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Articles 61 - 90 of 267
Full-Text Articles in Materials Science and Engineering
A Study On Ultrasonic Energy Assisted Metal Processing : Its Correeltion With Microstructure And Properties, And Its Application To Additive Manufacturing., Anagh Deshpande
Electronic Theses and Dissertations
Additive manufacturing or 3d printing is the process of constructing a 3-dimensional object layer-by-layer. This additive approach to manufacturing has enabled fabrication of complex components directly from a computer model (or a CAD model). The process has now matured from its earlier version of being a rapid prototyping tool to a technology that can fabricate service-ready components. Development of low-cost polymer additive manufacturing printers enabled by open source Fused Deposition Modeling (FDM) printers and printers of other technologies like SLA and binder jetting has made polymer additive manufacturing accessible and affordable. But the metal additive manufacturing technologies are still expensive …
Plasma Oxidation Of Liquid Precursors For Complex Metal Oxides., Babajide Patrick Ajayi
Plasma Oxidation Of Liquid Precursors For Complex Metal Oxides., Babajide Patrick Ajayi
Electronic Theses and Dissertations
Clean energy production and storage are two of the most significant challenges in the 21st century currently limited by the discovery and development of new and advanced materials. Complex oxides and alloys made using earth-abundant elements will play a crucial role in technology development moving forward, however, current preparation techniques are limited by their inability to produce complex oxides and alloys with precise composition control at fast timescales. A concept was proposed to produce mixed metal oxides with composition control through the oxidation of liquid precursors via plasma oxidation. It was hypothesized that the oxidation process can be completed …
Coupling Of Light's Orbital Angular Momentum To A Quantum Dot Ensemble, Alaa A. Bahamran
Coupling Of Light's Orbital Angular Momentum To A Quantum Dot Ensemble, Alaa A. Bahamran
Electronic Theses and Dissertations
We theoretically and experimentally investigate the transfer of orbital angular momentum from light to an ensemble of semiconductor-based nanostructures composed of lead sulfide quantum dots. Using an ensemble of quantum dots offers a higher cross-section and more absorption of twisted light fields compared to experimentally challenging single-nanostructure measurements. However, each quantum dot (except for on-center) sees a displaced light beam parallel to its own axis of symmetry. The transition matrix elements for the light-matter interaction are calculated by expressing the displaced light beam in terms of the appropriate light field centered on the nanoparticles. The resulting transition rate induced by …
Synergistic Environmental Aging Of Glass Reinforced Polymer Composites, Tianyi Lu
Synergistic Environmental Aging Of Glass Reinforced Polymer Composites, Tianyi Lu
Electronic Theses and Dissertations
Synergistic effects involved in the environmental degradation of Glass Reinforced Polymer (GRP) composites were examined and a novel synergistic aging model was proposed in this study. Six GRPs based on glass fibers with four different polymer resins and six pure polymer thermoplastic resins were exposed either individually or in combination to ultraviolet (UV) radiation, water condensation and elevated temperature for approximately 1000 h. The composites and polymers were monitored for weight changes as a function of time and their surfaces were examined after the tests using optical and scanning electron microscopes (SEM). Photodegradation of the polymer matrices was analyzed by …
Mechanical Properties Of 3d Printed Acrylonitrile Styrene Acrylate, William Cahyadi
Mechanical Properties Of 3d Printed Acrylonitrile Styrene Acrylate, William Cahyadi
Electronic Theses and Dissertations
Several studies have been conducted on FDM 3d printed materials such as PLA (Polylactic Acid) and ABS (Acrylonitrile Butadiene Styrene), however, not for ASA (Acrylonitrile Styrene Acrylate). The use of ASA has been increasing due to its resistance to UV, heat, and some chemicals. The resistance to UV prevents the material from degrading its material properties in common outdoor conditions, whereas resistance to heat and oil prevents the material from discoloration. This combination of effects allows designers to use ASA in outdoor applications, however, material properties for ASA in the FDM 3d printing manufacturing process are not well defined. It …
A Study Of The Effect Of Heat Treatment On 3d Printed Pla Impact Strength, Suresh Thota
A Study Of The Effect Of Heat Treatment On 3d Printed Pla Impact Strength, Suresh Thota
Electronic Theses and Dissertations
Environmental conditions have a significant effect on the mechanical properties of various materials. Environmental parameters such as temperature and humidity have a major impact on mechanical properties of materials such as compressive strength, tensile strength, bending strength and impact strength. The purpose of this research is to study how temperature and humidity affect the impact strength of 3D printed PLA plastic. Impact strength is the ability of a material to absorb energy subjected to an impact load by a pendulum. In this research, 3D printing was employed to produce PLA specimens which were later used for different experimental testings. For …
Utilizing Of Magnesium Oxysulfate Binders For Additive Construction Applications, Hatem Hashem Al-Masaeid
Utilizing Of Magnesium Oxysulfate Binders For Additive Construction Applications, Hatem Hashem Al-Masaeid
Electronic Theses and Dissertations
This dissertation is serving multiple transdisciplinary top-notch material design and technological topics. It is a proof of concept of the feasibility of 3D printing using Magnesium Oxysulfate (MOS) binder as an alternative to the ordinary Portland cement (OPC) to be utilized in terrestrial and extraterrestrial additive construction (AC) fields. MOS paste and mortar are characterized physically, chemically, and mechanically. The characterization results conducted in this research show how MOS’s properties can be controlled to match the 3D printing requirements by manipulating the MOS’s ingredients proportions.
Process-Property-Microstructure Relationships In Laser-Powder Bed Fusion Of 420 Stainless Steel., Subrata Deb Nath
Process-Property-Microstructure Relationships In Laser-Powder Bed Fusion Of 420 Stainless Steel., Subrata Deb Nath
Electronic Theses and Dissertations
Laser-powder bed fusion (L-PBF) is an additive manufacturing technique for fabricating metal components with complex design and customized features. However, only a limited number of materials have been widely studied using L-PBF. AISI 420 stainless steel, an alloy with a useful combination of high strength, hardness, and corrosion resistance, is an example of one such material where few L-PBF investigations have emerged to date. In this dissertation, L-PBF experiments were conducted using 420 stainless steel powders to understand the effects of chemical composition, particle size distribution and processing parameters on ensuing physical, mechanical and corrosion properties and microstructure in comparison …
Low Temperature Desiccants In Atmospheric Water Generation., Sunil Gupta
Low Temperature Desiccants In Atmospheric Water Generation., Sunil Gupta
Electronic Theses and Dissertations
Surging global water demand as well as changes to weather patterns and over exploitation of natural water sources, such as ground water, has made potable water a critical resource in many parts of the World already – one rapidly heading towards a crisis situation. Desalination has been adopted as a solution – this is however energy intensive and impractical for most of the developing countries - those most in need of water. A renewable source of energy is solar thermal and solar photovoltaic. A plentiful source of water is the humidity in the atmosphere. This research is to push the …
Nanoengineering Of Next Generation Silicone Rubber Materials For Extreme Applications, Monika Bleszynski
Nanoengineering Of Next Generation Silicone Rubber Materials For Extreme Applications, Monika Bleszynski
Electronic Theses and Dissertations
Silicone rubber materials are frequently used in extreme environments, including aviation, space, high voltage and other applications. In service, however, complex and difficult to predict damage mechanisms in the rubbers can occur which can lead to severe failures of essential infrastructural components. For example, Non-Ceramic Insulators (NCIs), which support some of the most critical high voltage lines in the world, regularly exhibit severe polymer aging due to environmental pollution, ultra-violet (UV) radiation, and dry band and corona arcing. Designing silicone rubbers to resist aging in these demanding environments is difficult and requires an interdisciplinary approach, including correctly assessing the actual …
Microstructure And Mechanical Properties Of Selective Laser Melted Superalloy Inconel 625., Md Ashabul Anam
Microstructure And Mechanical Properties Of Selective Laser Melted Superalloy Inconel 625., Md Ashabul Anam
Electronic Theses and Dissertations
Selective Laser Melting (SLM), a powder based Additive Manufacturing (AM) process, has gained considerable attention in the aerospace, biomedical and automotive industries due to its many potential benefits, such as, capability of fabricating complex three-dimensional components, shortened design to product time, reduction in process steps, component mass reduction and material flexibility. This process uses metallic powder and is capable of fabricating complex structures with excellent microstructure which make SLM not only an improvement over other manufacturing processes but also innovative material processing technology. Inconel 625, a nickel-based super alloy is widely popular in aerospace, chemical and nuclear industries. This alloy …
High Dynamic Range Optical Devices And Applications., Elijah Robert Jensen
High Dynamic Range Optical Devices And Applications., Elijah Robert Jensen
Electronic Theses and Dissertations
Much of what we know about fundamental physical law and the universe derives from observations and measurements using optical methods. The passive use of the electromagnetic spectrum can be the best way of studying physical phenomenon in general with minimal disturbance of the system in the process. While for many applications ambient visible light is sufficient, light outside of the visible range may convey more information. The signals of interest are also often a small fraction of the background, and their changes occur on time scales so quickly that they are visually imperceptible. This thesis reports techniques and technologies developed …
Modeling And Validations Of Control Parameters For Material Extrusion-Based Additive Manufacturing Of Thixotropic Aluminum Alloys., Lars Herhold
Electronic Theses and Dissertations
Additive Manufacturing (AM) with metals has been accomplished mainly through powder bed fusion processes. Initial experiments and simulations using Material Extrusion Additive Manufacturing (MEAM) have been performed by various researchers especially using low melting alloys. Recently Stratasys Inc. submitted a patent application for the use of their Material Extrusion technology also called Fused Deposition Modeling (FDM) where they describe the process using thixotropic semi-solid alloys. Currently this process using semi-solid, engineering type alloys such as A356 or THIXALLOY 540 aluminum have not been researched to evaluate the control parameters. This research combines the in-depth knowledge of applying thixotropic semi-solid aluminum …
Ultrasonic Nondestructive Evaluation Of Metal Additive Manufacturing., Venkata Karthik Nadimpalli
Ultrasonic Nondestructive Evaluation Of Metal Additive Manufacturing., Venkata Karthik Nadimpalli
Electronic Theses and Dissertations
Metal Additive Manufacturing (AM) is increasingly being used to make functional components. One of the barriers for AM components to become mainstream is the difficulty to certify them. AM components can have widely different properties based on process parameters. Improving an AM processes requires an understanding of process-structure-property correlations, which can be gathered in-situ and post-process through nondestructive and destructive methods. In this study, two metal AM processes were studied, the first is Ultrasonic Additive Manufacturing (UAM) and the second is Laser Powder Bed Fusion (L-PBF). The typical problems with UAM components are inter-layer and inter-track defects. To improve the …
Reactive Lamination Of Perovskite Solar Cells., Lyndie Burns
Reactive Lamination Of Perovskite Solar Cells., Lyndie Burns
Electronic Theses and Dissertations
Due to the growing demand for energy internationally and the environmental impact of other conventional energy technologies, solar power has been a growing area in the energy landscape. Perovskite research has increased substantially because of the high power conversion efficiencies, up to 22%, with many recent advances in the use of these organic-inorganic hybrid perovskites for photovoltaic cells. However, to bring perovskite solar cells into the industrial world, the overall cost of the manufacturing of the solar cell must be improved to compete with other well-developed photovoltaic technologies. Here is presented an alternative perovskite deposition method for methylammonium lead halide …
Materials Design With Polylactic Acid-Polyethylene Glycol Blends Using 3d Printing And For Medical Applications., Jeremiah R. Bauer
Materials Design With Polylactic Acid-Polyethylene Glycol Blends Using 3d Printing And For Medical Applications., Jeremiah R. Bauer
Electronic Theses and Dissertations
This thesis is an examination of two material systems derived from polylactic acid (PLA) and polyethylene glycol (PEG). PLA is a polymer commonly sourced from renewable sources such as starches and sugars. It is a relatively strong, biodegradable polymer, making it ideal for use in the body. Even though it has a relative high strength, PLA is also brittle leading to the use of plasticizers to increase flexibility. One such plasticizer is PEG, which is a material that can exist at room temperature as either a thin liquid, or a hard waxy solid depending on the molecular weight. The first …
Graphene Induced Formation Of Nanostructures In Composites, Chen Shen
Graphene Induced Formation Of Nanostructures In Composites, Chen Shen
Electronic Theses and Dissertations
Graphene induced nanostructures in graphene-based composites and the performance of these composites have been explored in this study. For the metallic nanoparticles decorated graphene aerogels composites, the fabrication of hierarchically structured, reduced graphene oxide (rGO) aerogels with heavily metallic nanoparticles was realized. Higher loading of palladium nanoparticles in graphene aerogels leads to improved hydrogen gas sensing performance. For polymer derived ceramics (PDCs) composites with anisotropic electrical properties, the fabrication of composites was realized by embedding anisotropic reduced graphene oxide aerogels (rGOAs) into the PDCs matrix. Raman spectroscopy and X-ray diffraction studies of PDCs composites with and without graphene indicate that …
Assessment Of Microstructure And Mechanical Behavior Of Materials And Phases Observed In Low-Enriched Uranium Monolithic Fuel Plates After Fabrication, Ryan Newell
Electronic Theses and Dissertations
Low enriched uranium (LEU) fuels are being developed to reduce the use of highly enriched uranium in power generation to reduce proliferation risks. Challenges arise in providing sufficient fissile U in LEU without reactor redesign. As such, a novel monolithic fuel plate design employs LEU alloyed with 10 wt. % Mo. Throughout fabrication of these fuel plates, metallurgical transformations and reactions take place as a result of elevated temperatures during processing. The transformations include decomposition of the metastable body-centered cubic γ phase in the fuel and metallurgical interactions at interfaces between fuel plate components. This work aims to provide further …
The Formation And Characterization Of Mesoscopic J- And H-Aggregates With Controlled Morphologies By The Co- And Templated Assembly Of Cyanine Dyes, Samuel Rhodes
Electronic Theses and Dissertations
The supramolecular aggregates of π-conjugated molecules have become an area of great interest to the scientific community in recent years for their promise in biosensors and optoelectronic devices. Among various supramolecular aggregates, J- and H-aggregates of πconjugated dye molecules are particularly interesting because of their unique optical and excitonic properties that are not given by individual molecules. H-aggregates are composed of dye molecules in a face-to-face stacking, giving rise to a blue-shifted absorption band compared with the monomer band and a strong emission quenching. In contrast, J-aggregates represent an edge-toedge stacking of dye molecules, showing a red-shifted absorption band with …
Novel Technique Of Fabrication Of Porous Copper And Copper Oxide To Improve The Lithium Ion Battery Performance, Raju Prasad Ghimire
Novel Technique Of Fabrication Of Porous Copper And Copper Oxide To Improve The Lithium Ion Battery Performance, Raju Prasad Ghimire
Electronic Theses and Dissertations
Due to widespread and long-term application, Lithium-ion batteries are considered as promising power sources for portable devices, satellites, medical instruments, computers, electric vehicles and grid application. It started to occupy the market once Sony commercialized in 1991. Rechargeable lithium ion batteries drawing people attention due to their peculiar properties such as high energy density and low self-discharge compared to other alkali metals. However, these widespread and long-term applications still require better batteries in terms of performance, safety and cost, which can be achieved by better utilization of anode materials and/or an optimized design of battery configuration. There are several challenges …
Development Of Material For 3d Printed Habitats With Extraplanetary Applications, Taylor Wait
Development Of Material For 3d Printed Habitats With Extraplanetary Applications, Taylor Wait
Electronic Theses and Dissertations
3D printing, also called Additive Manufacturing, has increasingly become a focus for research because of the potential to replace complicated assemblies or complex parts with a single printed item. The space industry is very interesting in studying 3d printing with parts being tested and used on rockets, a 3D printer being installed at the International Space Station and is being developed for use in manned exploration of extraplanetary bodies to build habitats. To encourage teams from around the world to develop technologies and materials for autonomous habitat construction using minimal Earth exports, NASA created the 3D Printed Habitat Challenge. NASA …
Electro-Magnetic Responsive Ni0.5zn0.5fe2o4 Nano-Particle Composite, Jaiprakash Kanagaraj
Electro-Magnetic Responsive Ni0.5zn0.5fe2o4 Nano-Particle Composite, Jaiprakash Kanagaraj
Electronic Theses and Dissertations
The purpose of this study is to simulate and synthesize a Radar (or Radiation) Absorbent Material (RAM) by using polymers and nickel zinc ferrite (Ni0.5Zn0.5Fe2O4) magnetic nanoparticles. There is an ardent desire in military, space and electronics for lighter, faster, cheaper and widespread bandwidth providing RAM materials. Electromagnetic property such as magnetic permeability and electric permittivity play a major in controlling the radiation. The appropriate combination of permeability and permittivity properties is acquired for the synthesis of RAM providing wide-ranging bandwidth. The apt property is achieved by rule of mixture, mixing of particular composition of epoxy polymer having low permeability …
Topology Optimization Of Lightweight Structural Composites Inspired By Cuttlefish Bone, Varun Kumar Gadipudi
Topology Optimization Of Lightweight Structural Composites Inspired By Cuttlefish Bone, Varun Kumar Gadipudi
Electronic Theses and Dissertations
Lightweight material structure is a crucial subject in product design. The lightweight material has high strength to weight proportion which turns into an immense fascination and a territory of investigation for the researchers as its application is wide and expanding consistently. Lightweight composite material design is accomplished by choice of the cellular structure and its optimization. Cellular structure is utilized as it has wide multifunctional properties with lightweight characteristics. Unless it has been topologically optimized, each part in a assembly most likely weighs more than it needs to. Additional weight implies abundance materials are being utilized, loads on moving parts …
Analysis Of 3d Printed Cylindrical Members, Salvador Caballero
Analysis Of 3d Printed Cylindrical Members, Salvador Caballero
Electronic Theses and Dissertations
Compressive analysis of a structural member is the determination of the axial capacity of the member when it is undergoing a load causing the member to fail in either a buckling or a crushing mode. 3D printed plastic columns have not been characterized and analyzed yet. However, this research characterizes 3D-printed PLA columns and provides parameters for future researchers to investigate. The literature describes the different industries that utilize 3D-printing. In this research, we introduce an innovative approach to investigate the stresses produced in a 3D printed composite member, made of PLA and locally available soil. The compressive testing will …
Regolith-Based Construction Materials For Lunar And Martian Colonies, Kevin Grossman
Regolith-Based Construction Materials For Lunar And Martian Colonies, Kevin Grossman
Electronic Theses and Dissertations
Humankind's ambitions of exploring our solar system and parts beyond depend heavily on our ability to collect resources from local environments at our destinations rather than bringing materials on the journey. This is a concept known as in-situ resource utilization (ISRU) and it is one that has been understood by every explorer and settler in the history of humankind. Regolith on the moon and Mars has been shown to be a particularly useful resource and has the ability to provide humans with resources including water, oxygen, construction material, fabric, radiation shielding, metals, and may more. This dissertation focuses on construction …
Influence Of Chitosan-Alginate Scaffold Stiffness On Bone Marrow Stromal Cell Differentiation, Isabel Arias Ponce
Influence Of Chitosan-Alginate Scaffold Stiffness On Bone Marrow Stromal Cell Differentiation, Isabel Arias Ponce
Electronic Theses and Dissertations
Tissue grafts are the gold standard for replacing large volume tissue defects. Yet, they present several risks, including infection, low functional outcomes, and reduced graft integrity. Tissue engineering (TE) combines cells and biomaterial scaffolds to foster tissue growth and remodeling. Bone marrow stromal cells (BMSCs) have been shown to respond to the stiffness of their microenvironment, resulting in differentiation into different lineages. 3D porous chitosan-alginate (CA) scaffolds have been previously demonstrated for bone TE with osteoblasts and BMSCs; however, only a single scaffold composition (4 wt%) was studied. Three CA scaffold compositions (2, 4, 6 wt% CA) were produced. Scanning …
Cell Printing: An Effective Advancement For The Creation Of Um Size Patterns For Integration Into Microfluidic Biomems Devices, Megan Aubin
Electronic Theses and Dissertations
The Body-on-a-Chip (BoaC) is a microfluidic BioMEMs project that aims to replicate major organs of the human body on a chip, providing an in vitro drug testing platform without the need to resort to animal model testing. Using a human model also provides significantly more accurate drug response data, and may even open the door to personalized drug treatments. Microelectrode arrays integrated with human neuronal or human cardiac cells that are positioned on the electrodes are essential components for BoaC systems. Fabricating these substrates relies heavily on chemically patterned surfaces to control the orientation and growth of the cells. Currently, …
Simultaneous Measurement Of Isotope-Free Tracer And Interdiffusion Coefficients In Sandwich Type Diffusion Couples, Esin Schulz
Simultaneous Measurement Of Isotope-Free Tracer And Interdiffusion Coefficients In Sandwich Type Diffusion Couples, Esin Schulz
Electronic Theses and Dissertations
The experimental determination of the tracer or self-diffusion coefficient as a function of composition can be quite burdensome in alloys since separate measurements must be carried out for each alloy composition. A new formalism recently developed by I.V. Belova, N.S. Kulkarni, Y.H. Sohn and G.E. Murch, based on linear response theory combined with the Boltzmann–Matano method allows determination of tracer and interdiffusion coefficients simultaneously from a single, isotope-free solid to solid diffusion couple experiment. In this study, for the first time, an experimental investigation with an analytical approach based on the new formalism has been carried out in the binary …
Advanced Nanoscale Characterization Of Plants And Plant-Derived Materials For Sustainable Agriculture And Renewable Energy, Mikhael Soliman
Advanced Nanoscale Characterization Of Plants And Plant-Derived Materials For Sustainable Agriculture And Renewable Energy, Mikhael Soliman
Electronic Theses and Dissertations
The need for nanoscale, non-invasive functional characterization has become more significant with advances in nano-biotechnology and related fields. Exploring the ultrastructure of plant cell walls and plant-derived materials is necessary to access a more profound understanding of the molecular interactions in the systems, in view of a rational design for sustainable applications. This, in turn, relates to the pressing requirements for food, energy and water sustainability experienced worldwide. Here we will present our advanced characterization approach to study the effects of external stresses on plants, and resulting opportunities for biomass valorization with an impact on the food-energy-water nexus. First, the …
Bio-Mimetic Design With 3d Printable Composites, Ramya Mitra Patnam Damodaram
Bio-Mimetic Design With 3d Printable Composites, Ramya Mitra Patnam Damodaram
Electronic Theses and Dissertations
Weight and stiffness are key factors in the advancement of materials and parts for use in numerous industries. Lightweight cellular structures are broadly utilized for this reason. However, these structures must satisfy several key constraints: they should be light yet structurally safe, sustainable in different loading conditions, resource efficient and easy to maintain. Bio-inspired materials/structures which results in desirable material features are a significant inspiration for engineered cellular structures. Cellular structures can be designed to have multifunctional properties along with lightweight characteristics. Currently, these structures with high strength to weight ratio are widely applied in many fields such as automotive, …