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Full-Text Articles in Materials Science and Engineering

Burner, Emitter, And Recuperator Development For Lightweight Thermophotovoltaic Power Supply, Lewis Fraas, Leonid Minkin, J. Avery, Hui She, L. Ferguson, Fatih Dogan Jun 2015

Burner, Emitter, And Recuperator Development For Lightweight Thermophotovoltaic Power Supply, Lewis Fraas, Leonid Minkin, J. Avery, Hui She, L. Ferguson, Fatih Dogan

Materials Science and Engineering Faculty Research & Creative Works

Like batteries, thermophotovoltaic generators produce DC electricity quietly. TPV uses infrared photovoltaic cells to convert infrared radiation from a combustion heated ceramic IR emitter. However, because the specific energy in a hydrocarbon fuel like propane or butane is 12,900 Wh/kg, much larger than the specific energy of 145 Wh/kg for a Li-ion battery, TPV is very promising as a lightweight DC power supply. A portable cylindrical thermophotovoltaic (TPV) battery replacement concept has been previously described. It consists of a cylindrical TPV receiver assembly using simple diffused junction GaSb IR cells along with a novel omega recuperator and a novel doped …


Tensile Test Design To Measure Interlayer Adhesion In Investment Casting Shells For Spalling Mitigation, Shelby Boyd, Alex Miller, Jameson Senger Jun 2015

Tensile Test Design To Measure Interlayer Adhesion In Investment Casting Shells For Spalling Mitigation, Shelby Boyd, Alex Miller, Jameson Senger

Materials Engineering

We designed a tensile test fixture for a 112 lbf capacity Instron load frame that imparts a normal force on the face of a button epoxied to an investment casting shell sample, delaminating the shell area attached to the button. Using a green standard shell (Group 1), a partially fired standard shell (Group 2), and a green shell with a different third coat (Group 3), we verified that the fixture can measure differences in strength between sample groups. We attached steel buttons to leveled samples with 0.05 mL of Hysol-Loctite 9340 epoxy, let it cure for 48 hours, and tested …


Chemical Oxidative Polymerization, Optical, Electrochemical And Kinetic Studies Of 8-Amino-2-Naphthol, Fatih Dogan, Ismet Kaya, Ali Bilici, Mehmet Yildirim Jun 2015

Chemical Oxidative Polymerization, Optical, Electrochemical And Kinetic Studies Of 8-Amino-2-Naphthol, Fatih Dogan, Ismet Kaya, Ali Bilici, Mehmet Yildirim

Materials Science and Engineering Faculty Research & Creative Works

Here the polymerization of 8-amino-2-naphthol (AN) is reported without use of an additional external template, surfactants or functional dopants. For this, NaOCl and hydrochloride acid solution (1.0 M) were used as oxidant and reaction medium, respectively. The structure of oligomer was elucidated by FT-IR, UV–vis and 1 H-NMR techniques. The number average molecular weight of oligomer was found to be 2200Da with a polydispersity index of 1.4 by size exclusion chromatography. This oligomer exhibited a multicolor emission behavior as it was excited at different wavelengths. Redox states were clarified by cyclic voltammetry (CV) technique and the relationship between anodic/cathodic peak …


Comparison Of Low-Temperature Co-Fired Ceramic And Direct Bonded Copper For Single Ended Primary Inductance Topology, Kristopher Cody Johnson May 2015

Comparison Of Low-Temperature Co-Fired Ceramic And Direct Bonded Copper For Single Ended Primary Inductance Topology, Kristopher Cody Johnson

Electrical Engineering Undergraduate Honors Theses

This work examines the thermal dissipation characteristics of Low-Temperature Co-fired Ceramic (LTCC) and Direct Bonded Copper (DBC) with the implementation of a Single Ended Primary Inductance Converter (SEPIC) topology. The advantages and disadvantages of the two substrates will be explored in addition to a description of the design and control of the SEPIC. It will be shown that the DBC implementation is superior with regards to thermal dissipation, but that LTCC has advantages in high- density packaging, RF applications, and embedded components. These substrates and converters provide many advantages in industrial applications that include automotive and grid level implementations. Additional …


Kinetics Of Corrosion Of Bn-Zro2-Sic Ceramics In Contact With Si-Killed Steel, Abhishek Kumar, Vivek Thapliyal, David G.C. Robertson, Jeffrey D. Smith May 2015

Kinetics Of Corrosion Of Bn-Zro2-Sic Ceramics In Contact With Si-Killed Steel, Abhishek Kumar, Vivek Thapliyal, David G.C. Robertson, Jeffrey D. Smith

Materials Science and Engineering Faculty Research & Creative Works

The mechanism and kinetics of corrosion of BN-ZrO2-SiC (MYCROSINT®SO43) by molten Si-killed steel was studied. Isothermal corrosion tests were performed for duration between 2 and 8 h. Refractory and steel composition and morphology changes were investigated. A kinetic model using process simulation software METSIM and thermochemical software FactSage was developed to understand refractory-steel interactions. The corrosion process showed a deviation from parabolic kinetics and was fitted by a combination of linear and parabolic terms. It was determined that corrosion of the BN-ZrO2-SiC refractory was governed by dissolution of SiC and BN and removal of ZrO2 …


High Pressure Behavior Of Mullite-Type Oxides: Phase Transitions, Amorphization, Negative Linear Compressibility And Microstructural Implications, Patricia Kalita May 2015

High Pressure Behavior Of Mullite-Type Oxides: Phase Transitions, Amorphization, Negative Linear Compressibility And Microstructural Implications, Patricia Kalita

UNLV Theses, Dissertations, Professional Papers, and Capstones

Even though mullite occurs rarely in nature, it is perhaps one of the most important phases in both traditional and advanced ceramics. Existing and emerging applications of mullite and mullite-type materials include: high-temperature composites, aerospace materials, ballistic shielding for military applications and even non-linear optical materials. There are many uncertainties regarding the basic physical properties of mullite-type materials, particularly in terms of their high-pressure structural stability and mechanical behavior that are important to address for emerging applications of mullites as engineering materials. This work is the first reported comprehensive investigation of the high –pressure structural behavior of several different mullites …


Reaction Kinetics Of Rare Earth And Actinide Materials, Brian Jon Jaques May 2015

Reaction Kinetics Of Rare Earth And Actinide Materials, Brian Jon Jaques

Boise State University Theses and Dissertations

This dissertation presents the effects of atmosphere, time, and energy input (thermal and mechanical) on the kinetics of gas-solid and solid-solid reactions in systems of dysprosium, uranium, oxygen, and nitrogen. Accordingly, Chapter Two presents a novel synthesis technique used to form DyN via a gas-solid reaction between dysprosium and nitrogen. DyN was rapidly formed through a mechanochemical process in a high energy ball mill at ambient temperatures. The progress of the reaction was quantified using in situ temperature and pressure measurements coupled with microscopy and x-ray diffraction. It was found that the rate of the nitridation reaction is controlled by …


Crystal Nucleation Of Palladium-Doped Lithium Disilicate Glass, Gregory Humble Apr 2015

Crystal Nucleation Of Palladium-Doped Lithium Disilicate Glass, Gregory Humble

Symposium of Student Scholars

The effect of concentration of palladium particles on crystal nucleation was investigated for lithium disilicate glass. The heterogeneous nucleation rate for 470°C and 480°C were calculated for a concentration of 0.001% palladium by weight. The DTA method of measuring nucleation and crystallization was used in this calculation.


Electrochemical Capture Of Co2 From Natural Gas Using A High-Temperature Ceramic-Carbonate Membrane, Jingjing Tong, Lingling Zhan, Jie Fang, Minfang Han, Kevin Huang Jan 2015

Electrochemical Capture Of Co2 From Natural Gas Using A High-Temperature Ceramic-Carbonate Membrane, Jingjing Tong, Lingling Zhan, Jie Fang, Minfang Han, Kevin Huang

Faculty Publications

This study reports the first investigation of using a ceramic-carbonate dual-phase membrane to electrochemically separate CO2 from a simulated natural gas. The CO2 permeation flux density was systematically studied as a function of temperature, CO2 partial pressure and time. As expected, the flux density was observed to increase with temperature and CO2 partial pressure. Long-term stability test showed that flux density experienced an initial performance-improving “break-in” period followed by a slow decay. Post-test microstructural analysis suggested that a gradual loss of carbonate during the test could be the cause of the flux-time behavior observed.


Method And System For Purifying Charged Radioisotopes, Cathy Sue Cutler, Gary John Ehrhardt, Hendrik Petrus Engelbrecht, D. E. Day Jan 2015

Method And System For Purifying Charged Radioisotopes, Cathy Sue Cutler, Gary John Ehrhardt, Hendrik Petrus Engelbrecht, D. E. Day

Materials Science and Engineering Faculty Research & Creative Works

The present invention provides a simple and inexpensive method for removing metal and other impurities in a radioisotope solution. The invention further includes the development of a new parent/daughter generator system for collecting the daughter isotope in a concentrated solution.


Methods Of Extrusion On Demand For High Solids Loading Ceramic Paste In Freeform Extrusion Fabrication, Wenbin Li, Amir Ghazanfari, Ming Leu, Robert Landers Jan 2015

Methods Of Extrusion On Demand For High Solids Loading Ceramic Paste In Freeform Extrusion Fabrication, Wenbin Li, Amir Ghazanfari, Ming Leu, Robert Landers

Faculty Publications, Mechanical Engineering

Fabrication of highly dense parts with complex geometry by paste-extrusion-based solid freeform fabrication processes requires a precise control of the extrusion flow rate to dispense material on demand, which is often referred as Extrusion-On-Demand (EOD). The extrusion process for aqueous ceramic pastes is complex and difficult to control due to their non-Newtonian behavior, compressibility and inhomogeneity. In this study, three methods of EOD (based on ram extruder, needle valve, and auger valve) are introduced and investigated for the extrusion of high solids loading (i.e., >50%, volumetric) aqueous alumina paste. Optimal extrusion process parameters for these methods are determined through printing …


Angiogenic Effect Of Bioactive Borate Glass Microfibers And Beads In The Hairless Mouse, Richard J. Watters, Roger F. Brown, D. E. Day Jan 2015

Angiogenic Effect Of Bioactive Borate Glass Microfibers And Beads In The Hairless Mouse, Richard J. Watters, Roger F. Brown, D. E. Day

Biological Sciences Faculty Research & Creative Works

The purpose of this project was to investigate the angiogenic mechanism of bioactive borate glass for soft tissue repair in a 'hairless' SKH1 mouse model. Subcutaneous microvascular responses to bioactive glass microfibers (45S5, 13-93B3, and 13-93B3Cu) and bioactive glass beads (13-93, 13-93B3, and 13-93B3Cu) were assessed via: noninvasive imaging of skin microvasculature; histomorphometry of microvascular densities; and quantitative PCR measurements of mRNA expression of VEGF and FGF-2 cytokines. Live imaging via dorsal skin windows showed the formation at two weeks of a halo-like structure infused with microvessels surrounding implanted borate-based 13-93B3 and 13-93B3Cu glass beads, a response not observed with …


Fundamental Studies Of Surfactant Templated Metal Oxide Materials Synthesis And Transformation For Adsorption And Energy Applications, Saikat Das Jan 2015

Fundamental Studies Of Surfactant Templated Metal Oxide Materials Synthesis And Transformation For Adsorption And Energy Applications, Saikat Das

Theses and Dissertations--Chemical and Materials Engineering

This work addresses fundamental aspects of designing templates and curing conditions for the synthesis of mesoporous metal oxide thin films. The first section addresses selection of cationic-carbohydrate surfactant mixtures to synthesize templated silica thin films for selective adsorption of simple carbohydrates based on molecular imprinting. Nuclear magnetic resonance and fluorescence spectroscopy results suggest a novel structure for mixtures of alkyl glucopyranosides or xylopyranosides with cationic (trimethylammonium) surfactants. Despite thermodynamically favorable mixing, the carbohydrate headgroups in the mixed micelle adopt an inverted configuration with their headgroups in the micelle core, and therefore are inaccessible for molecular imprinting. This orientation occurs even …


Fusion Welding Of Diboride-Carbide Ceramic Composites, Derek Scott King Jan 2015

Fusion Welding Of Diboride-Carbide Ceramic Composites, Derek Scott King

Doctoral Dissertations

"Plasma and pulsed plasma arc welding (PAW and PPAW) processes were used to fusion weld ZrB2 containing 20 vol% ZrC. Varying welding parameters resulted in changes in weld pool shape and size, and the size of ZrB2 grains within the fusion zone. For PAW processes that resulted in a keyhole fusion zone (full penetration), the arc to workpiece power transfer efficiency was estimated to be 2 grain lengths were observed to decrease between binary PAW FZs (~1 mm in length), and binary PPAW FZs (~0.8 mm in length), and an increasing aspect ratio for ZrB2 grains in …


Congenital Epidermoid Cyst Results In Muscle Fusion Defect In The Upper Lip, Fatih Dogan, Ibrahim Hakan Bucak Dec 2014

Congenital Epidermoid Cyst Results In Muscle Fusion Defect In The Upper Lip, Fatih Dogan, Ibrahim Hakan Bucak

Materials Science and Engineering Faculty Research & Creative Works

Epidermoid cysts are rarely detected malformations in the oral cavity. Their development sites are the sublingual, submaxillary, and submandibular spaces. In this paper, we report a three-month-old infant who was admitted to our hospital due upper lip swelling. Magnetic resonance imaging showed that she had a two-centimeter cystic lesion and fusion defects of orbicularis oris muscle. The cyst was surgically removed, and histopathological diagnosis was “epidermoid cyst.” In recent literature, we could not find reports related to orbicularis oris muscle fusion defects because of epidermoid cyst.


Interaction Of Bn-Zro2-Sic Ceramics With Inclusions In Si-Killed Steel, Abhishek Kumar, Vivek Thapliyal, Jeffrey D. Smith Nov 2014

Interaction Of Bn-Zro2-Sic Ceramics With Inclusions In Si-Killed Steel, Abhishek Kumar, Vivek Thapliyal, Jeffrey D. Smith

Materials Science and Engineering Faculty Research & Creative Works

Boron nitride (BN)-based ceramics are often used as containment refractory in thin-strip steel production. The interaction of this material (BN-ZrO2-SiC: -MYCROSINT® SO43) was studied using a steel-inclusion system in a laboratory setup. Isothermal interaction tests were performed to evaluate the interaction of inclusions with this refractory. It was determined that corrosion of the BN refractory occurs through a dissolution mechanism and it was more severe in contact with steel compared to slag. A thermodynamic model was developed using FactSage to study the change in liquid steel/slag composition with refractory interaction. Thermodynamic predictions were in agreement with the experimental …


Investigation Of The Performance Of Different Types Of Zirconium Microstructures Under Extreme Irradiation Conditions, Eric M. Acosta, Osman J. El-Atwani Aug 2014

Investigation Of The Performance Of Different Types Of Zirconium Microstructures Under Extreme Irradiation Conditions, Eric M. Acosta, Osman J. El-Atwani

The Summer Undergraduate Research Fellowship (SURF) Symposium

The safe and continued operation of the US nuclear power plants requires improvement of the radiation resistant properties of materials used in nuclear reactors. Zirconium is a material of particular interest due to its use in fuel cladding. Studies performed on other materials have shown that grain boundaries can play a significant role on the radiation resistant properties of a material. Thus, the focus of our research is to investigate the performance of different zirconium microstructures under irradiation conditions similar to those in commercial nuclear reactors. Analysis of the surface morphology of zirconium both pre- and post-irradiation was conducted with …


Microstructure Development Of Granular System During Compaction, Chen Shang, Marcial Gonzalez Aug 2014

Microstructure Development Of Granular System During Compaction, Chen Shang, Marcial Gonzalez

The Summer Undergraduate Research Fellowship (SURF) Symposium

Granular materials is the second most manipulated material in the industry today. They are easy to transport and more and more newly developed materials cannot stand the process of traditional casting, like energetic materials and bio-materials, but will survive the powder compaction process. Having a better understanding of the microstructure development of granular systems during compaction process, especially for particles that will heavily deform under loading, will give an insight of how to better process the powders to produce materials with overall better performance comparing to bulk materials. The main theory and mechanism applied are Hertz law and nonlocal contact …


In Vitro Assessment Of Laser Sintered Bioactive Glass Scaffolds With Different Pore Geometries, Krishna C. R. Kolan, Albin Thomas, Ming-Chuan Leu, Greg Hilmas Aug 2014

In Vitro Assessment Of Laser Sintered Bioactive Glass Scaffolds With Different Pore Geometries, Krishna C. R. Kolan, Albin Thomas, Ming-Chuan Leu, Greg Hilmas

Mechanical and Aerospace Engineering Faculty Research & Creative Works

The pore geometry of bioactive glass scaffolds intended for use in bone repair or replacement is one of the most important parameters that could determine the rate of bone regeneration. The pore geometry would also affect the mechanical properties of the scaffolds and their rate of degradation. Scaffolds with five different architectures, having ~50% porosity, were fabricated with silicate (13–93) and borate (13–93B3) based bioactive glasses using a laser sintering process. An established, late-osteoblasts/early-osteocytes cell line was used to perform cell proliferation tests on the scaffolds. The results indicated that the cells proliferate significantly more on the scaffolds which mimic …


The Electronic And Thermodynamic Properties Of Ca Doped Lafeo3: A First Principles Study Using Density Functional Theory, Davis George Daniel Aug 2014

The Electronic And Thermodynamic Properties Of Ca Doped Lafeo3: A First Principles Study Using Density Functional Theory, Davis George Daniel

Boise State University Theses and Dissertations

Density functional theory (DFT) was used to evaluate the electronic and thermodynamic properties of Ca-doped LaFeO3 (La1-xCaxFeO3-y). La1-xCaxFeO3-y exhibits ionic (O2- anions) and electronic conductivity at high temperatures and has potential applications in gas separation, syngas production and solid oxide fuel cell cathodes. DFT is a computational technique based on the First Principles of physics, derived from the theory of quantum mechanics. DFT approximates the ground state energy of a system and can subsequently determine many bulk properties such as lattice constants, magnetic states, band gap, density …


Modulating Notochordal Differentiation Of Human Induced Pluripotent Stem Cells Using Natural Nucleus Pulposus Tissue Matrix, Yongxing Liu, M. N. Rahaman, B. Sonny Bal Jul 2014

Modulating Notochordal Differentiation Of Human Induced Pluripotent Stem Cells Using Natural Nucleus Pulposus Tissue Matrix, Yongxing Liu, M. N. Rahaman, B. Sonny Bal

Materials Science and Engineering Faculty Research & Creative Works

Human induced pluripotent stem cells (hiPSCs) can differentiate into notochordal cell (NC)-like cells when cultured in the presence of natural porcine nucleus pulposus (NP) tissue matrix. The method promises massive production of high-quality, functional cells to treat degenerative intervertebral discs (IVDs). Based on our previous work, we further examined the effect of cell-NP matrix contact and culture medium on the differentiation, and further assessed the functional differentiation ability of the generated NC-like. The study showed that direct contact between hiPSCs and NP matrix can promote the differentiation yield, whilst both the contact and non-contact cultures can generate functional NC-like cells. …


Characterizing The Pore Structure Of Carbonated Natural Wollastonite, Chiara Villani, Robert Spragg, Raikhan Tokpatayeva, Jan Olek, W. Jason Weiss Jun 2014

Characterizing The Pore Structure Of Carbonated Natural Wollastonite, Chiara Villani, Robert Spragg, Raikhan Tokpatayeva, Jan Olek, W. Jason Weiss

International Conference on Durability of Concrete Structures

This paper focuses on examining the pore structure of a cementitious paste made with a calcium silicate (wollastonite) that reacts with carbon dioxide and water to form a hardened solid. The pore structure of the hardened solid has been characterized using vapor sorption and desorption, low-temperature differential scanning calorimetry (LT-DSC), and scanning electron microscopy (SEM). The total porosity was also measured using mass measurement in oven-dry and vacuum-saturated conditions. Evidence exists that support the hypothesis that the solid has two main pore sizes: large macropores (>10 nm) appear to form between the initial calcium silicate particles and small micropores …


Developent Of A Phospholipid Encapsulation Process For Quantum Dots To Be Used In Biologic Applications, Logan Grimes Jun 2014

Developent Of A Phospholipid Encapsulation Process For Quantum Dots To Be Used In Biologic Applications, Logan Grimes

Master's Theses

The American Cancer Society predicts that 1,665,540 people will be diagnosed with cancer, and 585,720 people will die from cancer in 2014. One of the most common types of cancer in the United States is skin cancer. Melanoma alone is predicted to account for 10,000 of the cancer related deaths in 2014. As a highly mobile and aggressive form of cancer, melanoma is difficult to fight once it has metastasized through the body. Early detection in such varieties of cancer is critical in improving survival rates in afflicted patients. Present methods of detection rely on visual examination of suspicious regions …


Material Composition And Toxicology Of Cosmetic Products, Hilda Gonzalez Jun 2014

Material Composition And Toxicology Of Cosmetic Products, Hilda Gonzalez

Materials Engineering

In today’s modern society, the U.S. Food and Drug Administration regulates many industries to protect consumers’ health; the cosmetics industry is not one of them. Through self-regulation, companies continue to sell products for topical use on the body that have been known to contain toxic chemicals with little to no testing on the effects they have on the human body. The purpose of this project was to determine the content of such known toxins in five different brands of face powders. X-Ray Diffraction (XRD) was used to verify the primary component and Inductively Coupled Plasma-Optical Emissions Spectroscopy (ICP-OES) was used …


Characterization Of 3d Interconnected Microstructural Network In Mixed Ionic And Electronic Conducting Ceramic Composites, William M. Harris, Kyle S. Brinkman, Ye Lin, Dong Su, Alex P. Cocco, Arata Nakajo, Matthew B. Degostin, Yu-Chen Karen Chen-Wiegart, Jun Wang, Fanglin Chen, Yong S. Chu, Wilson K. S. Chiu May 2014

Characterization Of 3d Interconnected Microstructural Network In Mixed Ionic And Electronic Conducting Ceramic Composites, William M. Harris, Kyle S. Brinkman, Ye Lin, Dong Su, Alex P. Cocco, Arata Nakajo, Matthew B. Degostin, Yu-Chen Karen Chen-Wiegart, Jun Wang, Fanglin Chen, Yong S. Chu, Wilson K. S. Chiu

Faculty Publications

The microstructure and connectivity of the ionic and electronic conductive phases in composite ceramic membranes are directly related to device performance. Transmission electron microscopy (TEM) including chemical mapping combined with X-ray nanotomography (XNT) have been used to characterize the composition and 3-D microstructure of a MIEC composite model system consisting of a Ce0.8Gd0.2O2 (GDC) oxygen ion conductive phase and a CoFe2O4 (CFO) electronic conductive phase. The microstructural data is discussed, including the composition and distribution of an emergent phase which takes the form of isolated and distinct regions. Performance implications are considered …


Ceramic Welds, And A Method For Producing The Same, Greg Hilmas, William Fahrenholtz, Jeremy Lee Watts, Harlan James Brown-Shaklee May 2014

Ceramic Welds, And A Method For Producing The Same, Greg Hilmas, William Fahrenholtz, Jeremy Lee Watts, Harlan James Brown-Shaklee

Materials Science and Engineering Faculty Research & Creative Works

A method of producing a ceramic weld, including identifying a ceramic first surface and a ceramic second surface to be bonded together, maintaining a non-oxidizing atmosphere over the first and second surfaces, and engaging the first and second surfaces to define a joint. An arc is generated between an electrode and the joint to create a liquid phase, and the liquid phase is cooled to yield a solid fusion layer, wherein the first and second surfaces are joined in the fusion layer.


Selection Of The Process Parameters For The Mass Plating Of Discrete Electronic Components, Ann Hopper May 2014

Selection Of The Process Parameters For The Mass Plating Of Discrete Electronic Components, Ann Hopper

Articles

The miniaturisation of electronic components coupled with requirements for high temperature lead free soldering has forced the improvement of the termination finish of surface mount components to meet the critical demands of the electronic industry. In the present work the processing parameters necessary to plate miniature multilayer varistors (MLV’s) have been explored. The tooling selected was a “Rotary flow-thru’ plater” which achieved high volume plating with


Thermodynamics And Reaction Kinetics During Mechanochemical Synthesis And Environmental Testing Of Lanthanide And Actinide Refractory Materials, Gordon Andrew Alanko May 2014

Thermodynamics And Reaction Kinetics During Mechanochemical Synthesis And Environmental Testing Of Lanthanide And Actinide Refractory Materials, Gordon Andrew Alanko

Boise State University Theses and Dissertations

High energy ball milling is a broad family of well-known techniques for materials processing that includes mechanochemical synthesis, in which the milled materials react during milling. The latter may involve components reacting in the solid, liquid, or gas phases, and the operative kinetics have hardly been studied. Several manufacturers of high energy ball mills have recently made available instrumented milling vessel lids. These lids are able to monitor the temperature of the lid and the gas pressure within the vessel in situ during milling experiments. This ability is a significant improvement over the ad hoc instrumentation setups sometimes discussed in …


Phase Transformations In Calcium Substituted Lanthanum Ferrite, Patrick M. Price May 2014

Phase Transformations In Calcium Substituted Lanthanum Ferrite, Patrick M. Price

Boise State University Theses and Dissertations

Increasing world energy demands are still heavily dependent on fossil fuels. To meet these demands, crude oil is increasingly being extracted from remote locations where natural gas pipelines do not exist. It is not profitable for oil and gas companies to transport natural gas by ship or truck from these remote locations so it is combusted on site in the form of gas flares. Critics oppose this practice due to the environmental impact from pollution and carbon emissions created during the flaring process. Oil and gas companies are eager to find profitable ways to eliminate natural gas lines in order …


Experimental Investigation Of Mechanical Behavior Of An Oxide/Oxide Ceramic Composite In Interlaminar Shear And Under Combined Tension-Torsion Loading, Skyler R. Hilburn Mar 2014

Experimental Investigation Of Mechanical Behavior Of An Oxide/Oxide Ceramic Composite In Interlaminar Shear And Under Combined Tension-Torsion Loading, Skyler R. Hilburn

Theses and Dissertations

Creep behavior in interlaminar shear of an oxide-oxide ceramic composite, Nextel 720™/aluminosilicate (N720/AS), was investigated at 1100°C in laboratory air and in steam. The interlaminar shear strength (ILSS) was determined as 7.65 MPa. The creep behavior was examined for interlaminar shear stresses in the 2-6 MPa range. Primary and secondary creep regimes were observed in all tests conducted in air and in steam. Tertiary creep was noted in the tests performed at 6 MPa. Larger creep strains and higher creep strain rates were produced in steam. Surprisingly, the presence of steam had a beneficial effect on creep lifetimes. It appears …