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Articles 31 - 60 of 146
Full-Text Articles in Materials Science and Engineering
Synthesis And Radical Polymerization Of N,N-Diallyl Phthalimide, Oytura S. Maksumova, Feruza A. Pulatova, Dilnozakhon I. Tursunova, Feruza A. Makhmudova
Synthesis And Radical Polymerization Of N,N-Diallyl Phthalimide, Oytura S. Maksumova, Feruza A. Pulatova, Dilnozakhon I. Tursunova, Feruza A. Makhmudova
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of this work is the synthesis of iodine N,N-diallylphthalimide and the study of its radical polymerization. In this regard, the synthesis of iodine N,N-diallylphthalimide was carried out in two stages: at the first stage, phthalic anhydride reacts with allylamine and forms allyl phthalimide, at the second stage, allyl phthalimide reacts with allyl iodide to form iodine N, N-diallyl phthalimide. Radical polymerization of the synthesized quaternary salt of N, N-diallyl phthalimide was studied in the presence of the initiator dinitrile azobisisobutyric acid at relatively low temperatures. Kinetic features of the polymerization reaction of iodine N, N-diallyl phthalimide were considered. …
Technology For Improving The Quality Of Graphite Enrichment By Chemical Treatment, Baxtiyor S. Sadullayev, Abror S. S. Usmonov
Technology For Improving The Quality Of Graphite Enrichment By Chemical Treatment, Baxtiyor S. Sadullayev, Abror S. S. Usmonov
CHEMISTRY AND CHEMICAL ENGINEERING
No abstract provided.
On The Possibility Of Using Qiziltepa Bentonite In Drilling, Farrukh B. Erkinov, Biloliddin B. Qobilov, Mukhammadamin Sh. Jololdinov
On The Possibility Of Using Qiziltepa Bentonite In Drilling, Farrukh B. Erkinov, Biloliddin B. Qobilov, Mukhammadamin Sh. Jololdinov
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of the study was to investigate the possibility of using natural bentonite samples obtained from the Qiziltepa district of Navoiy region in drilling operations. Within the scope of the study, the chemical and mineralogical compositions of the bentonite were determined using X-ray diffraction (XRD) and X-ray fluorescence (XRF) analysis methods. In addition, several enrichment methods for bentonite were tested under laboratory conditions. These included magnetic separation of the bentonite suspension formed with water, washing, and acid washing using oxalic acid for chemical enrichment. The chemical and mineralogical composition of the resulting samples was reanalyzed, relevant tables were compiled, …
Peculiarities Of Preparation Of Nanostructured Cerium-Doped Lutetium-Aluminium Garnet Powders Prepared By Sol-Gel Combustion Method, Eygeniy N. Poddenezhny, Ekaterina E. Trusova, Andrei A. Boiko, Vladimir S. Urbanovich
Peculiarities Of Preparation Of Nanostructured Cerium-Doped Lutetium-Aluminium Garnet Powders Prepared By Sol-Gel Combustion Method, Eygeniy N. Poddenezhny, Ekaterina E. Trusova, Andrei A. Boiko, Vladimir S. Urbanovich
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of the work is to study a new method of thermochemical synthesis of luminescent powder of lutetium-aluminium garnet activated by cerium ions (Lu3Al5O12:Се3+) using nitric acid salts of lutetium, aluminium and cerium, and a mixture of acetic acid and polyvinyl alcohol as a propellant. The synthesis process was carried out in a muffle furnace at an initial temperature of 350 ºC under conditions of limited presence of atmospheric air. The average size of the coherent scattering region for Lu3Al5O12:Се3+ obtained from the combustion …
Evaluation Of Coal Properties Used In A Cement Plant, Geun-Seong Lee, Farrukh B. Erkinov, Mastura Kh. Aripova
Evaluation Of Coal Properties Used In A Cement Plant, Geun-Seong Lee, Farrukh B. Erkinov, Mastura Kh. Aripova
CHEMISTRY AND CHEMICAL ENGINEERING
Coal is not only a heat source for clinker burning but also the coal ash after combustion plays a large role in the quality of clinker mixed with hot meals in the kiln. Since the properties of coal vary depending on the coalification and environment in which it was sedimented, the quality of coal supplying to cement plant can change greatly depending on the coal seam even if it is from the same coal mine. Therefore, the coal used in a cement plant should have its properties measured accurately through representative sampling whenever it is supplied to the plant, and …
Preparation Of Nano-Sized Silver Particles By Electrolysis From Silver-Containing Electrical Scrap, Umar A. Yakhyaev, Mastura Kh. Aripova, Ripsime V. Mkrtchyan, Dilrabo A. Mukhtorova
Preparation Of Nano-Sized Silver Particles By Electrolysis From Silver-Containing Electrical Scrap, Umar A. Yakhyaev, Mastura Kh. Aripova, Ripsime V. Mkrtchyan, Dilrabo A. Mukhtorova
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of the study was preparation of nanosized silver particles by electrolysis from silver-containing scrap from electrical engineering production. For this purpose, at the first stage, silver particles with a size of 0.2–2 microns were obtained by the cementation method, confirmed by the results of scanning electron microscopy. A silver anode for the electrolysis unit was created from the obtained silver particles by the melting method. At the second stage, electrolysis was carried out on a unit with rotating electrodes, in which the cathode was made of platinum. Optimum conditions for the electrolysis process, carried out at a voltage …
Synthesis Of Neodymium Oxide Nanotubes Via Chemical Deposition Followed By Thermal Treatment, Odiljon E. Abdurakhmonov, Mastura Kh. Aripova, Sherzod E. Abdurakhmonov, Zaynobiddin T. Matkarimov, Sultan Kh. Suleymanov, Natalya A. Kulagina
Synthesis Of Neodymium Oxide Nanotubes Via Chemical Deposition Followed By Thermal Treatment, Odiljon E. Abdurakhmonov, Mastura Kh. Aripova, Sherzod E. Abdurakhmonov, Zaynobiddin T. Matkarimov, Sultan Kh. Suleymanov, Natalya A. Kulagina
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of this work is to synthesize Nd2O3 nanotubes via chemical deposition followed by thermal treatment. Nd(OH)3 nanotubes were synthesized using Nd(NO3)3 as a precursor and NaOH as a precipitant. After thermal treatment, crystalline Nd2O3 nanotubes were obtained. Thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) were conducted to study the thermal effects and phase transitions during the synthesis. X-ray phase analysis (XRD) was used to determine the phase composition and crystal structure. In addition, the construction of the crystal lattice structure is carried out using programs.The morphological characteristics …
Bismuth Cuprates Produced By Solar Energy Showing Anomalous Resistance, Dilbara Dj. Gulamova, Sirojiddin Z. Mirzaev, Sirojiddin Kh. Bobokulov, Timur I. Gulamov
Bismuth Cuprates Produced By Solar Energy Showing Anomalous Resistance, Dilbara Dj. Gulamova, Sirojiddin Z. Mirzaev, Sirojiddin Kh. Bobokulov, Timur I. Gulamov
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of the study is to obtain bismuth superconducting cuprates with higher superconducting properties. The advantages of superconducting materials in power engineering, disadvantages of synthesis based on solid-phase and melt principles, and the prospect of using nontrivial methods to obtain high critical parameters are presented. The advantages of synthesis under the influence of concentrated solar energy are shown. In order to obtain a superconductor with high critical properties, a massive, long-term stable bismuth cuprate was synthesized using solar technology. It pushes out an external magnetic field and has a nanostructured layered microstructure with caverns containing submicron-sized particles. The phase …
Research Of Horse Oil Based Shampoo For Fine Hair Involving Local Oils And Enzyms Transesterification, Sherzod Y. Rakhmanov, Madina O. Khaydarova, Bonu G. Аrislonboyeva, Nilufar A. Khaydarova, Dilshod P. Rakhimov
Research Of Horse Oil Based Shampoo For Fine Hair Involving Local Oils And Enzyms Transesterification, Sherzod Y. Rakhmanov, Madina O. Khaydarova, Bonu G. Аrislonboyeva, Nilufar A. Khaydarova, Dilshod P. Rakhimov
CHEMISTRY AND CHEMICAL ENGINEERING
Currently, there are many shampoos, balms and various hair masks. Shampoo-tonics have also been introduced into production, providing temporary coloring without damaging the hair structure. In this research work, we set ourselves the task of conducting a study of a shampoo for soft hair that provides durability, granularity and shine to hair by transesterifying horse oil with the enzyme lipase and the surfactant sodium lauryl sulfate. Depending on the type of shampoo, we conducted a scientific study using the following experimental method. To add horse oil to the shampoo formula, we re-esterified mixtures of horse oil and sunflower oil in …
Effect Of Desorption On Photocatalytic Decomposition Of Methylene Blue Using Materials From Solid Wastes Of Production Of Molybdenum Oxides (Vi) And Titanium Dioxide, Dilshoda R. Tursunova, Shahlo Sh. Daminova, Rafael A. Nusretov, Ayipbergen Shiknazarov, Zuhra Ch. Kadirova
Effect Of Desorption On Photocatalytic Decomposition Of Methylene Blue Using Materials From Solid Wastes Of Production Of Molybdenum Oxides (Vi) And Titanium Dioxide, Dilshoda R. Tursunova, Shahlo Sh. Daminova, Rafael A. Nusretov, Ayipbergen Shiknazarov, Zuhra Ch. Kadirova
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of the work is to obtain and characterize a composite photocatalyst based on the spent catalyst of the Shurtan Mining and Chemical Combine based on titanium dioxide and molybdenum-containing waste of the Almalyk Mining and Metallurgical Combine and to identify factors influencing the process of photocatalytic decomposition of methylene blue in solution under the action of UV light. In this work, we studied the kinetics of photocatalytic decomposition of methylene blue on the surface of materials obtained from technogenic solid waste, which were thermally activated at a temperature of 600 ° C. It was found that desorption plays …
X-Ray Photoelectron Spectroscopy Investigation Of Surface Changes In Chalcocite And Enargite Minerals Following Oxidation Treatment, Berdakh T. Daniyarov, Miki Hajime, Baxtigul Y. Ruzieva, Shahlo Sh. Daminova
X-Ray Photoelectron Spectroscopy Investigation Of Surface Changes In Chalcocite And Enargite Minerals Following Oxidation Treatment, Berdakh T. Daniyarov, Miki Hajime, Baxtigul Y. Ruzieva, Shahlo Sh. Daminova
CHEMISTRY AND CHEMICAL ENGINEERING
Copper sulfide minerals, such as chalcocite (Cu₂S) and enargite (Cu₃AsS₄), are important sources of copper, which has wide applications in electronics, energy, and other industries. These minerals are traditionally processed using flotation methods, which are one of the most effective ways to extract copper from sulfide ores. However, the success of flotation of copper sulfides, such as chalcocite and enargite, strongly depends on changes in their surface properties, such as hydrophobicity or hydrophilicity, which can be modified by various chemical reagents. To further understand the impact of these chemical reagents on chalcocite and enargite minerals, X-ray photoelectron spectroscopy (XPS) was …
Synthesis And Study Of Complex Compounds With 1,3,4-Oxadiazole Derivatives Based On Ammonium Vanadate, Mehribon A. Pirimova, Shaxnoza A. Kadirova, Abduhakim A. Ziyayev
Synthesis And Study Of Complex Compounds With 1,3,4-Oxadiazole Derivatives Based On Ammonium Vanadate, Mehribon A. Pirimova, Shaxnoza A. Kadirova, Abduhakim A. Ziyayev
CHEMISTRY AND CHEMICAL ENGINEERING
This research work examines the synthesis, structure and properties of ammonium vanadate complex compounds based on 1,3,4-oxadiazole derivatives. Competing donor centers in coordination, electronic and geometric structures of the ligand molecule were studied based on quantum chemical calculations using the Gaussian09 LanL2DZ software package. Among the ligands, 2-carboxymethylthio-5-phenyl-1,3,4-oxadiazole ligand has been shown to have more competitive donor atoms than other ligands.
Structural Features And Morphology Of Biodegradable Composites Based On Polylactide And Corn Starch, Eygeniy N. Poddenezhny, Andrei A. Boiko, Ekaterina E. Trusova, Viktor M. Shapovalov
Structural Features And Morphology Of Biodegradable Composites Based On Polylactide And Corn Starch, Eygeniy N. Poddenezhny, Andrei A. Boiko, Ekaterina E. Trusova, Viktor M. Shapovalov
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of the work was to study the morphology and structural features of biodegradable composites based on polylactide, filled with corn starch formed by extrusion method. The characteristics of the obtained materials were investigated by scanning electron microscopy, X-ray diffraction, IR spectroscopy. It was established that the presence of polyethylene glycol PEG–4000 as a plasticizer and surfactant – glycerin monostearate in the initial mixture leads to the formation of a nonporous heterogeneous system, in which starch particles are statistically distributed in the matrix. The starch concentration in the composite varied from 20 to 55 wt. %. When the starch …
Influence Of Thermal Cycling On The Resistance Of Bismuth Cuprates Synthesized Using Solar Energy, Dilbara Dj. Gulamova, Sirojiddin Z. Mirzaev, Sirojiddin Kh. Bobokulov, Elyor B. Eshonkulov, Grigor I. Mamniashvili
Influence Of Thermal Cycling On The Resistance Of Bismuth Cuprates Synthesized Using Solar Energy, Dilbara Dj. Gulamova, Sirojiddin Z. Mirzaev, Sirojiddin Kh. Bobokulov, Elyor B. Eshonkulov, Grigor I. Mamniashvili
CHEMISTRY AND CHEMICAL ENGINEERING
A bulk superconducting ceramic synthesized using solar technology exhibits a sharp increase in resistance from zero to approximately 160Ω at 250 K. Four thermal cycling tests in the range of 79-360 K revealed a tendency for the temperature transition interval to narrow and a comparatively sharp jump at 290 K, suggesting a superconducting transition. The effect of stress concentration at grain boundaries during four cycles leads to an increase in the superconducting transition temperature due to the cumulative rise in stress and pinning force. The assumption that these effects are caused by superconducting homologous phases is based on the manifestation …
The Effect Of B2o3 On The Structure And Properties Of The Glasses Of The Na2o–Cao–Mgo–Sio2–P2o5 System, Mihail V. Dyadenko, Ivan A. Levitskiy, Irina I. Kurilo, Alexander S. Glinskii
The Effect Of B2o3 On The Structure And Properties Of The Glasses Of The Na2o–Cao–Mgo–Sio2–P2o5 System, Mihail V. Dyadenko, Ivan A. Levitskiy, Irina I. Kurilo, Alexander S. Glinskii
CHEMISTRY AND CHEMICAL ENGINEERING
The purpose of this work was to study the effect of boron oxide on the physico-chemical and technological properties of glasses of the Na2O–CaO–MgO–SiO2–P2O5 system. The study of crystallization ability, density, the temperature of the onset of softening, as well as the chemical stability of experimental glasses modified with boron oxide, made it possible to indirectly assess their ability to dissolve in aqueous solutions and show bioactive properties. The article presents the results of the influence of B2O3 on the viscosity of the studied glasses and the value of their …
Research Of The Decomposition Process Of Unenriched Phosphate Raw Materials Of Central Kyzylkum With Nitric And Sulfuric Acids, Husan A. Zikirov, Ruslan Ch. Yorbobaev, Kholtura Ch. Mirzakulov
Research Of The Decomposition Process Of Unenriched Phosphate Raw Materials Of Central Kyzylkum With Nitric And Sulfuric Acids, Husan A. Zikirov, Ruslan Ch. Yorbobaev, Kholtura Ch. Mirzakulov
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of the research is to establish the optimal technological parameters of the process of decomposition of unenriched phosphate raw materials of the Central Kyzylkum nitric and sulfuric acid for processing complex nitrogen-phosphorus fertilizers, to study the chemical composition, rheological properties. The coefficient of decomposition of unenriched phosphate raw materials, pH of acid pulp depending on various ratios and the total rate of nitric-sulfuric acid, as well as S:L of the environment are determined. The chemical and mineralogical composition of nitrosulphophosphate fertilizers formed after drying the ammoniated pulp are established.
Study Of Regularities Of Formation Of Hydroxyammonium Oligomers From Alkanolamine Of The Type Of Hexahydrosimtriazine And Epichlorohydrin, Nozima M. Ibragimova, Ravshan I. Adilov
Study Of Regularities Of Formation Of Hydroxyammonium Oligomers From Alkanolamine Of The Type Of Hexahydrosimtriazine And Epichlorohydrin, Nozima M. Ibragimova, Ravshan I. Adilov
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of the work is to study the patterns of formation of hydroxylammonium oligomers based on hexahydrosymtriazine with epichlorohydrin. The paper studies the interaction patterns of the alkanolamine hexahydrosimtriazine type - N, N', N'-tris (β-oxyethyl) hexahydro-S-triazine (THOHST)with epichlorohydrin (ECH). The reaction between TOEGT and ECH occurs at a noticeable rate, already at 0 oC. An increase in the reaction duration leads to a symbate increase in the molecular weight values, the concentration of hydrolyzed chlorine, a decrease in the content of epoxy groups, and the concentration of hydroxyl groups do not change within the experimental error. An increase …
O-Xloratsetiltimol Sintezi Va Uni Kimyoviy Modifikatsiyalash, Azimjon U. Choriev, Anvar K. Abdushukurov, Ilyos U. Normurodov, Sarvinoz K. Mirzayeva
O-Xloratsetiltimol Sintezi Va Uni Kimyoviy Modifikatsiyalash, Azimjon U. Choriev, Anvar K. Abdushukurov, Ilyos U. Normurodov, Sarvinoz K. Mirzayeva
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of the study is to develop a convenient method for the synthesis of O-chloroacetylthymol and to propose the mechanism of the O-chloroacetylation reaction. Thin-layer chromatography of chloroacetylation and nucleophilic substitution reaction products was studied and their composition was confirmed by reference substances. Nucleophilic exchange reactions of O-chloroacetylthymol with sodium oxalate, sodium tartrate, potassium rhodanides were studied. Favorable conditions for carrying out the nucleophilic exchange reaction were searched and 3 new substances unknown in the literature were synthesized. The structure of the synthesized substances was proved by IR and NMR spectra.
Study Of Crystallization Ability Of Glasses Synthesized In The Basalt-Quartz-Soda System, Eldor I. Ruzmatov, Mastura Kh. Aripova, Bahrom R. Ro'ziboyev
Study Of Crystallization Ability Of Glasses Synthesized In The Basalt-Quartz-Soda System, Eldor I. Ruzmatov, Mastura Kh. Aripova, Bahrom R. Ro'ziboyev
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of the work is to study the crystallization capacity of glasses synthesized in the basalt-quartz-soda system. The crystallization capacity of glasses was studied by the method of mass crystallization in the range of 600 oC and 1050 oC. The stages of spontaneous crystallization were determined by the DTA method. The density, TCLE, refractive index, compressive strength and frost resistance were studied. The crystalline phases of crystallized glasses were determined by the X-ray phase method. The presence of diopside and anorthite was revealed.
Influence Of The Granulometric Composition Of Carbonate Rocks On Glass Formation Processes In Float Glass Technology, Sergey P. Grechuha, Yury G. Pavliukevich, Ludmila F. Pаpko, Olesya M. Mozhdzher, Aleksandr P. Kravchuk
Influence Of The Granulometric Composition Of Carbonate Rocks On Glass Formation Processes In Float Glass Technology, Sergey P. Grechuha, Yury G. Pavliukevich, Ludmila F. Pаpko, Olesya M. Mozhdzher, Aleksandr P. Kravchuk
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of this work is to study the influence of the granulometric composition of dolomite and limestone of 0.1–1.0 mm, 1.0–1.6 mm, 1.6–2.5 mm fractions on the rate of glass formation processes in the synthesis of float glass. The dependence of the degree of decarbonization of dolomite and limestone on the dispersion of particles and the time of heat treatment has been established. According to the study of the influence of the granulometric composition of carbonate rocks on the melting characteristic of float glass, it can be concluded that it is possible to use the 1.0–1.6 mm fraction of …
Antibacterial Semi-Fritted Glazes Containing Iron (Iii) And Manganese (Iv) Oxides, Ivan A. Levitskiy, Mihail V. Dyadenko, Ekaterina E. Trusova
Antibacterial Semi-Fritted Glazes Containing Iron (Iii) And Manganese (Iv) Oxides, Ivan A. Levitskiy, Mihail V. Dyadenko, Ekaterina E. Trusova
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of this research work is production of colored antibacterial glaze coatings for ceramic products containing iron (III) and manganese (IV) oxides. The coatings are produced on the basis of multicalcium aluminoborosilicate frit, dolomite and iron or manganese oxides. The constant components in the raw mixture were feldspar, alumina, coal clay and kaolin. The coatings were obtained by finely grinding the components then applied to the dried semi-finished product and single fired at a temperature of 1200±5 °C for 60±2 minutes. The formation of the glaze layer, the decorative properties of coatings, and their physical and chemical and operational …
Synthesis Of Nanostructured Cerium-Doped Yttrium-Aluminum Garnets By Method Of Sol-Gel Burning In A Microwave Oven, Eygeniy N. Poddenezhny, Andrei A. Boiko, Ekaterina E. Trusova, Ekaterina R. Kravcova
Synthesis Of Nanostructured Cerium-Doped Yttrium-Aluminum Garnets By Method Of Sol-Gel Burning In A Microwave Oven, Eygeniy N. Poddenezhny, Andrei A. Boiko, Ekaterina E. Trusova, Ekaterina R. Kravcova
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of research is to study the new method of thermochemical synthesis of yttrium-aluminum garnet luminescent powder, cerium doped (Y3Al5O12:Се3+, YAG:Ce) using the nitric acid salts of yttrium, aluminum and cerium, with the mixture of carbamide and hexamethylenetetramine used as fuel. Synthesis was performed in a microwave oven with the power of 800 W and frequency of 2450 MHz in a porcelain crucible closed with a perforated heat-resistant cover. The average size of coherent scattering region (CSR) of YAG:Ce particles (nominal diameter D) obtained in the crucible during the microwave heating …
Synthesis, Crystal Structure, Hirshfeld Surface And Void Analysis Of 2-Amino-1h-Benzimidazolium 2-Hydroxybenzoate, Salmon M. Mukhammadiev, Daminbek A. Ziyatov, Zuhra Ch. Kadirova, Jamshid M. Ashurov, Shahlo Sh. Daminova
Synthesis, Crystal Structure, Hirshfeld Surface And Void Analysis Of 2-Amino-1h-Benzimidazolium 2-Hydroxybenzoate, Salmon M. Mukhammadiev, Daminbek A. Ziyatov, Zuhra Ch. Kadirova, Jamshid M. Ashurov, Shahlo Sh. Daminova
CHEMISTRY AND CHEMICAL ENGINEERING
The purpose of this work is determination of crystal structure and Hirschfeld surface void analysis for many intermolecular interactions in the crystal structure of 1,3-dihydro-2H-benzimidazole-2-iminium-2-hydroxy-5-sulfobenzoate.. For the first time, a new organic salt containing organic benzimidazolium cations and sulfosalicylic anions was synthesized and structurally characterized. Hirshfeld surface analysis confirm that in the crystal shape most remarkable contacts are H∙∙∙O (38%) and H∙∙∙H (29.7%) There are some π–π stacking interactions in the crystal shape.
Synthesis Of Cationite Based On Indene, A Secondary Product Of Hydrocarbons Pyrolysis, Saidmansur Sh. Saidobbozov, Suvonkul E. Nurmanov, Dilorom H. Mirkhamitova
Synthesis Of Cationite Based On Indene, A Secondary Product Of Hydrocarbons Pyrolysis, Saidmansur Sh. Saidobbozov, Suvonkul E. Nurmanov, Dilorom H. Mirkhamitova
CHEMISTRY AND CHEMICAL ENGINEERING
The purpose of the study is extraction of the indene from pyrolysis oil obtained from the pyrolysis of hydrocarbons at the Ustyurt gas processing plant. Indene is isolated by rectification from the composition of pyrolysis oil formed as a by-product of the process of hydrocarbons pyrolysis at the Ustyurt gas processing plant. Polymethyleneindenesulfocationite was synthesized on the basis of isolated indene, and its structure and physicochemical properties were determined. Chromatomass spectrum of pyrolysis oil was obtained and analyzed. The indene fraction and the synthesized polymethyleneindenesulfocationite were analyzed using IR spectroscopy and SEM (scanning electron microscopy). Thermal analysis of cationite was …
Preparation Of Keratin-Containing Protein Compounds From Chickens Feathers Using Hydrochloric Acid, Dilnozakhon I. Tursunova, Oytura S. Maksumova
Preparation Of Keratin-Containing Protein Compounds From Chickens Feathers Using Hydrochloric Acid, Dilnozakhon I. Tursunova, Oytura S. Maksumova
CHEMISTRY AND CHEMICAL ENGINEERING
The purpose of this work is the preparation of keratin-containing protein compounds from poultry processing waste by hydrolysis with hydrochloric acid, including treatment of the protein with 5% H2O2. The process of cleaning feather raw materials using water, liquid soap, NaClO3, C2H5OH, and H2O2, and the reaction of its hydrolysis with an aqueous solution of HCl have been studied. The influence of temperature and reaction duration on the hydrolysis process was studied, and its optimal mode was established. It has been shown that the process of …
Synthesis And Research Of Adsorbents And Catalysts Obtained By Processing Of Industrial Wastes, Shuhratqodir T. Gulyamov, Sherzod A. Омоnоv, Shaxnoz B. Jalalova, Dilnoza P. Turdieva, Rufatjon F. Boymonov
Synthesis And Research Of Adsorbents And Catalysts Obtained By Processing Of Industrial Wastes, Shuhratqodir T. Gulyamov, Sherzod A. Омоnоv, Shaxnoz B. Jalalova, Dilnoza P. Turdieva, Rufatjon F. Boymonov
CHEMISTRY AND CHEMICAL ENGINEERING
The purposes of the study are the synthesis of granular aluminum oxide and magnesium-aluminum spinel using various residues formed during thermochemical regeneration of adsorbents deactivated by chloride compounds, the physicochemical characteristics and catalytic properties of catalysts. The main parameters for processing aluminum-containing waste using sulfuric acid technology to produce pseudoboehmite have been identified. Adsorbents, as well as carriers and catalysts obtained using pseudoboehmite and alkaline waste have been studied using diffractometry, thermography and elemental analysis. The conditions for the synthesis of mechanically strong granules containing magnesium and calcium aluminates have been determined. Based on pseudoboehmite, aluminum oxide adsorbents with texture, …
Influence Of Solid-Phase And Melt Synthesis Methods On The Structure And Electrochemical Properties Of Na3fe2(Po4)3 Polycrystals, Adolf S. Nogai, Artur A. Nogai, Daniyar E. Uskenbaev, Eleonora A. Nogai, Alexander A. Bush
Influence Of Solid-Phase And Melt Synthesis Methods On The Structure And Electrochemical Properties Of Na3fe2(Po4)3 Polycrystals, Adolf S. Nogai, Artur A. Nogai, Daniyar E. Uskenbaev, Eleonora A. Nogai, Alexander A. Bush
CHEMISTRY AND CHEMICAL ENGINEERING
The article studies the influence of solid-phase and melt synthesis methods on the structure and electrochemical properties of the Na3Fe2(PO4)3 polycrystals. If the solid-phase synthesis of the Na3Fe2(PO4)3 polycrystals (type 1 of samples) is carried out using ceramic technology, initially glassy precursors are first obtained by melting the starting materials under the influence of optical radiation energy at the melt synthesis method, and the Na3Fe2(PO4)3 polycrystals are obtained after firing (type 2 of samples). With this method, the synthesis …
Study Of The Process Of Foam Formation During Nitric Acid Decomposition Of Dolomite Raw Materials, Oybek A. Mikhliev, Kholtura Ch. Mirzakulov, Ruslan Ch. Yorbobaev, Shahodat M. Olmurova
Study Of The Process Of Foam Formation During Nitric Acid Decomposition Of Dolomite Raw Materials, Oybek A. Mikhliev, Kholtura Ch. Mirzakulov, Ruslan Ch. Yorbobaev, Shahodat M. Olmurova
CHEMISTRY AND CHEMICAL ENGINEERING
The purpose of the work is acceleration of the process of nitrate decomposition of local dolomite raw materials and study its processing into MgOH, MgO, liquid and granular magnesium fertilizers. We studied the effect of "PAA-gel" and "Struktol SB 2195" on the foam expansion ratio and filtration rate, as well as the influence of acid concentration and temperature on the rheological properties of the acidic pulp and the liquid and solid phases formed during its separation. The qualitative and quantitative compositions were determined. As a result, an increase in the filtration rate and a decrease in the rate of foaming …
Microwave Synthesis Of Yttrium Oxide Nanostructure Powders, Doped With Ytterbium And Erbium Ions, Eygeniy N. Poddenezhny, Andrei A. Boiko, Olga V. Davydova, Ekaterina E. Trusova
Microwave Synthesis Of Yttrium Oxide Nanostructure Powders, Doped With Ytterbium And Erbium Ions, Eygeniy N. Poddenezhny, Andrei A. Boiko, Olga V. Davydova, Ekaterina E. Trusova
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of the study was to develop microwave synthesis of luminescent yttrium oxide powders doped with ytterbium and erbium ions (Y2O3:Yb3+, Er3+) in the process of homogeneous precipitation from a reaction mixture of yttrium, ytterbium and erbium chlorides. The characteristics of the obtained powders were studied by X-ray diffraction, scanning and passing electron microscopy, differential thermal analysis, IR spectroscopy and photoluminescence under IR excitation. From luminescence spectra of Y2O3:Yb3+, Er3+ samples obtained by excitation with an IR laser at a wavelength of 975 nm, …
Optical Glass With Increased Refractive Index Based Bao – B2o3 – Sio2 System, Yury G. Pavliukevich, Ludmila F. Pаpko, Ekaterina E. Trusova
Optical Glass With Increased Refractive Index Based Bao – B2o3 – Sio2 System, Yury G. Pavliukevich, Ludmila F. Pаpko, Ekaterina E. Trusova
CHEMISTRY AND CHEMICAL ENGINEERING
The aim of the research is to develop lead-free optical glass with increased refractive index based on BaO – B2O3 – SiO2 system. A study of technological and physical-chemical properties of glass was conducted. It has been shown that the glass of this system tends to the phase separation of segregation type. The area of glass composition with refractive index of 1.6195 – 1.6650 has been established. The peculiarities of influence of the modifiers – Al2O3 and oxides of the RO group – on the technological and optical properties of the glass of …