparticles, Abhishek Sharma, Navneet Kaur, Ayashkanta Nanda, Manvinder Kaur, Rajeev Sharma, Harvinder Singh Sohal Jan 2024

Recent Advances In Synthesis And Bio-Applications Of Natural Stabilizers For Metal Nanoparticles, Abhishek Sharma, Navneet Kaur, Ayashkanta Nanda, Manvinder Kaur, Rajeev Sharma, Harvinder Singh Sohal

Journal of Metals, Materials and Minerals

Due to their exceptional physicochemical properties, the synthesis and application of metal nano-particles gained significant traction and a grip in industries and scientific fields or regions. However, the thermodynamic instability of metal nanoparticles poses or leads to challenges in their controlled synthesis and stabilization. To address this stability and the immobilization strategies, natural polymers such as cellulose, starch, alginate, chitosan, and hyaluronic acid have been explored for their non-toxic, biodegradable, and environmentally friendly characteristics. Recent advances in nanotechnology have led to an increased focus on these natural polymer’s utilization as effective stabilizers for diverse metal nanoparticles. This review comprehensively examines …


Influence Of Bi Substitution On Structural And Optical Properties Of Lafeo3 Perovskite, Mohammed Sadok Mahboub, Ouarda Ben Ali, Soria Zeroual, Ghani Rihia, Mourad Mimouni, Imad Hamadneh, Samir Bayou, Hani Boulahbel, Adel Benarfa, Ferhat Rehouma Jan 2024

Influence Of Bi Substitution On Structural And Optical Properties Of Lafeo3 Perovskite, Mohammed Sadok Mahboub, Ouarda Ben Ali, Soria Zeroual, Ghani Rihia, Mourad Mimouni, Imad Hamadneh, Samir Bayou, Hani Boulahbel, Adel Benarfa, Ferhat Rehouma

Journal of Metals, Materials and Minerals

The sol-gel self-ignition method has successfully synthesized a series of homogenous perovskites La1-xBixFeO3 (x=0.0, 0.2, 0.4, 0.6, and 0.8) nanoparticles. Rietveld refinement results from XRD patterns revealed no secondary phases in pure and Bi-substituted LaFeO3 samples. The structural transition from orthorhombic at x = 0.0 until x=0.6 (space group Pbnm) to rhombohedral at x=0.8 (space group R3c) was observed. Lattice parameter values increase slightly with Bi concentration due to the substitution of Bi in the LaFeO3 structure. The average crystallite size D was found to vary between 19 nm and 50 nm. The combination of XRD and SEM demonstrated that …


Nanostructure Of Tio2 And Wo3 Multilayer Films Deposited On Ito Glass For Electrochromic Enhanced Photocatalytic Activity, Atsakorn Chuenkruit, Watcharaporn Thongjoon, Kamon Aiempanakit, Montri Aiempanakit, Chantana Aiempanakit Jan 2024

Nanostructure Of Tio2 And Wo3 Multilayer Films Deposited On Ito Glass For Electrochromic Enhanced Photocatalytic Activity, Atsakorn Chuenkruit, Watcharaporn Thongjoon, Kamon Aiempanakit, Montri Aiempanakit, Chantana Aiempanakit

Journal of Metals, Materials and Minerals

The photocatalytic activity (PA) by electrochromic (EC) enhancement of single and multilayer films of TiO2, WO3, TiO2/WO3, and WO3/TiO2 was investigated. All films were deposited from metal on an ITO glass substrate using direct current (DC) magnetron sputtering via an oblique angle deposition (OAD) technique at 85°. Subsequently, a thermal oxidation (TO) process at 500℃ was applied for the samples to form metal oxide films. The morphology, elemental composition, crystal structure, and optical properties were studied by using field emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDS), X-ray diffractometry (XRD), and UV-vis spectroscopy, respectively. The photocatalytic properties were investigated …


Surface Characteristics Evolution Of 316l Stainless Steel Induced By Tension Loading, Kanokwan Antanam, Surasak Kuimalee, Panya Buahombura, Waraporn Piyawit Jan 2024

Surface Characteristics Evolution Of 316l Stainless Steel Induced By Tension Loading, Kanokwan Antanam, Surasak Kuimalee, Panya Buahombura, Waraporn Piyawit

Journal of Metals, Materials and Minerals

316L stainless steel has been employed as a medical implant material owing to its advantageous biocompatibility and durability. The microstructure and surface characteristics of 316L play a crucial role in implant application. Diverse processing methods were utilized to modify the surface properties of 316L to customize the characteristics of medical devices. Mechanical deformation induces changes in the microstructure and causes changes in surface topography. In this study, we introduced deformation to 316L by applying uniaxial tension at strain values ranging from 2% to 25%. During sample preparation, electrochemical polishing was employed to eliminate the deformed layers generated by mechanical grinding. …


Sbr Elastomer Response To Renewable Diesel Blends: An Experimental Investigation, Andrias Rahman Wimada, Ni Putu Dian Nitamiwati, Fatimah Tresna Pratiwi, Maharanni Dewi Solikhah, Bina Restituta Barus, Eki Dwi Wijanarko, Riesta Anggarani, Lies Asiyah, Setyo Widodo, Arfi Thahar, Soni Solistia Wirawan Jan 2024

Sbr Elastomer Response To Renewable Diesel Blends: An Experimental Investigation, Andrias Rahman Wimada, Ni Putu Dian Nitamiwati, Fatimah Tresna Pratiwi, Maharanni Dewi Solikhah, Bina Restituta Barus, Eki Dwi Wijanarko, Riesta Anggarani, Lies Asiyah, Setyo Widodo, Arfi Thahar, Soni Solistia Wirawan

Journal of Metals, Materials and Minerals

To investigate the impact of Styrene Butadiene Rubber (SBR) exposure to renewable fuels during handling and storage processes, compatibility tests were conducted on three different renewable fuel mixtures: 30% biodiesel, 40% biodiesel, and 30% biodiesel + 10% hydrogenated vegetable oil. These tests involved static immersion experiments conducted at room temperature for a duration of 1000 h, following the ASTM D471 standards. Before and after the immersion tests, the physical properties and visually assessed elastomers concentrations were investigated by varying the SBR content. Additionally, the post-immersion fuel properties were examined. The results showed that mass and volume swelling increased with the …


Bifunctional Cationic Modification Of Modal Fabric For Sustainable In Textile Dyeing With Spent Coffee Grounds, Monthon Nakpathom, Rattanaphol Mongkholrattanasit, Sarute Ummartyotin, Pisutsaran Chitichotpanya, Nattaya Vuthiganond Jan 2024

Bifunctional Cationic Modification Of Modal Fabric For Sustainable In Textile Dyeing With Spent Coffee Grounds, Monthon Nakpathom, Rattanaphol Mongkholrattanasit, Sarute Ummartyotin, Pisutsaran Chitichotpanya, Nattaya Vuthiganond

Journal of Metals, Materials and Minerals

In order to dye cellulose or regenerated cellulose with natural dyes, toxic metal mordants are generally employed. In response to this issue, the novel bifunctional cationic agent was pretreated to modify modal (regenerated cellulose) fabric prior to dyeing to enhance the fiber-dye affinity. The cationization reaction was carried out using a compound containing bicationic sites, N,N'-(oxybis (ethane-2,1-diyl))bis(3-chloro-2-hydroxy-N,N-dimethylpropan-1-aminium. This unique cationic agent is capable of producing nonvolatile amine and has no odor problem. The successful cationic modification was confirmed through FTIR spectroscopy and zeta potential measurement. The cationized process was optimized at a cationic and sodium hydroxide concentration …


Designing Biphasic Nanocellulose Hydrogels To Mimic The Complex Cartilage-Bone Interface, Sairash Sairash, Sirinee Jirajessada, Supansa Yodmuang Jan 2024

Designing Biphasic Nanocellulose Hydrogels To Mimic The Complex Cartilage-Bone Interface, Sairash Sairash, Sirinee Jirajessada, Supansa Yodmuang

Journal of Metals, Materials and Minerals

Osteochondral lesions, which affect both the cartilage and the bone, present significant challenges in treatment due to the complex mechanical and biochemical properties of these tissues. A crucial consideration in developing tissue replacements for these lesions is the simultaneous regeneration of cartilage and calcified cartilage, which forms the transition zone to bone. Our current study aims to fabricate a bilayer polymeric hydrogel designed not only to support cartilage regeneration but also to serve as an interface between cartilage and bone. The bilayer hydrogel was created by combining oxidized bacterial nanocellulose, gelatin, and alginate in one layer, while the other layer …


The Impact Of Hot Rolling, Zn And Sn On The Mechanical And Corrosion Characteristics Of Mg-Zn-Ca Alloys, Halil Eren, Ali Güngör, Erkan Koç, Harun Çuğ Jan 2024

The Impact Of Hot Rolling, Zn And Sn On The Mechanical And Corrosion Characteristics Of Mg-Zn-Ca Alloys, Halil Eren, Ali Güngör, Erkan Koç, Harun Çuğ

Journal of Metals, Materials and Minerals

In this study, it was aimed to develop a biodegradable metallic plate that is an alternative to bioinert metal plates. The main advantage of using biodegradable materials for implants is that they can be gradually replaced with the patient's own tissue, which reduces the need for additional surgeries to remove the implant after it has served its purpose. Magnesium and its alloys can provide biocompatibility as orthopedic implant materials. Mg-Zn-Ca and Mg-Zn-Ca-Sn alloys were prepared using the gravity die casting method. Zn (1.0 wt% and 2.0 wt%) and Sn (0.0 wt%, 0.5 wt% and 1.0 wt%) ratios were used as …


Nutrient Retention And Availability Of Biochars Prepared By Co-Pyrolysis Of Vinasse With Sugarcane Filter Cake, Siraprapra Suwanree, Jesper T.N. Knijnenburg, Emirhan M. Ölҫer, Kaewta Jetsrisuparb Jan 2024

Nutrient Retention And Availability Of Biochars Prepared By Co-Pyrolysis Of Vinasse With Sugarcane Filter Cake, Siraprapra Suwanree, Jesper T.N. Knijnenburg, Emirhan M. Ölҫer, Kaewta Jetsrisuparb

Journal of Metals, Materials and Minerals

The disposal of vinasse, a nutrient-rich by-product of ethanol production, is challenging because of the low pH and emissions of harmful gases and smells. Here, biochars were produced by pyrolysis of mixtures of filter cake and vinasse (0.25 w/v to 1 w/v) at 550℃. The effects of filter cake to vinasse ratios on the biochar yield, pH, ash content, total nutrient (P, K, Ca, and Mg) content, and nutrient availability were investigated. Increasing the filter cake to vinasse ratio increased the biochar yield and ash content and lowered the biochar pH from 10.3 for 0.25-BC to 8.2 for filter cake …


Corrosion Behavior Of Ysz And Ysz/Nico Coatings On Inconel 625 Exposed Alkali Chlorides, Resetiana Dwi Desiati, Eni Sugiarti, Bambang Hermanto, Gerald Ensang Timuda, Hubby Izzuddin, Fraya Aulia Salsabilla, Anawati Anawati Jan 2024

Corrosion Behavior Of Ysz And Ysz/Nico Coatings On Inconel 625 Exposed Alkali Chlorides, Resetiana Dwi Desiati, Eni Sugiarti, Bambang Hermanto, Gerald Ensang Timuda, Hubby Izzuddin, Fraya Aulia Salsabilla, Anawati Anawati

Journal of Metals, Materials and Minerals

Alkali chloride attack on boiler pipe walls is considered the main problem of corrosion in the waste-to-energy (WTE) industry, even though uses superalloy. Electrophoretic deposited (EPD) yttria-stabilized zirconia (YSZ) coating is carried out to protect the Inconel 625 substrate. YSZ is deposited directly both on the Inconel 625 substrate and NiCo-Inconel 625. Corrosion resistance was conducted using the 3.5% NaCl electrochemical test and the hot salt corrosion test at 600°C in alkaline salt media such as NaCl, KCl, and CaCl2. The potentiodynamic polarization curve shows that the YSZ coating deposited on the substrate (single-layer) has a corrosion rate of 0.065 …


Study Of Titanium Alloy Ti–Al–Zr–Nb–V During Heating Under Deformation And Its Phase Transformation Features, Aidar Kenzhegulov, Axaule Mamaeva, Aleksander Panichkin, Akerke Imbarova, Balzhan Kshibekova, Rashida Aubakirova, Nazgul Toiynbaeva Jan 2024

Study Of Titanium Alloy Ti–Al–Zr–Nb–V During Heating Under Deformation And Its Phase Transformation Features, Aidar Kenzhegulov, Axaule Mamaeva, Aleksander Panichkin, Akerke Imbarova, Balzhan Kshibekova, Rashida Aubakirova, Nazgul Toiynbaeva

Journal of Metals, Materials and Minerals

An alloy based on Ti–Al–Zr–Nb–V was prepared and its deformation behavior at elevated temperatures was studied. The microstructure and phase of the alloys were characterized by optical microscopy, scanning electron microscopy, thermal analysis, and mechanical testing. The results showed that the Ti–Al–Zr–Nb–V alloy, when stretched, exhibits a superplasticity effect in the range of  975℃ to 1100℃, with an elongation of up to 400%. It was found that superplasticity develops in the temperature region of the α+β→β transition and is accompanied by a change in grain size and redistribution of alloying elements among phases.


One-Pot Microwave-Assisted Approach Of Polydiacetylene/Zinc Oxide Nanocomposite For Reversible Thermochromic, Chanita Khanantong, Thanutpon Srinopkun, Thitirut Boonmak, Jintana Siriboon Jan 2024

One-Pot Microwave-Assisted Approach Of Polydiacetylene/Zinc Oxide Nanocomposite For Reversible Thermochromic, Chanita Khanantong, Thanutpon Srinopkun, Thitirut Boonmak, Jintana Siriboon

Journal of Metals, Materials and Minerals

This study introduces a new technique to fabricate the reversible poly(PCDA/ZnO) nanocomposites thermochromism. Our preparation process is the solution-mixing method, which is supported by microwave synthesis time instead of ultrasonic bath or stirrer. The presence of ethanol molecules in aqueous media in the solution-mixing method induces dipolar polarization. In addition, the presence of Zn2+ leaking out of the ZnO can produce ionic polarization. These factors affect the shape of poly(PCDA/ZnO) nanocomposites based on their thermochromic properties. The optical properties of poly(PCDA/ZnO) nanocomposite were determined through UV-Vis absorption spectroscopy. The morphology of this nanocomposite was examined by scanning electron microscopy, and …


Green Synthesis Of Carbon Dots From Mangosteen Peel For Fluorescent Cancer Cells, Supaluck Amloy, Tanachporn Lukprang, Monthon Lertworapreecha, Pakorn Preechaburana Jan 2024

Green Synthesis Of Carbon Dots From Mangosteen Peel For Fluorescent Cancer Cells, Supaluck Amloy, Tanachporn Lukprang, Monthon Lertworapreecha, Pakorn Preechaburana

Journal of Metals, Materials and Minerals

Recently, carbon dots (CDs) have received significant attention owing to their outstanding optical properties, good solubility, and low toxicity. In this research, CDs were synthesized by a hydrothermal method based on an environmentally friendly and straightforward strategy, using only mangosteen peel and deionized water. The synthesized CDs had an average size of 3.09 ± 0.38 nm. The absorbance spectrum peak for the CDs was seen at 282 nm, and the central wavelength of fluorescence emission was observed at 433 nm under an excitation wavelength of 355 nm. An aqueous solution of CDs exhibited bright green fluorescence when observed with the …


Fabrication Of Porous Geopolymers Utilizing Aluminum Wastes As Foaming Agent, Siriwan Chokkha, Jiratchaya Ayawanna, Anurat Poowancum, Thanasak Singlaem, Pusit Mitsomwang Jan 2024

Fabrication Of Porous Geopolymers Utilizing Aluminum Wastes As Foaming Agent, Siriwan Chokkha, Jiratchaya Ayawanna, Anurat Poowancum, Thanasak Singlaem, Pusit Mitsomwang

Journal of Metals, Materials and Minerals

Porous geopolymers (PG) are attractive due to their simple fabrication and diverse applications. This work presents a method for fabricating PG by using aluminum salt slag (ASS) as a foaming agent and metakaolin (MK) as the precursor. Sodium silicate (Na2SiO3) and sodium hydroxide (NaOH) are used as alkali activator solutions. The results show that the PG is fabricated by using the sequence mixing method. ASS was milled to a size of 4 µm, then mixed with an NaOH solution for 30 min. After that, MK and Na2SiO3 solution were added. The weight ratio of Na2SiO3/NaOH and solid/liquid was 2.0 and …


Influence Of Annealing Times For W Films On The Structure And Electrochromic Properties Of Anodized Wo3 Films, Watcharaporn Thongjoon, Kamon Aiempanakit, Montri Aiempanakit, Chantana Aiempanakit Jan 2024

Influence Of Annealing Times For W Films On The Structure And Electrochromic Properties Of Anodized Wo3 Films, Watcharaporn Thongjoon, Kamon Aiempanakit, Montri Aiempanakit, Chantana Aiempanakit

Journal of Metals, Materials and Minerals

WO3 films were prepared from annealed W films by anodization and annealing at 450℃ for 1 h. The sputtered W films were annealed before anodization at different times for 0.5 h to 2 h, followed by immediate removal from the furnace (quenching) or slow cooling (cool-down). The WO3 films exhibited a different preferred orientation between the (200) and (222) planes. The morphological structure of the WO3 films depended on the annealing time and cooling features of the W films. The WO3 films for the cool-down condition had smaller grains and more pores than the quenching condition. The WO3 films prepared …


Fabrication And Characterization Of Sb-Doped Mxene Prepared By Hydrothermal Method For Use As A Sensing Electrode For Heavy Metal Detection, Siranaree Phoohadsuan, Thitima Maturos Daniels, Mati Horprathum, Nichaphat Thongsai, Eakkasit Punrat Jan 2024

Fabrication And Characterization Of Sb-Doped Mxene Prepared By Hydrothermal Method For Use As A Sensing Electrode For Heavy Metal Detection, Siranaree Phoohadsuan, Thitima Maturos Daniels, Mati Horprathum, Nichaphat Thongsai, Eakkasit Punrat

Journal of Metals, Materials and Minerals

MXene, a two-dimensional material with favorable physicochemical characteristics, has demonstrated outstanding efficiency in a wide range of applications because of their superior properties, such as higher surface area and conductivity, and facile surface modification. In this study, antimony (Sb) doped MXenes were synthesized via a simple hydrothermal method, employing various Sb concentrations ranging from 5%w/w to 25%w/w. The successful preparation of the Sb-doped MXene (Sb@MXene) was confirmed by an X-ray diffraction (XRD) method. Physical morphologies examined through field-emission scanning electron microscopy (FE-SEM) depict the presence of Sb nanoparticles with the size of about 80 nm on the surface and interlayer …


Realizing Fast Plating/Stripping Of High-Performance Zn Metal Anode With A Low Zn Loading, Zhuo Li, Tamene Tadesse Beyene, Kai Zhu, Dianxue Cao Jan 2024

Realizing Fast Plating/Stripping Of High-Performance Zn Metal Anode With A Low Zn Loading, Zhuo Li, Tamene Tadesse Beyene, Kai Zhu, Dianxue Cao

Journal of Metals, Materials and Minerals

Zn metal batteries and capacitors (ZMBs/ZMCs) are gaining significant attention due to their low cost, high safety, and high theoretical capacity. However, the low utilization of Zn metal decreases the coulombic efficiency. Here, we present a novel approach to enhance the conductivity of host materials by utilizing a 3D conductive structural network of copper mesh. The 3D copper mesh serves as a high-conductive matrix and additionally coating it with Zn serves as a Zn source. Finally, a flexible reduced graphene oxide (rGO) was deposited on the Zn-coated copper mesh as an anode protective layer. The conductive copper mesh renders a …


The Effects Of The Crystallinity Index Of Cellulose On The Flexural Properties Of Hybrid-Cellulose Epoxy Composites, Nathawat Poopakdee, Warut Thammawichai Jan 2024

The Effects Of The Crystallinity Index Of Cellulose On The Flexural Properties Of Hybrid-Cellulose Epoxy Composites, Nathawat Poopakdee, Warut Thammawichai

Journal of Metals, Materials and Minerals

This work investigated the effects of the crystallinity index (CI) of cellulose on the flexural properties of hybrid-cellulose epoxy composites. The CI was varied by combining cellulose microfibrils (CMF) and microcrystalline cellulose (MCC), extracted from coir and eucalyptus, respectively, in various mixing ratios. From the XRD analysis, it was shown that the CI values and the CMF/MCC content follow a parabolic-fitting pattern, reaching a maximum value of 82.06% for the CMF/MCC of 30/70. The composites with cellulose of different CI values were fabricated and the flexural properties were measured. The results showed that the flexural strength increased as the CI …


Maintenance Of The Deteriorated Infrastructure In Thailand, Pakawat Sancharoen, Sothyrak Rath, Dong Viet Phuong Tran, Pitichon Klomjit, Somnuk Tangtermsirikul Jan 2024

Maintenance Of The Deteriorated Infrastructure In Thailand, Pakawat Sancharoen, Sothyrak Rath, Dong Viet Phuong Tran, Pitichon Klomjit, Somnuk Tangtermsirikul

Journal of Metals, Materials and Minerals

Infrastructure has been aged and deteriorated by various causes. Maintenance of its safety and serviceability are crucial and many countries have raised concerns about the existing infrastructure. Infrastructure in Thailand has been also aged. This paper shows results of studies relating to maintenance of infrastructure in Thailand. Inspection of the existing infrastructure in Bangkok was conducted by both visual and non-destructive testing (NDT) showing many deteriorations, and damages. Most of the deteriorations are caused by low concrete covering depth and water leakage. While in marine environment, chloride attack is the main cause. Evaluation criteria for NDT results are studied and …


Properties Of Acrylonitrile-Butadiene-Styrene Nanocomposites Adding Ammonia Plasma Treated Carbon Nanotubes/Graphene Nanoplatelets For Electronic Discharge Application, Sorawit Duangsripat, Pajaera Patanathabutr, Nattakarn Hongsriphan Jan 2024

Properties Of Acrylonitrile-Butadiene-Styrene Nanocomposites Adding Ammonia Plasma Treated Carbon Nanotubes/Graphene Nanoplatelets For Electronic Discharge Application, Sorawit Duangsripat, Pajaera Patanathabutr, Nattakarn Hongsriphan

Journal of Metals, Materials and Minerals

Carbon-based nanofillers have been applied in various products, especially electrical and electronic products. It could be used to modify electrical conductivity of the integrated circuit (IC) polymeric packaging in order to prevent electrostatic discharge that would damage electronic integrity. This research reported the influence of ammonia plasma functionalization and its concentration on electrical, mechanical and thermal properties of Acrylonitrile-Butadiene-Styrene (ABS) reinforced with a mixture of CNTs and GNPs. Nanocomposites were successfully compounded using a twin-screw extruder, which firstly the masterbatch was prepared and then mixed with neat polymer into various concentrations (2 wt%, 4 wt%, 6 wt%, and 8 wt%). …